JP5441406B2 - カプセル化されたデバイスおよび製造方法 - Google Patents
カプセル化されたデバイスおよび製造方法 Download PDFInfo
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Images
Classifications
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K50/00—Organic light-emitting devices
- H10K50/80—Constructional details
- H10K50/84—Passivation; Containers; Encapsulations
- H10K50/844—Encapsulations
- H10K50/8445—Encapsulations multilayered coatings having a repetitive structure, e.g. having multiple organic-inorganic bilayers
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K30/00—Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
- H10K30/80—Constructional details
- H10K30/88—Passivation; Containers; Encapsulations
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K59/00—Integrated devices, or assemblies of multiple devices, comprising at least one organic light-emitting element covered by group H10K50/00
- H10K59/80—Constructional details
- H10K59/87—Passivation; Containers; Encapsulations
- H10K59/873—Encapsulations
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E10/00—Energy generation through renewable energy sources
- Y02E10/50—Photovoltaic [PV] energy
- Y02E10/549—Organic PV cells
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- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Optics & Photonics (AREA)
- Electroluminescent Light Sources (AREA)
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- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
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Description
アクリラート単量体の様々なブレンドを用いてポリマーフィルムを作製した。表1に、その配合を示す。トリプロピレングリコールジアクリラートを用いて作製したポリマー層は、例えば、“Plasma treatment of PET and acrylic coating surfaces−I.In−situ XPS measurements”,Shi等,J.Adhesion Sci.Technol.,第14巻,第12号,1485〜1498頁(2000)(参照により本発明に含める)で説明されている。調合物1(トリプロピレングリコールジアクリラートを包含する)は、その他の調合物との比較のベースとして用いられた。
多層遮断物でカプセル化されたガラス基板上のCa切り取り試片の透過における変化は、遮断構造の有効性を試験する優れた手段である。図6A〜Cに示される実施例において、酸化物層(厚さ100nm)、および、6対のポリマー/酸化物対[ポリマー(0.5μm)/酸化物(40nm)]による多層構造を構成した。カプセル化されたCa切り取り試片を、400時間、60℃、90%RHでエージングした。図6Aによれば、調合物4(5.5×1020n/mlのエーテル結合)は透過の増加を示さないことがわかり、従って遮断物の不良はない。図6Bによれば、調合物1(3.6×1021n/mlのエーテル結合)は、カルシウム領域の端部において透過の増加を示すことがわかる。図6Cにおいて、カルシウム領域全体がフェージングし、調合物5(3.2×1021n/mlのエーテル結合)の場合は極端な遮断物の不良を示す。図6Dは、酸化物層(厚さ100nm)、および、わずか3対のポリマー/酸化物対[ポリマー(0.7μm)/酸化物(40nm)]によって構成された多層構造を有するCa切り取り試片を示す。このようなポリマー層は、表1に記載の調合物7を用いて作製された。この調合物はポリブタジエンジメタクリラート(PBDM)をベースとしており、スピン・オン・コーティングによって付着させた。サンプルを、500時間、60℃、90%RHでエージングした。図6Dによれば、調合物7(0n/mlのエーテル結合)は、透過の増加を示さないことがわかり、従って遮断物の不良はない。
OLEDの試験用画素上に様々なポリマー調合物を用いて積重ね遮断物を形成した。これらサンプルを500時間貯蔵し、水分への曝露を回避するために乾燥ボックス中で試験した。24時間にわたり差を目視で観察した。
表3に示される配合に従って減結合ポリマー層を作製した。前駆体ブレンドの付着効率を測定し、平均分子量を計算した。
Claims (13)
- 有機発光デバイス、液晶ディスプレイ、発光ダイオード、発光ポリマー、電気泳動インクを用いた電子標識、エレクトロルミネセンスデバイス、リン光デバイス、集積回路、電荷結合素子、金属センサーパッド、マイクロディスクレーザー、エレクトロクロミック素子、フォトクロミック素子、超小型電子機械式システム、太陽電池、またはこれらの組み合わせであるデバイスをカプセル化する方法であって:
基板を用意すること;
少なくとも1個の該デバイスを該基板に隣接させて配置すること;および、
少なくとも1つの積重ね遮断物を該デバイスに隣接させて付着させること、を含み、
ここで、該積重ね遮断物の少なくとも1つは、少なくとも1つの遮断層、および、少なくとも1つの減結合ポリマー層を含み、そして、該減結合ポリマー層の少なくとも1つは、ポリマー前駆体のブレンドから作製され、ここで、該ブレンドが
60〜90重量%のポリブタジエンジメタクリラート及び/またはドデカンジオールジメタクリラート;
0〜20重量%のモノアクリラート;
0〜20重量%のトリアクリラート;
1〜10%の光開始剤、を含む、上記方法。 - 該ポリマー前駆体のブレンドは、少なくとも275の平均分子量を有する、請求項1に記載の方法。
- 前記ポリブタジエンジメタクリラート及び/またはドデカンジオールジメタクリラートが、65〜75重量%の量で存在する、請求項1または2に記載の方法。
- 前記モノアクリラートが、10〜20重量%の量で存在する、請求項1から3のいずれか1項に記載の方法。
- 前記トリアクリラートが、5〜15重量%の量で存在する、請求項1から4のいずれか1項に記載の方法。
- 前記光開始剤が、1〜3重量%の量で存在する、請求項1から5のいずれか1項に記載の方法。
- 前記ポリマー前駆体のブレンドが:
65〜75重量%のドデカンジオールジメタクリラート;
10〜20重量%のラウリルアクリラート;
5〜15重量%のトリメチロールプロパントリアクリラート;
1〜3重量%の光開始剤、
を含む、請求項1または2に記載の方法。 - カプセル化された、有機発光デバイス、液晶ディスプレイ、発光ダイオード、発光ポリマー、電気泳動インクを用いた電子標識、エレクトロルミネセンスデバイス、リン光デバイス、集積回路、電荷結合素子、金属センサーパッド、マイクロディスクレーザー、エレクトロクロミック素子、フォトクロミック素子、超小型電子機械式システム、太陽電池、またはこれらの組み合わせであるデバイスであって:
基板;
該基板に隣接する少なくとも1個の該デバイス;および、
該デバイスに隣接する少なくとも1つの積重ね遮断物、
を含み、ここで、該積重ね遮断物の少なくとも1つは、少なくとも1つの遮断層、および、少なくとも1つの減結合ポリマー層を含み、ここで、該減結合ポリマー層の少なくとも1つは、ポリマー前駆体のブレンドから作製され、ここで、該ブレンドが
60〜90重量%のポリブタジエンジメタクリラート及び/またはドデカンジオールジメタクリラート;
0〜20重量%のモノアクリラート;
0〜20重量%のトリアクリラート;
1〜10%の光開始剤、を含む、上記デバイス。 - 前記ポリブタジエンジメタクリラート及び/またはドデカンジオールジメタクリラートが、65〜75重量%の量で存在する、請求項8に記載のカプセル化されたデバイス。
- 前記モノアクリラートが、10〜20重量%の量で存在する、請求項8または9に記載のカプセル化されたデバイス。
- 前記トリアクリラートが、5〜15重量%の量で存在する、請求項8から10のいずれか1項に記載のカプセル化されたデバイス。
- 前記光開始剤が、1〜3重量%の量で存在する、請求項8から11のいずれか1項に記載のカプセル化されたデバイス。
- 前記ポリマー前駆体のブレンドが:
65〜75重量%のドデカンジオールジメタクリラート;
10〜20重量%のラウリルアクリラート;
5〜15重量%のトリメチロールプロパントリアクリラート;
1〜3重量%の光開始剤、
を含む、請求項8または9に記載のカプセル化されたデバイス。
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US11/509,837 US7767498B2 (en) | 2005-08-25 | 2006-08-24 | Encapsulated devices and method of making |
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KR (1) | KR101156427B1 (ja) |
CN (1) | CN101292373B (ja) |
AT (1) | ATE509378T1 (ja) |
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- 2006-08-25 CN CN200680039424.2A patent/CN101292373B/zh active Active
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KR20080045243A (ko) | 2008-05-22 |
EP1925043A1 (en) | 2008-05-28 |
US20070049155A1 (en) | 2007-03-01 |
ATE509378T1 (de) | 2011-05-15 |
WO2007025140A1 (en) | 2007-03-01 |
TW200715500A (en) | 2007-04-16 |
CN101292373B (zh) | 2010-05-26 |
EP1925043B1 (en) | 2011-05-11 |
US7767498B2 (en) | 2010-08-03 |
TWI313918B (en) | 2009-08-21 |
CN101292373A (zh) | 2008-10-22 |
JP2009506171A (ja) | 2009-02-12 |
KR101156427B1 (ko) | 2012-06-21 |
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