KR101130871B1 - 파이프 반응기를 이용한 폴리에스터 제조 방법 - Google Patents

파이프 반응기를 이용한 폴리에스터 제조 방법 Download PDF

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KR101130871B1
KR101130871B1 KR1020057023136A KR20057023136A KR101130871B1 KR 101130871 B1 KR101130871 B1 KR 101130871B1 KR 1020057023136 A KR1020057023136 A KR 1020057023136A KR 20057023136 A KR20057023136 A KR 20057023136A KR 101130871 B1 KR101130871 B1 KR 101130871B1
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pipe
polyester
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outlet
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Korean (ko)
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KR20060012660A (ko
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브루스 로저 데브루인
리차드 길 보너
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이스트만 케미칼 컴파니
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Assigned to 그루포 페트로테멕스 에스.에이. 데 씨.브이. reassignment 그루포 페트로테멕스 에스.에이. 데 씨.브이. 권리의 전부이전등록 Assignors: 이스트만 케미칼 컴파니
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/785—Preparation processes characterised by the apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/81—Preparation processes using solvents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181—Acids containing aromatic rings
    • C08G63/183—Terephthalic acids

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
KR1020057023136A 2003-06-06 2004-05-26 파이프 반응기를 이용한 폴리에스터 제조 방법 Expired - Lifetime KR101130871B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/456,309 2003-06-06
US10/456,309 US7135541B2 (en) 2003-06-06 2003-06-06 Polyester process using a pipe reactor
PCT/US2004/016465 WO2005000461A1 (en) 2003-06-06 2004-05-26 Polyester process using a pipe reactor

Publications (2)

Publication Number Publication Date
KR20060012660A KR20060012660A (ko) 2006-02-08
KR101130871B1 true KR101130871B1 (ko) 2012-03-28

Family

ID=33490133

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020057023136A Expired - Lifetime KR101130871B1 (ko) 2003-06-06 2004-05-26 파이프 반응기를 이용한 폴리에스터 제조 방법

Country Status (17)

Country Link
US (1) US7135541B2 (https=)
EP (1) EP1631379B1 (https=)
JP (1) JP4938446B2 (https=)
KR (1) KR101130871B1 (https=)
CN (1) CN100512948C (https=)
AR (1) AR044620A1 (https=)
BR (1) BRPI0410976B1 (https=)
CA (1) CA2527018C (https=)
ES (1) ES2483899T3 (https=)
MX (1) MXPA05013165A (https=)
MY (1) MY141971A (https=)
PL (1) PL1631379T3 (https=)
PT (1) PT1631379E (https=)
RU (1) RU2342406C2 (https=)
SI (1) SI1631379T1 (https=)
TW (1) TWI351413B (https=)
WO (1) WO2005000461A1 (https=)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6906164B2 (en) 2000-12-07 2005-06-14 Eastman Chemical Company Polyester process using a pipe reactor
US7332548B2 (en) 2004-03-04 2008-02-19 Eastman Chemical Company Process for production of a polyester product from alkylene oxide and carboxylic acid
US7943094B2 (en) * 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
US7649109B2 (en) 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
US7863477B2 (en) 2007-03-08 2011-01-04 Eastman Chemical Company Polyester production system employing hot paste to esterification zone
US7829653B2 (en) 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor
US7872089B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Multi-level tubular reactor with internal tray
US7858730B2 (en) 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
US7842777B2 (en) 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US7868129B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Sloped tubular reactor with spaced sequential trays
US7847053B2 (en) 2007-07-12 2010-12-07 Eastman Chemical Company Multi-level tubular reactor with oppositely extending segments
US7872090B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Reactor system with optimized heating and phase separation
US7868130B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Multi-level tubular reactor with vertically spaced segments
DE102009016819B4 (de) * 2009-04-09 2011-12-15 Carl Zeiss Optronics Gmbh Verfahren zur Detektion wenigstens eines Objekts und/oder wenigstens einer Objektgruppe, Computerprogramm, Computerprogammprodukt, Stereokameraeinrichtung, aktiv Strahlung aussendendes Bildsensorsystem und Überwachungsvorrichtung
CN112023852B (zh) * 2019-06-03 2023-05-09 中国石油化工股份有限公司 一种苯部分加氢制备环己烯的生产装置

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002046266A2 (en) * 2000-12-07 2002-06-13 Eastman Chemical Company Low cost polyester process using a pipe reactor

Family Cites Families (246)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2905707A (en) 1959-09-22 Production of bis
GB115812A (en) 1915-08-30 1919-04-10 Charles Franklin Kettering Improvements in Ignition Systems for Internal Combustion Engines.
US2361717A (en) 1940-09-12 1944-10-31 Du Pont Process for making polyamides
US2753249A (en) 1950-10-06 1956-07-03 Exxon Research Engineering Co Catalytic polymerization apparatus
US2709642A (en) 1951-12-03 1955-05-31 Exxon Research Engineering Co Chemical reactor
US2973341A (en) 1956-01-25 1961-02-28 Glanzstoff Ag Continuous process for production of a polyethylene terephthalate condensate
NL108873C (https=) 1957-01-17
US2829153A (en) 1957-03-04 1958-04-01 Du Pont Continuous ester interchange process
NL96710C (https=) 1957-09-28
US3254965A (en) 1958-11-28 1966-06-07 Phillips Petroleum Co Polymerization control apparatus
US3113843A (en) 1959-01-27 1963-12-10 Du Pont Apparatus for separating a vapor from a viscous material such as molten polymer
US3192184A (en) 1959-03-19 1965-06-29 Du Pont Prepolymerization process
NL255414A (https=) 1959-08-31
US3052711A (en) 1960-04-20 1962-09-04 Du Pont Production of di(beta-hydroxyethyl) terephthalate
US3110547A (en) 1961-07-26 1963-11-12 Du Pont Polymerization process
US3161710A (en) 1961-07-27 1964-12-15 Du Pont Polymerization process for polyester films
GB988548A (en) 1961-08-30 1965-04-07 Goodyear Tire & Rubber Method for preparing polyester resins
BE634031A (https=) 1962-06-23
NL130338C (https=) 1963-06-11 1900-01-01
US3241926A (en) 1963-11-15 1966-03-22 Monsanto Co Apparatus for continuously polycondensing polymethylene glycol esters of aromatic dicarboxylic acids
NO116966B (https=) 1964-06-01 1969-06-16 Consanto Co
DE1240286B (de) 1965-01-02 1967-05-11 Basf Ag Verfahren zur kontinuierlichen Emulsions-polymerisation olefinisch ungesaettigter Verbindungen
NL131998C (https=) 1965-06-09
US3442868A (en) 1965-07-20 1969-05-06 Teijin Ltd Novel process for the preparation of polyester
CH487345A (de) 1965-11-11 1970-03-15 Karl Fischer App Und Rohrleitu Verfahren zur Förderung eines dampfförmigen Stoffes und Anwendung dieses Verfahrens
ES337977A1 (es) 1966-03-23 1968-03-16 Fiber Industries Inc Un procedimiento para la produccion de polimeros lineales de bajo peso molecular de acido tereftalico y etilenglicol.
US3496220A (en) 1966-04-04 1970-02-17 Mobil Oil Corp Esterification process
GB1111815A (en) 1966-04-22 1968-05-01 Ici Ltd Polyester preparation
CH465875A (de) 1966-09-16 1968-11-30 Inventa Ag Verfahren zur kontinuierlichen Herstellung von Polyestern
US3590072A (en) 1966-11-18 1971-06-29 Monsanto Co Method for direct esterification of terephthalic acid with ethylene glycol
US3639448A (en) 1966-12-30 1972-02-01 Mitsubishi Chem Ind Process for producing bis(beta-hydroxyethyl)-terephthalate and/or prepolymer thereof
US3487049A (en) 1967-01-04 1969-12-30 Du Pont Process for producing polyethylene terephthalate
US3522214A (en) 1967-04-13 1970-07-28 Mobil Oil Corp Process and apparatus for polymerizing liquids
GB1154538A (en) 1967-04-19 1969-06-11 Mobil Oil Corp Esterifying Viscous Reaction Mixtures
US3595846A (en) 1967-05-02 1971-07-27 Michelin & Cie Continuous chemical reactions
US3497743A (en) 1967-06-16 1970-02-24 United Aircraft Corp Annular multiple beam contoured cathode device
US3496146A (en) 1967-08-23 1970-02-17 Du Pont Preparation of glycol terephthalate linear polyester by direct esterification of terephthalic acid
US4020049A (en) 1967-09-14 1977-04-26 The Goodyear Tire & Rubber Company Process for preparing polyester resin
US3551396A (en) 1968-01-05 1970-12-29 Gulf Oil Canada Ltd Continuous vinyl polymerization process
NL6809754A (https=) 1968-04-11 1969-10-14
US3609125A (en) 1968-04-24 1971-09-28 Asahi Chemical Ind Polyesterification process and apparatus
FR1583867A (https=) 1968-05-15 1969-12-05
US3590070A (en) 1968-06-03 1971-06-29 Celanese Corp Recycle of terephthalic acid in the production of a bis(2-hydroxyalkyl) terephthalate
US3651125A (en) 1968-08-12 1972-03-21 Eastman Kodak Co Continuous method for formation of a liquid monomer for a condensation polymer
US3646102A (en) 1968-08-28 1972-02-29 Idemitsu Kosan Co Method for continuously preparing polycarbonate oligomer
NL160174C (nl) 1968-12-12 1979-10-15 Snia Viscosa Inrichting voor het volumetrisch afvoeren van een viskeuze vloeistof uit een ruimte voor het continu behandelen van polymeren.
CH521400A (de) 1969-01-24 1972-04-15 Inventa Ag Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polylactamen
US3697579A (en) 1969-09-18 1972-10-10 Allied Chem Method of esterifying a polycarboxylic acid with a glycol
US3689461A (en) 1969-09-18 1972-09-05 Allied Chem Process for the preparation of linear condensation polyesters
BE759208A (fr) 1969-11-22 1971-05-21 Basf Ag Procede de preparation continue de
US3644096A (en) 1970-03-30 1972-02-22 Eastman Kodak Co Apparatus for use in a continuous flow reaction for producing a monomer and/or a protopolymer
US3684459A (en) 1970-08-20 1972-08-15 Phillips Fibers Corp Plug metered evaporative reaction tube
NL7016364A (https=) 1970-10-21 1972-04-25
GB1380266A (en) 1971-05-21 1975-01-08 Agfa Gevaert Process for the semi-continuous preparation of high-molecular weight linear polyesters
DE2145761C3 (de) 1971-09-14 1978-06-15 Davy International Ag, 6000 Frankfurt Verfahren zur Einführung pulverförmiger Terephthalsäure in ein Reaktionsgemisch aus teilweise mit Diolen veresterter Terephthalsäure
US3740267A (en) 1971-09-22 1973-06-19 Allied Chem Method of cleaning apparatus used in processing polyethylene terephthalate
US3819585A (en) 1971-09-30 1974-06-25 Monsanto Co Polyester esterification under two different pressures
GB1395551A (en) 1971-12-29 1975-05-29 Kanebo Ltd Method of producing polyesters
DE2200832A1 (de) 1972-01-08 1973-07-12 Schwarza Chemiefaser Verfahren zur kontinuierlichen herstellung von oligomeren des bis - (betahydroxyaethyl) - terephthalates
FR2168990A1 (en) 1972-01-28 1973-09-07 Schwarza Chemiefaser Bis-(beta-hydroxyethyl) terephthalate oligomers prodn - by continuous reaction in stirred still and flow tube
BE780142A (en) 1972-03-02 1972-09-04 Sandoz Sa Polyester prepn - by solid phase condensation in heated tubular reactors under vacuum with opt heated transport screws
JPS4894795A (https=) 1972-03-18 1973-12-06
DE2227091A1 (de) 1972-06-03 1973-12-13 Davy Ashmore Ag Verfahren zur herstellung von hochpolymeren, insbesondere spinnfaehigen, polyestermassen
JPS5534822B2 (https=) 1972-07-14 1980-09-09
ZA734645B (en) * 1972-07-21 1974-04-24 Ici Ltd Manufacture of polyesters
JPS537477B2 (https=) 1972-07-31 1978-03-17
US4100142A (en) 1972-09-13 1978-07-11 Fiber Industries, Inc. Polyester process and product
JPS49105893A (https=) 1973-02-07 1974-10-07
GB1474524A (https=) 1973-07-06 1977-05-25
US3927983A (en) 1973-09-19 1975-12-23 Monsanto Co Continuous staged isobaric stirred polymerization apparatus
GB1486409A (en) 1973-11-06 1977-09-21 Agfa Gevaert Process for the preparation of high-molecular weight polyesters
JPS5082197A (https=) 1973-11-21 1975-07-03
CA1024294A (en) 1974-02-27 1978-01-10 Du Pont Of Canada Limited Control in preparing polyamides by continuous polymerization
US4077945A (en) 1974-03-23 1978-03-07 Zimmer Aktiengesellschaft Process for making linear polyesters from ethylene glycol and terephthalic acid
JPS5129460A (en) 1974-09-02 1976-03-12 Asahi Chemical Ind Esuterukahoho narabini sochi
DE2443566A1 (de) 1974-09-12 1976-04-01 Basf Ag Verfahren zum kontinuierlichen herstellen von polyamiden
DE2504258A1 (de) 1975-02-01 1976-08-05 Dynamit Nobel Ag Verfahren und apparatur zur herstellung von oligomeren alkylenterephthalaten
JPS51100036A (ja) 1975-03-03 1976-09-03 Mitsubishi Rayon Co Esuterukahoho
FR2302778A1 (fr) 1975-03-05 1976-10-01 Rhone Poulenc Ind Appareil et procede de preparation de polyesters
DE2514116C3 (de) 1975-03-29 1983-03-17 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen Herstellung von linearen, hochmolekularen Polybutylenterephthalaten
JPS51127031A (en) 1975-04-23 1976-11-05 Fuji Photo Film Co Ltd Preparation of polyethylene terephthalate
JPS51136788A (en) 1975-05-21 1976-11-26 Kuraray Co Ltd Continuo us process for preparing polyester using terephthalic acid
JPS51136789A (en) 1975-05-21 1976-11-26 Kuraray Co Ltd Continuous process for preparing polyest er using terephthalic acid
US4028307A (en) 1975-05-30 1977-06-07 Fiber Industries, Inc. Preparation of polyesters using salts of substituted quaternary ammonium bases
JPS5251495A (en) 1975-10-23 1977-04-25 Mitsubishi Chem Ind Ltd A continuous process for preparing polyester
US4118582A (en) 1975-10-28 1978-10-03 E. I. Du Pont De Nemours And Company Purification of spent ethylene glycol
JPS5271432A (en) 1975-12-09 1977-06-14 Teijin Ltd Cntinuus feeding of terephthalic acid and alkylene gylcol
JPS5278845A (en) 1975-12-24 1977-07-02 Mitsubishi Rayon Co Ltd Esterification
JPS5827782B2 (ja) 1975-12-30 1983-06-11 東レ株式会社 エステルカホウホウ
DE2559290B2 (de) 1975-12-31 1979-08-02 Davy International Ag, 6000 Frankfurt Verfahren zur kontinuierlichen Herstellung von hochmolekularem PoIyäthylenterephthalat
JPS5833855B2 (ja) 1976-01-12 1983-07-22 東レ株式会社 エステル化方法
US4079046A (en) 1976-06-03 1978-03-14 Monsanto Company, St. Louis, Missouri Multiple polyesterification process
JPS52150496A (en) 1976-06-09 1977-12-14 Mitsubishi Gas Chem Co Inc Preparation of polycaronate oligomers
US4046718A (en) 1976-06-17 1977-09-06 The Dow Chemical Company Polymerization method employing tubular reactor
US4089888A (en) 1976-07-12 1978-05-16 Idemitsu Petrochemical Co. Ltd. Method for producing a polycarbonate oligomer
JPS5331793A (en) 1976-09-06 1978-03-25 Toray Ind Inc Preparation of particle-containing polyester
JPS5334894A (en) 1976-09-14 1978-03-31 Toray Ind Inc Preparation of polyester
US4097468A (en) 1977-03-15 1978-06-27 Allied Chemical Corporation Process for preparing polyesters
US4146729A (en) 1977-04-07 1979-03-27 E. I. Du Pont De Nemours And Company Process for preparing poly(ethylene terephthalate)
US4110316A (en) 1977-04-14 1978-08-29 E. I. Du Pont De Nemours And Company Improved process for preparing poly(ethylene terephthalate)
DE2719967A1 (de) 1977-05-04 1978-11-09 Bayer Ag Kontinuierliches verfahren zur durchfuehrung von stofftransportbedingten reaktionen
GB1558910A (en) 1977-05-04 1980-01-09 Bayer Ag Continuous process for the production of polybutylene terephthalates
IT1097584B (it) 1977-08-24 1985-08-31 Basf Ag Processo ed apparecchio per la preparazione di poliesteri macronolecolari linerai
JPS5441833A (en) 1977-09-02 1979-04-03 Toray Ind Inc Method of esterification
JPS5476535A (en) 1977-11-22 1979-06-19 Toray Ind Inc Esterification
JPS5479242A (en) 1977-12-05 1979-06-25 Teijin Ltd Method of esterification
US4365078A (en) 1977-12-16 1982-12-21 The Goodyear Tire & Rubber Company Process for charging dry terephthalic acid into a reactor
CA1115446A (en) 1977-12-16 1981-12-29 Lawrence E. Shelley Process
JPS6017291B2 (ja) 1978-01-25 1985-05-02 東レ株式会社 ポリエステルの製造方法
JPS54157536A (en) 1978-05-29 1979-12-12 Toray Ind Inc Esterification process
JPS5543128A (en) 1978-09-22 1980-03-26 Toray Ind Inc Production of polyester film with high transparency
JPS55108422A (en) 1979-02-15 1980-08-20 Toray Ind Inc Batch-wise esterification
US4230818A (en) 1979-03-01 1980-10-28 The Goodyear Tire & Rubber Company Reduction of glycol ethers in polyesters
US4254246A (en) 1979-03-26 1981-03-03 Davy International Ag Column system process for polyester plants
JPS55135133A (en) 1979-04-10 1980-10-21 Mitsubishi Chem Ind Ltd Continuous production of polyester
PL127634B1 (en) 1979-05-23 1983-11-30 Inst Chemii Przemyslowej Continuous process for manufacturing polyesters and apparatus therefor
US4238593B1 (en) 1979-06-12 1994-03-22 Goodyear Tire & Rubber Method for production of a high molecular weight polyester prepared from a prepolymer polyester having an optional carboxyl content
US4223124A (en) 1979-06-22 1980-09-16 The Goodyear Tire & Rubber Company Method for producing polyesters containing low amounts of ether by-products
JPS5645704A (en) 1979-09-21 1981-04-25 Hitachi Ltd Method and apparatus for removal of volatile substances from high-viscous substance
BR7906279A (pt) 1979-10-01 1981-04-07 Nippon Ester Co Ltd Apereicoamento em processo continuo para produzir poliester e em processo para produzir uma fibra fiada a partir de polimero de poli(tereftalato de etileno)
US4452956A (en) 1979-11-09 1984-06-05 Union Carbide Corporation Discrete spiral flow imparting device
SU973552A1 (ru) 1980-02-12 1982-11-15 Всесоюзный научно-исследовательский институт синтетических волокон Непрерывный способ получени полиэтилентерефталата
US4289871A (en) 1980-03-27 1981-09-15 Allied Chemical Corporation Method to increase reactor capacity for polycondensation of polyesters
JPS57101A (en) 1980-06-04 1982-01-05 Mitsui Petrochem Ind Ltd Method and apparatus for polymerization
DE3025574A1 (de) 1980-07-05 1982-02-04 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von polyestern
DE3047474C2 (de) * 1980-12-17 1983-05-11 Didier Engineering Gmbh, 4300 Essen Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polyestern
US4499226A (en) 1981-03-20 1985-02-12 The Goodyear Tire & Rubber Company High clarity colorless polyesters
US4346193A (en) 1981-05-04 1982-08-24 Atlantic Richfield Company Continuous process for making star-block copolymers
JPS5823829A (ja) 1981-07-17 1983-02-12 イ−・アイ・デユポン・デ・ニモアス・アンド・カンパニ− 合成重合体仕上げ装置
US4397343A (en) 1981-08-31 1983-08-09 The Coe Manufacturing Co. Log scanning in veneer lathe to determine optimum yield axis
US4410750A (en) 1981-12-14 1983-10-18 Exxon Research And Engineering Co. Preparation of linear olefin products
JPS58129020A (ja) 1982-01-27 1983-08-01 Toray Ind Inc ポリエステルの製造方法
PL136188B1 (en) 1982-04-16 1986-02-28 Inst Chemii Przemyslowej Continuous process for manufacturing polyesters and apparatus therefor
JPS5947226A (ja) 1982-09-09 1984-03-16 Toyobo Co Ltd ポリエステルの製造法
JPS5953530A (ja) 1982-09-22 1984-03-28 Toyobo Co Ltd ポリエステルの製造方法
US4548788A (en) 1982-09-24 1985-10-22 Cosden Technology, Inc. Apparatus for producing styrenic/alkenylnitrile copolymers
US4542196A (en) 1982-09-24 1985-09-17 Cosden Technology, Inc. Process for producing styrenic/alkenylnitrile copolymers
US4550149A (en) 1982-09-24 1985-10-29 Cosden Technology, Inc. Process for producing styrenic/alkenylnitrile copolymers
US4551309A (en) 1982-09-24 1985-11-05 Cosden Technology, Inc. Apparatus for producing styrenic/alkenylnitrile copolymers
US4551510A (en) 1982-09-24 1985-11-05 Cosden Technology, Inc. Process for producing styrenic/alkenylnitrile copolymers
US4555384A (en) 1982-09-24 1985-11-26 Cosden Technology, Inc. Apparatus for producing styrenic/alkenylnitrile copolymers
US4440924A (en) 1982-10-05 1984-04-03 Toyo Boseki Kabushiki Kaisha Process for production of polyester
JPS5968326A (ja) 1982-10-13 1984-04-18 Toyobo Co Ltd ポリエステルの製造法
JPS5971326A (ja) 1982-10-15 1984-04-23 Toyobo Co Ltd ポリエステルの製造法
US4831108A (en) 1983-02-16 1989-05-16 Amoco Corporation Polycondensation process with mean dispersion residence time
JPS6015421A (ja) 1983-07-06 1985-01-26 Nippon Ester Co Ltd ポリエステルの製造方法
JPS6072845A (ja) 1983-09-28 1985-04-24 Nippon Ester Co Ltd テレフタル酸グリコ−ルエステルの連続製造法
JPS60115551A (ja) 1983-11-25 1985-06-22 Nippon Ester Co Ltd エステル化方法
JPS60120839A (ja) 1983-12-02 1985-06-28 Nippon Ester Co Ltd テレフタル酸とエチレングリコ−ルとのスラリ−の連続供給法
JPS60163918A (ja) 1984-02-06 1985-08-26 Toyobo Co Ltd ポリエステルの連続製造方法
JPS60226846A (ja) 1984-04-26 1985-11-12 Nippon Ester Co Ltd エステル化方法
JPH0641513B2 (ja) 1984-11-20 1994-06-01 三菱レイヨン株式会社 ポリエステルの製造法
US4554343A (en) 1984-11-23 1985-11-19 Eastman Kodak Company Process for the production of high molecular weight polyester
US4675377A (en) 1985-03-11 1987-06-23 General Electric Company Process for continuous preparation of polyphenylene oxide in agitated reaction zones
DE3544551C2 (de) 1985-12-17 2002-02-28 Zimmer Ag Verfahren zur kontinuierlichen Herstellung von hochmolekularem Polybutylenterephthalat
JPH06104718B2 (ja) 1986-03-07 1994-12-21 コニカ株式会社 ポリエステルの製造方法
US4670580A (en) 1986-03-31 1987-06-02 Celanese Corporation Process for preparing oligomeric glycol esters of dicarboxylic acids
US4721575A (en) 1986-04-03 1988-01-26 Vertech Treatment Systems, Inc. Method and apparatus for controlled chemical reactions
JPS62292831A (ja) 1986-06-12 1987-12-19 Teijin Ltd ポリエステルの連続重合法
EP0254304B1 (en) 1986-07-25 1994-09-21 Dainippon Ink And Chemicals, Inc. Process for producing high impact styrene resin by continuous bulk polymerization
JP2512491B2 (ja) 1987-08-27 1996-07-03 旭化成工業株式会社 ポリエステルの連続重合方法
JPH0813786B2 (ja) 1987-10-15 1996-02-14 日本エステル株式会社 エステル化方法
DE3820362A1 (de) 1988-06-15 1990-03-15 Basf Ag Verfahren zur kontinuierlichen herstellung von linearen thermoplastischen polyestern
US5041525A (en) 1988-09-30 1991-08-20 E. I. Du Pont De Nemours And Company Process for manufacture of shaped polyethylene terephthalate structures in the presence of molecular sieve catalyst
US5413861A (en) 1988-10-17 1995-05-09 Dextor Corporation Semiconductor device encapsulated with a flame retardant epoxy molding compound
US5194525A (en) 1988-12-12 1993-03-16 Dainippon Ink And Chemicals, Inc. Continuous mass polymerization process for making styrene copolymers
US5162488A (en) 1989-05-22 1992-11-10 Hoechst Celanese Corporation Catalyst system and process for preparing polyethylene terephthalate
JPH03192118A (ja) 1989-12-21 1991-08-22 Toray Ind Inc ポリエステルの製造方法
FR2660663B1 (fr) 1990-04-05 1993-05-21 Rhone Poulenc Fibres Procede pour l'obtention de polyterephtalate d'ethylene modifie, fibres exemptes de boulochage issues du polymere ainsi modifie.
JPH03292323A (ja) 1990-04-10 1991-12-24 Fuji Photo Film Co Ltd ポリエステルの製造方法
US5064935A (en) 1990-08-01 1991-11-12 E. I. Dupont De Nemours And Company Continuous process for preparing poly(butylene terephthalate) oligomer or poly(butylene isophthalate) oligomer
KR940009419B1 (ko) 1991-02-07 1994-10-13 한국과학기술연구원 색조가 우수한 폴리에스테르의 제조방법
EP0501543B1 (en) 1991-02-28 1998-05-20 Agfa-Gevaert N.V. Process for the production of polyesters with increased electroconductivity
DE69214686T2 (de) 1991-02-28 1997-06-05 Agfa Gevaert Nv Verfahren zur Herstellung von Polyestern mit verbesserter thermooxydativer Stabilität
JPH05222180A (ja) 1992-02-17 1993-08-31 Fuji Photo Film Co Ltd ポリエステルの製造法
DE4235785A1 (de) 1992-10-23 1994-05-11 Basf Ag Verfahren und Vorrichtung zur kontinuierlichen Polymerisation
DE4240588A1 (de) 1992-12-03 1994-06-09 Bayer Ag Verfahren zur Herstellung von Polycarbonaten
US5650536A (en) 1992-12-17 1997-07-22 Exxon Chemical Patents Inc. Continuous process for production of functionalized olefins
JP3336658B2 (ja) 1993-02-26 2002-10-21 三菱化学株式会社 テレフタル酸の連続エステル化方法
US5385773A (en) 1993-04-27 1995-01-31 Eastman Chemical Company Copolyester of cyclohexanenedimethanol and process for producing such polyester
US5294305A (en) 1993-05-06 1994-03-15 Mobile Process Technology, Inc. Ethylene glycol recovery process
US5340907A (en) 1993-06-28 1994-08-23 Eastman Chemical Company Copolyester of cyclohexanedimethanol and process for producing such polyester
JP3309502B2 (ja) 1993-07-12 2002-07-29 大日本インキ化学工業株式会社 生分解性ポリエステル系ポリマーの連続製造法
US5411665A (en) 1993-07-20 1995-05-02 Scraggs; Charles R. Methods for reducing and separating emulsions and homogeneous components from contaminated water
US5599900A (en) 1993-10-18 1997-02-04 E. I. Du Pont De Nemours And Company Polyesters production process
JPH07118208A (ja) 1993-10-19 1995-05-09 Nippon Ester Co Ltd テレフタル酸のエステル化方法
EP0650995B1 (de) 1993-11-02 2000-01-05 Bayer Ag Verfahren zur Herstellung von Asparaginsäure-haltigen Polymeren
JP3375403B2 (ja) 1993-12-20 2003-02-10 日本エステル株式会社 ポリエステルの製造方法
TW330940B (en) 1993-12-22 1998-05-01 Mitsui Petroleum Chemicals Ind A method of manufacturing polyesters
CA2139061C (en) 1993-12-28 1998-12-08 Mitsui Chemicals, Inc. Process for preparing polyester
JP3710067B2 (ja) 1994-02-25 2005-10-26 三菱化学ポリエステルフィルム株式会社 ポリエステルの製造方法
US5464590A (en) 1994-05-02 1995-11-07 Yount; Thomas L. Reactor trays for a vertical staged polycondensation reactor
US5466419A (en) 1994-05-02 1995-11-14 Yount; Thomas L. Split flow reactor trays for vertical staged polycondensation reactors
DE4419397A1 (de) 1994-06-03 1995-12-14 Zimmer Ag Verfahren zur mehrstufigen Vakuumerzeugung bei der Polyester-Herstellung
JP3395423B2 (ja) 1995-01-20 2003-04-14 三菱化学株式会社 ポリエステル
US5811496A (en) 1995-12-21 1998-09-22 E.I. Du Pont De Nemours And Company Process for polymerization of polyester oligomers
AU4696896A (en) 1995-01-20 1996-08-07 E.I. Du Pont De Nemours And Company Process for polymerization of polyester oligomers
US5476919A (en) * 1995-02-21 1995-12-19 Minnesota Mining And Manufacturing Company Process for esterification
US5466765A (en) 1995-03-09 1995-11-14 Eastman Chemical Company Vaccum system for controlling pressure in a polyester process
DE19511483A1 (de) 1995-03-29 1996-10-02 Bayer Ag Verfahren zur Herstellung von thermoplastischem Polycarbonat
JPH08283394A (ja) 1995-04-10 1996-10-29 Mitsui Petrochem Ind Ltd ポリエチレンテレフタレートの製造方法
JPH08283398A (ja) 1995-04-14 1996-10-29 Nippon Ester Co Ltd ポリエステルの製造方法
DE19524181A1 (de) 1995-07-03 1997-01-09 Basf Ag Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren
DE19524180A1 (de) 1995-07-03 1997-01-09 Basf Ag Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren
EP0755945B1 (de) 1995-07-26 1998-11-25 Sulzer Chemtech AG Verfahren und Einrichtung zum Durchführen einer Polymerisation in einem Rohrreaktor
DE19530765A1 (de) 1995-08-22 1997-02-27 Basf Ag Kontinuierliches Verfahren zur Herstellung von expandierbaren Styrolpolymerisaten
DE19537930B4 (de) 1995-10-12 2006-02-23 Zimmer Ag Verfahren zur Herstellung von klarsichtigem Polyester
KR100443389B1 (ko) 1995-12-14 2004-11-16 이.아이,듀우판드네모아앤드캄파니 폴리에스테르 예비중합체의 제조 방법
TW381104B (en) 1996-02-20 2000-02-01 Eastman Chem Co Process for preparing copolyesters of terephthalic acid, ethylene glycol, and 1,4-cyclohexanedimethanol
DE19608614A1 (de) 1996-03-06 1997-09-11 Basf Ag Verfahren zur Aufarbeitung von Dihydroxyverbindungen enthaltenden Rückständen
PT889922E (pt) * 1996-03-28 2002-10-31 Du Pont Aparelho e processo para a preparacao de uma reaccao de policondensacao
DE19618678A1 (de) 1996-05-09 1997-11-13 Basf Ag Verfahren zur Herstellung von Polystyrol durch kontinuierliche anionische Polymerisation
US5898058A (en) 1996-05-20 1999-04-27 Wellman, Inc. Method of post-polymerization stabilization of high activity catalysts in continuous polyethylene terephthalate production
JPH1036495A (ja) 1996-07-25 1998-02-10 Nippon Ester Co Ltd 透明性に優れたポリエステルの連続製造法
DE19634450A1 (de) 1996-08-26 1998-03-05 Basf Ag Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen
US5922828A (en) 1996-09-03 1999-07-13 Hoechst Celanese Corp. Process for producing polyethylene terephthalate using a specific catalyst stabilizer system
TW541321B (en) 1996-09-04 2003-07-11 Hitachi Ltd Process and apparatus for continuous polycondensation
JP3836228B2 (ja) 1996-12-26 2006-10-25 三井化学株式会社 分離流による重合方法
JP3489382B2 (ja) 1997-03-19 2004-01-19 株式会社日立製作所 連続重縮合装置及び方法
US6103859A (en) 1997-04-09 2000-08-15 Eastman Chemical Company Late addition of supplemental ethylene glycol in the preparation of copolyesters
TW482790B (en) 1997-05-06 2002-04-11 Teijin Ltd Method for continuous production of polyester
JP3489408B2 (ja) 1997-09-19 2004-01-19 株式会社日立製作所 ポリエステルの連続製造装置
US5932105A (en) 1997-10-01 1999-08-03 Mobile Process Technology, Co. Method of polyester manufacturing using crossflow membrane filtration
JPH11106489A (ja) 1997-10-03 1999-04-20 Nippon Ester Co Ltd ポリエステル樹脂及びその製造方法
JPH11217429A (ja) 1998-02-05 1999-08-10 Nippon Ester Co Ltd ポリエステル樹脂の製造方法
KR100348238B1 (ko) 1998-02-27 2002-08-09 미쓰이 가가쿠 가부시키가이샤 신규 폴리에스테르 및 그의 제조방법
US6113997A (en) 1998-05-26 2000-09-05 Shell Oil Company Process to prepare a polyester resin
US6252034B1 (en) * 1998-06-04 2001-06-26 Teljin Limited Process for producing a polycarbonate resin
FR2780986B1 (fr) 1998-07-10 2000-09-29 Electrolyse L Procede de transformation de structures chimiques dans un fluide sous pression et en temperature et dispositif pour sa mise en oeuvre
US6069228A (en) 1998-08-17 2000-05-30 E. I. Du Pont De Nemours And Company Process for preparing polyamides
JP2000095851A (ja) 1998-09-22 2000-04-04 Hitachi Ltd ポリエチレンテレフタレートの製造方法
US6127493A (en) 1998-11-04 2000-10-03 Arteva North America S.A.R.L. Pressure polymerization of polyester
US6111064A (en) 1998-11-04 2000-08-29 The Regents Of The University Of California Pressure polymerization of polyester
US6339031B1 (en) 1998-12-29 2002-01-15 Seng C. Tan Microcellular carbon foams and microcellular C/C composites fabricated therefrom
AR024361A1 (es) 1999-06-15 2002-10-02 Dow Chemical Co Proceso y aparato para preparar una composicion utilizando un reactor continuo y mezclador en serie
BE1012770A3 (nl) 1999-07-02 2001-03-06 Ineos Nv Werkijze en inrichting voor het industrieel aanmaken van producten door middel van een alkoxylatiereactie.
US6623643B2 (en) 1999-11-19 2003-09-23 Microtek Medical Holdings, Inc. Process for treatment of aqueous environments containing a water soluble polymer
US6359106B1 (en) 2000-03-09 2002-03-19 Hitachi, Ltd. Production process and production apparatus for polybutylene terephthalate
EP1310496B1 (en) * 2000-08-11 2006-12-06 Kureha Corporation Process for the preparation of cyclic esters and method for purification of the same
DE10048003A1 (de) 2000-09-26 2002-04-11 Basell Polypropylen Gmbh Verfahren zur Voraktivierung von Katalysatoren
DE10126133B4 (de) 2001-05-29 2007-03-29 Karl-Heinz Wiltzer Verfahren und Vorrichtung zur Herstellung von hochviskosen oder hochstabilisierten Polykondensaten und entmonomerisiertem PA 6
KR100891603B1 (ko) 2001-07-10 2009-04-08 가부시끼가이샤 구레하 폴리에스테르 제조방법 및 반응 장치
DE10224883B4 (de) * 2001-07-27 2010-07-29 Heidelberger Druckmaschinen Ag Trockenstation und Verfahren zum Trocknen von bedruckten Bogen
US6672373B2 (en) 2001-08-27 2004-01-06 Idalex Technologies, Inc. Method of action of the pulsating heat pipe, its construction and the devices on its base
US7067088B2 (en) 2002-01-12 2006-06-27 Saudi Basic Industries Corporation Stratified flow chemical reactor
US7074879B2 (en) * 2003-06-06 2006-07-11 Eastman Chemical Company Polyester process using a pipe reactor

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002046266A2 (en) * 2000-12-07 2002-06-13 Eastman Chemical Company Low cost polyester process using a pipe reactor

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