JP2007532761A5 - - Google Patents

Info

Publication number

JP2007532761A5

JP2007532761A5 JP2007508536A JP2007508536A JP2007532761A5 JP 2007532761 A5 JP2007532761 A5 JP 2007532761A5 JP 2007508536 A JP2007508536 A JP 2007508536A JP 2007508536 A JP2007508536 A JP 2007508536A JP 2007532761 A5 JP2007532761 A5 JP 2007532761A5

Authority

JP

Japan

Prior art keywords

less

polymer

adhesive

weight

preferred

Prior art date

2005-04-13

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Granted

Links

• Espacenet
• Global Dossier
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• 229920000642 polymer Polymers 0.000 claims description 240
• 239000000203 mixture Substances 0.000 claims description 160
• -1 polyethylene Polymers 0.000 claims description 116
• 239000000853 adhesive Substances 0.000 claims description 106
• 230000001070 adhesive effect Effects 0.000 claims description 105
• 229920001577 copolymer Polymers 0.000 claims description 74
• 239000004743 Polypropylene Substances 0.000 claims description 60
• QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 59
• 229920001155 polypropylene Polymers 0.000 claims description 54
• 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 54
• VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 48
• 239000005977 Ethylene Substances 0.000 claims description 48
• 125000000524 functional group Chemical group 0.000 claims description 43
• 229920005989 resin Polymers 0.000 claims description 39
• 239000011347 resin Substances 0.000 claims description 39
• 150000001336 alkenes Chemical class 0.000 claims description 34
• 239000002253 acid Substances 0.000 claims description 33
• 239000004711 α-olefin Substances 0.000 claims description 33
• 238000002844 melting Methods 0.000 claims description 30
• 230000008018 melting Effects 0.000 claims description 30
• 125000003118 aryl group Chemical group 0.000 claims description 27
• 150000002148 esters Chemical class 0.000 claims description 24
• 230000004927 fusion Effects 0.000 claims description 24
• 238000007306 functionalization reaction Methods 0.000 claims description 23
• 239000002667 nucleating agent Substances 0.000 claims description 21
• 229920000098 polyolefin Polymers 0.000 claims description 20
• VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 claims description 19
• JRZJOMJEPLMPRA-UHFFFAOYSA-N 1-nonene Chemical compound CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims description 18
• 150000001875 compounds Chemical class 0.000 claims description 17
• RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 16
• KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 15
• KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 15
• LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 claims description 14
• 239000013032 Hydrocarbon resin Substances 0.000 claims description 14
• 125000004432 carbon atom Chemical group C* 0.000 claims description 14
• 150000003505 terpenes Chemical class 0.000 claims description 14
• 235000007586 terpenes Nutrition 0.000 claims description 14
• 229920006270 hydrocarbon resin Polymers 0.000 claims description 12
• 229920000573 polyethylene Polymers 0.000 claims description 12
• 239000004698 Polyethylene Substances 0.000 claims description 11
• 150000007513 acids Chemical class 0.000 claims description 11
• 150000003839 salts Chemical class 0.000 claims description 11
• IAQRGUVFOMOMEM-UHFFFAOYSA-N butene Natural products CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 claims description 10
• 150000001735 carboxylic acids Chemical class 0.000 claims description 9
• 150000001408 amides Chemical class 0.000 claims description 8
• 239000002023 wood Substances 0.000 claims description 8
• 125000001931 aliphatic group Chemical group 0.000 claims description 7
• 230000008859 change Effects 0.000 claims description 7
• 239000002655 kraft paper Substances 0.000 claims description 7
• KWKAKUADMBZCLK-UHFFFAOYSA-N 1-octene Chemical compound CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 claims description 6
• WSSSPWUEQFSQQG-UHFFFAOYSA-N 4-methyl-1-pentene Chemical compound CC(C)CC=C WSSSPWUEQFSQQG-UHFFFAOYSA-N 0.000 claims description 6
• 229920006271 aliphatic hydrocarbon resin Polymers 0.000 claims description 6
• 150000003097 polyterpenes Chemical class 0.000 claims description 6
• 229920005604 random copolymer Polymers 0.000 claims description 6
• 239000003784 tall oil Substances 0.000 claims description 6
• 229920000181 Ethylene propylene rubber Polymers 0.000 claims description 5
• YWAKXRMUMFPDSH-UHFFFAOYSA-N pentene Chemical compound CCCC=C YWAKXRMUMFPDSH-UHFFFAOYSA-N 0.000 claims description 5
• 150000004756 silanes Chemical class 0.000 claims description 5
• LDTAOIUHUHHCMU-UHFFFAOYSA-N 3-methylpent-1-ene Chemical compound CCC(C)C=C LDTAOIUHUHHCMU-UHFFFAOYSA-N 0.000 claims description 4
• 150000008282 halocarbons Chemical class 0.000 claims description 4
• 150000003949 imides Chemical class 0.000 claims description 4
• ZGEGCLOFRBLKSE-UHFFFAOYSA-N methylene hexane Natural products CCCCCC=C ZGEGCLOFRBLKSE-UHFFFAOYSA-N 0.000 claims description 4
• 229920005629 polypropylene homopolymer Polymers 0.000 claims description 4
• CRSBERNSMYQZNG-UHFFFAOYSA-N 1 -dodecene Natural products CCCCCCCCCCC=C CRSBERNSMYQZNG-UHFFFAOYSA-N 0.000 claims description 3
• 229920002367 Polyisobutene Polymers 0.000 claims description 3
• AFFLGGQVNFXPEV-UHFFFAOYSA-N n-decene Natural products CCCCCCCCC=C AFFLGGQVNFXPEV-UHFFFAOYSA-N 0.000 claims description 3
• 239000005011 phenolic resin Substances 0.000 claims description 3
• SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 2
• 239000004712 Metallocene polyethylene (PE-MC) Substances 0.000 claims description 2
• 150000008065 acid anhydrides Chemical class 0.000 claims description 2
• 150000005690 diesters Chemical class 0.000 claims description 2
• 229940069096 dodecene Drugs 0.000 claims description 2
• 229920001002 functional polymer Polymers 0.000 claims 7
• 239000003925 fat Substances 0.000 claims 1
• 239000003054 catalyst Substances 0.000 description 108
• 239000000178 monomer Substances 0.000 description 83
• 238000000034 method Methods 0.000 description 59
• 239000001993 wax Substances 0.000 description 57
• 229920001971 elastomer Polymers 0.000 description 36
• 239000004615 ingredient Substances 0.000 description 31
• 239000000243 solution Substances 0.000 description 30
• 239000000758 substrate Substances 0.000 description 29
• PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 28
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 27
• 238000006243 chemical reaction Methods 0.000 description 27
• VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 27
• 239000000523 sample Substances 0.000 description 26
• 239000002904 solvent Substances 0.000 description 26
• 239000000126 substance Substances 0.000 description 26
• 150000008064 anhydrides Chemical class 0.000 description 25
• 150000001993 dienes Chemical class 0.000 description 25
• 238000006116 polymerization reaction Methods 0.000 description 25
• 230000008569 process Effects 0.000 description 23
• 239000005060 rubber Substances 0.000 description 21
• IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 20
• FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 19
• KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical group C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 18
• 239000012190 activator Substances 0.000 description 18
• 239000000654 additive Substances 0.000 description 18
• 239000000835 fiber Substances 0.000 description 18
• 238000002156 mixing Methods 0.000 description 18
• 239000003921 oil Substances 0.000 description 18
• 238000005481 NMR spectroscopy Methods 0.000 description 17
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 17
• 238000009826 distribution Methods 0.000 description 16
• 150000003254 radicals Chemical class 0.000 description 16
• 239000000806 elastomer Substances 0.000 description 15
• 239000000463 material Substances 0.000 description 15
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 14
• 229920001519 homopolymer Polymers 0.000 description 14
• 238000001542 size-exclusion chromatography Methods 0.000 description 14
• 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 13
• 239000003999 initiator Substances 0.000 description 12
• 238000012360 testing method Methods 0.000 description 12
• YBYIRNPNPLQARY-UHFFFAOYSA-N 1H-indene Natural products C1=CC=C2CC=CC2=C1 YBYIRNPNPLQARY-UHFFFAOYSA-N 0.000 description 11
• 239000003963 antioxidant agent Substances 0.000 description 11
• 235000006708 antioxidants Nutrition 0.000 description 11
• 238000002425 crystallisation Methods 0.000 description 11
• 230000008025 crystallization Effects 0.000 description 11
• 125000004122 cyclic group Chemical group 0.000 description 11
• 238000010438 heat treatment Methods 0.000 description 11
• 239000007788 liquid Substances 0.000 description 11
• RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 description 10
• OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 10
• HQQADJVZYDDRJT-UHFFFAOYSA-N ethene;prop-1-ene Chemical group C=C.CC=C HQQADJVZYDDRJT-UHFFFAOYSA-N 0.000 description 10
• 239000004014 plasticizer Substances 0.000 description 10
• VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 10
• OKTJSMMVPCPJKN-OUBTZVSYSA-N Carbon-13 Chemical compound [13C] OKTJSMMVPCPJKN-OUBTZVSYSA-N 0.000 description 9
• 238000009472 formulation Methods 0.000 description 9
• 239000000123 paper Substances 0.000 description 9
• 229920001083 polybutene Polymers 0.000 description 9
• 229920005606 polypropylene copolymer Polymers 0.000 description 9
• 239000000047 product Substances 0.000 description 9
• 229920001576 syndiotactic polymer Polymers 0.000 description 9
• PBKONEOXTCPAFI-UHFFFAOYSA-N 1,2,4-trichlorobenzene Chemical compound ClC1=CC=C(Cl)C(Cl)=C1 PBKONEOXTCPAFI-UHFFFAOYSA-N 0.000 description 8
• ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 description 8
• 239000003607 modifier Substances 0.000 description 8
• 238000000926 separation method Methods 0.000 description 8
• 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 8
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
• HECLRDQVFMWTQS-RGOKHQFPSA-N 1755-01-7 Chemical compound C1[C@H]2[C@@H]3CC=C[C@@H]3[C@@H]1C=C2 HECLRDQVFMWTQS-RGOKHQFPSA-N 0.000 description 7
• NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 7
• 239000004831 Hot glue Substances 0.000 description 7
• XYLMUPLGERFSHI-UHFFFAOYSA-N alpha-Methylstyrene Chemical compound CC(=C)C1=CC=CC=C1 XYLMUPLGERFSHI-UHFFFAOYSA-N 0.000 description 7
• 229920006125 amorphous polymer Polymers 0.000 description 7
• 229910052799 carbon Inorganic materials 0.000 description 7
• 239000003431 cross linking reagent Substances 0.000 description 7
• 238000000113 differential scanning calorimetry Methods 0.000 description 7
• 239000011521 glass Substances 0.000 description 7
• VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 7
• 239000011976 maleic acid Substances 0.000 description 7
• 230000000707 stereoselective effect Effects 0.000 description 7
• SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 6
• IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
• MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 description 6
• VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 6
• VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 description 6
• 229920000265 Polyparaphenylene Polymers 0.000 description 6
• GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
• 238000007334 copolymerization reaction Methods 0.000 description 6
• LPIQUOYDBNQMRZ-UHFFFAOYSA-N cyclopentene Chemical compound C1CC=CC1 LPIQUOYDBNQMRZ-UHFFFAOYSA-N 0.000 description 6
• HBGGXOJOCNVPFY-UHFFFAOYSA-N diisononyl phthalate Chemical compound CC(C)CCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCC(C)C HBGGXOJOCNVPFY-UHFFFAOYSA-N 0.000 description 6
• 239000000975 dye Substances 0.000 description 6
• 230000000694 effects Effects 0.000 description 6
• 239000000945 filler Substances 0.000 description 6
• 238000005227 gel permeation chromatography Methods 0.000 description 6
• 238000005259 measurement Methods 0.000 description 6
• 238000004806 packaging method and process Methods 0.000 description 6
• 230000000379 polymerizing effect Effects 0.000 description 6
• HJWLCRVIBGQPNF-UHFFFAOYSA-N prop-2-enylbenzene Chemical class C=CCC1=CC=CC=C1 HJWLCRVIBGQPNF-UHFFFAOYSA-N 0.000 description 6
• 229920001384 propylene homopolymer Polymers 0.000 description 6
• 238000001644 13C nuclear magnetic resonance spectroscopy Methods 0.000 description 5
• 229920002799 BoPET Polymers 0.000 description 5
• 239000005041 Mylar™ Substances 0.000 description 5
• NRCMAYZCPIVABH-UHFFFAOYSA-N Quinacridone Chemical compound N1C2=CC=CC=C2C(=O)C2=C1C=C1C(=O)C3=CC=CC=C3NC1=C2 NRCMAYZCPIVABH-UHFFFAOYSA-N 0.000 description 5
• 230000000996 additive effect Effects 0.000 description 5
• 150000001298 alcohols Chemical class 0.000 description 5
• 150000001412 amines Chemical class 0.000 description 5
• 239000011230 binding agent Substances 0.000 description 5
• 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 5
• 125000005842 heteroatom Chemical group 0.000 description 5
• 239000000155 melt Substances 0.000 description 5
• 229910052751 metal Inorganic materials 0.000 description 5
• 239000002184 metal Substances 0.000 description 5
• 239000012968 metallocene catalyst Substances 0.000 description 5
• UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 5
• 229910052757 nitrogen Inorganic materials 0.000 description 5
• 239000002530 phenolic antioxidant Substances 0.000 description 5
• 229920000728 polyester Polymers 0.000 description 5
• 229920006395 saturated elastomer Polymers 0.000 description 5
• 239000000377 silicon dioxide Substances 0.000 description 5
• 238000001374 small-angle light scattering Methods 0.000 description 5
• 229920002554 vinyl polymer Polymers 0.000 description 5
• LRTOHSLOFCWHRF-UHFFFAOYSA-N 1-methyl-1h-indene Chemical compound C1=CC=C2C(C)C=CC2=C1 LRTOHSLOFCWHRF-UHFFFAOYSA-N 0.000 description 4
• NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 4
• VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
• UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
• CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 4
• KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 4
• 239000002318 adhesion promoter Substances 0.000 description 4
• 230000003078 antioxidant effect Effects 0.000 description 4
• TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 4
• BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 4
• 229920001400 block copolymer Polymers 0.000 description 4
• 238000009835 boiling Methods 0.000 description 4
• 150000001732 carboxylic acid derivatives Chemical class 0.000 description 4
• 239000003086 colorant Substances 0.000 description 4
• 238000001816 cooling Methods 0.000 description 4
• 239000013078 crystal Substances 0.000 description 4
• 239000010408 film Substances 0.000 description 4
• 229920000578 graft copolymer Polymers 0.000 description 4
• NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 4
• 229920001580 isotactic polymer Polymers 0.000 description 4
• 239000012299 nitrogen atmosphere Substances 0.000 description 4
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 4
• 239000002994 raw material Substances 0.000 description 4
• 230000009257 reactivity Effects 0.000 description 4
• 125000003808 silyl group Chemical group [H][Si]([H])([H])[*] 0.000 description 4
• 239000002002 slurry Substances 0.000 description 4
• 238000000638 solvent extraction Methods 0.000 description 4
• 239000007921 spray Substances 0.000 description 4
• 239000007858 starting material Substances 0.000 description 4
• 238000012719 thermal polymerization Methods 0.000 description 4
• LWNGJAHMBMVCJR-UHFFFAOYSA-N (2,3,4,5,6-pentafluorophenoxy)boronic acid Chemical compound OB(O)OC1=C(F)C(F)=C(F)C(F)=C1F LWNGJAHMBMVCJR-UHFFFAOYSA-N 0.000 description 3
• OJOWICOBYCXEKR-KRXBUXKQSA-N (5e)-5-ethylidenebicyclo[2.2.1]hept-2-ene Chemical compound C1C2C(=C/C)/CC1C=C2 OJOWICOBYCXEKR-KRXBUXKQSA-N 0.000 description 3
• JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 3
• JTXUVHFRSRTSAT-UHFFFAOYSA-N 3,5,5-trimethylhex-1-ene Chemical compound C=CC(C)CC(C)(C)C JTXUVHFRSRTSAT-UHFFFAOYSA-N 0.000 description 3
• INYHZQLKOKTDAI-UHFFFAOYSA-N 5-ethenylbicyclo[2.2.1]hept-2-ene Chemical compound C1C2C(C=C)CC1C=C2 INYHZQLKOKTDAI-UHFFFAOYSA-N 0.000 description 3
• 239000004322 Butylated hydroxytoluene Substances 0.000 description 3
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• 239000011324 bead Substances 0.000 description 3
• LGBAGUMSAPUZPU-UHFFFAOYSA-N bis(9-methyldecyl) benzene-1,2-dicarboxylate Chemical compound CC(C)CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCCC(C)C LGBAGUMSAPUZPU-UHFFFAOYSA-N 0.000 description 3
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• 238000004364 calculation method Methods 0.000 description 3
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• 239000003795 chemical substances by application Substances 0.000 description 3
• LDHQCZJRKDOVOX-NSCUHMNNSA-N crotonic acid Chemical compound C\C=C\C(O)=O LDHQCZJRKDOVOX-NSCUHMNNSA-N 0.000 description 3
• NLDGJRWPPOSWLC-UHFFFAOYSA-N deca-1,9-diene Chemical compound C=CCCCCCCC=C NLDGJRWPPOSWLC-UHFFFAOYSA-N 0.000 description 3
• 230000007423 decrease Effects 0.000 description 3
• JLTDJTHDQAWBAV-UHFFFAOYSA-O dimethyl(phenyl)azanium Chemical compound C[NH+](C)C1=CC=CC=C1 JLTDJTHDQAWBAV-UHFFFAOYSA-O 0.000 description 3
• 239000002270 dispersing agent Substances 0.000 description 3
• 230000008030 elimination Effects 0.000 description 3
• 238000003379 elimination reaction Methods 0.000 description 3
• 125000005678 ethenylene group Chemical group [H]C([*:1])=C([H])[*:2] 0.000 description 3
• 125000002573 ethenylidene group Chemical group [*]=C=C([H])[H] 0.000 description 3
• 239000001530 fumaric acid Substances 0.000 description 3
• 229920005555 halobutyl Polymers 0.000 description 3
• 125000004968 halobutyl group Chemical group 0.000 description 3
• 150000002430 hydrocarbons Chemical group 0.000 description 3
• 239000002198 insoluble material Substances 0.000 description 3
• 230000014759 maintenance of location Effects 0.000 description 3
• LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 3
• 229920003052 natural elastomer Polymers 0.000 description 3
• 229920001194 natural rubber Polymers 0.000 description 3
• 239000004745 nonwoven fabric Substances 0.000 description 3
• 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 3
• 150000002894 organic compounds Chemical class 0.000 description 3
• 150000001451 organic peroxides Chemical class 0.000 description 3
• 230000003647 oxidation Effects 0.000 description 3
• 238000007254 oxidation reaction Methods 0.000 description 3
• NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 description 3
• FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 3
• RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 3
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