JP2016179935A5 - - Google Patents

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JP2016179935A5
JP2016179935A5 JP2016090381A JP2016090381A JP2016179935A5 JP 2016179935 A5 JP2016179935 A5 JP 2016179935A5 JP 2016090381 A JP2016090381 A JP 2016090381A JP 2016090381 A JP2016090381 A JP 2016090381A JP 2016179935 A5 JP2016179935 A5 JP 2016179935A5
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hydrogenated
mbh
polygermane
hydrogenating agent
hpa
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JP2016090381A
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JP2016179935A (ja
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Priority claimed from DE102009056731A external-priority patent/DE102009056731A1/de
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一実施形態によると、水素化は−６０℃〜２００℃の範囲から選択される温度で行うことが可能である。温度範囲は好ましくは−３０℃〜４０℃であり、より好ましくは−１０℃〜２５℃であってもよい。更に、水素化は1Pa〜2000hPa、好ましくは 1hPa〜1500hPa、より好ましくは20hPa〜1200hPaの範囲から選択される圧力下で行うことが可能である。よって、従来技術に比べると、水素化の条件は圧力も温度も低い穏やかものに設定される。このようにして、比較的不安定なハロゲン化ポリゲルマンでさえよい収率と高い転換率で水素化されうる。

Claims (2)

  1. プラズマ化学的に生成されたハロゲン化ポリゲルマンを、水素化される前に溶媒で希釈した後、−６０〜２００℃の温度、１Ｐａ〜２０００ｈＰａの圧力で、金属水素化物及び／又は半金属水素化物から選択される水素化合物の水素化剤と反応させて水素化することを特徴とする純粋化合物または複数の化合物の混合物としての水素化ポリゲルマンを製造する方法。
  2. 前記水素化剤は、ＭＨ、ＭＢＨ4、ＭＢＨ4-xＲx、ＭＡｌＨ4、ＡｌＨxＲ3-x、及びこれらの混合物を含むグループから選択されることを特徴とする請求項１に記載の方法。
JP2016090381A 2009-12-04 2016-04-28 水素化ポリゲルマンの製造方法及び水素化ポリゲルマン Pending JP2016179935A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009056731.3 2009-12-04
DE102009056731A DE102009056731A1 (de) 2009-12-04 2009-12-04 Halogenierte Polysilane und Polygermane

Related Parent Applications (1)

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JP2012541533A Division JP6297778B2 (ja) 2009-12-04 2010-12-06 水素化ポリゲルマンの製造方法及び水素化ポリゲルマン

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JP2016179935A JP2016179935A (ja) 2016-10-13
JP2016179935A5 true JP2016179935A5 (ja) 2017-01-05

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JP2012541538A Ceased JP2013512844A (ja) 2009-12-04 2010-12-06 ハロゲン化ポリシランを生成する方法
JP2012541535A Pending JP2013512842A (ja) 2009-12-04 2010-12-06 塩素化オリゴゲルマンとその製造方法
JP2012541539A Pending JP2013512845A (ja) 2009-12-04 2010-12-06 水素化ポリゲルマシランを製造するための方法および水素化ポリゲルマシラン
JP2012541533A Expired - Fee Related JP6297778B2 (ja) 2009-12-04 2010-12-06 水素化ポリゲルマンの製造方法及び水素化ポリゲルマン
JP2012541537A Expired - Fee Related JP5731531B2 (ja) 2009-12-04 2010-12-06 反応速度論的に安定した塩素化ポリシラン、この製造及び使用
JP2016090381A Pending JP2016179935A (ja) 2009-12-04 2016-04-28 水素化ポリゲルマンの製造方法及び水素化ポリゲルマン

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Application Number Title Priority Date Filing Date
JP2012541538A Ceased JP2013512844A (ja) 2009-12-04 2010-12-06 ハロゲン化ポリシランを生成する方法
JP2012541535A Pending JP2013512842A (ja) 2009-12-04 2010-12-06 塩素化オリゴゲルマンとその製造方法
JP2012541539A Pending JP2013512845A (ja) 2009-12-04 2010-12-06 水素化ポリゲルマシランを製造するための方法および水素化ポリゲルマシラン
JP2012541533A Expired - Fee Related JP6297778B2 (ja) 2009-12-04 2010-12-06 水素化ポリゲルマンの製造方法及び水素化ポリゲルマン
JP2012541537A Expired - Fee Related JP5731531B2 (ja) 2009-12-04 2010-12-06 反応速度論的に安定した塩素化ポリシラン、この製造及び使用

Country Status (9)

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US (7) US9139702B2 (ja)
EP (7) EP2507169A1 (ja)
JP (6) JP2013512844A (ja)
CN (3) CN102639644A (ja)
BR (2) BR112012014106A2 (ja)
CA (2) CA2782226A1 (ja)
DE (1) DE102009056731A1 (ja)
TW (7) TW201139283A (ja)
WO (7) WO2011067417A1 (ja)

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