EA200001135A1 - Способ получения изоксазолин-3-ил-ацилбензолов - Google Patents

Способ получения изоксазолин-3-ил-ацилбензолов

Info

Publication number
EA200001135A1
EA200001135A1 EA200001135A EA200001135A EA200001135A1 EA 200001135 A1 EA200001135 A1 EA 200001135A1 EA 200001135 A EA200001135 A EA 200001135A EA 200001135 A EA200001135 A EA 200001135A EA 200001135 A1 EA200001135 A1 EA 200001135A1
Authority
EA
Eurasian Patent Office
Prior art keywords
formula
alkyl
preparation
izoxazolin
acylbenzenes
Prior art date
Application number
EA200001135A
Other languages
English (en)
Other versions
EA007095B1 (ru
Inventor
Йоахим Райнхаймер
Вольфганг Фон-Дейн
Йоахим Гебхардт
Михаэль Ракк
Рене Лохтман
Норберт Гётц
Михаэль Кейль
Маттиас Витшель
Хельмут Хаген
Ульф Мисслитц
Эрнст Бауманн
Original Assignee
Басф Акциенгезельшафт
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19820722A external-priority patent/DE19820722C1/de
Priority claimed from DE19852095A external-priority patent/DE19852095A1/de
Application filed by Басф Акциенгезельшафт filed Critical Басф Акциенгезельшафт
Publication of EA200001135A1 publication Critical patent/EA200001135A1/ru
Publication of EA007095B1 publication Critical patent/EA007095B1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/06—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by nitrosation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/10—Preparation of nitro compounds by substitution of functional groups by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/44—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by —CHO groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/62—Preparation of compounds containing amino groups bound to a carbon skeleton by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32—Oximes
    • C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/48—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C255/50—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton to carbon atoms of non-condensed six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C07C315/04—Preparation of sulfones; Preparation of sulfoxides by reactions not involving the formation of sulfone or sulfoxide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D261/00—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings
    • C07D261/02—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings
    • C07D261/04—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/10—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a carbon chain containing aromatic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Изобретение относится к способу получения изоксазолов формулы Iгде заместители имеют следующее значение:R- водород, C-Cалкил,R- C-Cалкил,R, R, R- водород, C-Cалкил или Rи Rобразуют вместе связь,R- гетероциклическое кольцо,n равно 0, 1 или 2;включающему получение промежуточного соединения формулы VIгде R, R, Rи Rимеют вышеприведенное значение, и последующее взаимодействие с получением соединений формулы I.Изобретение относится также к новым промежуточным продуктам для получения соединений формулы I и к новым способам получения промежуточных продуктов.Международная заявка была опубликована вместе с отчетом о международном поиске.
EA200001135A 1998-05-11 1999-05-04 Способ получения изоксазолин-3-ил-ацилбензолов EA007095B1 (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19820722A DE19820722C1 (de) 1998-05-11 1998-05-11 Verfahren zur Herstellung von Benzoylpyrazolen
DE19852095A DE19852095A1 (de) 1998-11-12 1998-11-12 Verfahren zur Herstellung von 2-Alkyl-3-(4,5-dihydroisoxazol-3-yl)-acylbenzolen
PCT/EP1999/003006 WO1999058509A1 (de) 1998-05-11 1999-05-04 Verfahren zur herstellung von isoxazolin-3-yl-acylbenzolen

Publications (2)

Publication Number Publication Date
EA200001135A1 true EA200001135A1 (ru) 2001-06-25
EA007095B1 EA007095B1 (ru) 2006-06-30

Family

ID=26046070

Family Applications (3)

Application Number Title Priority Date Filing Date
EA200500510A EA010633B1 (ru) 1998-05-11 1999-05-04 Новые бензальдоксимы, способ получения бензальдоксимов и его применение
EA200500509A EA009301B1 (ru) 1998-05-11 1999-05-04 Способ получения производных тиоэфиров и его применение
EA200001135A EA007095B1 (ru) 1998-05-11 1999-05-04 Способ получения изоксазолин-3-ил-ацилбензолов

Family Applications Before (2)

Application Number Title Priority Date Filing Date
EA200500510A EA010633B1 (ru) 1998-05-11 1999-05-04 Новые бензальдоксимы, способ получения бензальдоксимов и его применение
EA200500509A EA009301B1 (ru) 1998-05-11 1999-05-04 Способ получения производных тиоэфиров и его применение

Country Status (24)

Country Link
US (6) US6525204B1 (ru)
EP (4) EP2325176B1 (ru)
JP (2) JP4786032B2 (ru)
KR (1) KR100604302B1 (ru)
CN (3) CN1255377C (ru)
AT (2) ATE552249T1 (ru)
AU (1) AU772781B2 (ru)
BR (1) BR9910326B1 (ru)
CA (3) CA2727762C (ru)
CZ (2) CZ299064B6 (ru)
DE (1) DE59914392D1 (ru)
DK (2) DK1077955T3 (ru)
EA (3) EA010633B1 (ru)
ES (2) ES2381758T3 (ru)
HU (1) HUP0102843A3 (ru)
IL (1) IL139277A0 (ru)
NO (1) NO318079B1 (ru)
NZ (1) NZ508648A (ru)
PL (2) PL209931B1 (ru)
PT (2) PT1077955E (ru)
SI (2) SI1852424T1 (ru)
SK (4) SK288033B6 (ru)
TR (1) TR200003332T2 (ru)
WO (1) WO1999058509A1 (ru)

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DE102011080020A1 (de) 2011-07-28 2012-09-13 Bayer Cropscience Ag Verwendung von Saatgutbehandlungs-Wirkstoffen aus der Gruppe der Dicarboximid-Fungizide als Safener
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DE102011079991A1 (de) 2011-07-28 2012-09-13 Bayer Crop Science Ag Verwendung von Saatgutbehandlungs-Wirkstoffen aus der Gruppe der Nicotinoid-Insektizide als Safener
DE102011080007A1 (de) 2011-07-28 2012-09-13 Bayer Cropscience Ag Verwendung von Saatgutbehandlungs-Wirkstoffen aus den Gruppen der Conazole- und Triazol-Fungizide als Safener
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CN102584735A (zh) * 2011-12-13 2012-07-18 大连理工大学 一种异噁唑类化合物的制备方法
CN105357968A (zh) 2012-10-19 2016-02-24 拜尔农科股份公司 包含羧酰胺衍生物的活性化合物复配物
CN103467300B (zh) * 2013-08-19 2016-02-24 浙江工业大学 一种邻硝基苯甲醛类化合物的合成方法
CN105481787B (zh) * 2015-11-30 2018-04-20 湖南海利化工股份有限公司 3‑(2‑甲基‑6‑硝基苯基)‑4,5‑二氢异噁唑的制备方法
CN106928159A (zh) * 2017-03-01 2017-07-07 安徽丰乐农化有限责任公司 3‑(3‑溴‑2‑甲基‑6‑甲基磺酰基苯基)‑4,5‑二氢化异恶唑的提纯方法
CN107011278B (zh) * 2017-04-06 2019-03-22 湘潭大学 3,4,5-,三取代-4,5-二氢异噁唑、衍生物及其合成方法及用途
CN107162944B (zh) * 2017-04-27 2019-02-26 湖南化工研究院有限公司 2,3-二甲基苯甲硫醚的制备方法
CN107325091B (zh) * 2017-07-13 2019-09-20 湖南海利化工股份有限公司 一种苯吡唑草酮的制备方法
CN107652246B (zh) * 2017-09-25 2020-08-25 江苏乾元生物科技有限公司 一种3-[3-溴-2-甲基-6-(甲基磺酰基)苯基]-4,5-二氢化异噁唑的制备方法
CN108863969B (zh) * 2018-06-30 2022-05-24 华南理工大学 一种4-烯丙基-3,5-二取代异噁唑的合成方法
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CN108947923A (zh) * 2018-08-28 2018-12-07 常州大学 一种3-(2-甲基-6-甲硫基)苯基-4,5-二氢异恶唑的制备方法
US20220400668A1 (en) 2018-10-03 2022-12-22 Basf Se Microemulsion compositions of topramezone
CN109438380B (zh) * 2018-11-19 2022-04-22 华南理工大学 一种合成4-(n,n-二烷基-2-丙炔-1-氨基)异恶唑的方法
WO2020152200A1 (en) 2019-01-25 2020-07-30 Basf Se Process for preparation of heteroarylketones
CN110183392B (zh) * 2019-06-14 2023-03-28 河北医科大学 一种3-取代苯基-4，5-二氢异噁唑衍生物的制备方法及其用途和中间体
CN112552178B (zh) * 2019-09-25 2023-07-18 江西天宇化工有限公司 一种苯甲硫醚类化合物合成中的副产物的回收利用方法
CN112694427B (zh) * 2019-10-23 2022-11-18 江西天宇化工有限公司 一种制备2,3-二甲基苯甲硫醚的方法
CN114644622B (zh) * 2020-12-17 2022-10-18 山东省联合农药工业有限公司 一种含异噁唑啉的吡啶联苯类化合物及其制备方法与用途
CN114797738B (zh) * 2022-04-30 2024-04-02 兰升生物科技集团股份有限公司 改进的管式反应器、使用该管式反应器的生产设备及使用它们制备磺酰基化合物的方法
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BR9910326B1 (pt) 2010-12-14
SK287476B6 (sk) 2010-11-08
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PL344332A1 (en) 2001-11-05
SK287758B6 (sk) 2011-09-05
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US6525204B1 (en) 2003-02-25
US7309802B2 (en) 2007-12-18
SI1852424T1 (sl) 2012-05-31
EP1077955A1 (de) 2001-02-28
CA2727762C (en) 2013-09-10
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ES2381758T3 (es) 2012-05-31
IL139277A0 (en) 2001-11-25
KR20010043497A (ko) 2001-05-25
CA2331816A1 (en) 1999-11-18
EP1852424A2 (de) 2007-11-07
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NO20005652L (no) 2000-11-09
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