CN103300450B - Preparation method of raw dendrobium officinale pulp beverage - Google Patents
Preparation method of raw dendrobium officinale pulp beverage Download PDFInfo
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Abstract
The invention discloses a preparation method of a raw dendrobium officinale pulp beverage. The preparation method comprises the following steps of: (1), baking a fresh dendrobium officinale branch to be purple, adding water to the baked fresh dendrobium officinale branch for pulping, so as to obtain a primary serous fluid; (2), carrying out insulation treatment on the primary serous fluid, boiling and filtering the primary serous fluid, so as to obtain filter residue; (3) adding water to the filter residue for pulping, boiling and filtering the filter residue again to obtain the filter residue, repeating the sub-steps for a plurality of times, adding water to the final filter residue for the pulping, so as to obtain secondary serous fluid; (4), adding a cellulolytic enzyme into the secondary serous fluid for carrying out enzymolysis, so as to obtain an enzymolysis solution; (5) boiling and filtering the enzymolysis solution, to obtain the filter residue; (6) adding water into the filter residue for the pulping, boiling and filtering the filter residue again, to obtain the filter residue, and repeating the sub-steps for a plurality of times; (7) mixing all the filter solutions, boiling and sterilizing the mixed filter solution, so as to obtain the raw dendrobium officinale pulp beverage. The preparation method provided by the invention has the advantages that dendrobium officinale is baked, the filter residue is subjected to enzymolysis treatment, the extraction rate of functionality polyose and flavone is improved, the content of dietary fiber in the beverage is increased, and the prepared beverage color is bright and stable.
Description
Technical field
The present invention relates to health food development technical field, be specifically related to a kind of preparation method of dendrobium candidum primary pulp drink.
Background technology
Dendrobium candidum contains dendrobium polysaccharide, flavones, protein, 17 seed amino acids and inorganic elements etc., it is sweet in flavor and cold in property, there is reinforcing stomach reg fluid, nourishing Yin and clearing heat function, be described as first of " Chinese nine immortal grass ", have good curative effect in diseases such as treatment enterogastric diseases, cataract, arthritis, Buerger's disease and chronic pharyngitis.
Candidum tissue culturing seedling and relevant health-product market are in the high speed stage of growth, and development space is huge.According to the relevent statistics, at present annual dendrobium candidum market demand is more than 1,000,000 kilograms for root, and the medicine using dendrobium candidum as raw material, the health products output value exceed hundred million yuan of hundreds ofs.These medicines and health food seem a lot, but formulation is mostly fairly simple, and preparation method taking to the roughing of fresh goods or Tiepi Fengdou dry product as main, product is single, utilization rate of active components is lower.
The Chinese patent literature that is CN1307901A as publication number discloses a kind of processing method of iron-sheet dendrobe fresh product, fresh dendrobium candidum of gathering is placed in to Ozone Water and soaks 20-40 minute, then use clear water rinsing, after rinsing is complete, dry, the method for pulverizing by vacuum refrigeration is made pulvis.In the dendrobium candidum powder that described processing method obtains, contain more crude fibre, after soaking, edible residue is more, and mouthfeel is not good enough.
The Chinese patent literature that is CN1754564A as notification number discloses a kind of method that the fresh dendrobium candidum young stem and leaf of gathering is added to honey and makes through cleaning, decoct juice, concentration operation honey dendrobium candidum extract processed; It is raw material that the method has adopted dendrobium candidum young stem and leaf, but polysaccharide accumulation deficiency in young stem and leaf, in the honey dendrobium candidum extract processed that not only makes to obtain, most important functional component (being polysaccharide) content is less, and this valuable ingredient of traditional Chinese medicine of dendrobium candidum is caused to the waste of raw material.
Publication number is the preparation method that the Chinese patent literature of CN100497396A discloses a kind of dendrobium candidum polysaccharide extractive, comprises degreasing, extraction, concentrated, alcohol precipitation, dry, and finally obtaining molecular weight is 1～300,000, and polyoses content is 25%～50%(weight).This preparation method is not used to the flavones being rich in dendrobium candidum, protein, amino acid and trace element, and raw material availability is also lower.
Publication number is the preparation method that the Chinese patent literature of CN102008654A discloses a kind of dendrobium officinale fresh juice stock solution, the method by after fresh dendrobium candidum washing and sterilizing through the separation of squeezing the juice, vacuum outgas, add pectase and cellulase to make hydrolyzed pectin by large molecule hydrolyzed pectin, to reduce viscosity.But pectase is processed also can be by polysaccharide hydrolysis, make the dendrobium officinale fresh juice stock solution obtaining lose due effect.
Summary of the invention
The invention provides a kind of preparation method of dendrobium candidum primary pulp drink, in the dendrobium candidum primary pulp drink that utilizes this preparation method to obtain, be rich in the functional component such as polysaccharide, flavones, and bright-colored stable, and the utilization rate of dendrobium candidum is up to more than 70%.
A preparation method for dendrobium candidum primary pulp drink, comprising:
(1) get the fresh branch of dendrobium candidum, be baked to and be purple, the making beating that adds water, makes just slurries;
(2) by boiling after first slurries insulation processing, filter, get filter residue;
(3) filter residue is added water again making beating, boils, and filters, and gets filter residue, and after repeated several times, the filter residue making beating that adds water makes secondary slurries;
(4) carry out enzymolysis toward adding cellulase in secondary slurries, obtain enzymolysis liquid;
(5) enzymolysis liquid is boiled, filters, get filter residue,
(6) filter residue is added water again making beating, boils, and filters, and gets filter residue, repeated several times;
(7) merge all filtrate, boil sterilization, make dendrobium candidum primary pulp drink.
In step (1), add water before making beating, fresh the dendrobium candidum after baking branch is cut into chunks, length 0.1～1.0cm; More preferably 0.2cm.Shorter dendrobium candidum stem section is more conducive to the stripping of functional polysaccharide and flavones.
As preferably, baking temperature is 85～95 DEG C, and baking time is 10～30min.As further preferred, baking temperature is 95 DEG C, and baking time is 15min.High-temperature baking can not only be removed herbaceous taste, plays the effect completing; And in bake process, the anthocyanin in dendrobium candidum reacts with functional polysaccharide, flavones, make the color of primary pulp drink more bright-coloured and stable.
After having toasted, add clean clear water making beating, make functional polysaccharide, flavones and anthocyanin stripping in dendrobium candidum.While adding water making beating, material-water ratio is preferably 1:5～7.
For making more anthocyanin stripping, in step (2), the first slurries that obtain are incubated to a period of time at a certain temperature, heat-retaining condition is preferably: 50～55 DEG C of temperature, time 30～120min; More preferably: temperature 50 C, time 30min.Under this heat-retaining condition, anthocyanin stripping substantially.
In step (3), in first slurries after insulation, add the water of 8～10 times of amounts of dendrobium candidum raw material, after boiling 3～8min, filter, get the filter residue after filtration, add the water making beating of 3～5 times of amounts of filter residue, obtain secondary slurries, as without special appointment, dendrobium candidum raw material of the present invention refers to fresh of dendrobium candidum.
Slurries are boiled and not only play the effect of sterilizing but also greatly improved functional polysaccharide, flavones extraction efficiency.As preferably, in step (3), the number of times of described repetition is at least 3 times, and the recovery rate that can further improve functional polysaccharide, flavones is boiled in repeatedly adding water making beating.
After the making beating that repeatedly adds water is boiled, most of free functional polysaccharide, flavones stripping substantially, recovery rate cannot improve again.But because the main component of filter residue is cellulose, between cellulosic molecule, also fetter some functional polysaccharide, flavones, and cellulose is water insoluble and common organic solvents, makes this part bound functional polysaccharide, the flavones also cannot stripping.
Therefore in step of the present invention (4), in secondary slurries, add cellulase, utilize cellulase to carry out enzymolysis to cellulose.As preferably, the addition of described cellulase is 5-15U/g dendrobium candidum raw material, more preferably 10U/g dendrobium candidum raw material.1U refers at 50 DEG C, pH5.0, and under the condition of reaction 30min, degraded CMC(carboxymethyl cellulose per minute) the required enzyme amount of generation 1 μ g reduced sugar (with glucose meter).
As preferably, enzymolysis time is 10～40min, and enzymolysis pH is 4.8～5.2, and hydrolysis temperature is 45～55 DEG C.As further preferred, enzymolysis time is 30min, and enzymolysis pH is 5.0, and hydrolysis temperature is 50 DEG C.When enzymolysis, be equipped with stirring, to increase the contact area of filter residue and cellulase, improve enzymolysis efficiency.After enzymolysis, the functional polysaccharide, the flavones that are not only fettered by cellulose are released, and have also obtained many cellulosic water-soluble enzymolysis things.
After stirring enzymolysis completes, enzymolysis liquid boiled to 3～8min and filter.Get the filter residue after filtration, add the water making beating of 3～5 times of amounts of filter residue.As preferably, in step (6), the number of times of described repetition is at least 3 times, and the recovery rate that can further improve functional polysaccharide, flavones is boiled in repeatedly adding water making beating.
As preferably, in the boiling part of step (3) and step (6), in slurries, add appropriate dried peppermint leaf.The dendrobium candidum primary pulp drink so obtaining not only has the fragrance of dendrobium candidum, also has the refrigerant mouthfeel of peppermint, and being more of value to promotes the production of body fluid quenches one's thirst, moistening lung health.
The present invention also provides the dendrobium candidum being made by described preparation method primary pulp drink.In this dendrobium candidum primary pulp drink, anthocyanin content > 0.3 μ g/mL, flavones content > 0.4 μ g/mL, functional polysaccharide content > 1.5mg/mL.
Compared with prior art, beneficial effect of the present invention is:
(1) the present invention carries out the extraction of functional component again after dendrobium candidum is toasted, and is conducive to functional polysaccharide, flavones stripping, and makes the dendrobium candidum primary pulp drink that makes bright-colored, stable;
(2) the present invention utilizes cellulase to carry out enzymolysis to cellulose, increase on the one hand the recovery rate to compositions such as functional polysaccharides in dendrobium candidum, make on the other hand cellulose Partial digestion, be dissolved in the soluble dietary fiber that becomes body health benefits in beverage, also can too far consequently do not cause to functional polysaccharide degraded the reduction of health-care efficacy simultaneously;
(3) preparation method of the present invention is simple to operate, and energy-conserving and environment-protective, cost are low; Functional component rich content in the dendrobium candidum primary pulp drink making, has good health-care efficacy.
Brief description of the drawings
Fig. 1 is the preparation method's of dendrobium candidum primary pulp drink of the present invention flow chart.
Detailed description of the invention
The preparation flow of dendrobium candidum primary pulp drink of the present invention as shown in Figure 1, is described in further detail preparation method of the present invention below in conjunction with the drawings and specific embodiments.
Embodiment 1
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.1cm toast 40min at 85 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:6, and making beating obtains just slurries;
(2) first slurries are incubated to 60min at 55 DEG C; After insulation, add the water of 8 times of amounts of dendrobium candidum raw material, filter after boiling 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 5U/g dendrobium candidum raw material; Enzymolysis 20min at approximately 5.0,48 DEG C of pH, obtains enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 3 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, boil, make dendrobium candidum primary pulp drink; And calculate the fresh branch utilization rate of dendrobium candidum; Computing formula is:
In formula, M is the fresh branch weight of dendrobium candidum before baking, and x is the fresh branch of dendrobium candidum moisture, m
1for final filter residue dry weight.
In the present embodiment, the fresh branch utilization rate of dendrobium candidum is 77%.
Embodiment 2
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.2cm toast 15min at 95 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:5, and making beating obtains just slurries;
(2) first slurries are incubated to 30min at 50 DEG C; After insulation, add the water of 10 times of amounts of dendrobium candidum raw material, filter after boiling 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 3 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 10U/g dendrobium candidum raw material; Enzymolysis 30min at approximately 5.0,50 DEG C of pH, obtains enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 77%.
Embodiment 3
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.8cm toast 30min at 90 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:7, and making beating obtains slurries;
(2) first slurries are incubated to 120min at 50 DEG C; After insulation, add the water of 9 times of amounts of dendrobium candidum raw material, filter after boiling 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 15U/g dendrobium candidum raw material; Be enzymolysis 10min at 5.0 left and right, 52 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 72%.
Embodiment 4
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 1cm toast 40min at 85 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:7, and making beating obtains slurries;
(2) first slurries are incubated to 100min at 55 DEG C; After insulation, add the water of 10 times of amounts of dendrobium candidum raw material, filter after boiling 8min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 15U/g dendrobium candidum raw material; Be enzymolysis 40min at 5.0 left and right, 50 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 8min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 71%.
Embodiment 5
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.2cm toast 20min at 95 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:6, and making beating obtains just slurries;
(2) first slurries are incubated to 120min at 55 DEG C; After insulation, add the water of 8 times of amounts of dendrobium candidum raw material, filter after boiling 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 10U/g dendrobium candidum raw material; Be enzymolysis 10min at 5.0 left and right, 48 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 3 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 75%.
Embodiment 6
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.1cm toast 15min at 90 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:5, and making beating obtains just slurries;
(2) first slurries are incubated to 120min at 55 DEG C; After insulation, add the water of 8 times of amounts of dendrobium candidum raw material, filter after boiling 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 15U/g dendrobium candidum raw material; Be enzymolysis 10min at 5.0 left and right, 52 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 3 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 78%.
Embodiment 7
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.5cm toast 30min at 85 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:7, and making beating obtains just slurries;
(2) first slurries are incubated to 30min at 52 DEG C; After insulation, add the water of 9 times of amounts of dendrobium candidum raw material, filter after boiling 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 5U/g dendrobium candidum raw material; Be enzymolysis 20min at 5.0 left and right, 50 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 3 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 72%.
Embodiment 8
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.3cm toast 15min at 85 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:6, and making beating obtains just slurries;
(2) first slurries are incubated to 30min at 50 DEG C; After insulation, add the water of 9 times of amounts of dendrobium candidum raw material, filter after boiling 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 10U/g dendrobium candidum raw material; Be enzymolysis 30min at 5.0 left and right, 50 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 75%.
Embodiment 9
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.2cm toast 20min at 95 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:7, and making beating obtains just slurries;
(2) first slurries are incubated to 60min at 50 DEG C; After insulation, add the water of 10 times of amounts of dendrobium candidum raw material, filter after boiling 8min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 10U/g dendrobium candidum raw material; Be enzymolysis 30min at 5.0 left and right, 50 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 8min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 76%.
Embodiment 10
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 1cm toast 30min at 95 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:7, and making beating obtains just slurries;
(2) first slurries are incubated to 60min at 50 DEG C; After insulation, add the water of 9 times of amounts of dendrobium candidum raw material, filter after boiling 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 3 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 5U/g dendrobium candidum raw material; Be enzymolysis 40min at 5.0 left and right, 55 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 70%.
Embodiment 11
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.8cm toast 15min at 85 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:6, and making beating obtains just slurries;
(2) first slurries are incubated to 120min at 50 DEG C; After insulation, add the water of 10 times of amounts of dendrobium candidum raw material, filter after boiling 8min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 10U/g dendrobium candidum raw material; Be enzymolysis 40min at 5.0 left and right, 45 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 8min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 74%.
Embodiment 12
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 0.2cm toast 20min at 85 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:7, and making beating obtains just slurries;
(2) first slurries are incubated to 30min at 55 DEG C; After insulation, add the water of 8 times of amounts of dendrobium candidum raw material, filter after boiling 3min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 3 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 15U/g dendrobium candidum raw material; Be enzymolysis 20min at 5.0 left and right, 50 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 75%.
Embodiment 13
(1) by fresh dendrobium candidum defoliation, clean, dry, be cut into the stem section that length is 1cm toast 15min at 95 DEG C after; Getting material-water ratio is dendrobium candidum stem section and the clean clear water of 1:6, and making beating obtains just slurries;
(2) first slurries are incubated to 60min at 50 DEG C; After insulation, add the water of 10 times of amounts of dendrobium candidum raw material, filter after boiling 8min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 5 times of amounts, making beating obtains secondary slurries;
(3) in secondary slurries, add cellulase, addition is 10U/g dendrobium candidum raw material; Be enzymolysis 30min at 5.0 left and right, 55 DEG C at pH, obtain enzymolysis liquid;
(4) filter after enzymolysis liquid is boiled to 5min, filtrate is preserved; Filter residue is repeated to " add water and pull an oar-boil-filtration " three times, get the water that filter residue adds 4 times of amounts, pull an oar, filter, get filtrate;
(5) merge all filtrate, sterilizing, makes dendrobium candidum primary pulp drink; And utilize the method for embodiment 1 to calculate the fresh branch utilization rate of the present embodiment, be 71%.
In the dendrobium candidum primary pulp drink that embodiment 1～13 is obtained, the content of functional polysaccharide and flavones is measured, and measurement result is as shown in table 1.
The content of polysaccharide and flavones in the each embodiment dendrobium candidum of table 1 primary pulp drink
The dendrobium candidum primary pulp drink color that above embodiment makes is all bright-coloured stable, the content of comprehensive function polysaccharide and flavones, dendrobium candidum primary pulp drink the best that embodiment 2 obtains.
Comparative example 1
Utilize respectively the method identical with embodiment 1～13 to prepare dendrobium candidum primary pulp drink, but in step (1) fresh dendrobium candidum without toasting the making beating that directly adds water.Content to functional polysaccharide, flavones in the dendrobium candidum primary pulp drink obtaining detects, and testing result is as shown in table 2.
Table 2 toasts the impact of dendrobium candidum stem section on extraction effect
Claims (5)
1. a preparation method for dendrobium candidum primary pulp drink, comprising:
(1) get the fresh branch of dendrobium candidum, be baked to and be purple, the making beating that adds water, makes just slurries;
(2) by boiling after first slurries insulation processing, filter, get filter residue;
(3) filter residue is added water again making beating, boils, and filters, and gets filter residue, and after repeated several times, the filter residue making beating that adds water makes secondary slurries;
(4) carry out enzymolysis toward adding cellulase in secondary slurries, obtain enzymolysis liquid;
(5) enzymolysis liquid is boiled, filters, get filter residue,
(6) filter residue is added water again making beating, boils, and filters, and gets filter residue, repeated several times;
(7) merge all filtrate, boil sterilization, make dendrobium candidum primary pulp drink;
In step (1), baking temperature is 85～95 DEG C, and baking time is 10～30min;
In step (2), the temperature that insulation is processed is 50～55 DEG C, time 30～120min;
In step (3), the number of times of described repetition is at least 3 times;
In step (4), the addition of cellulase is 5-15U/g dendrobium candidum raw material;
In step (4), enzymolysis time is 10～40min, and enzymatic hydrolysis system pH is 4.8～5.2, and hydrolysis temperature is 45～55 DEG C.
2. preparation method as claimed in claim 1, is characterized in that, in step (1), adds water before making beating, fresh the dendrobium candidum after baking branch is cut into chunks, and length 0.1～1.0cm.
3. preparation method as claimed in claim 1, is characterized in that, in step (6), the number of times of described repetition is at least 3 times.
4. the dendrobium candidum primary pulp drink that the preparation method as described in as arbitrary in claim 1～3 makes.
5. dendrobium candidum primary pulp drink as claimed in claim 4, it is characterized in that, anthocyanin content > 0.3 μ g/mL, flavones content > 0.4 μ g/mL, functional polysaccharide content > 1.5mg/mL.
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