JPWO2020033819A5

JPWO2020033819A5 -

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Publication number: JPWO2020033819A5
Authority: JP; Japan
Prior art keywords: electrolytic capacitor; solid electrolytic; dihydrothieno; capacitor according; dioxin
Prior art date: 2022-03-02
Legal status : Granted

Application number

JP2021507053A

Other languages

English (en)

Japanese (ja)

Other versions

JP2021534579A (ja

JP7442502B2 (ja

Publication date

2022-03-02

2019-08-09 Application filed filed Critical

2019-08-09 Priority claimed from PCT/US2019/045887 external-priority patent/WO2020033819A1/en

2021-12-09 Publication of JP2021534579A publication Critical patent/JP2021534579A/ja

2022-03-02 Publication of JPWO2020033819A5 publication Critical patent/JPWO2020033819A5/ja

2024-03-04 Application granted granted Critical

2024-03-04 Publication of JP7442502B2 publication Critical patent/JP7442502B2/ja

Status Active legal-status Critical Current

2039-08-09 Anticipated expiration legal-status Critical

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239000003990 capacitor Substances 0.000 claims abstract description 171
239000007784 solid electrolyte Substances 0.000 claims abstract description 42
229920001940 conductive polymer Polymers 0.000 claims abstract description 40
239000007787 solid Substances 0.000 claims abstract description 38
239000002245 particle Substances 0.000 claims abstract description 32
239000011248 coating agent Substances 0.000 claims abstract description 26
238000000576 coating method Methods 0.000 claims abstract description 26
YTPLMLYBLZKORZ-UHFFFAOYSA-N Thiophene Chemical group C=1C=CSC=1 YTPLMLYBLZKORZ-UHFFFAOYSA-N 0.000 claims abstract description 14
229920000642 polymer Polymers 0.000 claims description 75
-1 2,3-dihydrothieno [3,4-b]-[1,4] dioxin-2-yl Chemical group 0.000 claims description 72
239000002253 acid Substances 0.000 claims description 21
239000011734 sodium Substances 0.000 claims description 18
229910052708 sodium Inorganic materials 0.000 claims description 16
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 15
125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims description 13
239000002923 metal particle Substances 0.000 claims description 11
239000012298 atmosphere Substances 0.000 claims description 10
239000003431 cross linking reagent Substances 0.000 claims description 10
239000000463 material Substances 0.000 claims description 10
229920005989 resin Polymers 0.000 claims description 10
239000011347 resin Substances 0.000 claims description 10
GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 9
125000004311 dioxin-2-yl group Chemical group [H]C1=C([H])OC(*)=C([H])O1 0.000 claims description 8
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 8
229910052715 tantalum Inorganic materials 0.000 claims description 7
229910052783 alkali metal Inorganic materials 0.000 claims description 6
238000011084 recovery Methods 0.000 claims description 6
229930192474 thiophene Natural products 0.000 claims description 6
150000001340 alkali metals Chemical class 0.000 claims description 5
125000000217 alkyl group Chemical group 0.000 claims description 5
230000015556 catabolic process Effects 0.000 claims description 5
125000005843 halogen group Chemical group 0.000 claims description 4
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 4
239000001294 propane Substances 0.000 claims description 3
FBRGJGRMDGNNRL-UHFFFAOYSA-N azanium 4-(2,3-dihydrothieno[3,4-b][1,4]dioxin-3-ylmethoxy)butane-2-sulfonate Chemical compound O1C=2C(OCC1COCCC(S(=O)(=O)[O-])C)=CSC2.[NH4+] FBRGJGRMDGNNRL-UHFFFAOYSA-N 0.000 claims description 2
QKEREOORBDZEBA-UHFFFAOYSA-M potassium 4-(2,3-dihydrothieno[3,4-b][1,4]dioxin-3-ylmethoxy)butane-2-sulfonate Chemical compound O1C=2C(OCC1COCCC(S(=O)(=O)[O-])C)=CSC2.[K+] QKEREOORBDZEBA-UHFFFAOYSA-M 0.000 claims description 2
LZHCEOYHBZYMQZ-UHFFFAOYSA-M sodium 1-(2,3-dihydrothieno[3,4-b][1,4]dioxin-3-ylmethoxy)heptane-3-sulfonate Chemical compound O1C=2C(OCC1COCCC(S(=O)(=O)[O-])CCCC)=CSC2.[Na+] LZHCEOYHBZYMQZ-UHFFFAOYSA-M 0.000 claims description 2
HVBRCYUJKTYVBD-UHFFFAOYSA-M sodium 1-(2,3-dihydrothieno[3,4-b][1,4]dioxin-3-ylmethoxy)octane-3-sulfonate Chemical compound O1C=2C(OCC1COCCC(S(=O)(=O)[O-])CCCCC)=CSC2.[Na+] HVBRCYUJKTYVBD-UHFFFAOYSA-M 0.000 claims description 2
OAJZFHFBPIVWMO-UHFFFAOYSA-M sodium 3-(2,3-dihydrothieno[3,4-b][1,4]dioxin-3-ylmethoxy)-1-fluoropropane-1-sulfonate Chemical compound O1C=2C(OCC1COCCC(S(=O)(=O)[O-])F)=CSC2.[Na+] OAJZFHFBPIVWMO-UHFFFAOYSA-M 0.000 claims description 2
ZMANZCXQSJIPKH-UHFFFAOYSA-O triethylammonium ion Chemical compound CC[NH+](CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-O 0.000 claims description 2
ZYNOESUJJLFWCB-UHFFFAOYSA-M sodium 4-(2,3-dihydrothieno[3,4-b][1,4]dioxin-3-ylmethoxy)butane-2-sulfonate Chemical group O1C=2C(OCC1COCCC(S(=O)(=O)[O-])C)=CSC2.[Na+] ZYNOESUJJLFWCB-UHFFFAOYSA-M 0.000 claims 1
238000010586 diagram Methods 0.000 abstract 1
239000010410 layer Substances 0.000 description 64
238000000034 method Methods 0.000 description 42
239000006185 dispersion Substances 0.000 description 27
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 26
PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 25
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 23
239000003792 electrolyte Substances 0.000 description 22
229910052751 metal Inorganic materials 0.000 description 22
239000002184 metal Substances 0.000 description 22
239000002904 solvent Substances 0.000 description 21
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 16
239000000843 powder Substances 0.000 description 16
230000008569 process Effects 0.000 description 16
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 15
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 15
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
229910052709 silver Inorganic materials 0.000 description 15
239000004332 silver Substances 0.000 description 15
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 14
239000000853 adhesive Substances 0.000 description 14
230000001070 adhesive effect Effects 0.000 description 14
229910052759 nickel Inorganic materials 0.000 description 13
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 12
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 12
125000002887 hydroxy group Chemical group [H]O* 0.000 description 12
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 12
150000003839 salts Chemical class 0.000 description 12
239000000243 solution Substances 0.000 description 12
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 11
239000000203 mixture Substances 0.000 description 11
238000003466 welding Methods 0.000 description 11
229920001609 Poly(3,4-ethylenedioxythiophene) Polymers 0.000 description 10
150000001450 anions Chemical class 0.000 description 10
229910052799 carbon Inorganic materials 0.000 description 10
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 9
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 9
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 9
229910052802 copper Inorganic materials 0.000 description 9
239000010949 copper Substances 0.000 description 9
239000000178 monomer Substances 0.000 description 9
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 8
VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical class [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 8
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 8
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 8
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 8
150000001875 compounds Chemical class 0.000 description 8
239000008188 pellet Substances 0.000 description 8
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 7
238000007743 anodising Methods 0.000 description 7
239000011230 binding agent Substances 0.000 description 7
229920001577 copolymer Polymers 0.000 description 7
235000014113 dietary fatty acids Nutrition 0.000 description 7
239000000194 fatty acid Substances 0.000 description 7
229930195729 fatty acid Natural products 0.000 description 7
150000008040 ionic compounds Chemical class 0.000 description 7
229920001223 polyethylene glycol Polymers 0.000 description 7
YXFVVABEGXRONW-UHFFFAOYSA-N toluene Substances CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 7
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MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 6
229920003171 Poly (ethylene oxide) Polymers 0.000 description 6
239000002202 Polyethylene glycol Substances 0.000 description 6
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 6
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 6
DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical compound OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 description 6
150000007513 acids Chemical class 0.000 description 6
125000001931 aliphatic group Chemical group 0.000 description 6
229910052782 aluminium Inorganic materials 0.000 description 6
JFDZBHWFFUWGJE-UHFFFAOYSA-N benzonitrile Chemical compound N#CC1=CC=CC=C1 JFDZBHWFFUWGJE-UHFFFAOYSA-N 0.000 description 6
150000002739 metals Chemical class 0.000 description 6
229920000172 poly(styrenesulfonic acid) Polymers 0.000 description 6
229940005642 polystyrene sulfonic acid Drugs 0.000 description 6
239000011148 porous material Substances 0.000 description 6
238000007639 printing Methods 0.000 description 6
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 6
230000000452 restraining effect Effects 0.000 description 6
239000000126 substance Substances 0.000 description 6
HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 description 6
229910052718 tin Inorganic materials 0.000 description 6
229910052719 titanium Inorganic materials 0.000 description 6
239000010936 titanium Substances 0.000 description 6
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 5
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
229910045601 alloy Inorganic materials 0.000 description 5
239000000956 alloy Substances 0.000 description 5
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
238000002048 anodisation reaction Methods 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 5
239000002019 doping agent Substances 0.000 description 5
239000008151 electrolyte solution Substances 0.000 description 5
239000007789 gas Substances 0.000 description 5
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 5
229910052737 gold Inorganic materials 0.000 description 5
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239000011261 inert gas Substances 0.000 description 5
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229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 5
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LDMOEFOXLIZJOW-UHFFFAOYSA-N 1-dodecanesulfonic acid Chemical class CCCCCCCCCCCCS(O)(=O)=O LDMOEFOXLIZJOW-UHFFFAOYSA-N 0.000 description 4
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239000001257 hydrogen Substances 0.000 description 4
229910052739 hydrogen Inorganic materials 0.000 description 4
150000002576 ketones Chemical class 0.000 description 4
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150000003457 sulfones Chemical class 0.000 description 3
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229910052725 zinc Inorganic materials 0.000 description 3
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JP2021507053A 2018-08-10 2019-08-09 固有導電性ポリマーを含む固体電解キャパシタ Active JP7442502B2 (ja)