CN100376585C - 用于填充橡胶的封端巯基硅烷偶联剂 - Google Patents
用于填充橡胶的封端巯基硅烷偶联剂 Download PDFInfo
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Abstract
Description
硅烷 | α | β | Ex.4 | Ex.3 | Ex.1 | Ex.2 | γ | γ |
加入重 | --- | 7.4 | 7.4 | 7.4 | 7.4 | 8.3 | 3.18 | 6.35 |
在100℃下的Mooney | ||||||||
粘度ML1+4 | 130 | 67 | 65 | 58 | 73 | 63 | 74 | 121 |
在135℃下的Mooney早期硫化 | ||||||||
MS1+,t<sub>3</sub>,分钟MS1+,t<sub>18</sub>, | 9.511.0 | 6.710.1 | 4.35.9 | 6.37.8 | 2.23.2 | 6.37.7 | 6.38.4 | 2.83.7 |
ODR@149℃,弧度1°,30分钟计时器 | ||||||||
M<sub>1</sub>.,dN-MM<sub>H</sub>,dN-Mt<sub>s1</sub>,分钟t90,分钟 | 26.944.55.410.5 | 8.530.84.817.8 | 8.531.02.58.0 | 7.231.43.88.0 | 9.334.81.68.1 | 7.830.53.87.5 | 11.527.83.815.1 | 14.833.92.015.0 |
物理性能,固化190@149℃ | ||||||||
硬度,Shore A伸长率,% | 66900 | 57400 | 59540 | 60520 | 62490 | 60450 | 52360 | 过早硫化 |
100%模量,kg/cm<sup>2</sup>200%模量,kg/cm<sup>2</sup>300%模量,kg/cm<sup>2</sup>拉伸强度kg/cm<sup>2</sup> | 10.515.524.6137.1 | 19.056.9128.0208.1 | 19.049.2101.2234.8 | 18.346.496.3218.0 | 22.559.8116.0237.6 | 23.266.1129.4222.9 | 15.545.0104.8139.2 | 未固化 |
动态性能@0.15%应变,10Hz,扭力模式(第二次撞击) | ||||||||
G′@0℃,x10<sup>7</sup>G′@60℃,x10<sup>7</sup>G″@0℃,x10<sup>7</sup>G″@60℃,x10<sup>6</sup>Tan delta@0℃Tan deIta@60℃比率,0℃/60℃ | 26.812.72.8711.20.10700.08761.22 | 5.922.761.262.480.21240.092.36 | 9.224.261.814.000.19680.09392.10 | 9.423.891.843.850.19520.09881.98 | 1.265.362.144.940.1690.0921.84 | 6.413.021.32.710.2020.0892.25 | 3.171.755.692.130.2020.1211.67 | |
热成形,100℃环境,18.5%压缩,143psi(99KPa)负荷,25分钟 | ||||||||
Delta T,℃永久变形,% | 66*** | 136.3 | 2210.9 | 198.8 | 188.0 | 176.9 | ||
***9%脱层 |
试验 | A | B | C | |||
phr DPG在100℃下的Mooney粘度ML 1+4在135℃下的Mooney早期硫化M<sub>v</sub>MS1+,t<sub>3</sub>,分钟MS1+,t<sub>18</sub>,分钟 | 2.0075412.53.6 | 0.5------15.324.1 | 1.25------6.28.3 | |||
ODR@149℃,弧度1°,30分钟计时器 | ||||||
M<sub>L</sub>,dN-MM<sub>H</sub>,dN-Mt<sub>S</sub>1,分钟t90,分钟 | 9.835.71.88.0 | 9.428.88.022.5 | 8.633.43.411.8 | |||
物理性能,固化t90@149℃ | ||||||
硬度,Shore A伸长率,%100%模量,kg/cm<sup>2</sup>200%模量,kg/cm<sup>2</sup>300%模量,kg/cm<sup>2</sup>拉伸强度,kg/cm<sup>2</sup>DIN磨损,毫米<sup>3</sup> | 6355021.155.5106.923685 | 5962019.042.980.9209.569 | 6256022.555.5106.2234.172 | |||
动态性能@10Hz,0.15%应变,扭力模式 | ||||||
G′@0℃,X10<sup>7</sup>G′@60℃,X10<sup>7</sup>G″@0℃,X10<sup>7</sup>G″@60℃,X10<sup>6</sup>Tan delta @0℃Tan delta @60℃比率,0℃/60℃ | 14.86.2323.06.550.15510.10531.47 | 14.15.9726.47.300.18720.11891.57 | 12.65.6422.16.010.17530.10351.69 |
硅烷 | 无 | TESPT | TESPT | Acetyl | Acetyl | Acetyl | Acetyl |
添加硫 | -- | 2 | 4 | 2 | X2 | ---4 | X4 |
Mooney早期硫化@135℃ | |||||||
MVMS1+,t<sub>3</sub>,分钟MS1+,t<sub>18</sub>,分钟Mooney 粘度@100℃ML1+4 | 515.05.896 | 424.35.378 | 404.35.376 | 366.98.274 | 337.48.871 | ||
ODR@149℃,弧度1°,12分钟计时器 | |||||||
M<sub>L</sub>,dN-mM<sub>H</sub>,dN-mt<sub>s</sub>1,分钟t90,分钟 | 19.759.73.55.7 | 14.957.42.85.6 | 14.054.22.85.9 | 12.252.04.37.5 | 11.552.83.87.1 | 10.449.34.78.2 | 10.249.84.48.2 |
物理性能,固化t90@149℃ | |||||||
硬度,Shore A伸长率,%100%模量,kg/cm<sup>2</sup>200%模量,kg/cm<sup>2</sup>300%模量,kg/cm<sup>2</sup>拉伸强度,kg/cm<sup>2</sup>DIN磨损,毫米<sup>3</sup>Akron磨损,毫米<sup>3</sup> | 6763019.736.658.3187.O860.46 | 6757023.950.686.5204.6750.48 | 6657025.354.191.4222.2670.35 | 6654026.756.297.7201.1740.39 | 6644026.759.1103.3174.4710.41 | 6650026.755.5963189.8650.45 | 6646027.459.8105.5189.1730.44 |
硅烷 | A | B | B | C | C | D | D | E | E | F | F | G | H | H |
添加S加入量Mooney 粘度@100℃ML1+4 | 7.094 | 6.3674 | X6.3674 | 6.3372 | X6.33-- | 7.4562 | X7.45-- | 9.6955 | X9.69-- | 12.6750 | X12.67-- | 9.6252 | 6.766 | X6.7-- |
Mooney早期硫化@135℃ | ||||||||||||||
MS1+,t<sub>3</sub>,分钟MS1+,t<sub>18</sub>,分钟 | 6.28.9 | 9.912.6 | 9.011.5 | 6.99.3 | 7.510.2 | 6.37.6 | 6.37.8 | 10.411.7 | 9.611.7 | 13.014.6 | 11.913.9 | 16.819.0 | 8.39.9 | 7.79.6 |
ODR@149℃,弧度1°,30分钟计时器 | ||||||||||||||
M<sub>L</sub>,dN-mM<sub>H</sub>,dN-mt<sub>s1</sub>,分钟t90,分钟 | 9.631.84.517.6 | 8.129.55.410.4 | 8.134.55.114.1 | 8.732.04.111 | 8.536.74.511.5 | 7.929.93.68.0 | 7.733.93.57.5 | 6.727.85.611.3 | 6.832.35.59.8 | 5.726.87.012.3 | 5.730.76.811.0 | 5.531.69.114.1 | 8.230.14.59.5 | 7.934.64.49.0 |
物理性能,固化t90@149℃ | ||||||||||||||
硬度,shore A伸长率,%100%模量,kg/cm<sup>2</sup>200%模量,kg/cm<sup>2</sup>300%模量,kg/cm<sup>2</sup>拉伸强度,kg/cm<sup>2</sup>DIN 磨损,毫米<sup>3</sup> | 5742020.458.4123.7210.971 | 5856016.940.184.4210.369 | 6044022.559.8123.0211.676 | 6466017.638.773.8225.0114 | 6657022.554.8105.5250.397 | 5963015.534.571.7223.6131 | 6054019.049.9104.1236.290 | 5360014.134.577.3227.899 | 5549017.649.2105.5213.792 | 5174012.727.455.5205.3-- | 5461.015.536.671.0186.3-- | 5660015.535.969.6175.8157 | 5861016.238.080.2234.1127 | 6054020.452.7108.3244.794 |
热成形@100℃,17.5%压缩,99KPa静态,25分钟试验 | ||||||||||||||
Delta T,℃永久变形,% | 13.36.2 | 18.910.5 | 13.36.3 | 32.225.3 | 18.312.3 | 21.114.5 | 13.39.8 | 12.25.0 | 8.94.6 | ---- | ---- | 10.57.0 | 18.911.0 | 12.27.7 |
动态性能@0.15%应变,10Hz,扭力模式 | ||||||||||||||
G′@0℃,达因/厘米<sup>2</sup>X10<sup>7</sup>G′@60℃,达因/厘米<sup>2</sup>X10<sup>7</sup>G″@0℃,达因/厘米<sup>2</sup>X10<sup>7</sup>G″@60℃,达因/厘米<sup>2</sup>X10<sup>6</sup>Tan delta@0℃Tan delta@60℃比率,0℃/60℃ | 6.733.001.462.930.2160.0982.22 | 12.85.132.445.230.1910.1021.88 | 12.45.152.434.470.1960.0872.26 | 20.18.733.398.350.1680.0961.75 | 16.62.677.065.330.1610.0752.15 | 12.85.102.475.790.1920.1141.68 | 10.41.934.053.210.1850.0792.34 | 4.802.440.982.140.2050.0882.33 | 4.620.822.001.270.1770.0642.77 | 6.402.421.272.340.1990.0972.05 | 5.931.132.171.230.1910.0573.35 | 9.291.883.643.080.2020.0852.39 | 10.14.182.074.620.2050.1101.86 | 9.541.763.722.720.1840.0732.52 |
硅烷 | I | J | K | K | L | L | M | M | N | N | O | O | P | Q |
添加S加入量 | 9.1 | 6.7 | 5.96 | X5.96 | 7.08 | X7.08 | 5.54 | X5.54 | 8.19 | X8.19 | 9.31 | X9.31 | 8.14 | 8.46 |
Mooney粘度@100℃ | ||||||||||||||
ML1+4 | 55 | 69 | 73 | -- | 63 | -- | 71 | -- | 65 | -- | 54 | -- | 52 | 63 |
Mooney早期硫化@135℃ | ||||||||||||||
Ms1+,t<sub>3</sub>,分钟Ms1+,t<sub>18</sub>,分钟 | 11.513.5 | 2.53.5 | 4.65.6 | 4.35.6 | 4.55.3 | 4.65.6 | 4.75.8 | 4.96.1 | 9.412.6 | 8.911.9 | 11.513.2 | 11.213.3 | 8.910.7 | 9.511.3 |
ODR@149℃,弧度1°,分钟计时器 | ||||||||||||||
M<sub>L</sub>,dN-mM<sub>H</sub>,dN-mt<sub>s1</sub>,分钟t90,分钟 | 6.235.06.311.3 | 8.832.51.917.0 | 9.529.82.816.8 | 9.034.12.815.3 | 6.827.52.811.3 | 7.731.32.89.5 | 9.433.93.013.5 | 9.338.12.911.8 | 8.634.55.312.0 | 8.537.04.811.9 | 6.730.75.610.3 | 6.634.75.910.9 | 7.038.44.810.5 | 6.837.65.510.0 |
物理性能,固化t90@149℃ | ||||||||||||||
硬度,shore A伸长率,%100%模量,kg/cm<sup>2</sup>200%模量,kg/cm<sup>2</sup>300%模量,kg/cm<sup>2</sup>拉伸强度,kg/cm<sup>2</sup>DIN磨损,亳米<sup>3</sup> | 6256019.047.8107.5210.9133 | 6l44019.051.3109.0198.288 | 6150019.043.684.4184.9113 | 6547020.451.3105.5208.l103 | 5658014.833.769.6199.0133 | 5856017.642.991.4234.896 | 6653021.147.187.9196.91O1 | 6553022.555.5105.5225.796 | 6164017.641.580.9227.1100 | 6359021.152.7100.5241.994 | 5758015.534.571.7203.2113 | 5853018.346.492.8208.197 | 6764021.148.586.5219.4141 | 6658022.552.794.2210.9132 |
热成形@100℃,17.5%压缩,99KPa静态负荷,25分钟试验 | ||||||||||||||
Delta T,℃永久变形,% | 12.87.9 | 15.610.8 | 21.713.7 | 16.18.7 | 28.923.2 | 16.711.2 | 25.017.3 | 16.79.2 | 21.116.8 | 15.612.6 | 14.411.0 | 10.07.5 | 17.212.7 | 15.010.8 |
动态性能@0.15%应变,10Hz,扭力模式 | ||||||||||||||
G′@0℃达因/厘米<sup>2</sup>x10<sup>7</sup>G″@60℃,达因/厘米<sup>2</sup>x10<sup>7</sup>G″@0℃达因/厘米<sup>2</sup>x10<sup>7</sup>G″@60℃达因/厘米<sup>2</sup>x10<sup>7</sup>Tan delta@0℃Tan delta@60℃比率,0℃/60℃ | 17.92.996.386.830.1670.1071.56 | 10.82.163.924.870.2010.1241.67 | 18.26.603.279.410.1800.1431.26 | 16.12.705.865.920.1670.1011.65 | 10.14.302.125.320.2100.1241.69 | 8.941.733.652.920.1930.0802.41 | 27.79.544.3314.00.1560.1471.06 | 22.23.397.799.170.1560.1181.30 | 14.95.722.935.750.1560.10l1.95 | 12.42.334.853.620.1870.0752.49 | 10.24.252.064.060.2020.0962.10 | 8.101.552.802.440.1920.0872.21 | 27.63.7210.812.40.1350.1151.18 | 23.83.599.049.610.1510.1061.42 |
Claims (18)
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US5656697P | 1997-08-21 | 1997-08-21 | |
US06/056,566 | 1997-08-21 | ||
PCT/US1998/017391 WO1999009036A1 (en) | 1997-08-21 | 1998-08-21 | Blocked mercaptosilane coupling agents for filled rubbers |
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CNA2007101424877A Division CN101139355A (zh) | 1997-08-21 | 1998-08-21 | 用于填充橡胶的封端巯基硅烷偶联剂 |
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CN1242774A CN1242774A (zh) | 2000-01-26 |
CN100376585C true CN100376585C (zh) | 2008-03-26 |
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CNA2007101424877A Pending CN101139355A (zh) | 1997-08-21 | 1998-08-21 | 用于填充橡胶的封端巯基硅烷偶联剂 |
CNB988015625A Expired - Lifetime CN100376585C (zh) | 1997-08-21 | 1998-08-21 | 用于填充橡胶的封端巯基硅烷偶联剂 |
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Country Status (12)
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US (12) | US6414061B1 (zh) |
EP (3) | EP1270581B1 (zh) |
JP (2) | JP2001505225A (zh) |
KR (2) | KR100674059B1 (zh) |
CN (2) | CN101139355A (zh) |
AT (1) | ATE239737T1 (zh) |
AU (1) | AU8917998A (zh) |
BR (1) | BR9806096B1 (zh) |
DE (1) | DE69814353T3 (zh) |
ES (2) | ES2458563T3 (zh) |
PT (1) | PT958298E (zh) |
WO (1) | WO1999009036A1 (zh) |
Cited By (1)
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