JP2020533423A - シリコーンポリエーテルコポリマー、それを含むシーラント、および関連する方法 - Google Patents
シリコーンポリエーテルコポリマー、それを含むシーラント、および関連する方法 Download PDFInfo
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- JP2020533423A JP2020533423A JP2019570952A JP2019570952A JP2020533423A JP 2020533423 A JP2020533423 A JP 2020533423A JP 2019570952 A JP2019570952 A JP 2019570952A JP 2019570952 A JP2019570952 A JP 2019570952A JP 2020533423 A JP2020533423 A JP 2020533423A
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- polyether
- silicone
- sealant
- compound
- Prior art date
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- 238000000034 method Methods 0.000 title claims abstract description 68
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- 239000007809 chemical reaction catalyst Substances 0.000 claims abstract description 31
- 238000006482 condensation reaction Methods 0.000 claims abstract description 20
- 125000004432 carbon atom Chemical group C* 0.000 claims description 62
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- 238000012956 testing procedure Methods 0.000 description 1
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- 150000003608 titanium Chemical class 0.000 description 1
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- LSZKGNJKKQYFLR-UHFFFAOYSA-J tri(butanoyloxy)stannyl butanoate Chemical compound [Sn+4].CCCC([O-])=O.CCCC([O-])=O.CCCC([O-])=O.CCCC([O-])=O LSZKGNJKKQYFLR-UHFFFAOYSA-J 0.000 description 1
- YZVRVDPMGYFCGL-UHFFFAOYSA-N triacetyloxysilyl acetate Chemical compound CC(=O)O[Si](OC(C)=O)(OC(C)=O)OC(C)=O YZVRVDPMGYFCGL-UHFFFAOYSA-N 0.000 description 1
- LTQZKHRCYAXPAZ-UHFFFAOYSA-N triazin-4-ylsulfonylurea Chemical compound NC(=O)NS(=O)(=O)C1=CC=NN=N1 LTQZKHRCYAXPAZ-UHFFFAOYSA-N 0.000 description 1
- 150000003852 triazoles Chemical class 0.000 description 1
- 125000001425 triazolyl group Chemical group 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- FOQJQXVUMYLJSU-UHFFFAOYSA-N triethoxy(1-triethoxysilylethyl)silane Chemical compound CCO[Si](OCC)(OCC)C(C)[Si](OCC)(OCC)OCC FOQJQXVUMYLJSU-UHFFFAOYSA-N 0.000 description 1
- PGVSPORIGRCPMG-UHFFFAOYSA-N triethoxy(1-triethoxysilylhexyl)silane Chemical group CCCCCC([Si](OCC)(OCC)OCC)[Si](OCC)(OCC)OCC PGVSPORIGRCPMG-UHFFFAOYSA-N 0.000 description 1
- ALVYUZIFSCKIFP-UHFFFAOYSA-N triethoxy(2-methylpropyl)silane Chemical compound CCO[Si](CC(C)C)(OCC)OCC ALVYUZIFSCKIFP-UHFFFAOYSA-N 0.000 description 1
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- FZMJEGJVKFTGMU-UHFFFAOYSA-N triethoxy(octadecyl)silane Chemical compound CCCCCCCCCCCCCCCCCC[Si](OCC)(OCC)OCC FZMJEGJVKFTGMU-UHFFFAOYSA-N 0.000 description 1
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- VTHOKNTVYKTUPI-UHFFFAOYSA-N triethoxy-[3-(3-triethoxysilylpropyltetrasulfanyl)propyl]silane Chemical compound CCO[Si](OCC)(OCC)CCCSSSSCCC[Si](OCC)(OCC)OCC VTHOKNTVYKTUPI-UHFFFAOYSA-N 0.000 description 1
- JXUKBNICSRJFAP-UHFFFAOYSA-N triethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CCO[Si](OCC)(OCC)CCCOCC1CO1 JXUKBNICSRJFAP-UHFFFAOYSA-N 0.000 description 1
- CPRPKIMXLHBUGA-UHFFFAOYSA-N triethyltin Chemical compound CC[Sn](CC)CC CPRPKIMXLHBUGA-UHFFFAOYSA-N 0.000 description 1
- 125000002023 trifluoromethyl group Chemical group FC(F)(F)* 0.000 description 1
- JBYXACURRYATNJ-UHFFFAOYSA-N trimethoxy(1-trimethoxysilylhexyl)silane Chemical compound CCCCCC([Si](OC)(OC)OC)[Si](OC)(OC)OC JBYXACURRYATNJ-UHFFFAOYSA-N 0.000 description 1
- XYJRNCYWTVGEEG-UHFFFAOYSA-N trimethoxy(2-methylpropyl)silane Chemical compound CO[Si](OC)(OC)CC(C)C XYJRNCYWTVGEEG-UHFFFAOYSA-N 0.000 description 1
- UBMUZYGBAGFCDF-UHFFFAOYSA-N trimethoxy(2-phenylethyl)silane Chemical compound CO[Si](OC)(OC)CCC1=CC=CC=C1 UBMUZYGBAGFCDF-UHFFFAOYSA-N 0.000 description 1
- JCGDCINCKDQXDX-UHFFFAOYSA-N trimethoxy(2-trimethoxysilylethyl)silane Chemical compound CO[Si](OC)(OC)CC[Si](OC)(OC)OC JCGDCINCKDQXDX-UHFFFAOYSA-N 0.000 description 1
- NMEPHPOFYLLFTK-UHFFFAOYSA-N trimethoxy(octyl)silane Chemical compound CCCCCCCC[Si](OC)(OC)OC NMEPHPOFYLLFTK-UHFFFAOYSA-N 0.000 description 1
- LFRDHGNFBLIJIY-UHFFFAOYSA-N trimethoxy(prop-2-enyl)silane Chemical compound CO[Si](OC)(OC)CC=C LFRDHGNFBLIJIY-UHFFFAOYSA-N 0.000 description 1
- AXNJHBYHBDPTQF-UHFFFAOYSA-N trimethoxy(tetradecyl)silane Chemical compound CCCCCCCCCCCCCC[Si](OC)(OC)OC AXNJHBYHBDPTQF-UHFFFAOYSA-N 0.000 description 1
- ASEGJSMHCHEQSA-UHFFFAOYSA-N trimethoxy(undec-10-enyl)silane Chemical compound CO[Si](OC)(OC)CCCCCCCCCC=C ASEGJSMHCHEQSA-UHFFFAOYSA-N 0.000 description 1
- MAFQBSQRZKWGGE-UHFFFAOYSA-N trimethoxy-[2-[4-(2-trimethoxysilylethyl)phenyl]ethyl]silane Chemical compound CO[Si](OC)(OC)CCC1=CC=C(CC[Si](OC)(OC)OC)C=C1 MAFQBSQRZKWGGE-UHFFFAOYSA-N 0.000 description 1
- SCRSFLUHMDMRFP-UHFFFAOYSA-N trimethyl-(methyl-octyl-trimethylsilyloxysilyl)oxysilane Chemical compound CCCCCCCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C SCRSFLUHMDMRFP-UHFFFAOYSA-N 0.000 description 1
- LAGQNGWYNLUQRI-UHFFFAOYSA-N trioctylmethylammonium bis(trifluoromethylsulfonyl)imide Chemical compound FC(F)(F)S(=O)(=O)[N-]S(=O)(=O)C(F)(F)F.CCCCCCCC[N+](C)(CCCCCCCC)CCCCCCCC LAGQNGWYNLUQRI-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- HQUQLFOMPYWACS-UHFFFAOYSA-N tris(2-chloroethyl) phosphate Chemical compound ClCCOP(=O)(OCCCl)OCCCl HQUQLFOMPYWACS-UHFFFAOYSA-N 0.000 description 1
- NCPXQVVMIXIKTN-UHFFFAOYSA-N trisodium;phosphite Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])[O-] NCPXQVVMIXIKTN-UHFFFAOYSA-N 0.000 description 1
- 239000002383 tung oil Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 239000010456 wollastonite Substances 0.000 description 1
- 229910052882 wollastonite Inorganic materials 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 229940043810 zinc pyrithione Drugs 0.000 description 1
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/10—Block- or graft-copolymers containing polysiloxane sequences
- C08L83/12—Block- or graft-copolymers containing polysiloxane sequences containing polyether sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/42—Block-or graft-polymers containing polysiloxane sequences
- C08G77/46—Block-or graft-polymers containing polysiloxane sequences containing polyether sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
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Abstract
Description
本出願は、2017年6月26日に出願された米国仮出願第62/524,637号、第62/524,636号、および第62/524,639号に対する優先権および全ての利点を主張し、これらの内容は、参照により本明細書に組み込まれる。
−CH2−CH(R3)−[D2]m−O−[C2H4O]x[C3H6O]y[C4H8O]z−[D2]m−CH(R3)−CH2−、
式中、各R3は、1〜6個の炭素原子を有する独立したヒドロカルビル基、アルコキシ基、シリル基、またはHであり、各D2は、1〜6個の炭素原子を有する独立して選択される二価の基であり、下付き文字mは、0または1であり、下付き文字xは、0〜999であり、下付き文字yは、1〜1000であり、下付き文字zは、0〜999であり、下付き文字x、y、およびzによって示される単位は、ポリエーテル部分Yにおいてランダム化されたまたはブロック形態であり得る。
CH2C(R3)−[D2]m−O−[C2H4O]x[C3H6O]y[C4H8O]z−[D2]m−C(R3)CH2、
乾燥した4つ口フラスコを温度制御された発熱ブロック内に配置し、機械式撹拌機、温度計、滴下漏斗、および還流冷却器を取り付けた。フラスコをN2でパージし、ポリエーテル化合物をその中に配置した。フラスコを加熱し、断続的なN2パージを伴って真空下で2時間105℃に保持した。次に、フラスコを85℃に冷却した。ヒドロシリル化触媒を追加した(5ppm、MMに溶解した0−0719の1重量%溶液)。鎖延長化有機シリコーン化合物を液滴で添加した。断熱的な発熱を5〜10℃の温度の上昇を伴って観察し、それに応じて鎖延長化有機シリコーン化合物の添加を調整することで反応温度を約95℃に保つ。反応が完了したとみなされるまで、つまり1H NMRまたはFTIRによってSiHが検出されなくなるまで、反応温度を約95℃の時間(T1)で保つ。末端保護化有機シリコーン化合物を液滴で添加した。断熱的な発熱を約5℃の温度の上昇を伴って観察した。次に、反応を完了まで約95℃に加熱し、時間(T2)で保ち、1H NMRによって観測されるC=Cが過剰な場合は、追加の末端保護化有機シリコーン化合物を追加した。反応は、C=Cがなくなるか、または開始時の量の2%未満のいずれかになると完了したと見なした(1H NMRによる)。全てのC=Cが消費されるが、残留SiHがまだ存在する場合(1H NMRまたはFTIRによる)は、残留SiHを除去するためにATMSを超過して添加した。完了したら、反応混合物を加熱し、真空下で2時間105℃に保ち、全ての揮発物を除去した。次いで、フラスコの内容物を室温まで冷却し、N2流下でナルゲン容器に封入する。完成した材料は、シリコーンポリエーテルコポリマーと称した。
調製例1に示される手順に従って、シリコーンポリエーテルコポリマーを調製した。以下の表2は、ポリエーテル化合物、鎖延長化有機シリコーン化合物(CEOC)、および末端保護化有機シリコーン化合物(EOC)の相対量を示す。
乾燥した4つ口フラスコを温度制御された発熱ブロック内に配置し、機械式撹拌機、温度計、滴下漏斗、および還流冷却器を取り付けた。フラスコをN2でパージし、ポリエーテル化合物をその中に配置した。フラスコを加熱し、断続的なN2パージを伴って真空下で2時間105℃に保持した。次に、フラスコを85℃に冷却した。末端保護化有機シリコーン化合物を反応フラスコに負荷する。ヒドロシリル化触媒を追加した(5ppm、MMに溶解した0−0719の1重量%溶液)。断熱的な発熱を5〜10℃の温度の上昇を伴って観察した。反応が完了したとみなされるまで、つまり1H NMRまたはFTIRによってSiHが検出されなくなるまで、反応温度を約95℃の時間(T1)で保つ。鎖延長化有機シリコーン化合物を液滴で添加した。断熱的な発熱を5〜10℃の温度の上昇を伴って観察し、それに応じて鎖延長化有機シリコーン化合物の添加を調整することで反応温度を約95℃に保つ。次に、反応を完了まで約95℃に加熱し、時間(T2)で保ち、1H NMRによって観測されるC=Cが過剰な場合は、追加の末端保護化有機シリコーン化合物を追加した。反応は、C=Cがなくなるか、または開始時の量の2%未満のいずれかになると完了したと見なした(1H NMRによる)。全てのC=Cが消費されるが、残留SiHがまだ存在する場合(1H NMRまたはFTIRによる)は、残留SiHを除去するためにATMSを超過して添加した。完了したら、反応混合物を加熱し、真空下で2時間105℃に保ち、全ての揮発物を除去した。次いで、フラスコの内容物を室温まで冷却し、N2流下でナルゲン容器に封入する。完成した材料は、シリコーンポリエーテルコポリマーと称した。
調製例2に示される手順に従って、シリコーンポリエーテルコポリマーを調製した。以下の表3は、ポリエーテル化合物、鎖延長化有機シリコーン化合物(CEOC)、および末端保護化有機シリコーン化合物(EOC)の相対量を示す。
乾燥した4つ口フラスコを温度制御された発熱ブロック内に配置し、機械式撹拌機、温度計、滴下漏斗、および還流冷却器を取り付けた。フラスコをN2でパージし、ポリエーテル化合物をその中に配置した。フラスコを加熱し、断続的なN2パージを伴って真空下で2時間105℃に保持した。次に、フラスコを85℃に冷却した。次いで、連鎖延長化有機シリコーン化合物および末端保護化有機シリコーン化合物をフラスコに負荷する。ヒドロシリル化触媒を追加し(5ppm、MMに溶解した0−0719の1重量%溶液)、断熱的な発熱を5〜10℃の温度の上昇を伴って観察した。次に、反応が完了するまで、すなわち1H NMRによりC=Cがなくなるか、または開始時の量の2%未満のいずれかになるまで、反応物を約95℃に加熱し、時間(T1)で保つ。C=Cが残留した場合、追加の末端保護化有機シリコーン化合物を追加した。全てのC=Cが消費されるが、残留SiHがまだ存在する場合(1H NMRまたはFTIRによる)は、残留SiHを除去するためにATMSを超過して添加した。完了したら、反応混合物を加熱し、真空下で2時間105℃に保ち、全ての揮発物を除去した。次いで、フラスコの内容物を室温まで冷却し、N2流下でナルゲン容器に封入する。完成した材料は、シリコーンポリエーテルコポリマーと称した。
調製例3に示される手順に従って、シリコーンポリエーテルコポリマーを調製した。以下の表4は、この例で使用した、ポリエーテル化合物、鎖延長化有機シリコーン化合物(CEOC)、および末端保護化有機シリコーン化合物(EOC)の相対量を示す。
例1〜8のシリコーンポリエーテルコポリマーの各々の30gの試料を、Flacktekスピードミキサ用の40g容量ポリプロピレンミキシングカップ中で0.03gのジブチルスズジラウレートと混合し、2000rpmで1分間混合した。混合物を、サイズが10cmx10cmのエッジガード付きのテフロンプレート上に配置した。テフロンプレートは、50%の湿度に制御され、23℃の温度に制御された部屋に配置した。プレートは、硬化させるために7日間部屋に置いた後、大気中の水分量は調整されていない50℃に設定された空気循環オーブンに移され、4日間オーブンに保持した。最後に、試料をオーブンから取り出し、室温まで冷却した。ドッグボーンの標本を、引張り試験をのために炭素鋼のダイで試料から切断し、示差走査熱量測定(DSC)のために試料から小さな断片を切断した。
アミノエチルアミノプロピルトリメトキシシラン(接着促進剤として)およびジブチルスズジラウレート(触媒として)のプレミックス溶液を1オンスのガラスバイアル内で組み合わせた。次に、この溶液を明白な淡黄色が得られるまで手で混合し、混合物を後の配合プロセスで使用するために取っておいた。
例3のシリコーンポリエーテルコポリマーを使用して、例12のシーラント調製手順に従ってシーラントを調製した。
例4のシリコーンポリエーテルコポリマーを使用して、例12のシーラント調製手順に従ってシーラントを調製した。
例5のシリコーンポリエーテルコポリマーを使用して、例12のシーラント調製手順に従ってシーラントを調製した。
実施例9〜11の物理的および硬化特性を、以下のそれぞれの手順に従って評価した。
Claims (25)
- 式Xg[ZjYo]cを有するシリコーンポリエーテルコポリマーであって、各Xが、式(I)または(II)のうちの1つを有する独立したシリコーン部分であり、
式中、各R1が、1〜18個の炭素原子を有する独立して選択される置換または非置換ヒドロカルビル基であり、各R2が、1〜18個の炭素原子を有する独立して選択される置換または非置換ヒドロカルビル基であり、各D1が、2〜18個の炭素原子を有する独立して選択される二価の炭化水素基であり、各下付き文字aが、独立して0または1であり、各下付き文字bが、独立して0または1であり、下付き文字cが、1〜150であり、各下付き文字dが、1〜1000であり、各下付き文字eが、独立して1または2であり、各X内でfが1の場合に、bが1であるという条件で、各下付き文字fが、独立して0または1であり、下付き文字gが、>1であり、下付き文字hが、下付き文字dによって示される各部分において0〜2から独立して選択され、各下付き文字jが、独立して>0および<2であり、下付き文字cによって示される各部分でj+o=2であるという条件で、各下付き文字oが、独立して>0および<2であり、下付き文字tが、≧0であり、下付き文字uが、>0である、シリコーンポリエーテルコポリマー。 - 前記シリコーンポリエーテルコポリマーが以下の式を有し、
- (i)各ポリエーテル部分Yが、式−O−(CnH2nO)w−を有するポリエーテル基を含み、式中、下付き文字nが、下付き文字wによって示される各部分において2〜4から独立して選択され、下付き文字wが、1〜1000であるか、(ii)各ポリエーテル部分Yが、少なくとも約100の数平均分子量を有するか、(iii)少なくとも1個のポリエーテル部分Yが、ポリヒドロキシルポリエーテルであるか、または(vi)(i)−(iii)の組み合わせである、請求項1または2に記載のシリコーンポリエーテルコポリマー。
- 各ポリエーテル部分Yが、以下の式を有し、
−CH2−CH(R3)−[D2]m−O−[C2H4O]x[C3H6O]y[C4H8O]z−[D2]m−CH(R3)−CH2−、
式中、各R3が、1〜6個の炭素原子を有する独立したヒドロカルビル基、アルコキシ基、シリル基、またはHであり、各D2が、1〜6個の炭素原子を有する独立して選択される二価の基であり、下付き文字mが、0または1であり、下付き文字xが、0〜999であり、下付き文字yが、1〜1000であり、下付き文字zが、0〜999であり、下付き文字x、y、およびzによって示される単位が、前記ポリエーテル部分Yにおいてランダム化されたまたはブロック形態であり得る、請求項1〜3のいずれか一項に記載のシリコーンポリエーテルコポリマー。 - (i)各R3が、メチルであるか、(ii)各下付き文字mが、1であり、および各D2が、CH2であるか、または(iii)(i)および(ii)の両方である、請求項4に記載のシリコーンポリエーテルコポリマー。
- (i)各R1が、メチルであるか、(ii)各R2が、プロピルであるか、(iii)各下付き文字aが、0であるか、(iv)各D1が、C2H4であるか、または(v)(i)〜(iv)の任意の組み合わせである、請求項1〜5のいずれか一項に記載のシリコーンポリエーテルコポリマー。
- シリコーンポリエーテルコポリマーを調製する方法であって、前記方法が、
ヒドロシリル化触媒の存在下で、平均で2個以上の末端不飽和基を有するポリエーテル化合物、鎖延長化有機シリコーン化合物、および末端保護化有機シリコーン化合物を反応させて、前記シリコーンポリエーテルコポリマーを得ることを含み、
前記シリコーンポリエーテルコポリマーが、請求項1〜6のいずれか一項に記載のシリコーンポリエーテルコポリマーである、方法。 - 前記ポリエーテル化合物が以下の式を有し、
Y1[R4]i、
式中、各R4が、2〜14個の炭素原子を有する独立して選択される不飽和基であり、下付き文字iが、>1であり、Y1が、式−O−(CnH2nO)w−を有するポリエーテル基を含む独立して選択されるポリエーテル部分であり、下付き文字nが、下付き文字wによって示される各部分において2〜4から独立して選択され、下付き文字wが、1〜1000である、請求項7に記載の方法。 - 前記ポリエーテル化合物において、
(i)前記ポリエーテル部分Y1が、以下の式を有し、
−O−[C2H4O]x[C3H6O]y[C4H8O]z−、
式中、各下付き文字xが、0〜999であり、各下付き文字yが、独立して1〜1000であり、各下付き文字zが、独立して0〜999であり、下付き文字x、y、およびzによって示される単位が、前記ポリエーテル部分Y1においてランダム化されたもしくはブロック形態であり得るか、
(ii)各R4が、以下の式を有し、
CH2C(R3)−[D2]m−、
式中、各R3が、1〜6個の炭素原子を有する独立したヒドロカルビル基、アルコキシ基、シリル基、またはHであり、各D2が、1〜6個の炭素原子を有する独立して選択される二価の基であり、下付き文字mが、0または1であるか、または
(iii)(i)および(ii)の両方である、請求項8に記載の方法。 - 式CH2C(R3)−[D2]m−の各R4において、(i)各R3が、メチルであるか、(ii)各下付き文字mが、1であり、および各D2が、CH2であるか、または(iii)(i)および(ii)の両方である、請求項9に記載の方法。
- 前記鎖延長化有機シリコーン化合物が、(i)直鎖状水素化シリコーン官能性有機シリコーン化合物か、(ii)分枝状水素化シリコーン官能性有機シリコーン化合物か、または(iii)(i)および(ii)の両方を含む、請求項7〜10のいずれか一項に記載の方法。
- 前記鎖延長化有機シリコーン化合物が、前記直鎖状水素化シリコーン官能性有機シリコーン化合物を含み、前記直鎖状水素化シリコーン官能性有機シリコーン化合物が、以下の式を有し、
- 前記末端保護化有機シリコーン化合物が、式(III)または(IV)を有し、
- (i)前記ヒドロシリル化触媒の存在下で、前記ポリエーテル化合物および前記鎖延長化有機シリコーン化合物を反応させて、鎖延長シリコーンポリエーテル化合物を得、ヒドロシリル化触媒の存在下で、前記鎖延長シリコーンポリエーテル化合物および前記末端保護化有機シリコーン化合物を反応させて、前記シリコーンポリエーテルコポリマーを得るか、
(ii)前記ヒドロシリル化触媒の存在下で、前記ポリエーテル化合物および前記末端保護化有機シリコーン化合物を反応させて、末端保護シリコーンポリエーテル化合物を得、前記ヒドロシリル化触媒の存在下で、前記末端保護シリコーンポリエーテル化合物および前記鎖延長化有機シリコーン化合物を反応させて、前記シリコーンポリエーテルコポリマーを得るか、または
(iii)(i)および(ii)の両方を含む、請求項7〜13のいずれか一項に記載の方法。 - (i)前記ヒドロシリル化触媒の存在下で、前記ポリエーテル化合物および前記鎖延長化有機シリコーン化合物を反応させて、前記鎖延長シリコーンポリエーテル化合物を得ることを含み、前記鎖延長シリコーンポリエーテル化合物が、以下の式を有し、
- 前記連鎖延長シリコーンポリエーテル化合物において、
(i)各ポリエーテル部分Y1が、以下の式を有し、
−O−[C2H4O]x[C3H6O]y[C4H8O]z−、
式中、各下付き文字xが、0〜999であり、各下付き文字yが、独立して1〜1000であり、各下付き文字zが、独立して0〜999であり、下付き文字x、y、およびzによって示される単位が、前記ポリエーテル部分Y1においてランダム化されたもしくはブロック形態であり得るか、
(ii)各R4が、以下の式を有し、
CH2C(R3)−[D2]m−、
式中、各R3が、1〜6個の炭素原子を有する独立したヒドロカルビル基、アルコキシ基、シリル基、またはHであり、各D2が、1〜6個の炭素原子を有する独立して選択される二価の基であり、下付き文字mが、0または1であるか、または
(iii)(i)および(ii)の両方を含む、請求項15に記載の方法。 - 式CH2C(R3)−[D2]m−の各R4において、(i)各R3が、メチルであるか、(ii)各下付き文字mが、1であり、および各D2が、CH2であるか、または(iii)(i)および(ii)の両方である、請求項16に記載の方法。
- 請求項7〜17のいずれか一項に記載の方法に従って調製された、シリコーンポリエーテルコポリマー。
- シーラントであって、
シリコーンポリエーテルコポリマーと、
縮合反応触媒と、を含み、
前記シリコーンポリエーテルコポリマーが、請求項1〜5、および15のいずれか一項に記載のシリコーンポリエーテルコポリマーである、シーラント。 - (i)充填剤;(ii)充填処理剤;(iii)架橋剤;(iv)表面改質剤;(v)乾燥剤;(vi)増量剤;(vii)殺生物剤;(viii)難燃剤;(ix)可塑剤;(x)末端遮断剤;(xi)接合剤(xii)老化防止添加剤;(xiii)水放出剤;(xiv)顔料;(xv)レオロジー調整剤;(xvii)担体;(xii)粘着付与剤;(xiii)腐食阻害剤;(xix)触媒阻害剤;(xx)接着促進剤;(xxi)粘度調整剤;(xxii)UV吸収剤;(xxiii)抗酸化剤;(xxiv)光安定剤;または(xxv)(i)−(xxiv)の組み合わせをさらに含む、請求項19に記載のシーラント。
- 前記シーラントが、前記充填剤、前記架橋剤、前記増量剤、前記可塑剤、および前記接着促進剤を含む、請求項20に記載のシーラント。
- 請求項19〜21のいずれか一項に記載のシーラントの硬化生成物。
- 基材と、前記基材上に配置される請求項22に記載の硬化生成物と、を含む複合物品。
- 複合物品を調製する方法であって、前記方法が、
基材上にシーラントを配置することと、
シーラントを硬化させて、前記基材上に硬化生成物を得、それにより前記複合物品を形成することとを含み、
前記シーラントが、請求項19〜21のいずれか一項に記載のシーラントである、方法。 - 2つの要素間に画定された空間を封止する方法であって、前記方法が、
前記空間にシーラントを適用することと、
前記空間内の前記シーラントを硬化させ、それにより前記空間を封止することとを含み、
前記シーラントが、請求項19〜21のいずれか一項に記載のシーラントである、方法。
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