JP7391857B2 - 周期的堆積プロセスによって基材上に遷移金属含有膜を形成する方法、遷移金属ハロゲン化物化合物を反応チャンバーに供給する方法、及び関連蒸着装置 - Google Patents
周期的堆積プロセスによって基材上に遷移金属含有膜を形成する方法、遷移金属ハロゲン化物化合物を反応チャンバーに供給する方法、及び関連蒸着装置 Download PDFInfo
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- JP7391857B2 JP7391857B2 JP2020543099A JP2020543099A JP7391857B2 JP 7391857 B2 JP7391857 B2 JP 7391857B2 JP 2020543099 A JP2020543099 A JP 2020543099A JP 2020543099 A JP2020543099 A JP 2020543099A JP 7391857 B2 JP7391857 B2 JP 7391857B2
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- transition metal
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- halide compound
- metal halide
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- 229910052723 transition metal Inorganic materials 0.000 title claims description 210
- 150000003624 transition metals Chemical class 0.000 title claims description 200
- 239000000758 substrate Substances 0.000 title claims description 131
- 238000000034 method Methods 0.000 title claims description 109
- 150000001875 compounds Chemical class 0.000 title claims description 101
- 238000006243 chemical reaction Methods 0.000 title claims description 84
- 125000004122 cyclic group Chemical group 0.000 title claims description 60
- 238000005137 deposition process Methods 0.000 title claims description 47
- 230000008021 deposition Effects 0.000 title description 75
- 239000002243 precursor Substances 0.000 claims description 164
- 239000000376 reactant Substances 0.000 claims description 131
- 239000007789 gas Substances 0.000 claims description 130
- 238000000151 deposition Methods 0.000 claims description 103
- 239000003446 ligand Substances 0.000 claims description 70
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 45
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 45
- 229910017052 cobalt Inorganic materials 0.000 claims description 44
- 239000010941 cobalt Substances 0.000 claims description 44
- 230000008569 process Effects 0.000 claims description 41
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 37
- 239000000463 material Substances 0.000 claims description 37
- 229910052760 oxygen Inorganic materials 0.000 claims description 37
- 239000001301 oxygen Substances 0.000 claims description 37
- 229910052739 hydrogen Inorganic materials 0.000 claims description 36
- 239000001257 hydrogen Substances 0.000 claims description 36
- 238000000231 atomic layer deposition Methods 0.000 claims description 30
- 229910052757 nitrogen Inorganic materials 0.000 claims description 29
- 150000003623 transition metal compounds Chemical class 0.000 claims description 27
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 25
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 24
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 23
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 23
- 239000003638 chemical reducing agent Substances 0.000 claims description 23
- 229910000314 transition metal oxide Inorganic materials 0.000 claims description 21
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 19
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(II) oxide Inorganic materials [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims description 18
- 229910052799 carbon Inorganic materials 0.000 claims description 14
- 239000010949 copper Substances 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 14
- UORVGPXVDQYIDP-UHFFFAOYSA-N borane Chemical compound B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 claims description 13
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 claims description 12
- GVPFVAHMJGGAJG-UHFFFAOYSA-L cobalt dichloride Chemical compound [Cl-].[Cl-].[Co+2] GVPFVAHMJGGAJG-UHFFFAOYSA-L 0.000 claims description 12
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 claims description 12
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 11
- 229910052802 copper Inorganic materials 0.000 claims description 11
- IUYLTEAJCNAMJK-UHFFFAOYSA-N cobalt(2+);oxygen(2-) Chemical compound [O-2].[Co+2] IUYLTEAJCNAMJK-UHFFFAOYSA-N 0.000 claims description 10
- 229910052759 nickel Inorganic materials 0.000 claims description 10
- 230000000737 periodic effect Effects 0.000 claims description 10
- 238000005229 chemical vapour deposition Methods 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 9
- 230000015572 biosynthetic process Effects 0.000 claims description 8
- 150000002431 hydrogen Chemical class 0.000 claims description 8
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 8
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 229910000085 borane Inorganic materials 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 6
- 238000004891 communication Methods 0.000 claims description 6
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 6
- 125000004433 nitrogen atom Chemical group N* 0.000 claims description 6
- 238000003786 synthesis reaction Methods 0.000 claims description 6
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 5
- 229910021381 transition metal chloride Inorganic materials 0.000 claims description 5
- 238000007740 vapor deposition Methods 0.000 claims description 5
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 4
- 229910000077 silane Inorganic materials 0.000 claims description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 3
- XKLVLDXNZDIDKQ-UHFFFAOYSA-N butylhydrazine Chemical group CCCCNN XKLVLDXNZDIDKQ-UHFFFAOYSA-N 0.000 claims description 3
- AVWLPUQJODERGA-UHFFFAOYSA-L cobalt(2+);diiodide Chemical compound [Co+2].[I-].[I-] AVWLPUQJODERGA-UHFFFAOYSA-L 0.000 claims description 3
- ZOCHARZZJNPSEU-UHFFFAOYSA-N diboron Chemical compound B#B ZOCHARZZJNPSEU-UHFFFAOYSA-N 0.000 claims description 3
- PZPGRFITIJYNEJ-UHFFFAOYSA-N disilane Chemical compound [SiH3][SiH3] PZPGRFITIJYNEJ-UHFFFAOYSA-N 0.000 claims description 3
- VEDJZFSRVVQBIL-UHFFFAOYSA-N trisilane Chemical compound [SiH3][SiH2][SiH3] VEDJZFSRVVQBIL-UHFFFAOYSA-N 0.000 claims description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims description 2
- BZRRQSJJPUGBAA-UHFFFAOYSA-L cobalt(ii) bromide Chemical compound Br[Co]Br BZRRQSJJPUGBAA-UHFFFAOYSA-L 0.000 claims description 2
- VXGHASBVNMHGDI-UHFFFAOYSA-N digermane Chemical compound [Ge][Ge] VXGHASBVNMHGDI-UHFFFAOYSA-N 0.000 claims description 2
- 229910001882 dioxygen Inorganic materials 0.000 claims description 2
- 229910000078 germane Inorganic materials 0.000 claims description 2
- 125000004430 oxygen atom Chemical group O* 0.000 claims description 2
- 229910021558 transition metal bromide Inorganic materials 0.000 claims description 2
- 229910021561 transition metal fluoride Inorganic materials 0.000 claims description 2
- 229910021573 transition metal iodide Inorganic materials 0.000 claims description 2
- 150000001805 chlorine compounds Chemical class 0.000 claims 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 1
- 238000005234 chemical deposition Methods 0.000 claims 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 claims 1
- 239000010408 film Substances 0.000 description 108
- -1 for example Chemical class 0.000 description 36
- 239000010410 layer Substances 0.000 description 29
- 229910052751 metal Inorganic materials 0.000 description 25
- 239000002184 metal Substances 0.000 description 25
- 238000010926 purge Methods 0.000 description 21
- 239000004065 semiconductor Substances 0.000 description 16
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 14
- 229910052717 sulfur Inorganic materials 0.000 description 14
- 125000001183 hydrocarbyl group Chemical group 0.000 description 13
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 13
- 239000011593 sulfur Substances 0.000 description 13
- 150000002429 hydrazines Chemical class 0.000 description 12
- 229910052711 selenium Inorganic materials 0.000 description 12
- 239000011669 selenium Substances 0.000 description 12
- 239000012686 silicon precursor Substances 0.000 description 12
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 11
- 239000012707 chemical precursor Substances 0.000 description 11
- 241000894007 species Species 0.000 description 11
- 229910000428 cobalt oxide Inorganic materials 0.000 description 9
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 8
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 8
- 229910052796 boron Inorganic materials 0.000 description 8
- 239000006227 byproduct Substances 0.000 description 8
- 230000008901 benefit Effects 0.000 description 7
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 7
- 150000001721 carbon Chemical group 0.000 description 7
- 235000012431 wafers Nutrition 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 229910021580 Cobalt(II) chloride Inorganic materials 0.000 description 6
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 6
- 150000001298 alcohols Chemical class 0.000 description 6
- 125000003342 alkenyl group Chemical group 0.000 description 6
- 125000000217 alkyl group Chemical group 0.000 description 6
- 230000004888 barrier function Effects 0.000 description 6
- 150000001735 carboxylic acids Chemical class 0.000 description 6
- 239000012159 carrier gas Substances 0.000 description 6
- 239000003989 dielectric material Substances 0.000 description 6
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 6
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 6
- 239000012528 membrane Substances 0.000 description 6
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 6
- 239000012688 phosphorus precursor Substances 0.000 description 6
- 239000002356 single layer Substances 0.000 description 6
- 239000010409 thin film Substances 0.000 description 6
- 125000003837 (C1-C20) alkyl group Chemical group 0.000 description 5
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 5
- 150000001299 aldehydes Chemical class 0.000 description 5
- 150000004820 halides Chemical class 0.000 description 5
- 230000007246 mechanism Effects 0.000 description 5
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 5
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 4
- 125000004429 atom Chemical group 0.000 description 4
- VURFVHCLMJOLKN-UHFFFAOYSA-N diphosphane Chemical compound PP VURFVHCLMJOLKN-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000011261 inert gas Substances 0.000 description 4
- 238000002347 injection Methods 0.000 description 4
- 239000007924 injection Substances 0.000 description 4
- 230000004048 modification Effects 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 4
- 150000003138 primary alcohols Chemical class 0.000 description 4
- 150000003333 secondary alcohols Chemical class 0.000 description 4
- 150000003509 tertiary alcohols Chemical class 0.000 description 4
- 229910021350 transition metal silicide Inorganic materials 0.000 description 4
- MDAXKAUIABOHTD-UHFFFAOYSA-N 1,4,8,11-tetraazacyclotetradecane Chemical compound C1CNCCNCCCNCCNC1 MDAXKAUIABOHTD-UHFFFAOYSA-N 0.000 description 3
- XQQZRZQVBFHBHL-UHFFFAOYSA-N 12-crown-4 Chemical compound C1COCCOCCOCCO1 XQQZRZQVBFHBHL-UHFFFAOYSA-N 0.000 description 3
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- KWYHDKDOAIKMQN-UHFFFAOYSA-N N,N,N',N'-tetramethylethylenediamine Chemical compound CN(C)CCN(C)C KWYHDKDOAIKMQN-UHFFFAOYSA-N 0.000 description 3
- 238000000277 atomic layer chemical vapour deposition Methods 0.000 description 3
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 3
- 235000019253 formic acid Nutrition 0.000 description 3
- 239000001307 helium Substances 0.000 description 3
- 229910052734 helium Inorganic materials 0.000 description 3
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229910001507 metal halide Inorganic materials 0.000 description 3
- 238000001451 molecular beam epitaxy Methods 0.000 description 3
- DWFKOMDBEKIATP-UHFFFAOYSA-N n'-[2-[2-(dimethylamino)ethyl-methylamino]ethyl]-n,n,n'-trimethylethane-1,2-diamine Chemical compound CN(C)CCN(C)CCN(C)CCN(C)C DWFKOMDBEKIATP-UHFFFAOYSA-N 0.000 description 3
- DIHKMUNUGQVFES-UHFFFAOYSA-N n,n,n',n'-tetraethylethane-1,2-diamine Chemical compound CCN(CC)CCN(CC)CC DIHKMUNUGQVFES-UHFFFAOYSA-N 0.000 description 3
- UKODFQOELJFMII-UHFFFAOYSA-N pentamethyldiethylenetriamine Chemical compound CN(C)CCN(C)CCN(C)C UKODFQOELJFMII-UHFFFAOYSA-N 0.000 description 3
- 239000011574 phosphorus Substances 0.000 description 3
- 229910052698 phosphorus Inorganic materials 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000009738 saturating Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- YFNKIDBQEZZDLK-UHFFFAOYSA-N triglyme Chemical compound COCCOCCOCCOC YFNKIDBQEZZDLK-UHFFFAOYSA-N 0.000 description 3
- MBYLVOKEDDQJDY-UHFFFAOYSA-N tris(2-aminoethyl)amine Chemical compound NCCN(CCN)CCN MBYLVOKEDDQJDY-UHFFFAOYSA-N 0.000 description 3
- 238000005019 vapor deposition process Methods 0.000 description 3
- UJTDKNZVLGVLFT-UHFFFAOYSA-N 1,2-Bis(methylthio)ethane Chemical compound CSCCSC UJTDKNZVLGVLFT-UHFFFAOYSA-N 0.000 description 2
- DIIIISSCIXVANO-UHFFFAOYSA-N 1,2-Dimethylhydrazine Chemical compound CNNC DIIIISSCIXVANO-UHFFFAOYSA-N 0.000 description 2
- WLDGDTPNAKWAIR-UHFFFAOYSA-N 1,4,7-trimethyl-1,4,7-triazonane Chemical compound CN1CCN(C)CCN(C)CC1 WLDGDTPNAKWAIR-UHFFFAOYSA-N 0.000 description 2
- HRFJEOWVAGSJNW-UHFFFAOYSA-N 1,4,8,11-tetramethyl-1,4,8,11-tetrazacyclotetradecane Chemical compound CN1CCCN(C)CCN(C)CCCN(C)CC1 HRFJEOWVAGSJNW-UHFFFAOYSA-N 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 2
- PWJHXHMUGFXPSN-UHFFFAOYSA-N 1,7-dioxa-4,10-diazacyclododecane Chemical compound C1COCCNCCOCCN1 PWJHXHMUGFXPSN-UHFFFAOYSA-N 0.000 description 2
- MIOCUERTSIJEDP-UHFFFAOYSA-N 2-diethylphosphanylethyl(diethyl)phosphane Chemical compound CCP(CC)CCP(CC)CC MIOCUERTSIJEDP-UHFFFAOYSA-N 0.000 description 2
- QPRQEDXDYOZYLA-UHFFFAOYSA-N 2-methylbutan-1-ol Chemical compound CCC(C)CO QPRQEDXDYOZYLA-UHFFFAOYSA-N 0.000 description 2
- UDQOBFJTYHSIPJ-UHFFFAOYSA-N 3-diethylphosphanylpropyl(diethyl)phosphane Chemical compound CCP(CC)CCCP(CC)CC UDQOBFJTYHSIPJ-UHFFFAOYSA-N 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 2
- ZTQSAGDEMFDKMZ-UHFFFAOYSA-N Butyraldehyde Chemical compound CCCC=O ZTQSAGDEMFDKMZ-UHFFFAOYSA-N 0.000 description 2
- STLRZBGWSTVCGW-UHFFFAOYSA-L CN(CCN(C)C)C.[Co](Cl)Cl Chemical compound CN(CCN(C)C)C.[Co](Cl)Cl STLRZBGWSTVCGW-UHFFFAOYSA-L 0.000 description 2
- 241000579895 Chlorostilbon Species 0.000 description 2
- 229910021592 Copper(II) chloride Inorganic materials 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- CJKRXEBLWJVYJD-UHFFFAOYSA-N N,N'-diethylethylenediamine Chemical compound CCNCCNCC CJKRXEBLWJVYJD-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 2
- 125000003172 aldehyde group Chemical group 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 238000003877 atomic layer epitaxy Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- UBEWDCMIDFGDOO-UHFFFAOYSA-N cobalt(II,III) oxide Inorganic materials [O-2].[O-2].[O-2].[O-2].[Co+2].[Co+3].[Co+3] UBEWDCMIDFGDOO-UHFFFAOYSA-N 0.000 description 2
- QTMDXZNDVAMKGV-UHFFFAOYSA-L copper(ii) bromide Chemical compound [Cu+2].[Br-].[Br-] QTMDXZNDVAMKGV-UHFFFAOYSA-L 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 150000004985 diamines Chemical class 0.000 description 2
- SBZXBUIDTXKZTM-UHFFFAOYSA-N diglyme Chemical compound COCCOCCOC SBZXBUIDTXKZTM-UHFFFAOYSA-N 0.000 description 2
- 239000010976 emerald Substances 0.000 description 2
- 229910052876 emerald Inorganic materials 0.000 description 2
- 238000010574 gas phase reaction Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 2
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 2
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
- HDZGCSFEDULWCS-UHFFFAOYSA-N monomethylhydrazine Chemical compound CNN HDZGCSFEDULWCS-UHFFFAOYSA-N 0.000 description 2
- MFIGJRRHGZYPDD-UHFFFAOYSA-N n,n'-di(propan-2-yl)ethane-1,2-diamine Chemical compound CC(C)NCCNC(C)C MFIGJRRHGZYPDD-UHFFFAOYSA-N 0.000 description 2
- VGIVLIHKENZQHQ-UHFFFAOYSA-N n,n,n',n'-tetramethylmethanediamine Chemical compound CN(C)CN(C)C VGIVLIHKENZQHQ-UHFFFAOYSA-N 0.000 description 2
- DMQSHEKGGUOYJS-UHFFFAOYSA-N n,n,n',n'-tetramethylpropane-1,3-diamine Chemical compound CN(C)CCCN(C)C DMQSHEKGGUOYJS-UHFFFAOYSA-N 0.000 description 2
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 2
- 150000002894 organic compounds Chemical class 0.000 description 2
- 125000002524 organometallic group Chemical group 0.000 description 2
- 229910000073 phosphorus hydride Inorganic materials 0.000 description 2
- 229920000768 polyamine Polymers 0.000 description 2
- 229920000570 polyether Polymers 0.000 description 2
- 150000003254 radicals Chemical class 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 229930195734 saturated hydrocarbon Natural products 0.000 description 2
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Images
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- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
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- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
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- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
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- C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
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- C23C16/406—Oxides of iron group metals
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
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- C23C16/45553—Atomic layer deposition [ALD] characterized by the use of precursors specially adapted for ALD
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
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- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/28—Manufacture of electrodes on semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/268
- H01L21/283—Deposition of conductive or insulating materials for electrodes conducting electric current
- H01L21/285—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation
- H01L21/28506—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers
- H01L21/28512—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers on semiconductor bodies comprising elements of Group IV of the Periodic Table
- H01L21/28568—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers on semiconductor bodies comprising elements of Group IV of the Periodic Table the conductive layers comprising transition metals
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- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/70—Manufacture or treatment of devices consisting of a plurality of solid state components formed in or on a common substrate or of parts thereof; Manufacture of integrated circuit devices or of parts thereof
- H01L21/71—Manufacture of specific parts of devices defined in group H01L21/70
- H01L21/768—Applying interconnections to be used for carrying current between separate components within a device comprising conductors and dielectrics
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
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- H01L21/70—Manufacture or treatment of devices consisting of a plurality of solid state components formed in or on a common substrate or of parts thereof; Manufacture of integrated circuit devices or of parts thereof
- H01L21/71—Manufacture of specific parts of devices defined in group H01L21/70
- H01L21/768—Applying interconnections to be used for carrying current between separate components within a device comprising conductors and dielectrics
- H01L21/76838—Applying interconnections to be used for carrying current between separate components within a device comprising conductors and dielectrics characterised by the formation and the after-treatment of the conductors
- H01L21/76877—Filling of holes, grooves or trenches, e.g. vias, with conductive material
- H01L21/76879—Filling of holes, grooves or trenches, e.g. vias, with conductive material by selective deposition of conductive material in the vias, e.g. selective C.V.D. on semiconductor material, plating
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L23/00—Details of semiconductor or other solid state devices
- H01L23/52—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames
- H01L23/522—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames including external interconnections consisting of a multilayer structure of conductive and insulating layers inseparably formed on the semiconductor body
- H01L23/532—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames including external interconnections consisting of a multilayer structure of conductive and insulating layers inseparably formed on the semiconductor body characterised by the materials
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- H01L21/71—Manufacture of specific parts of devices defined in group H01L21/70
- H01L21/768—Applying interconnections to be used for carrying current between separate components within a device comprising conductors and dielectrics
- H01L21/76838—Applying interconnections to be used for carrying current between separate components within a device comprising conductors and dielectrics characterised by the formation and the after-treatment of the conductors
- H01L21/76841—Barrier, adhesion or liner layers
- H01L21/76843—Barrier, adhesion or liner layers formed in openings in a dielectric
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- H01L23/52—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames
- H01L23/522—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames including external interconnections consisting of a multilayer structure of conductive and insulating layers inseparably formed on the semiconductor body
- H01L23/532—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames including external interconnections consisting of a multilayer structure of conductive and insulating layers inseparably formed on the semiconductor body characterised by the materials
- H01L23/53204—Conductive materials
- H01L23/53209—Conductive materials based on metals, e.g. alloys, metal silicides
- H01L23/53228—Conductive materials based on metals, e.g. alloys, metal silicides the principal metal being copper
- H01L23/53238—Additional layers associated with copper layers, e.g. adhesion, barrier, cladding layers
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Description
本開示は、2018年2月15日に出願され、「A METHOD OF FORMING A TRANSITION METAL CONTAINING FILM ON A SUBSTRATE BY A CYCLICAL DEPOSITION PROCESS, A METHOD FOR SUPPLYING A TRANSITION METAL HALIDE COMPOUND TO A REACTION CHAMBER, AND RELATED VAPOR DEPOSITION APPARATUS」と題された米国特許出願第15/897,578号の利益を主張し、これを参照によって本明細書に組み込む。
本願で特許請求される発明は、ヘルシンキ大学(the University of Helsinki)とASM Microchemistry Oyとの間の共同研究協約によって、又は共同研究協約のために、及び/又は共同研究協約に関連してなされた。当協約は、特許請求される発明がなされた日及びその日以前に発効しており、特許請求される発明は、当協約の範囲内で取り組まれた活動の結果としてなされたものである。
(付加体)n-M-Xa (I)
式中、「付加体」のそれぞれは、付加体形成配位子であり、単座、二座、又は多座付加体形成配位子又はその混合物となるよう独立して選択されることができ、単座形成配位子の場合、nは1~4であり、二座又は多座付加体形成配位子の場合、nは1~2であり、Mは、例えば、コバルト(Co)、銅(Cu)、又はニッケル(Ni)などの遷移金属であり、Xaのそれぞれは別の配位子であり、ハロゲン化物又は他の配位子となるように独立して選択されることができ、ここでaは、1~4であり、一部の例では、aは2である。
RIRII-N-NRIIIRIV (II)
式中、RIは、炭化水素基、例えば、直鎖、分枝鎖、環状、芳香族又は置換炭化水素基など、から選択されることができ、RII、RIII、RIV基のそれぞれは、水素基又は炭化水素基、例えば、直鎖、分枝鎖、環状、芳香族又は置換炭化水素基など、であるように独立して選択されることができる。
R1-OH (III)
式中、R1は、直鎖又は分岐鎖C1-C20アルキル、又はメチル、エチル、プロピル、ブチル、ペンチル又はヘキシルなどのアルケニル基である。第一級アルコールの例には、メタノール、エタノール、プロパノール、ブタノール、2-メチルプロパノール及び2-メチルブタノールが含まれる。
R3-CHO (VI)
式中、R3は、水素及びメチル、エチル、プロピル、ブチル、ペンチル又はヘキシルなどの直鎖又は分岐鎖C1-C20アルキル及びアルケニル基からなる群から選択される。いくつかの実施形態では、R3は、メチル又はエチルからなる群から選択される。例示的な化合物は、限定されないが、式(VI)によると、ホルムアルデヒド、アセトアルデヒド、及びブチルアルデヒドである。
OHC-R4-CHO (VII)
式中、R4は直鎖又は分岐鎖C1-C20飽和又は不飽和炭化水素である。別の方法として、アルデヒド基は相互に直接結合されてもよい(R4はnullである)。
R5-COOH (VIII)
式中、R5は、水素又はメチル、エチル、プロピル、ブチル、ペンチル又はヘキシル、例えば、メチル又はエチルなどの直鎖もしくは分岐鎖C1-C20アルキル又はアルケニル基である。いくつかの実施形態では、R5は、直鎖又は分岐鎖C1-C3アルキル又はアルケニル基である。式(VII)による化合物の例は、ギ酸、プロパン酸及び酢酸であり、いくつかの実施形態ではギ酸(HCOOH)である。
202 基材
204 誘電材料
206 バリア材料
208 金属相互接続材料
210 キャッピング層
400 蒸着装置
402 反応チャンバー
404 サセプタ
406 基材
408 シャワーヘッドガス分配器
410A、410B 前駆体供給源容器
410C パージガス容器
412A、412B 導管
414 加熱部
416 遷移金属ハロゲン化物
418 蒸気通路
420 システム動作及び制御機構
Claims (22)
- 周期的堆積プロセスにより基材上に遷移金属含有膜を形成する方法であって、
前記基材を、二座窒素含有付加配位子を含む遷移金属ハロゲン化物化合物を含む第一の気相反応物質と接触させることと、
前記基材を酸素前駆体を含む第二の気相反応物質と接触させて遷移金属酸化物を堆積させることとを含む、方法。 - 前記二座窒素含有付加配位子が二つの窒素原子を含み、各々の窒素原子が少なくとも一つの炭素原子に結合されている、請求項1に記載の方法。
- 前記遷移金属ハロゲン化物化合物が遷移金属塩化物を含む、請求項1に記載の方法。
- 前記遷移金属塩化物化合物が、塩化コバルト、塩化ニッケル、又は塩化銅のうちの少なくとも一つを含む、請求項3に記載の方法。
- 前記遷移金属塩化物化合物が、塩化コバルト(TMEDA)、又は塩化ニッケル(TMPDA)のうちの少なくとも一つを含む、請求項4に記載の方法。
- 前記酸素前駆体が、オゾン(O3)、分子状酸素(O2)、酸素原子(O)、酸素プラズマ、酸素ラジカル、酸素励起種、水(H2O)、及び過酸化水素(H2O2)からなる群から選択される、請求項1に記載の方法。
- 前記遷移金属酸化物が、酸化コバルト(II)(CoO)を実質的に含む、請求項6に記載の方法。
- 前記遷移金属酸化物を還元剤前駆体と接触させることを更に含み、それによって元素遷移金属を形成する、請求項6に記載の方法。
- 前記還元剤前駆体が、フォーミングガス(H2+N2)、アンモニア(NH3)、ヒドラジン(N2H4)、水素分子(H2)、水素原子(H)、水素プラズマ、水素ラジカル、水素励起種、アルコール、アルデヒド、カルボン酸、ボラン、又はアミンのうちの少なくとも一つを含む、請求項8に記載の方法。
- 第三級ブチルヒドラジン(C4H12N2)、水素(H2)、水素(H2)プラズマ、アンモニア(NH3)、アンモニア(NH3)プラズマ、ヒドラジン(N2H4)、シラン(SiH4)、ジシラン(Si2H6)、トリシラン(Si3H8)、ゲルマン(GeH4)、ジゲルマン(Ge2H6)、ボラン(BH3)、及びジボラン(B2H6)からなる群から選択される還元剤前駆体を含む、第三の気相反応物質に前記基材を接触させることを更に含む、請求項1に記載の方法。
- 前記遷移金属含有膜が、元素コバルト、元素ニッケル、又は元素銅のうちの少なくとも一つを含む、請求項1に記載の方法。
- 前記周期的堆積プロセスが、原子層堆積プロセスを含む、請求項1に記載の方法。
- 前記周期的堆積プロセスが周期的化学気相堆積プロセスを含む、請求項1に記載の方法。
- 周期的堆積プロセスにより基材上に遷移金属含有膜を形成する方法であって、
前記基材を二座窒素付加体形成配位子を含む遷移金属ハロゲン化物化合物を含む第一の気相反応物質と接触させることと、
前記基材を酸素前駆体を含む第二の気相反応物質と接触させて遷移金属酸化物を堆積させることと、を含み、
前記遷移金属が、銅(Cu)、ニッケル(Ni)、及びコバルト(Co)からなる群から選択される、周期的堆積プロセスにより基材上に遷移金属含有膜を形成する方法。 - 前記遷移金属ハロゲン化物化合物が、遷移金属塩化物、遷移金属ヨウ化物、遷移金属フッ化物、又は遷移金属臭化物からなる群から選択される、請求項14に記載の方法。
- 前記遷移金属ハロゲン化物化合物が、塩化コバルト(TMEDA)、臭化コバルト(TMEDA)、ヨウ化コバルト(TMEDA)、塩化コバルト(TMPDA)、又は塩化ニッケル(TMPDA)のうちの少なくとも一つを含む、請求項14に記載の方法。
- 付加体形成配位子を含む前記遷移金属ハロゲン化物化合物が、遷移金属ハロゲン化物化合物及び二座窒素付加体形成配位子を50℃未満の温度で組み合わせることを含む、ワンステップ合成プロセスを利用して合成される、請求項14に記載の方法。
- 二座窒素含有付加配位子を含む遷移金属ハロゲン化物化合物を、反応チャンバーに供給して、周期的堆積プロセスにより基材上に遷移金属含有膜を形成するための方法であって、
前記遷移金属ハロゲン化物化合物を収容するように構成された第1の前駆体供給源容器を提供することと、
酸素前駆体を収容するように構成された第2の前駆体供給源容器を提供することと、
前記反応チャンバーに前記第1及び第2の前駆体供給源容器を流体連結させることと、
前記前駆体供給源容器内に含まれる前記遷移金属ハロゲン化物化合物を50℃より高い温度に加熱することと、
少なくとも0.001ミリバ-ルの前記遷移金属ハロゲン化物化合物の蒸気圧を生成することと、
前記遷移金属ハロゲン化物化合物を前記反応チャンバーに供給することと、
前記酸素前駆体を前記反応チャンバーに供給して遷移金属酸化物を堆積させることと、を含む、二座窒素含有付加配位子を含む遷移金属ハロゲン化物化合物を、反応チャンバーに供給して、周期的堆積プロセスにより基材上に遷移金属含有膜を形成するための方法。 - 前記遷移金属ハロゲン化物化合物が、塩化コバルト(TMEDA)、塩化ニッケル(TMPDA)のうちの少なくとも一つを含む、請求項18に記載の方法。
- 反応性揮発性化学物質を利用して、周期的堆積プロセスにより基材上に遷移金属含有膜を形成するための蒸着装置であって、
反応チャンバーと、
前記反応チャンバーに配置された基材と、
前記反応チャンバーと流体連通する第1の前駆体供給源容器と、
前記反応チャンバーと流体連通する第2の前駆体供給源容器と、
前記第1の前駆体供給源容器に配置された二座窒素含有付加配位子を含む、遷移金属ハロゲン化物化合物と、
前記第2の前駆体供給源容器に配置された、遷移金属酸化物を堆積させるための酸素前駆体と、を備える、反応性揮発性化学物質を利用する蒸着装置。 - 前記遷移金属ハロゲン化物化合物が、塩化コバルト(TMEDA)、又は塩化ニッケル(TMPDA)のうちの少なくとも一つを含む、請求項20に記載の装置。
- 前記遷移金属ハロゲン化物化合物が、150℃未満の遷移金属化合物温度で0.001ミリバールを超える蒸気圧を示す、請求項20に記載の装置。
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CN111684105A (zh) | 2020-09-18 |
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WO2019158995A3 (en) | 2019-12-19 |
KR20200121798A (ko) | 2020-10-26 |
TW201934795A (zh) | 2019-09-01 |
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