JP6813586B2 - エアゾールフケ防止組成物 - Google Patents
エアゾールフケ防止組成物 Download PDFInfo
- Publication number
- JP6813586B2 JP6813586B2 JP2018543330A JP2018543330A JP6813586B2 JP 6813586 B2 JP6813586 B2 JP 6813586B2 JP 2018543330 A JP2018543330 A JP 2018543330A JP 2018543330 A JP2018543330 A JP 2018543330A JP 6813586 B2 JP6813586 B2 JP 6813586B2
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- Prior art keywords
- composition
- silicone
- cationic
- foaming
- group
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims description 197
- 208000001840 Dandruff Diseases 0.000 title claims description 20
- 239000000443 aerosol Substances 0.000 title description 14
- 230000002265 prevention Effects 0.000 title 1
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- 229920001296 polysiloxane Polymers 0.000 claims description 67
- -1 ethoxyl Chemical group 0.000 claims description 56
- 239000006260 foam Substances 0.000 claims description 35
- 239000002245 particle Substances 0.000 claims description 32
- 238000005187 foaming Methods 0.000 claims description 27
- 239000004094 surface-active agent Substances 0.000 claims description 27
- 239000003795 chemical substances by application Substances 0.000 claims description 24
- 239000004088 foaming agent Substances 0.000 claims description 22
- 230000003750 conditioning effect Effects 0.000 claims description 18
- 239000000126 substance Substances 0.000 claims description 17
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- 229920006317 cationic polymer Polymers 0.000 claims description 14
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- KAESVJOAVNADME-UHFFFAOYSA-N Pyrrole Chemical compound C=1C=CNC=1 KAESVJOAVNADME-UHFFFAOYSA-N 0.000 claims description 12
- 239000001294 propane Substances 0.000 claims description 8
- DDGPBVIAYDDWDH-UHFFFAOYSA-N 3-[dodecyl(dimethyl)azaniumyl]-2-hydroxypropane-1-sulfonate Chemical compound CCCCCCCCCCCC[N+](C)(C)CC(O)CS([O-])(=O)=O DDGPBVIAYDDWDH-UHFFFAOYSA-N 0.000 claims description 7
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- ILRSCQWREDREME-UHFFFAOYSA-N lauric acid amide propyl betaine Natural products CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims description 7
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- BTSZTGGZJQFALU-UHFFFAOYSA-N piroctone olamine Chemical compound NCCO.CC(C)(C)CC(C)CC1=CC(C)=CC(=O)N1O BTSZTGGZJQFALU-UHFFFAOYSA-N 0.000 claims description 7
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- 229940043810 zinc pyrithione Drugs 0.000 claims description 7
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 claims description 7
- CDOOAUSHHFGWSA-OWOJBTEDSA-N (e)-1,3,3,3-tetrafluoroprop-1-ene Chemical compound F\C=C\C(F)(F)F CDOOAUSHHFGWSA-OWOJBTEDSA-N 0.000 claims description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
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- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
- UOURRHZRLGCVDA-UHFFFAOYSA-D pentazinc;dicarbonate;hexahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[O-]C([O-])=O.[O-]C([O-])=O UOURRHZRLGCVDA-UHFFFAOYSA-D 0.000 claims description 6
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- 229940048842 sodium xylenesulfonate Drugs 0.000 claims description 5
- GOJYXPWOUJYXJC-UHFFFAOYSA-M sodium;2-[1-(2-hydroxyethyl)-2-undecyl-4,5-dihydroimidazol-1-ium-1-yl]acetate;hydroxide Chemical compound [OH-].[Na+].CCCCCCCCCCCC1=NCC[N+]1(CCO)CC([O-])=O GOJYXPWOUJYXJC-UHFFFAOYSA-M 0.000 claims description 5
- QUCDWLYKDRVKMI-UHFFFAOYSA-M sodium;3,4-dimethylbenzenesulfonate Chemical compound [Na+].CC1=CC=C(S([O-])(=O)=O)C=C1C QUCDWLYKDRVKMI-UHFFFAOYSA-M 0.000 claims description 5
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- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 4
- HLERILKGMXJNBU-UHFFFAOYSA-N norvaline betaine Chemical compound CCCC(C([O-])=O)[N+](C)(C)C HLERILKGMXJNBU-UHFFFAOYSA-N 0.000 claims description 4
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- 239000003381 stabilizer Substances 0.000 claims description 4
- NPNPZTNLOVBDOC-UHFFFAOYSA-N 1,1-difluoroethane Chemical compound CC(F)F NPNPZTNLOVBDOC-UHFFFAOYSA-N 0.000 claims description 3
- WCOXQTXVACYMLM-UHFFFAOYSA-N 2,3-bis(12-hydroxyoctadecanoyloxy)propyl 12-hydroxyoctadecanoate Chemical compound CCCCCCC(O)CCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCC(O)CCCCCC)COC(=O)CCCCCCCCCCC(O)CCCCCC WCOXQTXVACYMLM-UHFFFAOYSA-N 0.000 claims description 3
- LVZWSLJZHVFIQJ-UHFFFAOYSA-N Cyclopropane Chemical compound C1CC1 LVZWSLJZHVFIQJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000004338 Dichlorodifluoromethane Substances 0.000 claims description 3
- FPVVYTCTZKCSOJ-UHFFFAOYSA-N Ethylene glycol distearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCCCCCCCC FPVVYTCTZKCSOJ-UHFFFAOYSA-N 0.000 claims description 3
- 229940098691 coco monoethanolamide Drugs 0.000 claims description 3
- 235000019404 dichlorodifluoromethane Nutrition 0.000 claims description 3
- 239000011780 sodium chloride Substances 0.000 claims description 3
- 229940057400 trihydroxystearin Drugs 0.000 claims description 3
- 150000008282 halocarbons Chemical class 0.000 claims description 2
- YZUUTMGDONTGTN-UHFFFAOYSA-N nonaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCOCCO YZUUTMGDONTGTN-UHFFFAOYSA-N 0.000 claims description 2
- 238000010998 test method Methods 0.000 claims description 2
- 125000002091 cationic group Chemical group 0.000 description 80
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- OMDQUFIYNPYJFM-XKDAHURESA-N (2r,3r,4s,5r,6s)-2-(hydroxymethyl)-6-[[(2r,3s,4r,5s,6r)-4,5,6-trihydroxy-3-[(2s,3s,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]methoxy]oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)[C@H](O)[C@H](O)[C@H](O)O1 OMDQUFIYNPYJFM-XKDAHURESA-N 0.000 description 28
- 229920000926 Galactomannan Polymers 0.000 description 28
- 235000019698 starch Nutrition 0.000 description 26
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical group NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 25
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- 125000000217 alkyl group Chemical group 0.000 description 22
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- 239000013543 active substance Substances 0.000 description 20
- 150000003839 salts Chemical class 0.000 description 19
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 18
- 239000011734 sodium Substances 0.000 description 18
- 229910052708 sodium Inorganic materials 0.000 description 18
- 239000011701 zinc Substances 0.000 description 18
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 16
- 239000004368 Modified starch Substances 0.000 description 16
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 16
- 235000019426 modified starch Nutrition 0.000 description 16
- 229910052725 zinc Inorganic materials 0.000 description 16
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 15
- 229930182830 galactose Natural products 0.000 description 14
- 125000004432 carbon atom Chemical group C* 0.000 description 13
- 229920003118 cationic copolymer Polymers 0.000 description 13
- 239000004615 ingredient Substances 0.000 description 13
- 239000000047 product Substances 0.000 description 12
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 10
- 125000000129 anionic group Chemical group 0.000 description 10
- 239000002738 chelating agent Substances 0.000 description 10
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 9
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- FMRLDPWIRHBCCC-UHFFFAOYSA-L Zinc carbonate Chemical compound [Zn+2].[O-]C([O-])=O FMRLDPWIRHBCCC-UHFFFAOYSA-L 0.000 description 9
- 230000000844 anti-bacterial effect Effects 0.000 description 9
- 150000002148 esters Chemical class 0.000 description 9
- FJWSMXKFXFFEPV-UHFFFAOYSA-N prop-2-enamide;hydrochloride Chemical compound Cl.NC(=O)C=C FJWSMXKFXFFEPV-UHFFFAOYSA-N 0.000 description 9
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 8
- 239000002253 acid Substances 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 8
- VIDTVPHHDGRGAF-UHFFFAOYSA-N selenium sulfide Chemical compound [Se]=S VIDTVPHHDGRGAF-UHFFFAOYSA-N 0.000 description 8
- 238000006467 substitution reaction Methods 0.000 description 8
- 229910052717 sulfur Inorganic materials 0.000 description 8
- 239000002888 zwitterionic surfactant Substances 0.000 description 8
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 7
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- 239000000839 emulsion Substances 0.000 description 7
- 230000007062 hydrolysis Effects 0.000 description 7
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- 150000002500 ions Chemical class 0.000 description 7
- 229910052751 metal Inorganic materials 0.000 description 7
- 239000002184 metal Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 230000004048 modification Effects 0.000 description 7
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- 229910052757 nitrogen Inorganic materials 0.000 description 7
- WHMDPDGBKYUEMW-UHFFFAOYSA-N pyridine-2-thiol Chemical class SC1=CC=CC=N1 WHMDPDGBKYUEMW-UHFFFAOYSA-N 0.000 description 7
- 229960005265 selenium sulfide Drugs 0.000 description 7
- 239000011667 zinc carbonate Substances 0.000 description 7
- 235000004416 zinc carbonate Nutrition 0.000 description 7
- 229910000010 zinc carbonate Inorganic materials 0.000 description 7
- OYINQIKIQCNQOX-UHFFFAOYSA-M 2-hydroxybutyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCC(O)C[N+](C)(C)C OYINQIKIQCNQOX-UHFFFAOYSA-M 0.000 description 6
- 229920002907 Guar gum Polymers 0.000 description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 6
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- 238000009472 formulation Methods 0.000 description 6
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- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 5
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- 239000004480 active ingredient Substances 0.000 description 5
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- YBBJKCMMCRQZMA-UHFFFAOYSA-N pyrithione Chemical class ON1C=CC=CC1=S YBBJKCMMCRQZMA-UHFFFAOYSA-N 0.000 description 4
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- 125000006222 dimethylaminomethyl group Chemical group [H]C([H])([H])N(C([H])([H])[H])C([H])([H])* 0.000 description 3
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- UYMKPFRHYYNDTL-UHFFFAOYSA-N ethenamine Chemical compound NC=C UYMKPFRHYYNDTL-UHFFFAOYSA-N 0.000 description 3
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- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 3
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- 125000000400 lauroyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229940096989 lauryl aminopropylglycine Drugs 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 230000005291 magnetic effect Effects 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 150000005451 methyl sulfates Chemical class 0.000 description 1
- PGXWDLGWMQIXDT-UHFFFAOYSA-N methylsulfinylmethane;hydrate Chemical compound O.CS(C)=O PGXWDLGWMQIXDT-UHFFFAOYSA-N 0.000 description 1
- 229960000282 metronidazole Drugs 0.000 description 1
- VAOCPAMSLUNLGC-UHFFFAOYSA-N metronidazole Chemical compound CC1=NC=C([N+]([O-])=O)N1CCO VAOCPAMSLUNLGC-UHFFFAOYSA-N 0.000 description 1
- 229960002509 miconazole Drugs 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- SKDZEPBJPGSFHS-UHFFFAOYSA-N n,n-bis(2-hydroxyethyl)tetradecanamide Chemical compound CCCCCCCCCCCCCC(=O)N(CCO)CCO SKDZEPBJPGSFHS-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- MCVUKOYZUCWLQQ-UHFFFAOYSA-N n-tridecylbenzene Natural products CCCCCCCCCCCCCC1=CC=CC=C1 MCVUKOYZUCWLQQ-UHFFFAOYSA-N 0.000 description 1
- VWOIKFDZQQLJBJ-DTQAZKPQSA-N neticonazole Chemical compound CCCCCOC1=CC=CC=C1\C(=C/SC)N1C=NC=C1 VWOIKFDZQQLJBJ-DTQAZKPQSA-N 0.000 description 1
- 229950010757 neticonazole Drugs 0.000 description 1
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 229960004031 omoconazole Drugs 0.000 description 1
- JMFOSJNGKJCTMJ-ZHZULCJRSA-N omoconazole Chemical compound C1=CN=CN1C(/C)=C(C=1C(=CC(Cl)=CC=1)Cl)\OCCOC1=CC=C(Cl)C=C1 JMFOSJNGKJCTMJ-ZHZULCJRSA-N 0.000 description 1
- 239000010502 orange oil Substances 0.000 description 1
- 229960003483 oxiconazole Drugs 0.000 description 1
- QRJJEGAJXVEBNE-MOHJPFBDSA-N oxiconazole Chemical compound ClC1=CC(Cl)=CC=C1CO\N=C(C=1C(=CC(Cl)=CC=1)Cl)\CN1C=NC=C1 QRJJEGAJXVEBNE-MOHJPFBDSA-N 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000001254 oxidized starch Substances 0.000 description 1
- 235000013808 oxidized starch Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000011049 pearl Substances 0.000 description 1
- 229940086615 peg-6 cocamide Drugs 0.000 description 1
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 1
- 150000004965 peroxy acids Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-O phosphonium Chemical compound [PH4+] XYFCBTPGUUZFHI-UHFFFAOYSA-O 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 230000026731 phosphorylation Effects 0.000 description 1
- 238000006366 phosphorylation reaction Methods 0.000 description 1
- 229910052615 phyllosilicate Inorganic materials 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000011297 pine tar Substances 0.000 description 1
- 229940068124 pine tar Drugs 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 150000004291 polyenes Chemical class 0.000 description 1
- 229920002523 polyethylene Glycol 1000 Polymers 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- ONQDVAFWWYYXHM-UHFFFAOYSA-M potassium lauryl sulfate Chemical compound [K+].CCCCCCCCCCCCOS([O-])(=O)=O ONQDVAFWWYYXHM-UHFFFAOYSA-M 0.000 description 1
- 229940116985 potassium lauryl sulfate Drugs 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- QYUMESOEHIJKHV-UHFFFAOYSA-M prop-2-enamide;trimethyl(propyl)azanium;chloride Chemical compound [Cl-].NC(=O)C=C.CCC[N+](C)(C)C QYUMESOEHIJKHV-UHFFFAOYSA-M 0.000 description 1
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 1
- KCXFHTAICRTXLI-UHFFFAOYSA-N propane-1-sulfonic acid Chemical class CCCS(O)(=O)=O KCXFHTAICRTXLI-UHFFFAOYSA-N 0.000 description 1
- CIBMHJPPKCXONB-UHFFFAOYSA-N propane-2,2-diol Chemical compound CC(C)(O)O CIBMHJPPKCXONB-UHFFFAOYSA-N 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- NHARPDSAXCBDDR-UHFFFAOYSA-N propyl 2-methylprop-2-enoate Chemical compound CCCOC(=O)C(C)=C NHARPDSAXCBDDR-UHFFFAOYSA-N 0.000 description 1
- PNXMTCDJUBJHQJ-UHFFFAOYSA-N propyl prop-2-enoate Chemical compound CCCOC(=O)C=C PNXMTCDJUBJHQJ-UHFFFAOYSA-N 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- GGOZGYRTNQBSSA-UHFFFAOYSA-N pyridine-2,3-diol Chemical compound OC1=CC=CN=C1O GGOZGYRTNQBSSA-UHFFFAOYSA-N 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- MCJGNVYPOGVAJF-UHFFFAOYSA-N quinolin-8-ol Chemical compound C1=CN=C2C(O)=CC=CC2=C1 MCJGNVYPOGVAJF-UHFFFAOYSA-N 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000013557 residual solvent Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000006254 rheological additive Substances 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 238000006748 scratching Methods 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 150000003335 secondary amines Chemical class 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 229960005429 sertaconazole Drugs 0.000 description 1
- 229940095673 shampoo product Drugs 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- CQQFHQIXAHHOHI-UHFFFAOYSA-M sodium 3-[2-(dodecanoylamino)ethyl-(2-hydroxyethyl)amino]-2-hydroxypropane-1-sulfonate Chemical compound CCCCCCCCCCCC(=O)NCCN(CCO)CC(CS(=O)(=O)[O-])O.[Na+] CQQFHQIXAHHOHI-UHFFFAOYSA-M 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 description 1
- 229910000342 sodium bisulfate Inorganic materials 0.000 description 1
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 1
- 229940091855 sodium lauraminopropionate Drugs 0.000 description 1
- 229940057950 sodium laureth sulfate Drugs 0.000 description 1
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 1
- 235000019345 sodium thiosulphate Nutrition 0.000 description 1
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 description 1
- HWCHICTXVOMIIF-UHFFFAOYSA-M sodium;3-(dodecylamino)propanoate Chemical compound [Na+].CCCCCCCCCCCCNCCC([O-])=O HWCHICTXVOMIIF-UHFFFAOYSA-M 0.000 description 1
- LLKGTXLYJMUQJX-UHFFFAOYSA-M sodium;3-[2-carboxyethyl(dodecyl)amino]propanoate Chemical compound [Na+].CCCCCCCCCCCCN(CCC(O)=O)CCC([O-])=O LLKGTXLYJMUQJX-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000012916 structural analysis Methods 0.000 description 1
- 125000000547 substituted alkyl group Chemical group 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 239000000213 tara gum Substances 0.000 description 1
- 235000010491 tara gum Nutrition 0.000 description 1
- 239000010677 tea tree oil Substances 0.000 description 1
- 229940111630 tea tree oil Drugs 0.000 description 1
- DOMXUEMWDBAQBQ-WEVVVXLNSA-N terbinafine Chemical compound C1=CC=C2C(CN(C\C=C\C#CC(C)(C)C)C)=CC=CC2=C1 DOMXUEMWDBAQBQ-WEVVVXLNSA-N 0.000 description 1
- 229960002722 terbinafine Drugs 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 239000001585 thymus vulgaris Substances 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
- 150000003852 triazoles Chemical class 0.000 description 1
- 125000005209 triethanolammonium group Chemical class 0.000 description 1
- FZGFBJMPSHGTRQ-UHFFFAOYSA-M trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCOC(=O)C=C FZGFBJMPSHGTRQ-UHFFFAOYSA-M 0.000 description 1
- 229960004418 trolamine Drugs 0.000 description 1
- OBYIEPMKXIBQEV-UHFFFAOYSA-N undecyl hydrogen sulfate Chemical compound CCCCCCCCCCCOS(O)(=O)=O OBYIEPMKXIBQEV-UHFFFAOYSA-N 0.000 description 1
- 125000004417 unsaturated alkyl group Chemical group 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- IPCXNCATNBAPKW-UHFFFAOYSA-N zinc;hydrate Chemical compound O.[Zn] IPCXNCATNBAPKW-UHFFFAOYSA-N 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
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- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A61K8/41—Amines
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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Description
ヘアケア組成物は、組成物に洗浄性能を提供する約20重量%超の界面活性剤系を含み得る。界面活性剤系は、アニオン性界面活性剤及び/又は、アニオン性界面活性剤と、両性、双性イオン性、非イオン性及びこれらの混合物からなる群から選択される共界面活性剤との組み合わせを含む。洗浄性界面活性剤の種々の例及び説明が、米国特許第8,440,605号、米国特許出願公開第2009/155383号、及び米国特許出願公開第2009/0221463号に記述されており、参照によりそれら全体が本明細書に組み込まれる。
a)R1O(CH2CHR3O)ySO3M;
b)CH3(CH2)zCHR2CH2O(CH2CHR3O)ySO3M;及び
c)これらの混合物、からなる群から選択されるアニオン性界面活性剤も含むことができ、
式中、R1は、CH3(CH2)10を表し、R2は、H、又はz内の炭素原子の合計及びR2が8であるように1〜4個の炭素原子を含む炭化水素基を表し、R3は、H、又はCH3であり、yは0〜7であり、yがゼロ(0)でないときyの平均値は約1であり、Mは、一価の又は二価の正電気を帯びたカチオンである。
ヘアケア組成物は、ヘアケア組成物の約1重量%〜約5重量%、あるいは約2重量%〜約4重量%、あるいは約1重量%〜約3重量%の1種以上の粘度低減剤を含む。
組成物は、水混和性グリコール及び他のジオールを含むことができる。非限定的な例として、ジプロピレングリコール、トリプロピレングリコール、ジエチレングリコール、エチレングリコール、プロピレングリコール、1,3−プロパンジオール、2,2−プロパンジオール、1,2−ブタンジオール、1,3−ブタンジオール、1,4−ブタンジオール、2,3−ブタンジオール、1−プロペン、1,3,3,3テトラフルオロ−(1E)、及び2−メチル−2,4−ペンタンジオールが挙げられる。
本発明の組成物はまた、フケ防止剤を含有してもよい。フケ防止粒子の好適な非限定例には、ピリジンチオン塩、硫化セレン、粒子状硫黄、及びこれらの混合物が挙げられる。かかるフケ防止粒子は、組成物の必須成分と物理的及び化学的に適合する必要があり、製品の安定性、審美性又は性能を過度に損なってはならない。
ピリジンチオンフケ防止粒子、特に1−ヒドロキシ−2−ピリジンチオン塩は、本発明の組成物に用いる粒子状フケ防止剤の1つの実施形態である。ピリジンチオンフケ防止粒子の濃度は、典型的には組成物の約0.1重量%〜約10重量%の範囲である。一実施形態において、ピリジンチオンフケ防止粒子の濃度は、約0.1重量%〜約8重量%の範囲であり、更なる実施形態では、約0.3重量%〜約5重量%の範囲である。本発明の一実施形態において、ピリジンチオン塩は、亜鉛、銅、スズ、カドミウム、マグネシウム、アルミニウム及びジルコニウムなどの重金属から形成されるものを含む。本発明の一実施形態において、ピリジンチオン塩は、重金属亜鉛から形成され、更なる実施形態においては、(「ジンクピリジンチオン」又は「ZPT」として知られる)1−ヒドロキシ−2−ピリジンチオンの亜鉛塩であり、なお血小板状粒子形態の1−ヒドロキシ−2−ピリジンチオン塩の更なる実施形態においては、当該粒子は約20μまでの平均粒径を有する。本発明の一実施形態において、粒子は、約5μまで、更なる実施形態においては、約2.5μまでの平均粒径を有する。他のカチオン(例えば、ナトリウム)から形成される塩類もまた好適であり得る。ピリジンチオンフケ防止剤は、例えば、米国特許第2,809,971号、同第3,236,733号、同第3,753,196号、同第3,761,418号、同第4,345,080号、同第4,323,683号、同第4,379,753号、及び同第4,470,982号に記載されている。本明細書の組成物において、ZPTをフケ防止粒子として使用する際、毛髪の成長又は再生が刺激されるか、又は調節されるか、若しくはその両方が行われるか、又は脱毛が低減されるか又は阻害されるか、若しくは毛髪がより濃く若しくは豊かに見える可能性があると想到される。
ピリチオンの多価金属塩から選択されるフケ防止活性物質に加えて、本発明は、金属ピリチオン塩活性物質に加えて、1つ以上の抗真菌若しくは抗菌活性物質を更に含んでもよい。好適な抗菌活性物質としては、コールタール、硫黄、ウィットフィールド軟膏、カステラーニ塗布剤、塩化アルミニウム、ゲンチアナバイオレット、オクトピロックス(ピロクトンオラミン)、シクロピロックスオラミン、ウンデシレン酸及びその金属塩、過マンガン酸カリウム、硫化セレン、チオ硫酸ナトリウム、プロピレングリコール、ビターオレンジオイル、尿素調製物、グリセオフルビン、8−ヒドロキシキノリンシロキノール、チオベンダゾール、チオカルバメート、ハロプロジン、ポリエン、ヒドロキシピリドン、モルホリン、ベンジルアミン、アリルアミン(例えば、テルビナフィン)、ティーツリー油、クローブリーフ油、コリアンダー、パルマローザ、ベルベリン、タイムレッド、桂皮油、桂皮アルデヒド、シトロネル酸、ヒノキトール(hinokitol)、イクチオールペール(ichthyol pale)、Sensiva SC−50、Elestab HP−100、アゼライン酸、リチカーゼ、ヨードプロピニルブチルカルバメート(IPBC)、オクチルイソチアザリノンなどのイソチアザリノン及びアゾール、並びにこれらの組み合わせが挙げられる。本発明の一実施形態において、抗菌剤としては、イトラコナゾール、ケトコナゾール、硫化セレン及びコールタールが挙げられる。
アゾール抗菌剤としては、ベンズイミダゾールなどのイミダゾール、ベンゾチアゾール、ビフォナゾール、硝酸ブタコナゾール、クリムバゾール、クロトリマゾール、クロコナゾール、エベルコナゾール、エコナゾール、エルビオール、フェンチコナゾール、フルコナゾール、フルチマゾール、イソコナゾール、ケトコナゾール、ラノコナゾール、メトロニダゾール、ミコナゾール、ネチコナゾール、オモコナゾール、硝酸オキシコナゾール、セルタコナゾール、硝酸サルコナゾール、チオコナゾール、チアゾール、並びにテルコナゾール及びイトラコナゾールなどのトリアゾール、並びにこれらの組み合わせが挙げられる。組成物に存在する場合、アゾール抗菌有効成分は約0.01%〜約5%の量で含まれる。本発明の一実施形態において、アゾール抗菌有効成分は、組成物の約0.1重量%〜約3重量%、更なる実施形態においては約0.3重量%〜約2重量%の量で含まれる。本発明の一実施形態において、アゾール抗菌剤はケトコナゾールである。
硫化セレンは、本発明の抗菌組成物に用いるのに好適な粒子状フケ防止剤であり、その有効濃度は組成物の約0.1重量%〜約4重量%であり、本明細書の一実施形態においては約0.3重量%〜約2.5重量%、更なる実施形態においては約0.5重量%〜約1.5重量%の範囲である。硫化セレンは、一般的には、セレン1モル及び硫黄2モルを有する化合物とみなされるが、一般式SexSy(式中x+y=8)に従う環式構造であってもよい。前方レーザー光散乱装置(例えば、Malvern 3600装置)で測定した硫化セレンの平均粒径は、典型的には15μm未満であり、本発明の一実施形態においては、10μm未満である。硫化セレン化合物は、例えば、米国特許第2,694,668号、同第3,152,046号、同第4,089,945号、及び同第4,885,107号に記載されている。
d.角質溶解剤
e.追加の抗菌活性物質
本発明の追加の抗菌活性物質は、メラレウカ(茶木)及び炭の抽出物を含んでもよい。本発明はまた、抗菌活性物質の組み合わせを含んでもよい。このような組み合わせには、オクトピロックスとジンクピリチオンとの組み合わせ、パインタールとイオウとの組み合わせ、サリチル酸とジンクピリチオンとの組み合わせ、オクトピロックスとクリムバゾールとの組み合わせ、及びサリチル酸とオクトピロックスとの組み合わせ、ジンクピリチオンとクリムバゾール並びにこれらの混合物を挙げることができる。これらの有効成分は、本明細書で使用されるとき、約1%〜約4%、本発明の一実施形態においては約2%〜約4%のレベルで使用される。
ヘアケア組成物は、カチオン性ポリマーを更に含む。これらのカチオン性ポリマーは、(a)カチオン性グアーポリマー、(b)カチオン性非グアーガラクトマンナンポリマー、(c)カチオン性タピオカポリマー、(d)アクリルアミドモノマーとカチオン性モノマーとのカチオン性コポリマー、及び/又は(e)洗浄性界面活性剤と組み合わせた際にリオトロピック液晶を形成してもしなくてもよい、合成非架橋型カチオン性ポリマー、(f)カチオン性セルロースポリマーのうちの少なくとも1つを含み得る。更に、カチオン性ポリマーは、カチオン性ポリマーの混合物であってよい。
Yは、C1〜C22アルキル、アルコキシ、アルキリデン、アルキル、又はアリールオキシであり、
Ψは、C1〜C22のアルキル、アルキルオキシ、アルキルアリール又はアルキルアリールオキシであり、
Zは、C1〜C22のアルキル、アルキルオキシ、アリール又はアリールオキシであり、
R1は、H、C1〜C4の直鎖又は分枝鎖のアルキルであり、
sは、0又は1であり、nは、0又は≧1であり、
T及びR7は、C1〜C22アルキルであり、
X−は、ハロゲン、ヒドロキシド、アルコキシド、サルフェート又はアルキルサルフェートである。
本明細書に記載のヘアケア組成物は、ヘアケア組成物の約1重量%〜約10重量%の発泡剤、あるいは約2重量%〜約8重量%の発泡剤、及びあるいは約2.5重量%〜約7重量%の発泡剤を含んでもよい。
ヘアケア組成物は、有益剤を含む1種以上の任意成分を更に含み得る。好適な有益剤としては、コンディショニング剤、カチオン性ポリマーシリコーンエマルジョン、フケ防止活性物質、ゲルネットワーク、キレート剤、及びヒマワリ油又はヒマシ油等の天然油が挙げられるが、これらに限定されない。更なる好適な任意成分としては、香料、香料マイクロカプセル、着色剤、粒子、抗菌剤、消泡剤(foam busters)、帯電防止剤、レオロジー変性剤及び増粘剤、懸濁材料及び構造化剤、pH調整剤及び緩衝剤、防腐剤、パールエッセンス剤、溶媒、希釈剤、抗酸化剤、ビタミン並びにこれらの組み合わせが挙げられるが、これらに限定されない。
ヘアケア組成物のコンディショニング剤は、シリコーンコンディショニング剤であってよい。シリコーンコンディショニング剤は、揮発性シリコーン、不揮発性シリコーン、又はこれらの組み合わせを含んでもよい。シリコーンコンディショニング剤の濃度は、典型的には、組成物の約0.01重量%〜約10重量%、約0.1重量%〜約8重量%、約0.1重量%〜約5重量%、及び/又は約0.2重量%〜約3重量%の範囲である。好適なシリコーンコンディショニング剤、及びシリコーン用の任意選択の懸濁化剤の非限定的な例が、米国再発行特許第34,584号、米国特許第5,104,646号、及び米国特許第5,106,609号に記載されており、これらの記載を参照により本明細書に援用する。
種々のアニオン性及び非イオン性乳化剤をヘアケア組成物に使用することができる。アニオン性及び非イオン性乳化剤は、本質的にモノマー又はポリマーのいずれかであることができる。モノマーの例としては、アルキルエトキシレート、アルキルサルフェート、石鹸、及び脂肪酸エステル、並びにそれらの誘導体が例示として挙げられるが、これらに限定されない。ポリマーの例としては、ポリアクリレート、ポリエチレングリコール、及びブロックコポリマー、並びにこれらの誘導体が例示として挙げられるが、これらに限定されない。ラノリン、レシチン及びリグニンなどの天然の乳化剤、並びにそれらの誘導体も、有用な乳化剤の非限定的な例である。
ヘアケア組成物は、キレート剤を更に含むことができる。好適なキレート剤としては、A E Martell & R M Smith,Critical Stability Constants,Vol.1,Plenum Press,New York & London(1974)及びA E Martell & R D Hancock,Metal Complexes in Aqueous Solution,Plenum Press,New York & London(1996)に記載されるものが挙げられ、いずれも参照により本明細書に組み込まれる。キレート剤に関し、用語「塩及びそれらの誘導体」は、参照しているキレート剤と同じ官能構造(例えば、同じ化学主鎖)を含み、同様の又はより優れたキレート化特性を有する塩及び誘導体を意味する。塩及びそれらの誘導体としては、アルカリ金属、アルカリ土類、アンモニウム、置換アンモニウム塩(すなわち、モノエタノールアンモニウム、ジエタノールアンモニウム、トリエタノールアンモニウム)塩、酸性部分を有するキレート剤のエステル、及びこれらの混合物、特に、全てのナトリウム、カリウム又はアンモニウム塩が挙げられる。用語「誘導体」は、米国特許第5,284,972号に例示される化合物などの「キレート化界面活性剤」化合物、及び米国特許5,747,440号に開示されるポリマーEDDS(エチレンジアミン二コハク酸)などの、親キレート剤と同じ官能構造を有する1以上のキレート化基を含む大型分子も含む。
ヘアケア組成物は、(周囲条件下で)注ぐことが可能な液体の形態であってよい。したがって、かかる組成物は、典型的にキャリアを含み、これはヘアケア組成物の約40重量%〜約80重量%、あるいは約45重量%〜約75重量%、あるいは約50重量%〜約70重量%の濃度で存在する。キャリアは、水、又は水と有機溶媒との混和性混合物を含んでもよいが、一態様では、他の必須又は任意成分の微量成分として組成物中に偶然取り込まれる場合を除き、最小限の有機溶媒を含むか、又は有意の濃度の有機溶媒を含まない水を含んでもよい。
エアゾールフォームディスペンサは、ヘアケア組成物を保持するための収容容器を含んでもよい。収容容器は、プラスチック、金属、合金、積層体、及びこれらの組み合わせからなる群から選択される任意の好適な材料で作製されてもよい。一実施形態において、収容容器は、1回使い切りであり得る。一実施形態において、収容容器は、エアゾールフォームディスペンサから取り外し可能であり得る。あるいは、収容容器は、エアゾールフォームディスペンサと一体化してもよい。一実施形態において、2つ以上の収容容器が存在し得る。
泡沫密度
泡密度を、100mLのビーカーを質量計(mass balance)の上に配置し、ビーカーの質量を風袋引き(tarring)し、次いでエアゾール容器から100mLのビーカーに泡の体積が容器のへりより上になるまで製品を分配することにより測定する。泡は、泡にわたってへらで掻くことにより、ビーカーの上面と同じ高さになる。次いで、泡100mLの得られた質量を体積(100)で割り、g/mL単位の泡密度を求める。
頭皮上へのフケ防止活性物質の付着量は、熟練の美容師が従来の洗浄プロトコルに従い、個人の毛髪をフケ防止活性物質含有の組成物、例えば、本発明による組成物で洗浄することによって測定される。次いで、表面に開放端ガラスシリンダを保持できるよう毛髪を頭皮の領域上で分けて、同時に抽出溶液のアリコートを添加し撹拌した後、抗ふけ活性物質の内容物を回収し、HPLCのような従来の方法論に基づいて分析定量する。
Brookfield Engineering Laboratories(Stoughton,MA)製Cone/Plate Controlled Stress Brookfield Rheometer R/S Plusにより、配合物の粘度を測定する。使用されるコーン(スピンドルC−75−1)は、直径が75mm、角度が1°である。粘度は、一定のせん断速度2s−1及び温度26.5℃で定常状態の流動実験を使用して測定する。サンプル寸法は2.5mLであり、全測定読み取り時間は3分間である。
以下の実施例は、本明細書に述べられる本発明の実施形態を図示する。例示されたヘアケア組成物は、薄い界面活性剤相に、水、ポリマー、及び界面活性剤を、キシレンスルホン酸ナトリウム又はレオロジー変性剤とともに混合することにより製造することができる。界面活性剤は、pH7を目標として調整する。中和された界面活性剤相にジンクピリチオンと炭酸亜鉛固形物とを混合して分散させる。成分は周囲温度で完全に混合される。発泡剤、電解質、シリコーンエマルジョン、防腐剤及び芳香剤を含む追加の成分を、製品に添加してもよい。配合物分野の当業者の技術範囲内でヘアケア組成物の他の変形例が、本発明の趣旨及び範囲から逸脱することなく行われ得ることが理解されよう。本明細書における全ての部、比率(%)、及び比は、特に指定しない限り、重量基準である。特定の成分は、供給元から希釈溶液として供給され得る。記載される量は、特に指定しない限り、活性物質の重量%を表す。
2.ラウリル硫酸ナトリウム(Stepan Company製)
3.Amphosol HCA(Stepan Company製)
4.トリヒドロキシステアリン(Elementis Specialties製)
5.グリコールジステアレート(Golschmidt Chemical Company製)
6.U2 ZPT(Lonza製)
7.硫化セレン(Eskay Fine Chemicals製)
8.オクトピロックス(Clariant製)
9.炭酸亜鉛(Bruggeman Group製)
10.芳香剤(P&G製)
11.Jaguar C500(Solvay製、分子量500,000g/mol、電荷密度0.8meq/g)
12.ジメチコンDM5500、ワッカーシリコーン
13.塩酸(Mallinckrodt Baker Inc.製)
14.防腐剤Kathon CG(Akzo Nobel製)
15.塩化ナトリウムUSP(食品等級)、供給元:Morton
16.キシレンスルホン酸ナトリウム(Stepan Company製)
17.安息香酸ナトリウム(Kalama Chemical製)
18.水(Misty Mountain Spring Water製)
19.発泡剤A46(イソブタン及びプロパン)(18、Diversified Cpc International(Channahon US))
20.発泡剤HF0(トランス1,3,3,3テトラフルオロプロパ1エン)(19)(Honey Well製)
21.PEG8ジメチコンA208(20)(MW855)(Siltech製)
22.PEG8ジメチコンD208(20)MW2706(Siltech製)
表の結果は、ZPTの濃縮レベルを含有するエアゾールフォームからのZPTの平均付着量がほぼ2倍に増加したことを示している。この付着量の増加は、液体形態のシャンプー製品コントロールの投与重量の半分で送達される。更に、より高い密度を有する泡(チャートの例B及びF)は、A及びEのより低密度の例と体積基準で比較して、送達時、更に多くのZPTを送達する能力を有することを観察することができる。
A.
i.約18%〜約36%の1種以上のアニオン性界面活性剤と、
ii.0.01〜約5%の分子量約38〜約2800の1種以上の粘度調整剤と、
iii.約0.1〜約10%のフケ防止粒子と、
iv.約1%〜約10%の発泡剤と、を含み、
泡密度は、約0.05〜約0.25g/mLである、発泡組成物。
B.フケ防止付着量は、0.8マイクログラム/cm2以上である、A項に記載の発泡組成物。
C.泡密度は、0.1%〜約0.2%である、A及びB項に記載の発泡組成物。
D.(25℃で測定された)粘度は、9000cps未満である、A〜C項に記載の発泡組成物。
E.組成物は、約1%〜約5%の1種以上の両性/双性イオン性又は非イオン性共界面活性剤、及びこれらの混合物を更に含む、A〜D項に記載の発泡組成物。
F.粘度調整剤の分子量は、約75〜約350である、A〜E項に記載の発泡組成物。
G.フケ防止粒子は、フケ防止粒子の約1〜約5%である、A〜F項に記載の発泡組成物。
H.発泡剤は、約2%〜約8%である、A〜G項に記載の発泡組成物。
I.組成物は、0.1%〜5%の安定化剤を更に含む、A〜H項に記載の発泡組成物。
J.安定化剤は、トリヒドロキシステアリン、エチレングリコールジステアレートポリマー、及びこれらの混合物からなる群から選択される、A〜I項に記載の発泡組成物。
K.粘度調整剤は、エタノール、ジプロピレングリコール、キシレンスルホン酸ナトリウム、塩化ナトリウム、アルコキシル化シリコーン/エトキシル化シリコーン/プロポキシル化シリコーン/ポリオキシエチレンシリコーン/ポリオキシプロピレンシリコーン/ポリエチレングリコールシリコーン/PEG−8シリコーン/PEG−9シリコーン/PEG−nシリコーン/シリコーンエーテル(nは別の整数であると考えられる)、及びこれらの混合物からなる群から選択される、A〜J項に記載の発泡組成物。
L.フケ防止粒子は、ピリジンチオン塩、硫化セレン、粒子状硫黄、及びこれらの混合物からなる群から選択される、A〜K項に記載の発泡組成物。
M.フケ防止粒子は、ジンクピリチオンである、A〜L項に記載の発泡組成物。
N.組成物は、アゾール、オクトピロックス、及びこれらの混合物からなる群から選択されるフケ防止物質を更に含む、A〜M項に記載の発泡組成物。
O.共界面活性剤は、ラウリン酸アミドプロピルベタイン、ココアミドプロピルベタイン、ラウリルヒドロキシスルタイン、ラウロアンホ酢酸ナトリウム、ココモノエタノールアミド、及びこれらの混合物からなる群から選択される、A〜N項に記載の発泡組成物。
P.発泡剤は、プロパン、n−ブタン、イソブタン、シクロプロパン、及びこれらの混合物、並びにジクロロジフルオロメタン、1,1−ジクロロ−1,1,2,2−テトロフルオロエタン、1−クロロ−1,1−ジフルオロ−2,2−トリフルオロエタン、1−クロロ−1,1−ジフルオロエチレン、1,1−ジフルオロエタン、ジメチルエーテル、モノクロロジフルオロメタン、トランス−1,3,3,3−テトラフルオロプロペン、及びこれらの混合物などのハロゲン化炭化水素からなる群から選択される、A〜O項に記載の発泡組成物。
Q.発泡剤は、プロパン及びイソブテン、トランス−1,3,3,3−テトラフルオロプロペン、並びにこれらの混合物からなる群から選択される、A〜P項に記載の発泡組成物。
R.組成物は、カチオン性ポリマーを更に含む、A〜Q項に記載の発泡組成物。
S.組成物は、コンディショニング剤を更に含む、A〜R項に記載の発泡組成物。
T.コンディショニング剤は、シリコーンである、A〜S項に記載の発泡組成物。
Claims (10)
- i.全発泡組成物に基づいて、18%〜36%の1種以上のアニオン性界面活性剤と、
ii.全発泡組成物に基づいて、0.1〜5%の分子量38〜2800の1種以上の粘度調整剤であって、エタノール、ジプロピレングリコール、キシレンスルホン酸ナトリウム、塩化ナトリウム、アルコキシル化シリコーン/エトキシル化シリコーン/プロポキシル化シリコーン/ポリオキシエチレンシリコーン/ポリオキシプロピレンシリコーン/ポリエチレングリコールシリコーン/PEG−8シリコーン/PEG−9シリコーン/PEG−nシリコーン/シリコーンエーテル(nは別の整数であると考えられる)、及びこれらの混合物からなる群から選択される粘度調整剤と、
iii.全発泡組成物に基づいて、0.1〜10%のフケ防止粒子であって、前記フケ防止粒子は、ジンクピリチオンであるフケ防止粒子と、
iv.1%〜10%の発泡剤であって、1種以上の揮発性物質を含み、気体状態で、ヘアケア組成物の他の成分を粒子状又は飛沫形態で運ぶ発泡剤と、を含む、発泡組成物であって、
前記組成物は、全発泡組成物に基づいて、0.1%〜5%の安定化剤を更に含み、前記安定化剤は、トリヒドロキシステアリン、エチレングリコールジステアレートポリマー、及びこれらの混合物からなる群から選択され、
前記組成物は、全発泡組成物に基づいて、0.1重量%〜5重量%の塩基性炭酸亜鉛を、更に含み、
泡密度は、本明細書に記載の泡沫密度テスト方法に基づいて、0.05〜0.25g/mLであり、
フケ防止粒子付着量は、0.8マイクログラム/cm 2 以上である、
発泡組成物。 - 25℃で測定された粘度は、9000cps未満である、請求項1に記載の発泡組成物。
- 前記組成物は、全発泡組成物に基づいて、1%〜5%の1種以上の両性/双性イオン性又は非イオン性共界面活性剤及びこれらの混合物を更に含む、請求項1又は2に記載の発泡組成物。
- 前記粘度調整剤の分子量は、75〜350である、請求項1〜3のいずれか一項に記載の発泡組成物。
- 前記発泡剤は、全発泡組成物に基づいて、2%〜8%である、請求項1〜4のいずれか一項に記載の発泡組成物。
- 前記組成物は、アゾール、オクトピロックス、及びこれらの混合物からなる群から選択されるフケ防止物質を更に含む、請求項1〜5のいずれか一項に記載の発泡組成物。
- 前記共界面活性剤は、ラウリン酸アミドプロピルベタイン、ココアミドプロピルベタイン、ラウリルヒドロキシスルタイン、ラウロアンホ酢酸ナトリウム、ココモノエタノールアミド、及びこれらの混合物からなる群から選択される、請求項3〜6のいずれか一項に記載の発泡組成物。
- 前記発泡剤は、プロパン、n−ブタン、イソブタン、シクロプロパン、及びこれらの混合物、並びにジクロロジフルオロメタン、1,1−ジクロロ−1,1,2,2−テトロフルオロエタン、1−クロロ−1,1−ジフルオロ−2,2−トリフルオロエタン、1−クロロ−1,1−ジフルオロエチレン、1,1−ジフルオロエタン、ジメチルエーテル、モノクロロジフルオロメタン、トランス−1,3,3,3−テトラフルオロプロペン、及びこれらの混合物などのハロゲン化炭化水素からなる群から選択され、好ましくは、前記発泡剤は、プロパン及びイソブテン、トランス−1,3,3,3−テトラフルオロプロペン、及びこれらの混合物からなる群から選択される、請求項1〜7のいずれか一項に記載の発泡組成物。
- 前記組成物は、カチオン性ポリマーを更に含む、請求項1〜8のいずれか一項に記載の発泡組成物。
- 前記組成物は、コンディショニング剤を更に含み、好ましくは、前記コンディショニング剤は、シリコーンである、請求項1〜9のいずれか一項に記載の発泡組成物。
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