CN101198634A - 具有可接受乙醛产生率的高特性粘度熔体相聚酯聚合物 - Google Patents
具有可接受乙醛产生率的高特性粘度熔体相聚酯聚合物 Download PDFInfo
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- CN101198634A CN101198634A CNA2006800213942A CN200680021394A CN101198634A CN 101198634 A CN101198634 A CN 101198634A CN A2006800213942 A CNA2006800213942 A CN A2006800213942A CN 200680021394 A CN200680021394 A CN 200680021394A CN 101198634 A CN101198634 A CN 101198634A
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- C08G63/78—Preparation processes
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- C08G63/78—Preparation processes
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- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C08G63/82—Preparation processes characterised by the catalyst used
- C08G63/85—Germanium, tin, lead, arsenic, antimony, bismuth, titanium, zirconium, hafnium, vanadium, niobium, tantalum, or compounds thereof
- C08G63/86—Germanium, antimony, or compounds thereof
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- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/88—Post-polymerisation treatment
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- B29B9/16—Auxiliary treatment of granules
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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Abstract
Description
阶段 | 时间(min.) | 温度C° | 真空(torr) | 搅拌速度(rpm) |
1 | 0.1 | 285 | 730 | 0 |
2 | 10 | 285 | 730 | 150* |
3 | 2 | 285 | 140* | 300* |
4 | 1 | 285 | 140 | 300 |
5 | 10 | 285 | 51* | 300 |
6 | 5 | 285 | 51 | 300 |
7 | 1 | 285 | 4.5* | 300 |
8 | 20 | 285 | 4.5 | 300 |
9 | 2 | 285 | 0.8* | 30* |
10 | 500# | 285 | 0.8 | 30 |
样品# | 整理机时间(min) | XRFSb(ppm) | XRFP(ppm) | IhV(dL/g) | ItV(dL/g) | L*颜色 | b*颜色 | 游离AA(ppm) | AA产生率295/5(ppm) |
56 | 60.67 | 239 | 2 | 0.761 | 0.802 | 78.81 | 4.37 | 22.79 | 26.42 |
58 | 54.78 | 242 | 2 | 0.762 | 0.803 | 80.43 | 4.52 | 22.48 | 25.96 |
CB-12 | . | . | . | . | . | . | . | 1.06 | 20.08 |
阶段 | 时间(min) | 温度C° | 真空torr | 搅拌速度rpm |
1 | 0.1 | 285 | 730 | 0 |
2 | 10 | 285 | 730 | 150* |
3 | 2 | 285 | 140* | 300* |
4 | 1 | 285 | 140 | 300 |
5 | 10 | 285 | 51* | 300 |
6 | 5 | 285 | 51 | 300 |
7 | 1 | 285 | 4.5* | 300 |
8 | 20 | 285 | 4.5 | 300 |
9 | 2 | 285 | 0.8* | 30* |
10 | 58 | 285 | 0.8 | 30 |
11 | 3 | 285 | 650* | 30 |
12 | 2 | 285 | 650 | 30 |
13 | 1 | 285 | 0.5* | 45* |
14 | 5 | 285 | 0.5 | 45 |
样品# | 添加剂 | XRFSbppm | XRFPppm | P∶Sb摩尔比 | IhV | ItV | L*颜色 | b*颜色 | 游离AA(ppm) | 游离AA**的降低% | AA产生率295/5(ppm) | AA产生率**的降低% |
CB-12 | 1.06 | 20.08 | ||||||||||
70 | 无 | 243 | 2 | 0 | 0.84 | 0.891 | 76.44 | 4.6 | 22.08 | 3.5 | 25.3 | 1.2 |
71 | 无 | 243 | 1 | 0 | 0.83 | 0.88 | 79.7 | 4.44 | 24.74 | -8.2 | 25.76 | -0.6 |
64 | n.d.* | 244 | 3 | 0 | 0.833 | 0.883 | 79.09 | 5.41 | 21.78 | 4.7 | 25.73 | -0.5 |
61 | H3PO4 | 247 | 93 | 1.5 | 0.808 | 0.855 | 77.39 | 4.28 | 14.97 | 34.5 | 15.1 | 41.0 |
56 | H3PO4 | 243 | 129 | 2.1 | 0.761 | 0.791 | 78.83 | 3.94 | 10.59 | 53.7 | 17 | 33.6 |
67 | OPT | 246 | 34 | 0.5 | 0.843 | 0.894 | 78.79 | 3.9 | 21.46 | 6.2 | 24.88 | 2.8 |
65 | OPT | 246 | 67 | 1.1 | 0.814 | 0.862 | 80.26 | 4.08 | 20.09 | 12.2 | 16.47 | 35.7 |
63 | OPT | 246 | 109 | 1.7 | 0.799 | 0.845 | 80.35 | 4.42 | 17.89 | 21.8 | 22.1 | 13.7 |
样品# | 整理机时间(min) | XRFSb | XRF P | IhV | ItV | L*颜色 | b*颜色 |
(min) | (ppm) | (ppm) | (dL/g) | (dL/g) | CIELAB | CIELAB | |
1 | 77 | 235 | 1 | 0.788 | 0.832 | 79.7 | 3.41 |
2 | 84 | 238 | 1 | 0.807 | 0.854 | 78.78 | 2.88 |
6 | 67 | 240 | 2 | 0.783 | 0.827 | 81.58 | 4.13 |
8 | 92 | 233 | 1 | 0.821 | 0.87 | 78.35 | 4.97 |
样品# | 添加剂 | XRFSb | XRFP | P∶Sb摩尔比 | IhV | ItV | L*颜色 | b*颜色 | 游离AA | 游离AA的降低% | AA产生率295/5 | AA产生率的-降低% |
(ppm) | (ppm) | (dL/g) | (dL/9) | (ppm) | (ppm) | |||||||
CB-12 | 0.7 | 20.73 | ||||||||||
10 | None | 243 | 1 | 0.0 | 0.855 | 0.908 | 78.22 | 3.96 | 29.55 | -2.9 | 28.65 | -8.0 |
28 | None | 239 | 2 | 0.0 | 0.835 | 0.885 | 76.94 | 3.52 | 29.02 | -1.0 | 23.78 | 10.3 |
46 | None | 237 | 2 | 0.0 | 0.839 | 0.89 | 77.14 | 2.83 | 27.6 | 3.9 | 27.13 | -2.3 |
34 | H3PO4 | 236 | 65 | 1.1 | 0.779 | 0.822 | 76.03 | 2.93 | 16.89 | 41.2 | 19.39 | 26.9 |
20 | H3PO4 | 239 | 85 | 1.4 | 0.844 | 0.896 | 74.74 | 3.52 | 20.42 | 28.9 | 15.45 | 41.7 |
42 | H3PO4 | 241 | 95 | 1.5 | 0.805 | 0.852 | 77.86 | 2.59 | 14.37 | 50.0 | 17.03 | 35.8 |
30 | H3PO4 | 243 | 103 | 1.7 | 0.784 | 0.828 | 75.85 | 5.25 | 15.27 | 46.8 | 16.85 | 36.5 |
24 | H3PO4 | 232 | 133 | 2.3 | 0.769 | 0.811 | 77.53 | 3.68 | 14.48 | 49.6 | 17 | 35.9 |
38 | H3PO4 | 236 | 146 | 2.4 | 0.8 | 0.846 | 79.92 | 5.93 | 14.38 | 49.9 | 14.04 | 47.6 |
22 | OPT | 234 | 21 | 0.4 | 0.826 | 0.875 | 77.39 | 3.04 | 17.17 | 40.2 | 22.32 | 15.8 |
40 | OPT | 225 | 61 | 1.1 | 0.808 | 0.855 | 79.1 | 3.01 | 21.61 | 24.8 | 21.18 | 20.1 |
26 | OPT | 238 | 65 | 1.1 | 0.812 | 0.859 | 77.81 | 2.85 | 21.49 | 25.2 | 22.68 | 14.5 |
44 | OPT | 237 | 93 | 1.5 | 0.796 | 0.841 | 78.12 | 2.91 | 17.94 | 37.5 | 14.99 | 43.5 |
36 | OPT | 238 | 96 | 1.6 | 0.821 | 0.87 | 79.12 | 2.59 | 21.54 | 25.0 | 22.18 | 16.4 |
32 | OPT | 241 | 130 | 2.1 | 0.799 | 0.845 | 77.26 | 4.35 | 14.65 | 49.0 | 19.34 | 27.1 |
样品# | 添加剂 | 处理 | 游离AA(ppm) |
CB-12 | 无 | 0.74 | |
20 | H3PO4 | 无 | 7.18 |
20 | H3PO4 | 烘箱 | 0.97 |
样品# | 添加剂 | 混合并 | IhV | ItV | XRFSb | XRFP | L*颜色 | b*颜色 | 游离 | AA产生率 |
挤塑的 | (dL/g) | (dL/g) | (ppm) | (ppm) | AA(ppm) | 295/5(ppm) | ||||
147-4 | 无 | 否 | 0.75 | 0.79 | 248 | 8 | 83.62 | -1.76 | 0.32 | 16.195 |
147-1 | 无 | 是 | 0.676 | 0.708 | 250 | 8 | 61.49 | 0.81 | 12.18 | 21 |
147-2 | OPT | 是 | 0.645 | 0.674 | 246 | 97 | 59.22 | 0.41 | 14.34 | 17.39 |
147-3 | H3PO4 | 是 | 0.647 | 0.676 | 243 | 107 | 59.20 | 0.09 | 11.72 | 10.8 |
CB-12 | 0.75 | 17.57 |
阶段 | 时间Min. | 温度℃ | 真空Torr | 搅拌速度RPM |
1 | .1 | 270 | 730 | 0 |
2 | 5 | 270 | 730 | 0 |
3 | 5 | 270 | 730 | 0 |
4 | 5 | 270 | 730 | 15* |
5 | 4 | 270 | 730 | 35* |
6 | 2 | 270 | 730 | 75* |
7 | 5 | 270 | 730 | 75 |
样品# | 添加剂 | XRFSb | XRF P | IhV | ItV | 游离AA | AA产生率 | L* | b* |
(ppm) | (ppm) | (dL/g) | (dL/g) | (ppm) | 295/5(ppm) | 颜色 | 颜色 | ||
11 | 无 | 201 | 12 | 0.763 | 0.8 | 11.58 | 21.87 | 84.28 | 0.34 |
14 | H3PO4 | 199 | 92 | 0.729 | 0.76 | 7.85 | 13.01 | 84.17 | 0.07 |
CB-12 | 0.84 | 22.63 |
分类 | 红调色剂(ppm) | 蓝调色剂(ppm) | XRF P(ppm) | ItV(dL/g) | 游离AA(ppm) | AA产生率295/5(ppm) | L*颜色 | b*颜色 |
Sb | 6.29 | 12.58 | 87 | 0.848 | 14.51 | 11.54 | 74.3 | -2.9 |
CB-12 | 0.84 | 18.64 |
样品# | 添加剂 | 螺杆速度(rpm) | 大致时间(min) | IhV(dL/g) | ItV(dL/g) | XRFSb(ppm) | XRFP(ppm | 旧L*颜色 | 旧b*颜色 | 游离AA(ppm) | AA产生率295/5(ppm) |
干燥的 | 无 | 0 | 0 | 0.761 | 0.802 | 248 | 8 | 81.14 | -1.98 | 0.24 | 18.61 |
2 | 无 | 80 | 1 | 0.711 | 0.747 | 250 | 8 | 57.9 | 1.22 | 5.49 | 22.54 |
17 | 无 | 80 | 1 | 0.692 | 0.726 | 240 | 8 | 58.44 | 0.44 | 3.1 | 21.77 |
3 | 无 | 35 | 2.1 | 0.681 | 0.714 | 251 | 9 | 60.03 | 1.46 | 9.35 | 24.07 |
18 | 无 | 35 | 2.1 | 0.689 | 0.722 | 240 | 8 | 59.96 | 0.86 | 24.15 | |
18B/21 | 无 | 35 | 2.1 | 0.663 | 0.694 | 237 | 8 | 58.93 | 0.66 | 5.74 | 21.39 |
1 | 无 | 20 | 3.3 | 0.672 | 0.704 | 250 | 11 | 61.02 | 2.22 | 22.58 | 29.5 |
16 | 无 | 20 | 3.3 | 0.681 | 0.714 | 236 | 8 | 60.19 | 1.11 | 12.04 | 29.06 |
4 | OPT | 80 | 1 | 0.627 | 0.654 | 247 | 158 | 58.28 | 1.54 | 10.36 | 22.3 |
5 | OPT | 35 | 2.1 | 0.622 | 0.649 | 249 | 167 | 60.1 | 1.09 | 14.42 | 22.89 |
6 | OPT | 20 | 3.3 | 0.624 | 0.651 | 235 | 159 | 61.06 | 1.11 | 21.67 | 24.49 |
9 | PPA | 80 | 1 | 0.665 | 0.696 | 240 | 132 | 52.83 | 2.46 | 11.15 | |
9B/19 | PPA | 80 | 1 | 0.634 | 0.682 | 240 | 132 | 53.35 | 2.29 | 10.15 | 13.71 |
7 | PPA | 35 | 2.1 | 0.672 | 0.704 | 237 | 125 | 57.24 | 1.14 | 11.48 | 12.65 |
8 | PPA | 20 | 3.3 | 0.666 | 0.697 | 238 | 130 | 58.32 | 1.66 | 15.52 | 12.38 |
11 | H3PO4 | 80 | 1 | 0.687 | 0.72 | 238 | 97 | 55.39 | 0.13 | 9.12 | 10.46 |
12 | H3PO4 | 35 | 2.1 | 0.648 | 0.677 | 238 | 99 | 58.75 | 0.64 | 10.42 | |
12BC1/23 | H3PO4 | 35 | 2.1 | 0.673 | 0.705 | 248 | 105 | 59.63 | 0.41 | 10.46 | 10.67 |
12BC2/24 | H3PO4 | 35 | 2.1 | 0.657 | 0.687 | 230 | 94 | 59.55 | 0.3 | 10.16 | 11.1 |
10 | H3PO4 | 20 | 3.3 | 0.634 | 0.662 | 234 | 97 | 59.83 | 0.79 | 13.37 | 11.43 |
13 | 水 | 80 | 1 | 0.722 | 0.759 | 233 | 11 | 57.97 | 0.72 | 2.87 | 18.47 |
14 | 水 | 35 | 2.1 | 0.706 | 0.741 | 240 | 9 | 59.21 | 1.11 | 6.21 | 22.73 |
15 | 水 | 20 | 3.3 | 0.672 | 0.704 | 240 | 8 | 60.16 | 1.31 | 27.79 | |
15B/20 | 水 | 20 | 3.3 | 0.685 | 0.718 | 227 | 8 | 61.3 | 1.16 | 11.85 | 25.13 |
CB-121st | 0 | 0 | 0.797 | 0.843 | 0.77 | 22.12 | |||||
CB-12后一个 | 0 | 0 | 0.788 | 0.832 | 0.79 | 22.32 |
样品# | 添加剂 | XRFSb | XRFP | P∶Sb摩尔比 | IhV(dL/g) | It=V(dL/g) | L* | b* | 游离AA(ppm) | 游离AA的降低% | AA产生率295/5(ppm) | AA产生率的降低% |
070 | 无 | 261 | 3 | 0 | 0.777 | 0.82 | 84.69 | 3.67 | 13.23 | 1 | 20.38 | 5.5 |
093 | 无 | 265 | 2 | 0 | 0.756 | 0.797 | 82.33 | 2.29 | 13.95 | -4.4 | 20.765 | 3.7 |
17 | 无 | 244 | 4 | 0.1 | 0.77 | 0.812 | 82.42 | 2.19 | 14.345 | -7.3 | 22.265 | -3.2 |
122 | 无 | 258 | 3 | 0 | 0.767 | 0.809 | 82.13 | 2.8 | 11.94 | 10.7 | 22.85 | -6.0 |
113 | H3PO4 | 246 | 86 | 1.4 | 0.767 | 0.809 | 83.04 | 3.1 | 8.37 | 37.4 | 14.82 | 31.3 |
112 | H3PO4 | 255 | 199 | 3.1 | 0.708 | 0.743 | 81.3 | 2.57 | 7.765 | 41.9 | 18.135 | 15.9 |
116 | H3PO4 | 249 | 300 | 4.7 | 0.653 | 0.683 | 82.98 | 3.31 | 8.52 | 36.3 | 18.885 | 12.4 |
083 | OPT | 265 | 89 | 1.3 | 0.74 | 0.779 | 81.67 | 3.78 | 12.395 | 7.3 | 19.63 | 9.0 |
115 | OPT | 247 | 179 | 2.8 | 0.74 | 0.779 | 82.17 | 2.04 | 10.69 | 20 | 20.985 | 2.7 |
085 | OPT | 264 | 257 | 3.8 | 0.713 | 0.749 | 82.76 | 2.27 | 12.105 | 9.4 | 23.69 | -9.9 |
132 | OPT | 266 | 278 | 4.1 | 0.684 | 0.717 | 83.69 | 2.56 | 12.815 | 4.1 | 23.84 | -10.5 |
087 | TBP | 252 | 36 | 0.6 | 0.765 | 0.807 | 80.24 | 2.68 | 11.93 | 10.7 | 22.675 | -5.1 |
118 | TBP | 260 | 15 | 0.2 | 0.781 | 0.825 | 82.54 | 3.28 | 13.65 | -2.1 | 21.36 | 1.0 |
091 | 水 | 258 | 3 | 0.0 | 0.741 | 0.78 | 80.07 | 2.32 | 10.9 | 18.4 | 23.74 | -10.1 |
114 | 水 | 265 | 3 | 0 | 0.759 | 0.8 | 81.05 | 2.04 | 13.31 | 0.4 | 20.745 | 3.8 |
CB-12 | 0.79 | 18.28 |
起始原料 | 固态时间(h) | 添加剂 | IhV(dL/g) | ItV(dL/g) |
11 | 0 | 89ppm P,来自H3PO4 | 0.69 | 0.723 |
11 | 1 | 89ppm P,来自H3PO4 | 0.686 | 0.719 |
11 | 2 | 89ppm P,来自H3PO4 | 0.696 | 0.73 |
11 | 3 | 89ppm P,来自H3PO4 | 0.703 | 0.738 |
11 | 4 | 89ppm P,来自H3PO4 | 0.714 | 0.75 |
11 | 6 | 89ppm P,来自H3PO4 | 0.742 | 0.781 |
11 | 8 | 89ppm P,来自H3PO4 | 0.76 | 0.801 |
11 | 10 | 89ppm P,来自H3PO4 | 0.784 | 0.828 |
11 | 12 | 89ppm P,来自H3PO4 | 0.797 | 0.843 |
17 | 0 | 无 | 0.712 | 0.748 |
17 | 1 | 无 | 0.736 | 0.774 |
17 | 2 | 无 | 0.771 | 0.813 |
17 | 3 | 无 | 0.788 | 0.832 |
17 | 4 | 无 | 0.837 | 0.888 |
17 | 6 | 无 | 0.867 | 0.922 |
17 | 8 | 无 | 0.897 | 0.956 |
17 | 10 | 无 | 0.981 | 1.052 |
17 | 12 | 无 | 1.014 | 1.091 |
11 | 0 | 89ppm P,来自H3PO4 | 0.684 | 0.717 |
11 | 1 | 89ppm P,来自H3PO4 | 0.684 | 0.717 |
11 | 2 | 89ppm P,来自H3PO4 | 0.697 | 0.731 |
11 | 3 | 89ppm P,来自H3PO4 | 0.707 | 0.742 |
11 | 4 | 89ppm P,来自H3PO4 | 0.717 | 0.753 |
11 | 6 | 89ppm P,来自H3PO4 | 0.744 | 0.783 |
11 | 8 | 89ppm P,来自H3PO4 | 0.767 | 0.809 |
11 | 10 | 89ppm P,来自H3PO4 | 0.773 | 0.816 |
11 | 12 | 89ppm P,来自H3PO4 | 0.8 | 0.846 |
17 | 0 | 无 | 0.715 | 0.751 |
17 | 1 | 无 | 0.737 | 0.776 |
17 | 2 | 无 | 0.784 | 0.828 |
17 | 3 | 无 | 0.792 | 0.838 |
17 | 4 | 无 | 0.827 | 0.879 |
17 | 6 | 无 | 0.888 | 0.945 |
17 | 8 | 无 | 0.952 | 1.019 |
17 | 10 | 无 | 0.976 | 1.047 |
17 | 12 | 无 | 1.025 | 1.103 |
样品 | 催化剂体系 | 添加剂 | XRFSb(ppm) | XRFP(ppm) | IhV1(dL/g) | ItV(dL/g) | 游离AA(ppm) | AA产生率295/5(ppm) |
CB-12 | (ppm) | 0.87 | 20.52 | |||||
44 | 230 Sb&8 P | 无 | 246 | 7 | 0.758 | 0.799 | 8.03 | 17.37 |
45 | 230 Sb&8 P | H3PO4 | 245 | 55 | 0.747 | 0.787 | 5.48 | 11.98 |
46 | 230 Sb&55 P | 无 | 226 | 55 | 0.735 | 0.773 | 9.28 | 20.19 |
47 | 230 Sb&8 P | H3PO4 | 246 | 81 | 0.734 | 0.772 | 4.27 | 9.58 |
48 | 230Sb&55 P | H3PO4 | 229 | 120 | 0.729 | 0.767 | 7.99 | 18.48 |
49 | 230 Sb&8 P | H3PO4 | 243 | 94 | 0.726 | 0.763 | 4.17 | 11.12 |
50 | 230Sb&55 P | 无 | 231 | 56 | 0.737 | 0.776 | 10.74 | 22.41 |
55 | 230 Sb&55 P | H3PO4 | 231 | 138 | 0.717 | 0.753 | 6.37 | 15.94 |
52 | 230 Sb&8 P | 无 | 243 | 7 | 0.761 | 0.802 | 9.01 | 17.23 |
Claims (96)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US11/154,208 | 2005-06-16 | ||
US11/154,208 US8557950B2 (en) | 2005-06-16 | 2005-06-16 | High intrinsic viscosity melt phase polyester polymers with acceptable acetaldehyde generation rates |
PCT/US2006/023207 WO2006138406A2 (en) | 2005-06-16 | 2006-06-14 | High intrinsic viscosity melt phase polyester polymers with acceptable acetaldehyde generation rates |
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CN101198634B CN101198634B (zh) | 2011-05-25 |
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US (2) | US8557950B2 (zh) |
EP (1) | EP1891130B1 (zh) |
JP (2) | JP5307537B2 (zh) |
KR (1) | KR101317315B1 (zh) |
CN (1) | CN101198634B (zh) |
AR (1) | AR056383A1 (zh) |
BR (1) | BRPI0612239B1 (zh) |
CA (1) | CA2611949C (zh) |
ES (1) | ES2411681T3 (zh) |
MX (2) | MX363446B (zh) |
MY (1) | MY156241A (zh) |
PL (1) | PL1891130T3 (zh) |
PT (1) | PT1891130E (zh) |
RU (1) | RU2402575C2 (zh) |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN113512184A (zh) * | 2020-04-09 | 2021-10-19 | 中国石油化工股份有限公司 | 一种低乙醛瓶坯聚酯的生产方法及装置 |
CN113512184B (zh) * | 2020-04-09 | 2022-11-08 | 中国石油化工股份有限公司 | 一种低乙醛瓶坯聚酯的生产方法及装置 |
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MY156241A (en) | 2016-01-29 |
US20060287472A1 (en) | 2006-12-21 |
TW200704673A (en) | 2007-02-01 |
US8987408B2 (en) | 2015-03-24 |
BRPI0612239A2 (pt) | 2011-01-04 |
EP1891130A2 (en) | 2008-02-27 |
WO2006138406A3 (en) | 2007-03-29 |
PL1891130T3 (pl) | 2013-11-29 |
JP2013144811A (ja) | 2013-07-25 |
US8557950B2 (en) | 2013-10-15 |
EP1891130B1 (en) | 2013-05-08 |
CA2611949A1 (en) | 2006-12-28 |
RU2402575C2 (ru) | 2010-10-27 |
RU2008101675A (ru) | 2009-07-27 |
CA2611949C (en) | 2012-05-15 |
MX2007015306A (es) | 2008-02-21 |
WO2006138406A2 (en) | 2006-12-28 |
ES2411681T3 (es) | 2013-07-08 |
TWI429680B (zh) | 2014-03-11 |
EP1891130A4 (en) | 2009-08-05 |
JP5307537B2 (ja) | 2013-10-02 |
AR056383A1 (es) | 2007-10-10 |
KR101317315B1 (ko) | 2013-10-11 |
JP5695118B2 (ja) | 2015-04-01 |
JP2008544045A (ja) | 2008-12-04 |
US20140021652A1 (en) | 2014-01-23 |
KR20080019229A (ko) | 2008-03-03 |
PT1891130E (pt) | 2013-07-29 |
MX363446B (es) | 2019-03-22 |
CN101198634B (zh) | 2011-05-25 |
BRPI0612239B1 (pt) | 2017-04-25 |
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