JP2018535175A - ポリマーと金属酸化物との混合コーティングを有するガラス物品 - Google Patents
ポリマーと金属酸化物との混合コーティングを有するガラス物品 Download PDFInfo
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- JP2018535175A JP2018535175A JP2018517364A JP2018517364A JP2018535175A JP 2018535175 A JP2018535175 A JP 2018535175A JP 2018517364 A JP2018517364 A JP 2018517364A JP 2018517364 A JP2018517364 A JP 2018517364A JP 2018535175 A JP2018535175 A JP 2018535175A
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- Prior art keywords
- coating
- glass
- glass container
- coated
- metal oxide
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- 238000000576 coating method Methods 0.000 title claims abstract description 295
- 239000011248 coating agent Substances 0.000 title claims abstract description 281
- 229910044991 metal oxide Inorganic materials 0.000 title claims abstract description 66
- 150000004706 metal oxides Chemical class 0.000 title claims abstract description 66
- 229920000642 polymer Polymers 0.000 title description 72
- 239000000203 mixture Substances 0.000 claims abstract description 189
- 239000004642 Polyimide Substances 0.000 claims abstract description 109
- 229920001721 polyimide Polymers 0.000 claims abstract description 109
- 238000010438 heat treatment Methods 0.000 claims description 61
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 22
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 12
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 7
- 239000000523 sample Substances 0.000 description 88
- 238000012360 testing method Methods 0.000 description 57
- 238000000034 method Methods 0.000 description 41
- 239000012702 metal oxide precursor Substances 0.000 description 40
- 239000000126 substance Substances 0.000 description 33
- 239000000243 solution Substances 0.000 description 30
- 238000010586 diagram Methods 0.000 description 27
- 239000002243 precursor Substances 0.000 description 24
- PYGSKMBEVAICCR-UHFFFAOYSA-N hexa-1,5-diene Chemical group C=CCCC=C PYGSKMBEVAICCR-UHFFFAOYSA-N 0.000 description 19
- 239000007787 solid Substances 0.000 description 19
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 18
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- 239000013522 chelant Substances 0.000 description 16
- 230000008569 process Effects 0.000 description 16
- LSTSOJNBMMGIEY-UHFFFAOYSA-N butan-1-olate zirconium(4+) Chemical compound [Zr+4].CCCC[O-].CCCC[O-] LSTSOJNBMMGIEY-UHFFFAOYSA-N 0.000 description 15
- 239000003814 drug Substances 0.000 description 15
- 239000000463 material Substances 0.000 description 15
- 125000001971 neopentyl group Chemical group [H]C([*])([H])C(C([H])([H])[H])(C([H])([H])[H])C([H])([H])[H] 0.000 description 15
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- IWAUTUCYWHZANT-UHFFFAOYSA-M [Al+3].CC(C)[O-].CC(C)[O-].CC(=O)CC([O-])=O Chemical compound [Al+3].CC(C)[O-].CC(C)[O-].CC(=O)CC([O-])=O IWAUTUCYWHZANT-UHFFFAOYSA-M 0.000 description 12
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- 229910052726 zirconium Inorganic materials 0.000 description 9
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- 150000004645 aluminates Chemical class 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- 239000002585 base Substances 0.000 description 6
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- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
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- KVIKMJYUMZPZFU-UHFFFAOYSA-N propan-2-ol;titanium Chemical compound [Ti].CC(C)O.CC(C)O KVIKMJYUMZPZFU-UHFFFAOYSA-N 0.000 description 5
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- 239000000853 adhesive Substances 0.000 description 4
- 230000001070 adhesive effect Effects 0.000 description 4
- 239000005388 borosilicate glass Substances 0.000 description 4
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 description 4
- 230000008021 deposition Effects 0.000 description 4
- DYHSMQWCZLNWGO-UHFFFAOYSA-N di(propan-2-yloxy)alumane Chemical compound CC(C)O[AlH]OC(C)C DYHSMQWCZLNWGO-UHFFFAOYSA-N 0.000 description 4
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 229920003223 poly(pyromellitimide-1,4-diphenyl ether) Polymers 0.000 description 4
- 239000002356 single layer Substances 0.000 description 4
- 239000005361 soda-lime glass Substances 0.000 description 4
- 238000005728 strengthening Methods 0.000 description 4
- JMXKSZRRTHPKDL-UHFFFAOYSA-N titanium ethoxide Chemical compound [Ti+4].CC[O-].CC[O-].CC[O-].CC[O-] JMXKSZRRTHPKDL-UHFFFAOYSA-N 0.000 description 4
- 238000002834 transmittance Methods 0.000 description 4
- WOZZOSDBXABUFO-UHFFFAOYSA-N tri(butan-2-yloxy)alumane Chemical compound [Al+3].CCC(C)[O-].CCC(C)[O-].CCC(C)[O-] WOZZOSDBXABUFO-UHFFFAOYSA-N 0.000 description 4
- NXDMHKQJWIMEEE-UHFFFAOYSA-N 4-(4-aminophenoxy)aniline;furo[3,4-f][2]benzofuran-1,3,5,7-tetrone Chemical compound C1=CC(N)=CC=C1OC1=CC=C(N)C=C1.C1=C2C(=O)OC(=O)C2=CC2=C1C(=O)OC2=O NXDMHKQJWIMEEE-UHFFFAOYSA-N 0.000 description 3
- 229920013683 Celanese Polymers 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 229910004298 SiO 2 Inorganic materials 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
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- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical group [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 description 3
- 238000005496 tempering Methods 0.000 description 3
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Abstract
Description
ガラスバイアルの外面を、ジイソプロポキシドビスアセチルアセトネート及び6FDA−4−BDAFポリイミドを含むコーティング混合物で被覆し、TiO2及びポリイミドを含む固形コーティングを形成した。チタニウムジイソプロポキシドビスアセチルアセトネートの6FDA−4−BDAFポリイミドに重量比を、異なる試料で変化させた。
ガラスバイアルの外面を、ジルコニウム(IV)ジブトキシド(ビス−2,4−ペンタンジオナート)金属酸化物前駆体及び6FDA−4−BDAFポリイミドを含むコーティング混合物で被覆し、ZrO2及び6FDA−4−BDAFポリイミドを含む固形コーティングを形成した。ジルコニウム(IV)ジブトキシド(ビス−2,4−ペンタンジオナート)の6FDA−4−BDAFポリイミドに対する重量比を、異なる試料で変動させた。
ガラスバイアルの外面を、チタン(IV)ブトキシドポリマー及び6FDA−4−BDAFポリイミドを含むコーティング混合物で被覆し、TiO2及び6FDA−4−BDAFポリイミドを含む固形コーティングを形成した。チタン(IV)ブトキシドポリマーの6FDA−4−BDAFポリイミドに対する重量比は90/10であった。コーティングは、67.5質量%及び46.3体積%のTiO2を含んでいた。
ガラスバイアルの外面を、アルミニウム(ジイソプロポキシド)アセト酢酸エステルキレート及び6FDA−4−BDAFポリイミドを含むコーティング混合物で被覆し、Al2O3及びポリイミドを含む固形コーティングを形成した。チタニウムアルミニウム(ジイソプロポキシド)アセト酢酸エステルキレートの6FDA−4−BDAFポリイミドに対する重量比を、異なる試料で変動させた。この実施例は、四配位アルミネートが、本明細書に記載される方法に使用することができることを示している。
ガラスバイアルの外面を、アルミニウム−トリsec−ブトキシド及び6FDA−4−BDAFポリイミドを含むコーティング混合物で被覆し、Al2O3及びポリイミドを含む固形コーティングを形成した。アルミニウム−トリsec−ブトキシドの6FDA−4−BDAFポリイミドに対する重量比は90/10であった。コーティングは、78.8質量%及び59.5体積%のAl2O3を含んでいた。
ガラスバイアルの外面を、オルトケイ酸テトラエチル(TEOS)及び6FDA−4−BDAFポリイミドを含むコーティング混合物で被覆し、SiO2及びポリイミドを含む固形コーティングを形成した。TEOSの6FDA−4−BDAFポリイミドに対する重量比は50/50であった。コーティングは、22.38質量%及び14.35体積%のSiO2を含んでいた。
先の実施例に記載されるガラスバイアル(上述の方法で清浄及び調製した)を、メタノールで希釈した23.5質量%のアミノプロピルシルセスキオキサン水溶液(ABCR社から参照番号AB127715として市販される)で被覆し、2質量/体積%のシルセスキオキサン溶液を得た。バイアルを、80cm/分の引き上げ速度を用いて、シルセスキオキサン溶液でディップコーティングし、150℃で8分間、乾燥させた。PMDA−ODA(Sigma Aldrich社からKaptonポリイミドとして市販される)の第2のコーティングを、Fadeevらに対する米国特許出願公開第2013/0171456号明細書に記載されるように、シルセスキオキサンコーティングの上に施した。詳細には、10gのPMDA−ODAポリアミド酸溶液(12.0質量%±0.5質量%[80%NMP/20%キシレン]に1.16gのトリエチルアミンを加えることによって、ポリアミド酸をそのポリアミド酸塩に変換させた。強攪拌の後、28.84gのメタノールを加えて3質量%溶液を形成した。シルセスキオキサンで被覆後、噴霧法を使用して、バイアルを、メタノール中、0.5%のPMDA−ODAポリアミド酸塩で被覆した。被覆されたバイアルを、360℃で15分間硬化させ、320℃で5時間及び335℃で16時間、熱に曝露することによって脱パイロジェン化した。脱パイロジェンされていない(硬化されたままの)試料及び脱パイロジェン化された試料を、30Nの垂直荷重で、バイアル・オン・バイアルジグでスクラッチした。バイアルは、バイアル同士の接触試験における低い摩擦係数及び良好なガラス保護を示したが、黄色を呈していた。図13は、被覆されていないバイアル(511)、硬化されたままの比較例3のコーティングで被覆されたバイアル(518)、比較例3のコーティングで被覆され、300℃に12時間曝露されたバイアル(516)、比較例3のコーティングで被覆され、335℃に16時間曝露されたバイアル(517)、及び比較例3のコーティングで被覆され、320℃に5時間曝露されたバイアル(519)についてのCIE XYZ色座標を示している。McAdamsの楕円は、脱パイロジェン条件の前でさえ、被覆されていないバイアルに対する色差が目視で検出可能であることを示している。
ガラス容器の外面である第1の表面と、該第1の表面とは反対側の第2の表面とを含むガラス容器、及び
前記ガラス容器の前記第1の表面の少なくとも一部分に位置付けられたコーティング
を含む、薬剤用パッケージであって、前記コーティングが、
1つ以上のポリイミド組成物、及び
1つ以上の金属酸化物組成物
を含み、
前記1つ以上のポリイミド組成物と前記1つ以上の金属酸化物組成物とが、前記コーティングに混合されている、
薬剤用パッケージ。
前記1つ以上の金属酸化物組成物の前記1つ以上のポリイミド組成物に対する重量比が、約20/80〜約95/5であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングにおける前記1つ以上の金属酸化物組成物の総量が、約20質量%〜約95質量%であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングにおける前記1つ以上のポリイミド組成物の総量が、約5質量%〜約80質量%であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングにおけるポリイミドと金属酸化物との組合せが、前記コーティングの少なくとも約50質量%を構成することを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記1つ以上の金属酸化物組成物のうちの少なくとも1つが、ジルコニア、アルミナ、又はチタニアであることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングが、100nm以下の厚さを有することを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記1つ以上のポリイミド組成物がフッ素化されていることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングが、前記ガラス容器の前記第1の表面の少なくとも一部分に結合していることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングを有する前記ガラス容器の前記第1の表面の前記一部分が、約0.7以下の摩擦係数を有することを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングを有する前記ガラス容器の前記第1の表面の前記一部分が、少なくとも約250℃の温度で30分間の加熱処理の後に、約0.7以下の摩擦係数を保持することを特徴とする、実施形態10に記載の薬剤用パッケージ。
前記薬剤用パッケージを通る光透過率が、約400nm〜約700nmの各波長について、被覆されていない薬剤用パッケージを通る光透過率の約55%以上であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記薬剤用パッケージが、少なくとも約250℃の温度で30分間の加熱処理の後に、約400nm〜約700nmの各波長について、前記被覆されていない薬剤用パッケージを通る光透過率の約55%以上の前記薬剤用パッケージを通る光透過率を保持することを特徴とする、実施形態12に記載の薬剤用パッケージ。
前記1つ以上の金属酸化物組成物の前記1つ以上のポリイミド組成物に対する重量比が、90:10以上であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記1つ以上の金属酸化物組成物の前記1つ以上のポリイミド組成物に対する重量比が、約35/65以上であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記1つ以上の金属酸化物組成物の前記1つ以上のポリイミド組成物に対する重量比が、約50/50以上であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記1つ以上の金属酸化物組成物の前記1つ以上のポリイミド組成物に対する重量比が、約75/25以上であることを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングにおけるポリイミドと金属酸化物との組合せが、前記コーティングの少なくとも約90質量%を構成することを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングにおけるポリイミドと金属酸化物との組合せが、前記コーティングの少なくとも約95質量%を構成することを特徴とする、実施形態1に記載の薬剤用パッケージ。
前記コーティングにおけるポリイミドと金属酸化物との組合せが、前記コーティングの少なくとも約99質量%を構成することを特徴とする、実施形態1に記載の薬剤用パッケージ。
薬剤用パッケージの製造方法において、
ガラス容器の外面の第1の表面にコーティング混合物を堆積させる工程であって、該コーティング混合物が、
1つ以上の金属酸化物前駆体、及び
1つ以上のポリマー組成物、1つ以上のポリマー前駆体、又はその両方
を含む、工程と、
前記コーティング混合物を加熱して、前記ガラス容器の前記外面にコーティングを形成する工程であって、該コーティングが、
1つ以上のポリマー組成物、及び
1つ以上の金属酸化物組成物
を含む、工程と
を含む、方法。
少なくとも1つの金属酸化物前駆体が、チタネート、ジルコネート、アルミン酸ジルコニウム、アルミネート、若しくはそれらの加水分解物又はオリゴマーから選択されることを特徴とする、実施形態21に記載の方法。
少なくとも1つの金属酸化物前駆体が、テトラ−オルトチタネート、六配位キレート化チタネート、ポリマー性チタネート、若しくはそれらの加水分解物又はオリゴマーから選択されることを特徴とする、実施形態21に記載の方法。
少なくとも1つの金属酸化物前駆体が、テトラエチルオルトチタネート;テトラメチルオルトチタネート;テトライソプロピルオルトチタネート;テトラペンチルオルトチタネート;テトラオクチルオルトチタネート;テトラドデシルオルトチタネート;テトラ−2−エチルヘキシルオルトチタネート;テトラベンジルオルトチタネート;テトラシクロヘキシルオルトチタネート;テトラフェニルオルトチタネート;テトラエトキシエチルオルトチタネート;テトラ−n−ブチルチタネート;テトラキス(2−エチルヘキシル)チタネート;テトラ−ベータ−ナフチルオルトチタネート;若しくはそれらの加水分解物又はオリゴマーから選択される、テトラ−オルトチタネート若しくはそれらの加水分解物又はオリゴマーであることを特徴とする、実施形態21に記載の方法。
少なくとも1つの金属酸化物前駆体が、チタンアセチルアセトナート;ジイソプロポキシチタンビス(アセチルアセトナート);チタンアセチルアセトナートビス(ペンタン−2,4−ジオナト−O,O’)ビス(アルカノラト)チタン;ジイソプロポキシ−ビス(エチルアセトアセタト)チタン;チタン(IV)(トリエタノールアミナト)イソプロポキシド;若しくはそれらの加水分解物又はオリゴマーから選択される、六配位キレート化チタネート、若しくはそれらの加水分解物又はオリゴマーであることを特徴とする、実施形態21に記載の方法。
少なくとも1つの金属酸化物前駆体が、ジルコニウム含有金属酸化物前駆体であることを特徴とする、実施形態21に記載の方法。
前記ジルコニウム含有金属酸化物前駆体が、ジルコニウムアセチルアセトナート;ジルコニウムtert−ブトキシド;ジルコニウムヘキサフルオロアセチルアセトナート;ナフテン酸ジルコニウム;ジルコニウムプロポキシド;ジルコニウムイソプロポキシド;アルミン酸ジルコン;テトラ(2,2−ジアリルオキシメチル)ブチル、ジ(ジトリデシル)ホスフィトジルコネート;ネオペンチル(ジアリル)オキシ−トリネオデカノイルジルコネート;ネオペンチル(ジアリル)オキシ−トリ(ドデシル)ベンゼン−スルホニルジルコネート;ネオペンチル(ジアリル)オキシ−トリ(ジオクチル)ホスファトジルコネート;ネオペンチル(ジアリル)オキシ−トリ(ジオクチル)−ピロホスファトジルコネート;ネオペンチル(ジアリル)オキシ−トリ(N−エチレンジアミノ)エチルジルコネート;ネオペンチル(ジアリル)オキシ−トリ(m−アミノ)フェニルジルコネート;ネオペンチル(ジアリル)オキシ−トリメタクリルジルコネート;ネオペンチル(ジアリル)オキシ−トリアクリルジルコネート;ジネオペンチル(ジアリル)オキシ−ジパラアミノベンゾイルジルコネート;ジネオペンチル(ジアリル)オキシ−ジ(3−メルカプト)プロピオン酸ジルコネート;若しくはそれらの加水分解物又はオリゴマーから選択されることを特徴とする、実施形態26に記載の方法。
少なくとも1つの金属酸化物前駆体が、四配位アルミン酸金属酸化物前駆体であることを特徴とする、実施形態21に記載の方法。
ガラス容器の外面である第1の表面と、該第1の表面とは反対側の第2の表面とを含むガラス容器、及び
前記ガラス容器の前記第1の表面の少なくとも一部分に位置付けられたコーティング
を含む、薬剤用パッケージであって、前記コーティングが、
1つ以上のポリマー組成物、及び
1つ以上の金属酸化物組成物
を含み、
前記1つ以上のポリマー組成物及び前記1つ以上の金属酸化物組成物が、前記コーティングに混合されており、
前記1つ以上の金属酸化物組成物の前記1つ以上のポリマー組成物に対する重量比が約20/80〜約95/5であり、かつ
前記コーティングにおけるポリマーと金属酸化物との組合せが、前記コーティングの少なくとも約95質量%を構成する、
薬剤用パッケージ。
前記1つ以上のポリマー組成物の1つ以上がポリイミドであることを特徴とする、実施形態29に記載の薬剤用パッケージ。
102 ガラス本体
104 ガラス容器壁
106 内部容積
108 外面
110 内面
120 コーティング
122 外面
124 ガラス本体接触表面
200 バイアル・オン・バイアル試験用ジグ
210 第1のガラス容器
212 第1のクランプ
214 第1の固定アーム
216 第1のベース
220 第2のガラス容器
222 第2のクランプ
224 第2の固定アーム
226 第2のベース
230 接触点
Claims (10)
- ガラス容器の外面である第1の表面と、該第1の表面とは反対側の第2の表面とを含むガラス容器、及び
前記ガラス容器の前記第1の表面の少なくとも一部分に位置付けられたコーティング
を含む、薬剤用パッケージであって、前記コーティングが、
1つ以上のポリイミド組成物、及び
1つ以上の金属酸化物組成物
を含み、
前記1つ以上のポリイミド組成物と前記1つ以上の金属酸化物組成物とが、前記コーティングに混合されている、
薬剤用パッケージ。 - 前記1つ以上の金属酸化物組成物の前記1つ以上のポリイミド組成物に対する重量比が、約20/80〜約95/5であることを特徴とする、請求項1に記載の薬剤用パッケージ。
- 前記コーティングにおける前記1つ以上の金属酸化物組成物の総量が、約20質量%〜約95質量%であることを特徴とする、請求項1又は2に記載の薬剤用パッケージ。
- 前記コーティングにおける前記1つ以上のポリイミド組成物の総量が、約5質量%〜約80質量%であることを特徴とする、請求項1〜3のいずれか一項に記載の薬剤用パッケージ。
- 前記コーティングにおけるポリイミドと金属酸化物との組合せが、前記コーティングの少なくとも約50質量%を構成することを特徴とする、請求項1〜4のいずれか一項に記載の薬剤用パッケージ。
- 前記1つ以上の金属酸化物組成物のうちの少なくとも1つが、ジルコニア、アルミナ、又はチタニアであることを特徴とする、請求項1〜5のいずれか一項に記載の薬剤用パッケージ。
- 前記コーティングが、100nm以下の厚さを有することを特徴とする、請求項1〜6のいずれか一項に記載の薬剤用パッケージ。
- 前記1つ以上のポリイミド組成物がフッ素化されていることを特徴とする、請求項1〜7のいずれか一項に記載の薬剤用パッケージ。
- 前記コーティングを有する前記ガラス容器の前記第1の表面の前記一部分が、約0.7以下の摩擦係数を有することを特徴とする、請求項1〜8のいずれか一項に記載の薬剤用パッケージ。
- 前記コーティングを有する前記ガラス容器の前記第1の表面の前記一部分が、少なくとも約250℃の温度で30分間の加熱処理の後に、約0.7以下の摩擦係数を保持することを特徴とする、請求項9に記載の薬剤用パッケージ。
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RU2018118562A (ru) | 2019-12-02 |
US20230391506A1 (en) | 2023-12-07 |
TWI734711B (zh) | 2021-08-01 |
RU2729081C2 (ru) | 2020-08-04 |
CA3001514A1 (en) | 2017-05-04 |
US20210300625A1 (en) | 2021-09-30 |
TW201720778A (zh) | 2017-06-16 |
KR20180075547A (ko) | 2018-07-04 |
TW202146355A (zh) | 2021-12-16 |
EP4008695A1 (en) | 2022-06-08 |
RU2018118562A3 (ja) | 2020-03-19 |
MX2018005349A (es) | 2018-05-17 |
US11772846B2 (en) | 2023-10-03 |
US20170121058A1 (en) | 2017-05-04 |
CN108349789A (zh) | 2018-07-31 |
BR112018008744B1 (pt) | 2022-09-06 |
US20230391505A1 (en) | 2023-12-07 |
EP3368491B1 (en) | 2022-04-13 |
WO2017075435A1 (en) | 2017-05-04 |
CA3001514C (en) | 2024-06-04 |
BR112018008744A8 (pt) | 2019-02-26 |
AU2016343719A1 (en) | 2018-04-26 |
SG11201803373UA (en) | 2018-05-30 |
TWI825443B (zh) | 2023-12-11 |
KR102658016B1 (ko) | 2024-04-16 |
EP3368491A1 (en) | 2018-09-05 |
JP6993964B2 (ja) | 2022-01-14 |
AU2016343719B2 (en) | 2021-03-04 |
BR112018008744A2 (pt) | 2018-10-30 |
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