JP5823404B2 - Cnt導入金属繊維材料及びそのための方法 - Google Patents
Cnt導入金属繊維材料及びそのための方法 Download PDFInfo
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Description
本出願は、2007年1月3日に出願された米国特許出願第11/619,327号の一部継続出願である。本出願は、2009年4月10日に出願された米国特許仮出願第61/168,516号、2009年4月14日に出願された米国特許仮出願第61/169,055号、2009年2月27日に出願された米国特許仮出願第61/155,935号、2009年3月3日に出願された米国特許仮出願第61/157,096号、及び2009年5月29日に出願された米国特許仮出願第61/182,153号に対して米国特許法119条に基づく優先権を主張し、それらの全内容は参照により本出願に組み込まれる。
・201:バリアコーティングを受け入れ可能とするための金属繊維材料の機能化。
・202:金属繊維材料へのバリアコーティング及びCNT形成触媒の塗布。
・204:カーボンナノチューブ合成に十分な温度への金属繊維材料の加熱。
・204:触媒含浸金属繊維上でのCVD媒介成長によるCNT合成。
この実施例は、電気的及び熱的性質の向上を目標として、連続プロセスにおいてどのようにCNTが金属繊維材料に導入され得るかを示す。
この実施例は、機械的性質、特に、せん断強度のような界面特性の向上を目標として、連続プロセスにおいてどのようにCNTが金属繊維材料に導入され得るかを示す。
Claims (15)
- カーボンナノチューブ(CNT)導入金属繊維材料を含んで構成された複合材料であって、
前記カーボンナノチューブ導入金属繊維材料は、
巻取り可能な寸法の金属繊維材料と、
前記金属繊維材料の周囲に形状に合わせて配置され、メチルシロキサン等のアルコキシシラン、アルモキサン、スピンオンガラス及びガラスナノ粒子からなる群から選択される材料を含むバリアコーティングと、
前記金属繊維材料に導入されたカーボンナノチューブ(CNT)と、
を含んで構成され、
前記CNTは均一な長さと均一な分布とを有する複合材料。 - 前記CNTの成長に使用される遷移金属ナノ粒子をさらに含んで構成される請求項1に記載の複合材料。
- 前記金属繊維材料へのCNTの導入は、前記金属繊維材料へのCNTの直接結合、前記CNTと前記金属繊維材料との間に配置された遷移金属ナノ粒子触媒を介した間接結合、前記CNTと前記金属繊維材料との間に配置された遷移金属ナノ粒子とバリアコーティングとを介した間接結合、前記CNTと前記金属繊維材料との間に配置されたバリアコーティングを介した間接結合、及びこれらの組み合わせから選択される結合モチーフを含む請求項1に記載の複合材料。
- 前記CNTは、1ミクロンから500ミクロンの長さを有する請求項1に記載の複合材料。
- 界面活性剤、帯電防止剤、潤滑剤、シロキサン、アルコキシシラン、アミノシラン、シラン、シラノール、プリビニルアルコール、でんぷん、及びこれらの混合物から選択されるサイジング剤をさらに含んで構成された請求項1に記載の複合材料。
- エポキシ、ポリエステル、ビニルエステル、ポリエーテルイミド、ポリエーテルケトンケトン、ポリフタルアミド、ポリエーテルケトン、ポリエーテルエーテルケトン、ポリイミド、フェノールホルムアルデヒド、及びビスマレイミドから選択されるマトリックス材をさらに含んで構成される請求項1に記載の複合材料。
- (a)巻取り可能な寸法の金属繊維材料の表面に、メチルシロキサン等のアルコキシシラン、アルモキサン、スピンオンガラス及びガラスナノ粒子からなる群から選択される材料を含むバリアコーティングとカーボンナノチューブ(CNT)形成触媒とを配置することと、
(b)前記金属繊維材料上にカーボンナノチューブを合成し、これによりカーボンナノチューブ導入金属繊維材料を形成することと、
を含んで構成される連続CNT導入方法。 - 前記金属繊維上に前記バリアコーティング又は触媒を配置する前に、前記金属繊維材料からサイジング剤を除去することをさらに含んで構成される請求項7に記載の方法。
- 前記バリアコーティングを配置する工程は、前記金属繊維材料上への前記CNT形成触媒の配置と同時である請求項7に記載の方法。
- 前記バリアコーティングは、前記金属繊維材料上に前記CNT形成触媒を配置する直前に、前記金属繊維材料上に形状に合わせて配置される請求項7に記載の方法。
- 前記金属繊維材料上に前記CNT形成触媒を配置する前に、前記バリアコーティングを部分硬化させることをさらに含んで構成される請求項10に記載の方法。
- 前記金属繊維材料上に前記CNT形成触媒を配置した後に、前記バリアコーティングを硬化させることをさらに含んで構成される請求項11に記載の方法。
- 前記カーボンナノチューブ導入金属繊維材料にサイジング剤を塗布することをさらに含んで構成される請求項7に記載の方法。
- 前記カーボンナノチューブ導入繊維材料にマトリックス材を塗布することをさらに含んで構成される請求項7に記載の方法。
- a)前記金属繊維材料上に第1のタイプの第1の量のカーボンナノチューブを合成することと、
b)前期金属繊維材料上に第2のタイプの第2の量のカーボンナノチューブを合成することと、
をさらに含んで構成され、
カーボンナノチューブの前記第1のタイプは、前記金属繊維材料の少なくとも1つの第1の性質を変化させるために選択され、
カーボンナノチューブの前記第2のタイプは、前記金属繊維材料の少なくとも1つの第2の性質を変化させるために選択される請求項7に記載の方法。
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ZA201203253B (en) | 2013-01-30 |
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CA2779449A1 (en) | 2011-05-05 |
JP2013509504A (ja) | 2013-03-14 |
KR101770194B1 (ko) | 2017-09-05 |
US20150299849A1 (en) | 2015-10-22 |
EP2496413A1 (en) | 2012-09-12 |
CN102648088A (zh) | 2012-08-22 |
WO2011053459A1 (en) | 2011-05-05 |
US20160130147A1 (en) | 2016-05-12 |
KR20120101406A (ko) | 2012-09-13 |
EP2496413A4 (en) | 2014-04-23 |
AU2010313615B2 (en) | 2015-02-05 |
CN102648088B (zh) | 2015-09-09 |
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