JP2014519468A - ヘマタイトの調製方法 - Google Patents
ヘマタイトの調製方法 Download PDFInfo
- Publication number
- JP2014519468A JP2014519468A JP2014513014A JP2014513014A JP2014519468A JP 2014519468 A JP2014519468 A JP 2014519468A JP 2014513014 A JP2014513014 A JP 2014513014A JP 2014513014 A JP2014513014 A JP 2014513014A JP 2014519468 A JP2014519468 A JP 2014519468A
- Authority
- JP
- Japan
- Prior art keywords
- hematite
- aqueous composition
- basic aqueous
- iron
- reacting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims abstract description 230
- 239000011019 hematite Substances 0.000 title claims abstract description 204
- 229910052595 hematite Inorganic materials 0.000 title claims abstract description 204
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 title claims abstract description 204
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 309
- 239000000203 mixture Substances 0.000 claims abstract description 219
- 229910052742 iron Inorganic materials 0.000 claims abstract description 144
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 99
- 239000007791 liquid phase Substances 0.000 claims abstract description 45
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000007790 solid phase Substances 0.000 claims abstract description 18
- -1 iron ions Chemical class 0.000 claims description 132
- 239000002244 precipitate Substances 0.000 claims description 48
- 239000002253 acid Substances 0.000 claims description 35
- 238000002386 leaching Methods 0.000 claims description 31
- 239000007787 solid Chemical group 0.000 claims description 29
- 238000001556 precipitation Methods 0.000 claims description 28
- 239000000463 material Substances 0.000 claims description 26
- 238000006243 chemical reaction Methods 0.000 claims description 24
- 230000001376 precipitating effect Effects 0.000 claims description 24
- 150000002500 ions Chemical class 0.000 claims description 17
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 7
- 230000005484 gravity Effects 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 230000002708 enhancing effect Effects 0.000 claims description 5
- 229920002401 polyacrylamide Polymers 0.000 claims description 5
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 4
- 239000010881 fly ash Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 4
- 230000001737 promoting effect Effects 0.000 claims description 4
- 239000012071 phase Substances 0.000 claims description 3
- 229910000859 α-Fe Inorganic materials 0.000 claims description 3
- 239000011499 joint compound Substances 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 20
- 239000000243 solution Substances 0.000 description 17
- 239000002585 base Substances 0.000 description 14
- 230000035484 reaction time Effects 0.000 description 8
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 7
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 239000012452 mother liquor Substances 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 238000010908 decantation Methods 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 150000004677 hydrates Chemical class 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- 150000007513 acids Chemical class 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 238000001354 calcination Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 150000004679 hydroxides Chemical class 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 235000010755 mineral Nutrition 0.000 description 3
- 238000010899 nucleation Methods 0.000 description 3
- 238000000197 pyrolysis Methods 0.000 description 3
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 229910001566 austenite Inorganic materials 0.000 description 2
- 229910001570 bauxite Inorganic materials 0.000 description 2
- 229910052614 beryl Inorganic materials 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229910001610 cryolite Inorganic materials 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hcl hcl Chemical compound Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 229910052596 spinel Inorganic materials 0.000 description 2
- 239000011029 spinel Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000004931 aggregating effect Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 229910052598 goethite Inorganic materials 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000012510 hollow fiber Substances 0.000 description 1
- AEIXRCIKZIZYPM-UHFFFAOYSA-M hydroxy(oxo)iron Chemical compound [O][Fe]O AEIXRCIKZIZYPM-UHFFFAOYSA-M 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 229910052935 jarosite Inorganic materials 0.000 description 1
- 238000000622 liquid--liquid extraction Methods 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 1
- 239000011028 pyrite Substances 0.000 description 1
- 229910052683 pyrite Inorganic materials 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
- C01G49/06—Ferric oxide [Fe2O3]
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B21/00—Obtaining aluminium
- C22B21/0015—Obtaining aluminium by wet processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/12—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic alkaline solutions
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Geochemistry & Mineralogy (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Compounds Of Iron (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Investigating Or Analysing Biological Materials (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161493018P | 2011-06-03 | 2011-06-03 | |
| US61/493,018 | 2011-06-03 | ||
| PCT/CA2012/000541 WO2012162817A1 (en) | 2011-06-03 | 2012-06-04 | Methods for preparing hematite |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2014519468A true JP2014519468A (ja) | 2014-08-14 |
| JP2014519468A5 JP2014519468A5 (enExample) | 2015-07-23 |
Family
ID=47258226
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014513014A Pending JP2014519468A (ja) | 2011-06-03 | 2012-06-04 | ヘマタイトの調製方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US9150428B2 (enExample) |
| EP (1) | EP2714594A4 (enExample) |
| JP (1) | JP2014519468A (enExample) |
| CN (1) | CN103842296B (enExample) |
| AU (1) | AU2012262586B2 (enExample) |
| BR (1) | BR112013030819A2 (enExample) |
| CA (2) | CA2863755C (enExample) |
| RU (1) | RU2013157943A (enExample) |
| WO (1) | WO2012162817A1 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014508863A (ja) | 2011-03-18 | 2014-04-10 | オーバイト アルミナ インコーポレイテッド | アルミニウム含有材料から希土類元素を回収する方法 |
| EP3141621A1 (en) | 2011-05-04 | 2017-03-15 | Orbite Aluminae Inc. | Processes for recovering rare earth elements from various ores |
| CN104039706A (zh) | 2011-09-16 | 2014-09-10 | 奥贝特铝业有限公司 | 制备氧化铝和各种其他产品的工艺 |
| WO2013104059A1 (en) | 2012-01-10 | 2013-07-18 | Orbite Aluminae Inc. | Processes for treating red mud |
| US9181603B2 (en) | 2012-03-29 | 2015-11-10 | Orbite Technologies Inc. | Processes for treating fly ashes |
| CA2878744C (en) | 2012-07-12 | 2020-09-15 | Orbite Aluminae Inc. | Processes for preparing aluminum chloride and various other products by hcl leaching |
| WO2014047728A1 (en) | 2012-09-26 | 2014-04-03 | Orbite Aluminae Inc. | Processes for preparing alumina and magnesium chloride by hc1 leaching of various materials |
| JP2016504251A (ja) * | 2012-11-14 | 2016-02-12 | オーバイト アルミナ インコーポレイテッドOrbite Aluminae Inc. | アルミニウムイオンの精製方法 |
| CN104450790B (zh) * | 2014-12-22 | 2017-07-04 | 中国科学院新疆理化技术研究所 | 一种制备p‑铁素体修饰n‑赤铁矿异质结构的生物方法 |
| CN107233884B (zh) * | 2017-06-05 | 2020-06-30 | 云南驰宏锌锗股份有限公司 | 一种用于催化三价铁水解沉淀的铁磁性催化剂及其制备方法和应用 |
| AU2023352579A1 (en) * | 2022-09-26 | 2025-03-13 | Electrasteel, Inc. | Iron feedstock conversion system with improved efficiency |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5792527A (en) * | 1980-11-27 | 1982-06-09 | Sakai Chem Ind Co Ltd | Preparation of needle-like ferric oxide |
| JPS58181722A (ja) * | 1982-04-15 | 1983-10-24 | ジユ−ト−ヒエミ−・アクチエンゲゼルシヤフト | アルミニウムと鉄とを含有する酸性廃水の後処理方法 |
| JPH0517131A (ja) * | 1990-06-25 | 1993-01-26 | Nalco Australia Pty Ltd | アルミナ鉱石を精製してアルミナを回収する方法 |
| JPH0656429A (ja) * | 1992-07-31 | 1994-03-01 | Toda Kogyo Corp | 板状酸化鉄粒子粉末の製造法 |
| WO2007079532A1 (en) * | 2006-01-10 | 2007-07-19 | Murrin Murrin Operations Pty Ltd | Hematite precipitation |
| JP2010529289A (ja) * | 2007-05-21 | 2010-08-26 | エクスプロレイション オーバイト ヴイエスピーエー インコーポレイテッド | アルミニウム鉱石からアルミニウム及び鉄を抽出する方法 |
| US20110120267A1 (en) * | 2008-06-25 | 2011-05-26 | Eric Girvan Roche | Iron Precipitation |
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| US558726A (en) | 1896-04-21 | Process of producing hydrous chlorid of aluminium | ||
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| GB153500A (en) | 1920-01-19 | 1920-11-11 | Sven Emil Sieurin | An improved process of producing oxide of aluminium from chloride of aluminium |
| GB159086A (en) | 1920-01-19 | 1921-02-24 | Sven Emil Sieurin | An improved process of producing oxide of aluminium from chloride of aluminium |
| US1501873A (en) | 1922-03-27 | 1924-07-15 | Tyrer Daniel | Manufacture of red oxide of iron |
| GB195295A (en) | 1922-05-05 | 1923-03-29 | Alexandre Louis Pedemonte | Improvements in the manufacture of pure alumina |
| US1494029A (en) | 1922-05-17 | 1924-05-13 | Said Scofield | Process of separating the constituents of mineral silicates |
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| JP2010529289A (ja) * | 2007-05-21 | 2010-08-26 | エクスプロレイション オーバイト ヴイエスピーエー インコーポレイテッド | アルミニウム鉱石からアルミニウム及び鉄を抽出する方法 |
| US20110120267A1 (en) * | 2008-06-25 | 2011-05-26 | Eric Girvan Roche | Iron Precipitation |
Also Published As
| Publication number | Publication date |
|---|---|
| BR112013030819A2 (pt) | 2019-09-24 |
| US20140301920A1 (en) | 2014-10-09 |
| EP2714594A4 (en) | 2015-05-20 |
| CA2863755C (en) | 2016-04-26 |
| WO2012162817A1 (en) | 2012-12-06 |
| AU2012262586A1 (en) | 2013-05-02 |
| CN103842296A (zh) | 2014-06-04 |
| CN103842296B (zh) | 2016-08-24 |
| AU2012262586B2 (en) | 2015-05-14 |
| CA2834356C (en) | 2014-11-25 |
| US20160052796A1 (en) | 2016-02-25 |
| CA2863755A1 (en) | 2012-12-06 |
| US9150428B2 (en) | 2015-10-06 |
| RU2013157943A (ru) | 2015-07-20 |
| EP2714594A1 (en) | 2014-04-09 |
| CA2834356A1 (en) | 2012-12-06 |
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