CN1455661A - 含有生理活性玻璃的新型化妆、个人护理、清洁剂和营养增补剂组合物及其制备和使用方法 - Google Patents
含有生理活性玻璃的新型化妆、个人护理、清洁剂和营养增补剂组合物及其制备和使用方法 Download PDFInfo
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- CN1455661A CN1455661A CN01810211A CN01810211A CN1455661A CN 1455661 A CN1455661 A CN 1455661A CN 01810211 A CN01810211 A CN 01810211A CN 01810211 A CN01810211 A CN 01810211A CN 1455661 A CN1455661 A CN 1455661A
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- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
- 229940118257 zinc undecylenate Drugs 0.000 description 1
- UCRLQOPRDMGYOA-DFTDUNEMSA-L zinc;(4r)-4-[[(2s)-2-[[(4r)-2-[(1s,2s)-1-amino-2-methylbutyl]-4,5-dihydro-1,3-thiazole-4-carbonyl]amino]-4-methylpentanoyl]amino]-5-[[(2s,3s)-1-[[(3s,6r,9s,12r,15s,18r,21s)-3-(2-amino-2-oxoethyl)-18-(3-aminopropyl)-12-benzyl-15-[(2s)-butan-2-yl]-6-(carbox Chemical compound [Zn+2].C1SC([C@@H](N)[C@@H](C)CC)=N[C@@H]1C(=O)N[C@@H](CC(C)C)C(=O)N[C@H](CCC([O-])=O)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H]1C(=O)N[C@H](CCCN)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@H](CC=2C=CC=CC=2)C(=O)N[C@@H](CC=2NC=NC=2)C(=O)N[C@H](CC([O-])=O)C(=O)N[C@@H](CC(N)=O)C(=O)NCCCC1 UCRLQOPRDMGYOA-DFTDUNEMSA-L 0.000 description 1
- BOVNWDGXGNVNQD-UHFFFAOYSA-L zinc;2-hydroxybenzenesulfonate Chemical compound [Zn+2].OC1=CC=CC=C1S([O-])(=O)=O.OC1=CC=CC=C1S([O-])(=O)=O BOVNWDGXGNVNQD-UHFFFAOYSA-L 0.000 description 1
- 229940043798 zincon Drugs 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- 239000002076 α-tocopherol Substances 0.000 description 1
- 235000004835 α-tocopherol Nutrition 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/896—Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/22—Peroxides; Oxygen; Ozone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/04—Drugs for disorders of the alimentary tract or the digestive system for ulcers, gastritis or reflux esophagitis, e.g. antacids, inhibitors of acid secretion, mucosal protectants
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- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/14—Prodigestives, e.g. acids, enzymes, appetite stimulants, antidyspeptics, tonics, antiflatulents
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- A61P17/00—Drugs for dermatological disorders
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q9/00—Preparations for removing hair or for aiding hair removal
- A61Q9/02—Shaving preparations
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C12/00—Powdered glass; Bead compositions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/097—Glass compositions containing silica with 40% to 90% silica, by weight containing phosphorus, niobium or tantalum
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/11—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen
- C03C3/112—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/11—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen
- C03C3/112—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine
- C03C3/115—Glass compositions containing silica with 40% to 90% silica, by weight containing halogen or nitrogen containing fluorine containing boron
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- C03C4/0007—Compositions for glass with special properties for biologically-compatible glass
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- C03C4/00—Compositions for glass with special properties
- C03C4/0007—Compositions for glass with special properties for biologically-compatible glass
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- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2204/00—Glasses, glazes or enamels with special properties
- C03C2204/02—Antibacterial glass, glaze or enamel
Abstract
Description
原材料 |
Incromectant AQ |
Promyristyl PM-3 |
Dermol DPG-2B |
Transcutol CG |
甲氧基肉桂酸辛酯 |
Crodafos N3N |
三乙醇胺 |
邻氨基苯甲酸薄荷酯 |
矿物油 |
Incrodet TD7C |
Polyderm PPI SiWI |
PEG2 Oleamine |
Crodafos CAP |
Plantaren APB |
Polyderm PPI SiWS |
Finsolv TN |
Crodasinic O |
Dermol B-246 |
GE 1202 |
Crovol A-40 |
Crovol A-70 |
GE SF 96 350 cps |
Probutyl 14 |
Foamtaine CABG |
Dermol M5 |
PPG 10鲸蜡基醚 |
PEG7甘油基椰子酯 |
d-芋烯 |
Oleth-3 |
Stepanquat ML |
月桂基硫酸铵 |
Incromectant LQ |
Tergitol NP-9 |
椰油基羟基磺基甜菜碱 |
Crodesta SL-40*** |
POE20脱水山梨糖醇单油酸酯 |
丙二醇 |
乙醇 |
月桂酰-2硫酸钠 |
脱水山梨糖醇异硬脂酸酯 |
丙三醇 |
Procetyl AWS |
Crodafos SG |
Glycerox 767 |
Cocamide DEA |
Jojoba Oil |
Abil EM-90 |
原材料 |
Dermol M5 |
PPG10鲸蜡基醚 |
PEG7甘油基椰子酸酯 |
d-芋烯 |
Oleth-3 |
Stepanquat ML |
月桂基硫酸铵 |
Incromectant LQ |
Tergitol NP-9 |
椰油基羟基磺基甜菜碱 |
Crodesta SL-40 |
POE20脱水山梨糖醇单油酸酯 |
丙二醇 |
乙醇 |
月桂酰基-2硫酸钠 |
脱水山梨糖的异硬脂酸酯 |
甘油 |
Procetyl AWS |
Crodafos SG |
Glycerox 767 |
Cocamide DEA |
Jojoba Oil |
Incromectant AQ |
Foamtaine CABG(45%) |
Promyristyl PM-3 |
Abil EM-90 |
Dermol DPG-2B |
Transutol CG |
甲氧基肉桂酸辛酯 |
Crodafos N3N |
三乙醇胺 |
邻氨基苯甲酸薄荷基酯 |
矿物油 |
Incrodet TD7C |
Polyderm PPI SiWI |
PEG2 Oleamine |
Ctodafos CAP |
Plantaren APB |
Polyderm PPI SiWS |
Finsolv TN |
Crodsdinic O |
Dermol B-246 |
GE 1202 |
Crovol A-40 |
Crovol A-70 |
GESF 96(350 cps) |
Protutyl 14 |
试验菌 | 批号 | ||
枯草芽孢杆菌 | 1 | 2 | 3 |
1天 | 5 | 5 | 3 |
2天 | 2 | 2 | 1 |
3天 | 2 | 1 | 1 |
5天 | 2 | 0 | 0 |
试验菌 | 批号 | ||
金黄色葡萄球菌 | 1 | 2 | 3 |
1天 | 4 | 4 | 4 |
2天 | 3 | 3 | 2 |
3天 | 3 | 3 | 2 |
5天 | 3 | 2 | 2 |
试验菌 | 批号 | ||
铜绿假单胞杆菌 | 1 | 2 | 3 |
1天 | 4 | 4 | 3 |
2天 | 2 | 2 | 1 |
3天 | 2 | 2 | 0 |
5天 | 2 | 0 | 0 |
试验菌 | 批号 | ||
白色念株菌 | 1 | 2 | 3 |
1天 | 3 | 3 | 3 |
2天 | 0 | 1 | 1 |
3天 | 0 | 0 | 0 |
5天 | 0 | 0 | 0 |
试验菌 | 批号 | ||
黑曲霉 | 1 | 2 | 3 |
1天 | 5 | 5 | 5 |
2天 | 5 | 5 | 4 |
3天 | 3 | 3 | 2 |
5天 | 2 | 2 | 0 |
试验菌 | 玻璃量(mg) | ||||
枯草芽孢杆菌 | 10 | 100 | 200 | 500 | 1000 |
1天 | >105 | >105 | >104 | 0 | 0 |
2天 | >105 | >105 | >104 | 0 | 0 |
3天 | >105 | >105 | >104 | 0 | 0 |
5天 | >105 | >105 | + | - | - |
试验菌 | 玻璃量(mg) | ||||
金黄色葡萄球菌 | 10 | 100 | 200 | 500 | 1000 |
1天 | >105 | >105 | >104 | 0 | 0 |
2天 | >105 | >105 | >104 | 0 | 0 |
3天 | >105 | >105 | >104 | 0 | 0 |
5天 | >105 | >105 | + | - | - |
试验菌 | 玻璃量(mg) | ||||
铜绿假单胞菌 | 10 | 100 | 200 | 500 | 1000 |
1天 | >105 | >105 | >104 | 0 | 0 |
2天 | >105 | >105 | >104 | 0 | 0 |
3天 | >105 | >105 | >104 | 0 | 0 |
5天 | >105 | >105 | + | - | - |
试验菌 | 玻璃量(mg) | ||||
白色念球菌 | 10 | 100 | 200 | 500 | 1000 |
1天 | >105 | >105 | 0 | 0 | 0 |
2天 | >105 | >105 | >300 | 0 | 0 |
3天 | >105 | >105 | >300 | 0 | 0 |
5天 | >105 | >105 | + | + | + |
试验菌 | 玻璃量(mg) | ||||
黑曲霉 | 10 | 100 | 200 | 500 | 1000 |
1天 | n.d. | n.d. | n.d. | n.d. | n.d |
2天 | >105 | >300 | >30 | 0 | 0 |
3天 | >105 | >300 | >30 | 0 | 0 |
5天 | >105 | + | + | + | + |
含生物玻璃的载荷试验黑曲霉试验系列3AV99/020/01/11-V99/020/01/19含水溶液/上清液V99/020/02/02 O/W乳液V99/020/03/02 W/O乳液 | ||||||||
浓度 | ||||||||
循环0 | 循环1 | 循环2 | 循环3 | 循环4 | 循环5 | 循环6 | ||
水溶液(没有沉淀的上清液) (V99/020/01/11-19) | ||||||||
0.5% | - | +++ | +++ | +++ | +++ | +++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约105 |
0.8% | - | +++ | +++ | +++ | +++ | +++ | +++ | |
1% | - | +++ | +++ | +++ | +++ | +++ | +++ | |
2% | - | +++ | +++ | +++ | ||||
3% | - | +++ | +++ | +++ | +++ | +++ | +++ | |
5% | - | +++ | +++ | - | +++ | +++ | +++ | |
10% | - | +++ | - | - | +++ | +++ | +++ | |
15% | - | +++ | - | - | +++ | ++ | +++ | |
20% | - | - | - | - | +++ | +++ | +++ | |
O/W乳液(V99/020/02/02) | ||||||||
2% | - | +++ | +++ | + | +++ | ++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约105空白试验:不含生物玻璃 |
5% | - | - | - | - | + | - | + | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | ++ | + | ++ | |
20% | - | - | - | - | ++ | + | ++ | |
空白试验 | - | +++ | +++ | +++ | +++ | +++ | +++ | |
W/O乳液(V99/020/03/02) | ||||||||
2% | - | +++ | +++ | +++ | +++ | +++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约105空白试验:不含生物玻璃 |
5% | - | +++ | +++ | +++ | +++ | ++ | + | |
10% | - | +++ | - | - | - | |||
15% | - | - | - | - | - | - | + | |
20% | - | - | - | - | - | - | - | |
空白试验 | - | +++ | +++ | +++ | +++ | +++ | +++ |
含生物玻璃的载荷试验结果白色念珠菌试验系列3BV99/020/01/11-V99/020/01/19水溶液/上清液V99/020/02/02 O/W乳液V99/020/03/02 W/O乳液 | ||||||||
浓度 | ||||||||
循环0 | 循环1 | 循环2 | 循环3 | 循环4 | 循环5 | 循环6 | ||
水溶液(没有沉淀的上清液) (V99/020/01/11-19) | ||||||||
0.5% | - | - | - | ++ | +++ | +++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106 |
0.8% | - | - | - | + | +++ | +++ | +++ | |
1% | - | - | - | - | +++ | +++ | +++ | |
2% | - | - | - | - | - | ++ | +++ | |
3% | - | - | - | - | - | - | - | |
5% | - | - | - | - | - | - | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
O/W乳液(V99/020/02/02) | ||||||||
2% | - | - | - | - | - | - | - | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106空白试验:不含生物玻璃 |
5% | - | - | - | - | - | - | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
空白实验 | - | +++ | +++ | +++ | +++ | +++ | +++ | |
W/O乳液(V99/020/03/02) | ||||||||
2% | - | - | - | +++ | +++ | +++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106空白试验:不含生物玻璃 |
5% | - | - | + | - | - | - | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | +++ | +++ | +++ | +++ | +++ | +++ | |
空白试验 | - | - | - | - | - | - | - |
含生物玻璃的载荷试验大肠杆菌试验系列3CV99/020/01/11-V99/020/01/19含水溶液/上清液V99/020/02/02 O/W乳液V99/020/03/02 W/O乳液 | ||||||||
浓度 | ||||||||
循环0 | 循环1 | 循环2 | 循环3 | 循环4 | 循环5 | 循环6 | ||
水溶液(没有沉淀的上清液) (V99/020/01/11-19) | ||||||||
0.5% | - | - | + | - | +++ | +++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106 |
0.8% | - | - | + | - | - | - | - | |
1% | - | - | - | - | - | +++ | +++ | |
2% | - | - | - | - | - | - | +++ | |
3% | - | - | - | - | - | - | - | |
5% | - | - | - | - | - | - | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
O/W乳液 (V99/020/02/02) | ||||||||
2% | - | - | - | - | - | - | - | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106空白试验:不含生物玻璃 |
5% | - | - | - | - | - | - | - | |
10% | - | - | - | - | - | (+) | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
空白试验 | - | - | - | - | - | - | - | |
W/O乳液(V99/020/03/02) | ||||||||
2% | - | + | - | (+) | (++) | (++) | - | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106空白试验:不舍生物玻璃 |
5% | - | - | - | - | - | - | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
空白试验 | - | - | - | - | - | - | ++ |
含生物玻璃的载荷试验铜绿假单胞杆菌试验系列3DV99/020/01/11-V99/020/01/19含水溶液/上清液V99/020/02/02 O/W乳液V99/020/03/02 W/O乳液 | ||||||||
浓度 | ||||||||
循环0 | 循环1 | 循环2 | 循环3 | 循环4 | 循环5 | 循环6 | ||
水溶液(没有沉淀的上清液) (V99/020/01/11-19) | ||||||||
0.5% | - | - | - | - | +++ | +++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106 |
0.8% | - | - | +++ | +++ | +++ | +++ | +++ | |
1% | - | - | - | - | +++ | +++ | +++ | |
2% | - | - | - | +++ | +++ | +++ | +++ | |
3% | - | - | - | - | +++ | +++ | +++ | |
5% | - | - | - | - | - | + | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
O/W乳液(V99/020/02/02) | ||||||||
2% | - | - | - | - | - | - | - | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106空白试验:不含生物玻璃 |
5% | - | - | - | - | - | - | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
空白试验 | - | - | - | - | - | - | - | |
W/O乳液(V99/020/03/02) | ||||||||
2% | - | - | - | +++ | +++ | +++ | +++ | 解释:循环0:没有培养的斑循环1-6:用上述菌种培养的斑,样品瓶中的浓度大约106空白试验:不含生物玻璃 |
5%乳液 | - | - | - | - | - | - | - | |
10% | - | - | - | - | - | - | - | |
15% | - | - | - | - | - | - | - | |
20% | - | - | - | - | - | - | - | |
空白试验 | - | - | +++ | +++ | +++ | +++ | +++ |
生物玻璃的载荷试验试验系列7A黑曲霉/白色念株菌V99/020/06/01 O/W乳液(Dragil)未灭菌/PH未调节 | ||||||
产物NEO/W膏(Dragll) | 试验号V99/020/06/01 | 生产日期10/11/99 | 开始试验日期10/15/99 | |||
黑曲霉106CFU/ml | ||||||
Cons,No,MB99 | 生物玻璃% | 空白 | 循环1 | 循环2 | 循环3 | 开始试验前的PH值 |
1000 | a)2 | - | +++ | +++ | +++ | 10.9 |
1001 | b)5 | - | - | - | - | 11.6 |
1002 | c)10 | - | - | - | - | 11.8 |
1003 | d)15 | - | - | - | - | 12.1 |
1004 | e)20 | - | - | - | - | 12.2 |
1005 | f)none | - | +++ | +++ | +++ | 7.1 |
白色念株菌107CFU/ml | ||||||
Cons.No.MB99 | 生物玻璃% | 空白 | 循环1 | 循环2 | 循环3 | 开始试验前的PH值 |
1006 | a)2 | - | - | - | - | 10.9 |
1007 | b)5 | - | - | - | - | 11.6 |
1008 | c)10 | - | - | (+++P) | - | 11.8 |
1009 | d)15 | - | - | - | - | 12.1 |
1010 | e)20 | - | - | - | - | 12.2 |
1011 | f)none | - | +++ | +++ | +++ | 7.1 |
生物玻璃的载荷试验试验系列7B大肠杆菌/铜绿假单胞杆菌V99/020/06/01 O/W乳液(Dragil)未灭菌/PH未调节 | ||||||
产物NEO/W膏(Dragil) | 试验号V99/020/06/01 | 生产日期10/11/99 | 开始试验日期10/15/99 | |||
大肠杆菌107CFU/ml | ||||||
Cons.No.MB99 | 生物玻璃% | 空白 | 循环1 | 循环2 | 循环3 | 开始试验前的PH值 |
1012 | a)2 | - | - | - | - | 10.9 |
1013 | b)5 | - | - | - | - | 11.6 |
1014 | c)10 | - | - | - | - | 11.8 |
1015 | d)15 | - | - | - | - | 12.1 |
1016 | e)20 | - | - | - | - | 12.2 |
1017 | f)none | - | +++ | +++ | +++ | 7.1 |
铜绿假单胞杆菌107CFU/ml | ||||||
Cons.No.MB99 | 生物玻璃% | 空白 | 循环1 | 循环2 | 循环3 | 开始试验前的PH值 |
1018 | a)2 | - | - | - | - | 10.9 |
1019 | b)5 | - | - | - | - | 11.6 |
1020 | c)10 | - | - | - | - | 11.8 |
1021 | d)15 | - | - | - | - | 12.1 |
1022 | e)20 | - | - | - | - | 12.2 |
1023 | f)none | - | +++ | +++ | +++ | 7.1 |
生物玻璃的载荷试验试验系列7C金黄色葡萄球菌/大肠杆菌(PH已调节)V99/020/06/01 O/W 乳液(Dragil)未灭菌/PH未调节 | ||||||
产物NE O/W膏(Dragil) | 试验号V99/020/06/01 | 生产日期10/11/99 | 开始试验日期10/15/99 | |||
金黄色葡萄球菌107CFU/ml | ||||||
Cons.No.MB99 | 生物玻璃% | 空白 | 循环1 | 循环2 | 循环3 | 开始试验前的PH值 |
1024 | a)2 | - | - | - | - | 10.9 |
1025 | b)5 | - | - | - | - | 11.6 |
1026 | c)10 | - | - | - | - | 11.8 |
1027 | d)15 | - | - | - | - | 12.1 |
1028 | c)20 | - | - | - | - | 12.2 |
1029 | f)none | - | + | + | + | 7.1 |
大肠杆菌107CFU/ml(用调节过的PH值做对比试验) | ||||||
Cons.No.MB99 | 生物玻璃% | 空白 | 循环1 | 循环2 | 循环3 | PH/值11/09/99 |
1030 | a)2 | + | +++ | +++ | +++ | 8.5 |
1031 | b)5 | - | - | - | - | 10 |
1032 | c)10 | ++ | - | - | - | 10 |
1033 | d)15 | - | - | - | - | 10 |
1034 | e)20 | - | - | - | - | 10 |
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- 2001-03-27 BR BR0109603-6A patent/BR0109603A/pt not_active Application Discontinuation
- 2001-03-27 EP EP01922745A patent/EP1272144A4/en not_active Ceased
- 2001-03-27 WO PCT/US2001/009800 patent/WO2001072262A2/en active Search and Examination
- 2001-03-27 AU AU2001249510A patent/AU2001249510A1/en not_active Abandoned
- 2001-03-27 RU RU2002125871/15A patent/RU2251405C2/ru active
- 2001-03-27 CN CN01810211A patent/CN1455661A/zh active Pending
- 2001-03-27 PL PL01363113A patent/PL363113A1/xx not_active Application Discontinuation
- 2001-03-27 KR KR1020027012682A patent/KR20030019333A/ko not_active Application Discontinuation
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Also Published As
Publication number | Publication date |
---|---|
WO2001072262A3 (en) | 2001-10-25 |
RU2002125871A (ru) | 2004-03-20 |
WO2001072262A2 (en) | 2001-10-04 |
US20020086039A1 (en) | 2002-07-04 |
US8551508B2 (en) | 2013-10-08 |
AU2001249510A1 (en) | 2001-10-08 |
RU2251405C2 (ru) | 2005-05-10 |
EP1272144A4 (en) | 2006-04-26 |
US7250174B2 (en) | 2007-07-31 |
US20070275021A1 (en) | 2007-11-29 |
EP1272144A2 (en) | 2003-01-08 |
JP2004500404A (ja) | 2004-01-08 |
PL363113A1 (en) | 2004-11-15 |
KR20030019333A (ko) | 2003-03-06 |
BR0109603A (pt) | 2004-02-25 |
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