CN101980398A - 硫化锂的精制方法 - Google Patents

硫化锂的精制方法 Download PDF

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Publication number
CN101980398A
CN101980398A CN2010100021743A CN201010002174A CN101980398A CN 101980398 A CN101980398 A CN 101980398A CN 2010100021743 A CN2010100021743 A CN 2010100021743A CN 201010002174 A CN201010002174 A CN 201010002174A CN 101980398 A CN101980398 A CN 101980398A
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CN
China
Prior art keywords
lithium
lithium sulfide
sulfide
organic solvent
nmp
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Pending
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CN2010100021743A
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English (en)
Chinese (zh)
Inventor
清野美胜
千贺实
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Idemitsu Kosan Co Ltd
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Idemitsu Kosan Co Ltd
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Filing date
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Application filed by Idemitsu Kosan Co Ltd filed Critical Idemitsu Kosan Co Ltd
Publication of CN101980398A publication Critical patent/CN101980398A/zh
Pending legal-status Critical Current

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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562—Solid materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/06—Sulfates; Sulfites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/22—Alkali metal sulfides or polysulfides
    • C01B17/36—Purification
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0065—Solid electrolytes
    • H01M2300/0068—Solid electrolytes inorganic
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Secondary Cells (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN2010100021743A 2003-10-23 2004-10-15 硫化锂的精制方法 Pending CN101980398A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2003363403 2003-10-23
JP2003-363403 2003-10-23

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN2004800309857A Division CN1871177B (zh) 2003-10-23 2004-10-15 硫化锂的精制方法

Publications (1)

Publication Number Publication Date
CN101980398A true CN101980398A (zh) 2011-02-23

Family

ID=34510038

Family Applications (2)

Application Number Title Priority Date Filing Date
CN2010100021743A Pending CN101980398A (zh) 2003-10-23 2004-10-15 硫化锂的精制方法
CN2004800309857A Expired - Fee Related CN1871177B (zh) 2003-10-23 2004-10-15 硫化锂的精制方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN2004800309857A Expired - Fee Related CN1871177B (zh) 2003-10-23 2004-10-15 硫化锂的精制方法

Country Status (8)

Country Link
US (1) US8084160B2 (https=)
EP (1) EP1681263B1 (https=)
JP (1) JP4896520B2 (https=)
KR (1) KR101109821B1 (https=)
CN (2) CN101980398A (https=)
AT (1) ATE513788T1 (https=)
TW (1) TW200530121A (https=)
WO (1) WO2005040039A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110255587A (zh) * 2012-11-15 2019-09-20 阿克马法国公司 用于制备碱金属硫化物的方法

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US8012631B2 (en) 2005-12-09 2011-09-06 Idemitsu Kosan Co., Ltd Lithium ion conductive sulfide-based solid electrolyte and all-solid lithium battery using same
WO2009047977A1 (ja) 2007-10-11 2009-04-16 Idemitsu Kosan Co., Ltd. リチウムイオン伝導性固体電解質の製造方法
CN102099296A (zh) 2008-07-18 2011-06-15 里肯锂有限公司 从盐水中回收锂的方法
JP2010126422A (ja) 2008-11-28 2010-06-10 Panasonic Corp リチウム含有複合酸化物の製造方法および非水系二次電池
JP5448038B2 (ja) 2009-02-27 2014-03-19 公立大学法人大阪府立大学 硫化物固体電解質材料
JP5287739B2 (ja) 2009-05-01 2013-09-11 トヨタ自動車株式会社 固体電解質材料
JP5590836B2 (ja) 2009-09-09 2014-09-17 公立大学法人大阪府立大学 硫化物固体電解質
JP5168269B2 (ja) 2009-11-25 2013-03-21 トヨタ自動車株式会社 Ｌｉイオン伝導性材料およびリチウム電池
JP5629198B2 (ja) * 2009-12-04 2014-11-19 出光興産株式会社 アルカリ金属硫化物及びその製造方法
JP5141675B2 (ja) 2009-12-16 2013-02-13 トヨタ自動車株式会社 硫化物固体電解質材料の製造方法、硫化物固体電解質材料およびリチウム電池
KR101421905B1 (ko) 2010-08-05 2014-07-22 도요타 지도샤（주） 황화물 고체 전해질 유리, 리튬 고체 전지 및 황화물 고체 전해질 유리의 제조 방법
JP5729940B2 (ja) * 2010-08-13 2015-06-03 出光興産株式会社 固体電解質ガラス及びその製造方法
JP5521899B2 (ja) 2010-08-26 2014-06-18 トヨタ自動車株式会社 硫化物固体電解質材料およびリチウム固体電池
JP5349427B2 (ja) 2010-08-26 2013-11-20 トヨタ自動車株式会社 硫化物固体電解質材料、正極体およびリチウム固体電池
KR20140003514A (ko) * 2011-01-27 2014-01-09 이데미쓰 고산 가부시키가이샤 알칼리 금속 황화물과 도전제의 복합 재료
JP5708467B2 (ja) 2011-03-18 2015-04-30 トヨタ自動車株式会社 スラリー、固体電解質層の製造方法、電極活物質層の製造方法、および全固体電池の製造方法
JP5708233B2 (ja) 2011-05-18 2015-04-30 トヨタ自動車株式会社 硫化物固体電解質材料の製造方法および硫化物固体電解質材料
KR101963297B1 (ko) 2011-05-27 2019-03-28 알베마를 저머니 게엠베하 황화 리튬 준비 방법
DE102012209757A1 (de) * 2011-06-14 2012-12-20 Chemetall Gmbh Verfahren zur Herstellung eines kohlenstoffbeschichteten Lithiumsulfids und dessen Verwendung
JP5443445B2 (ja) 2011-07-06 2014-03-19 トヨタ自動車株式会社 硫化物固体電解質材料、リチウム固体電池、および、硫化物固体電解質材料の製造方法
JP5445527B2 (ja) 2011-07-13 2014-03-19 トヨタ自動車株式会社 硫化物固体電解質材料の製造方法
KR20140052058A (ko) 2011-09-22 2014-05-02 이데미쓰 고산 가부시키가이샤 이온 전도성 물질의 제조 방법
JP6234665B2 (ja) 2011-11-07 2017-11-22 出光興産株式会社 固体電解質
JP6203474B2 (ja) 2011-11-24 2017-09-27 出光興産株式会社 電極材料、電極及びそれを用いたリチウムイオン電池
JP6243103B2 (ja) 2012-06-29 2017-12-06 出光興産株式会社 正極合材
WO2014073197A1 (ja) 2012-11-06 2014-05-15 出光興産株式会社 固体電解質
JP5757284B2 (ja) 2012-12-27 2015-07-29 トヨタ自動車株式会社 硫化物固体電解質材料、リチウム固体電池、および、硫化物固体電解質材料の製造方法
JP6259617B2 (ja) 2013-04-24 2018-01-10 出光興産株式会社 固体電解質の製造方法
WO2014192309A1 (ja) 2013-05-31 2014-12-04 出光興産株式会社 固体電解質の製造方法
JP5673760B1 (ja) 2013-09-13 2015-02-18 トヨタ自動車株式会社 硫化物固体電解質の製造方法
CN103523806B (zh) * 2013-10-22 2014-11-12 瓮福（集团）有限责任公司 一种高纯度无水硫酸锂的制备方法
US10280109B2 (en) 2014-10-31 2019-05-07 Idemitsu Kosan Co., Ltd. Sulfide glass and crystalline solid electrolyte production method, crystalline solid electrolyte, sulfide glass and solid-state battery
JP6697398B2 (ja) 2014-12-16 2020-05-20 出光興産株式会社 硫化リチウム製造用装置及び硫化リチウムの製造方法
CN104609376A (zh) * 2015-01-30 2015-05-13 浙江工业大学 一种硫化锂粉体的制备方法
KR101684130B1 (ko) 2015-06-16 2016-12-07 현대자동차주식회사 리튬 이온 전도성 황화물의 제조방법, 이에 의하여 제조된 리튬 이온 전도성 황화물, 및 이를 포함하는 고체전해질, 전고체 배터리
CN105016310A (zh) * 2015-07-30 2015-11-04 广东先导稀材股份有限公司 一种高纯硫化锂的制备方法及装置
KR101930992B1 (ko) * 2016-02-15 2018-12-19 한양대학교 산학협력단 황화물계 고체 전해질의 제조방법, 이로부터 제조된 황화물계 고체 전해질 및 이를 포함하는 전고체 리튬 이차전지
KR101886036B1 (ko) 2016-08-22 2018-08-07 한국과학기술연구원 대기 안정성이 우수한 황화물계 고체전해질의 제조방법
JP6923173B2 (ja) 2016-12-14 2021-08-18 出光興産株式会社 硫黄含有複合体、その製造方法、及び固体電解質の製造方法
JP7294795B2 (ja) * 2017-11-17 2023-06-20 出光興産株式会社 硫化リチウム粉体、及びその製造方法
CN110790239B (zh) * 2019-08-26 2022-01-28 浙江工业大学 一种硫化锂粉体的机械球磨合成方法
CN112678781B (zh) * 2019-10-18 2022-04-15 天齐锂业（江苏）有限公司 硫化锂的制备方法
KR20220156838A (ko) * 2020-02-17 2022-11-28 솔리드 파워, 아이엔씨. 물-반응성 황화물 물질의 제조 방법
CN112624060B (zh) * 2020-12-31 2022-09-20 江西赣锋锂业股份有限公司 一种利用工业级丁基锂制备高纯硫化锂的方法
JP7120424B1 (ja) * 2021-09-30 2022-08-17 Ａｇｃ株式会社 硫化水素の精製方法、硫化リチウムの製造方法、硫化水素精製装置および硫化リチウム製造装置
KR102707192B1 (ko) * 2022-02-28 2024-09-20 주식회사 레이크테크놀로지 황화리튬 제조 장치
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KR102666522B1 (ko) * 2022-11-10 2024-05-16 전북대학교산학협력단 황화 리튬의 제조방법
KR20240112592A (ko) * 2023-01-12 2024-07-19 주식회사 이수스페셜티케미컬 황화 리튬의 제조 방법
DE102023102404A1 (de) 2023-02-01 2024-08-01 Albemarle Germany Gmbh Verfahren zur Herstellung von an Kohlenstoffverunreinigung reduziertem/Kohlenstoffverunreinigung freiem Lithiumsulfid, das Kohlenstoffverunreinigung reduzierte/Kohlenstoffverunreinigung freie Lithiumsulfid sowie dessen Verwendung zur Herstellung von Festelektrolyten und Feststoffbatterien
DE102023114082A1 (de) 2023-05-30 2024-12-05 Albemarle Germany Gmbh Verfahren zur Herstellung von an Kohlenstoffverunreinigung reduziertem/Kohlenstoffverunreinigung freiem Lithiumsulfid, das an Kohlenstoffverunreinigung reduzierte/Kohlenstoffverunreinigung freie Lithiumsulfid sowie dessen Verwendung zur Synthese von Festkörperelektrolyten und Herstellung von Feststoffbatterien
CN117163922B (zh) 2023-09-20 2024-03-26 天齐锂业股份有限公司 Ev级硫化锂及其制备方法
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CN110255587A (zh) * 2012-11-15 2019-09-20 阿克马法国公司 用于制备碱金属硫化物的方法

Also Published As

Publication number Publication date
US20070196739A1 (en) 2007-08-23
TWI366554B (https=) 2012-06-21
WO2005040039A1 (ja) 2005-05-06
TW200530121A (en) 2005-09-16
US8084160B2 (en) 2011-12-27
EP1681263A4 (en) 2008-06-25
EP1681263B1 (en) 2011-06-22
CN1871177B (zh) 2010-12-22
JPWO2005040039A1 (ja) 2007-03-01
EP1681263A8 (en) 2006-10-11
KR20060076316A (ko) 2006-07-04
CN1871177A (zh) 2006-11-29
JP4896520B2 (ja) 2012-03-14
ATE513788T1 (de) 2011-07-15
EP1681263A1 (en) 2006-07-19
KR101109821B1 (ko) 2012-03-13

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Application publication date: 20110223