JP2005276846A - 蛍光ランプ - Google Patents
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- H—ELECTRICITY
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- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
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- C09K11/7797—Borates
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- H01J61/02—Details
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- H—ELECTRICITY
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- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J61/00—Gas-discharge or vapour-discharge lamps
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- H01J61/38—Devices for influencing the colour or wavelength of the light
- H01J61/42—Devices for influencing the colour or wavelength of the light by transforming the wavelength of the light by luminescence
- H01J61/44—Devices characterised by the luminescent material
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- H—ELECTRICITY
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- H01J61/70—Lamps with low-pressure unconstricted discharge having a cold pressure < 400 Torr
- H01J61/76—Lamps with low-pressure unconstricted discharge having a cold pressure < 400 Torr having a filling of permanent gas or gases only
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- H—ELECTRICITY
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- H01J65/046—Lamps in which a gas filling is excited to luminesce by an external electromagnetic field or by external corpuscular radiation, e.g. for indicating plasma display panels by an external electromagnetic field the field being produced by using capacitive means around the vessel
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- H05B41/00—Circuit arrangements or apparatus for igniting or operating discharge lamps
- H05B41/14—Circuit arrangements
- H05B41/26—Circuit arrangements in which the lamp is fed by power derived from dc by means of a converter, e.g. by high-voltage dc
- H05B41/28—Circuit arrangements in which the lamp is fed by power derived from dc by means of a converter, e.g. by high-voltage dc using static converters
- H05B41/2806—Circuit arrangements in which the lamp is fed by power derived from dc by means of a converter, e.g. by high-voltage dc using static converters with semiconductor devices and specially adapted for lamps without electrodes in the vessel, e.g. surface discharge lamps, electrodeless discharge lamps
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Abstract
【解決手段】蛍光体被膜が、次の蛍光体、すなわち赤色蛍光体Rとして一般式(YxGdyEuz)BO3(ここで0≦x≦0.99、0≦y≦0.99、0.01≦z≦0.2及びx+y+z≒1)による混合ホウ酸塩、緑色蛍光体Gとして一般式(LnxCeyScwTbz)PO4(ここでLnはLa、Y又はGdの1つ又はこれらの元素の混合物であり、0.35≦x≦0.95、0≦y≦0.5、0≦w≦0.2、0.05≦z≦0.5でw+x+y+z≒1)による混合リン酸塩、青色蛍光体Bとして一般式(BaxEuy)MgAl10O17(ここで0.6≦x≦0.97、0.03≦y≦0.4及びx+y≒1)による混合アルミン酸塩を含み、混合物の重量割合は0.2<R<0.5、0.4<G<0.7、0.05<B<0.15及びR+G+B=1が当てはまる。
【選択図】 図6b
Description
赤色蛍光体Rとして一般式
(YxGdyEuz)BO3
(ここで0≦x≦0.99、0≦y≦0.99、0.01≦z≦0.2及びx+y+z≒1)による混合ホウ酸塩、
緑色蛍光体Gとして一般式
(LnxCeyScwTbz)PO4
(ここでLnはLa、Y又はGdの1つ又はこれらの元素の混合物であり、0.35≦x≦0.95、0≦y≦0.5、0≦w≦0.2、0.05≦z≦0.5でw+x+y+z≒1)による混合リン酸塩、
青色蛍光体Bとして一般式
(BaxEuy)MgAl10O17
(ここで0.6≦x≦0.97、0.03≦y≦0.4及びx+y≒1)による混合アルミン酸塩
を含み、混合物の重量割合は0.2<R<0.5、0.4<G<0.7、0.05<B<0.15及びR+G+B=1が当てはまることによって解決される。
本発明の有利な実施態様によれば、蛍光体の表面及び/又は蛍光体被膜の表面が保護被膜を備えている。本発明の他の有利な実施態様によれば、保護被膜がMgF2から成る。
光体の主放出は約610nm、緑色蛍光体の主放出は約540nm、青色蛍光体の主放出は約450nmに位置しなければならない(例えば、エイ・ダブリュ・トルントン「J.Opt.Soc.Am.61」(1971年)第1155頁参照)。
第1のクラスでは、入射した真空紫外線放射パワーの50%以上はホスト格子によって吸収され、このホスト格子から発光中心へ転移される。真空紫外線放射パワーの残余量は例えば活性剤原子によって直接吸収される。このための例は赤色蛍光体(YxGdyEuz)BO3である。三価ユーロピウムEu3+を用いて活性化した混合ホウ酸塩が使用される。x、y及びzに適した値は0≦x≦0.99、0≦y≦0.99、0.01≦z≦0.2、特に0.55≦x≦0.87、0.1≦y≦0.3及び0.03≦z≦0.15であり、その場合それぞれ境界条件x+y+z≒1が満たされる。青色蛍光体用の例は二価ユーロピウムEu2+を用いて活性化した混合アルミン酸塩(BaxEuy)MgAl10O17である。x及びyに適した値は0.6≦x≦0.97、0.03≦y≦0.4、特に0.8≦x≦0.95、0.05≦y≦0.2であり、その場合それぞれx+y≒1が当てはまる。
三価テルビウムTb3+を用いて活性化した緑色蛍光体用の例は、
1)混合アルミン酸塩(YxGdyTbz)3Al5O12、その場合0.1≦x≦0.99、0≦y≦0.9、0.03≦z≦0.4及びx+y+z≒1、特にy=0、0.8≦x≦0.99、0.01≦z≦0.2及びx+z≒1が当てはまり、
2)混合ケイ酸塩(YxScyTbz)2SiO5、その場合0.6≦x≦0.99、0≦y≦0.1、0.01≦z≦0.4及びx+y+z≒1が当てはまり、並びに
3)混合ホウ酸塩(YxGdyTbz)BO3、その場合0≦x≦0.99、0≦y≦0.99、0.01≦z≦0.4、特に0.55≦x≦0.8、0.1≦y≦0.3、0.03≦z≦0.2及びx+y+z≒1が当てはまる。
光帯域端が真空紫外線波長範囲の上限に接近すればする程、ホスト格子による真空紫外線の吸収が多くなる。極端な場合、専らホスト格子吸収が現れる、すなわち活性剤が有っても無くても同じ吸収が生ずる。
蛍光体のこのクラスの例としては一般式(LnxCeyScwTbz)PO4に応じて三価テルビウムTb3+を用いて活性化した混合リン酸塩がある。なお、Lnは元素ランタンLa、イットリウムY又はガドリニウムGdの1つ、又はこれらの元素の混合物を表す。x、y、w及びzに適した値は0.35≦x≦0.95、0≦y≦0.5、0≦w≦0.2、0.05≦z≦0.5、特にw=0、0.45≦x≦0.8、0.1≦y≦0.3、0.1≦z≦0.25であり、w+x+y+z≒1が当てはまる。
この場合、励起パワーは殆ど専ら活性剤Tb3+自体によって吸収される。波長254nmの放射によって励起する際に増感剤として必要なCe3+はこの場合このクラスの蛍光体に対する真空紫外線励起にはそれ程重要ではなく、ランプ効率を変えることなく、多分省略することができる。Ce3+がこれに関連してそもそも(たとえ小さくても)改善をもたらすか否かはまだ最終的に解明されていない。
図2は緑色蛍光体CeMgAl11O19:Tb3+の真空紫外線励起スペクトルを示す。
図3は青色蛍光体BaMgAl10O17:Eu2+の真空紫外線励起スペクトルを示す。
図4は赤色蛍光体(Y0.72Gd0.2Eu0.08)BO3の真空紫外線励起スペクトルを示す。
図5は緑色蛍光体(La0.43Ce0.39Tb0.18)PO4の真空紫外線励起スペクトルを示す。
図6aは本発明による3波長域発光形蛍光体被膜を備えた新形蛍光ランプの側面図を示す。
図6bは図6aのA−A線に沿って示した蛍光ランプの断面図を示す。
図7は図6a及び図6bに示された3波長域発光形蛍光ランプの発光スペクトルを示す。
第1の実施例は好適な発光スペクトルを有する赤色蛍光体である。この赤色蛍光体は三価ユーロピウムを用いて活性化した希土類−混合ホウ酸塩である。次の表1は異なった組成を有する蛍光体を示し、最初の組成はイットリウムY及びガドリニウムGdを含み、次の2つの組成はイットリウムのみ、又はガドリニウムのみを含む。図4には蛍光体No.1の励起スペクトルが示されている。
第2の実施例は好適な発光スペクトルを有する緑色蛍光体である。この緑色蛍光体は三価テルビウムを用いて活性化した希土類−混合リン酸塩である。次の表2は異なった組成を有する蛍光体を示し、その組成は一部がさらに共活性剤として三価セリウム又はスカンジウムをドープされている。最初の4つの蛍光体はランタンLaを含んでいる。次の4つの蛍光体ではランタンはイットリウムYによって置換され、その場合蛍光体No.8はさらにスカンジウムScを添加されている。最後の3つの蛍光体ではランタンはガドリニウムGdによって置換され、その場合最後の蛍光体にはさらにスカンジウムScが添加されている。図5は蛍光体(La0.44Ce0.43Tb0.13)PO4の励起スペクトルを示す。
第3の実施例は非常に好適な発光スペクトルを有する緑色蛍光体である。次の表3に示されているように、この緑色蛍光体は三価テルビウムを用いて活性化した2つのホウ酸イットリウムであり、その場合No.2はさらにガドリニウムを含んでいる。
第4の実施例は別の緑色蛍光体である。この緑色蛍光体は三価テルビウムを用いて活性化した希土類−混合ケイ酸塩であり、これは組成(Y0.924Sc0.002Tb0.074)SiO5に従ってイットリウム及びスカンジウムを含んでいる。次の値が検出された。EXe=0.94、QXe *=0.8。
第5の実施例は2つの別の緑色蛍光体である。この緑色蛍光体は三価テルビウムを用いて活性化した希土類−混合アルミン酸塩である。第1の蛍光体は次の組成(Y0.9Tb0.1)3Al5O12を持つアルミン酸イットリウムである。次の値が検出された。EXe=0.94、QXe *=0.76。特性上同じである第2の蛍光体ではイットリウムがガドリニウムによって20%置換されている。即ち(Y0.7Gd0.2Tb0.1)3Al5O12である。
第6の実施例は青色蛍光体である。この青色蛍光体は組成(Ba0.94Eu0.06)MgAl10O17に従って二価ユーロピウムを用いて活性化した混合アルミン酸塩である。次の値が検出された。EXe=0.96、QXe *=0.86。
図6aには特に照明用に適する蛍光ランプ1の側面図が示され、図6bにはその断面図が示されている。円筒状放電管2は0.7mmの厚みのDURAN(登録商標)ガラス(ショット社)から構成されて、約50mmの直径を有し、173hPaの圧力でキセノンが封入されている。放電管2の内部の中心軸線上には円形断面と2mmの直径とを有する特殊鋼製の棒から構成された内部電極3が配設されている。放電管2の外壁上には軸平行で12個に均等に分割された1mm幅及び8cm長の高導電性銀条帯が外部電極4として配設されている。放電管2の内壁は蛍光体膜6で被覆されている。この蛍光体膜6は青色成分B:(Ba0.94Eu0.06)MgAl10O17、緑色成分G:(La0.43Ce0.39Tb0.18)PO4及び赤色成分R:(Y0.72Gd0.2Eu0.08)BO3を有する3波長域発光形蛍光体混合物である。各成分はB:G:R=0.085:0.555:0.36の比で混合されている。内部電極3はエジソンねじ込み口金7によってパルス状の周期的な電圧が印加され、この電圧は外部電極に対して約4kVの大きさであり、約1.2μsの平均パルス継続時間と約25kHzのパルス周波数とを有している。それによって、40lm/Wのランプ効率が得られた。色温度は4000K、CIEに基づく標準色度図による色位置は座標x=0.38、y=0.377である。このランプの発光スペクトルは図6に示されている。
2 円筒状放電管
3 内部電極
4 外部電極
6 蛍光体膜
7 口金
Claims (3)
- ランプガラス球の内壁面上に蛍光体被膜を備え、ランプガラス球の内部に145nm〜185nmの範囲の波長を持つ真空紫外線放射が作られる蛍光ランプにおいて、蛍光体被膜が、次の蛍光体、すなわち
赤色蛍光体Rとして一般式
(YxGdyEuz)BO3
(ここで0≦x≦0.99、0≦y≦0.99、0.01≦z≦0.2及びx+y+z≒1)による混合ホウ酸塩、
緑色蛍光体Gとして一般式
(LnxCeyScwTbz)PO4
(ここでLnはLa、Y又はGdの1つ又はこれらの元素の混合物であり、0.35≦x≦0.95、0≦y≦0.5、0≦w≦0.2、0.05≦z≦0.5でw+x+y+z≒1)による混合リン酸塩、
青色蛍光体Bとして一般式
(BaxEuy)MgAl10O17
(ここで0.6≦x≦0.97、0.03≦y≦0.4及びx+y≒1)による混合アルミン酸塩
を含み、混合物の重量割合は0.2<R<0.5、0.4<G<0.7、0.05<B<0.15及びR+G+B=1が当てはまる
ことを特徴とする蛍光ランプ。 - 蛍光体の表面及び/又は蛍光体被膜の表面が保護被膜を備えていることを特徴とする請求項1記載の蛍光ランプ。
- 保護被膜がMgF2から成ることを特徴とする請求項2記載の蛍光ランプ。
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4311197A DE4311197A1 (de) | 1993-04-05 | 1993-04-05 | Verfahren zum Betreiben einer inkohärent strahlenden Lichtquelle |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP52154694A Division JP3714952B2 (ja) | 1993-04-05 | 1994-04-05 | 誘電体妨害放電蛍光ランプ |
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JP2005276846A true JP2005276846A (ja) | 2005-10-06 |
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Family Applications (6)
Application Number | Title | Priority Date | Filing Date |
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JP52154694A Expired - Fee Related JP3714952B2 (ja) | 1993-04-05 | 1994-04-05 | 誘電体妨害放電蛍光ランプ |
JP52154594A Expired - Lifetime JP3298886B2 (ja) | 1993-04-05 | 1994-04-05 | インコヒーレント放出放射源の作動方法 |
JP2001347842A Expired - Lifetime JP3715231B2 (ja) | 1993-04-05 | 2001-11-13 | インコヒーレント放出放射源の作動方法 |
JP2004162737A Withdrawn JP2004296446A (ja) | 1993-04-05 | 2004-06-01 | 蛍光ランプ |
JP2004162736A Pending JP2004303737A (ja) | 1993-04-05 | 2004-06-01 | 蛍光ランプ |
JP2005166606A Pending JP2005276846A (ja) | 1993-04-05 | 2005-06-07 | 蛍光ランプ |
Family Applications Before (5)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP52154694A Expired - Fee Related JP3714952B2 (ja) | 1993-04-05 | 1994-04-05 | 誘電体妨害放電蛍光ランプ |
JP52154594A Expired - Lifetime JP3298886B2 (ja) | 1993-04-05 | 1994-04-05 | インコヒーレント放出放射源の作動方法 |
JP2001347842A Expired - Lifetime JP3715231B2 (ja) | 1993-04-05 | 2001-11-13 | インコヒーレント放出放射源の作動方法 |
JP2004162737A Withdrawn JP2004296446A (ja) | 1993-04-05 | 2004-06-01 | 蛍光ランプ |
JP2004162736A Pending JP2004303737A (ja) | 1993-04-05 | 2004-06-01 | 蛍光ランプ |
Country Status (10)
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US (2) | US5714835A (ja) |
EP (4) | EP0738311B1 (ja) |
JP (6) | JP3714952B2 (ja) |
KR (1) | KR100299151B1 (ja) |
CN (1) | CN1066854C (ja) |
CA (2) | CA2159906C (ja) |
CZ (1) | CZ286740B6 (ja) |
DE (5) | DE4311197A1 (ja) |
HU (1) | HU215307B (ja) |
WO (2) | WO1994022975A1 (ja) |
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- 1994-04-05 EP EP00124154A patent/EP1076084B1/de not_active Expired - Lifetime
- 1994-04-05 JP JP52154694A patent/JP3714952B2/ja not_active Expired - Fee Related
- 1994-04-05 WO PCT/DE1994/000382 patent/WO1994022975A1/de active IP Right Grant
- 1994-04-05 EP EP00121142A patent/EP1078972B1/de not_active Expired - Lifetime
- 1994-04-05 JP JP52154594A patent/JP3298886B2/ja not_active Expired - Lifetime
- 1994-04-05 WO PCT/DE1994/000380 patent/WO1994023442A1/de active IP Right Grant
- 1994-04-05 HU HU9502905A patent/HU215307B/hu unknown
- 1994-04-05 EP EP94911103A patent/EP0733266B1/de not_active Expired - Lifetime
-
2001
- 2001-11-13 JP JP2001347842A patent/JP3715231B2/ja not_active Expired - Lifetime
-
2004
- 2004-06-01 JP JP2004162737A patent/JP2004296446A/ja not_active Withdrawn
- 2004-06-01 JP JP2004162736A patent/JP2004303737A/ja active Pending
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2005
- 2005-06-07 JP JP2005166606A patent/JP2005276846A/ja active Pending
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