CN103340411B - Lung moistening oil tea camellia honey - Google Patents
Lung moistening oil tea camellia honey Download PDFInfo
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- CN103340411B CN103340411B CN201310334397.3A CN201310334397A CN103340411B CN 103340411 B CN103340411 B CN 103340411B CN 201310334397 A CN201310334397 A CN 201310334397A CN 103340411 B CN103340411 B CN 103340411B
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Abstract
The invention discloses a lung moistening oil tea camellia honey relating to the technical field of medicines and health care. The lung moistening oil tea camellia honey is prepared from the following raw materials in parts by weight: 20-30 parts of oil tea seeds, 5-10 parts of peanuts, 3-5 parts of dried apple grunt, 10-20 parts of pure oil tea, 5-10 parts of tremella, 3-6 parts of grape pulp, 5-10 parts of bulbus fritillariae cirrhosae, 5-10 parts of lotus seeds, 1-3 parts of dried white radish, 3-6 parts of ladybell roots and 10-20 parts of honey. The lung moistening oil tea camellia honey has the effects of tonifying the spleen and reinforcing the stomach, reinforcing qi and nourishing blood, relaxing bowels, nourishing yin and engendering liquid, clearing heat and moistening the lung, descending qi and helping digestion, eliminating phlegm and lubricating the lung as well as detoxifying, has a better lubricating effect on the lung, not only can be used for treating cough caused by lung impairment by dryness evil, but also can be used for lubricating and tonifying the lung and avoiding impairing the lung by the dryness evil, and is suitable for all-aged men and women.
Description
Technical field
The present invention relates to medicines and health protection technical field, particularly a kind of moistening lung oil tea honey.
Background technology
Lung is human body vitals, is positioned at thoracic cavity, is covered in the heart.The main Physiological Function of lung is main gas, and department breathes, and main row water, towards hundred arteries and veins, cures mainly joint.Lung qi is reduced to basic operation form with Xuan Fasu.Lung position in the vital organs of the human body is the highest, cover all dirty, therefore there is the title of " canopy ".The lobe of the lung is tender and lovely, not invading of the cold-resistant all heresies of hot eliminating dampness; Lung is gone up again clearing the nasal passage, closes fur outward, closely linked with nature, is subject to outer evil invasion and attack, therefore there is the title of " tender dirty ".Lung happiness profit and dislike dry, the dryness evil impariment of the lung, thereby moistening lung can be safeguarded lung's normal function, avoids outside perverse trend invasion.
The food of moistening lung is many, and as Lilii Decoction: lily is removed to impurity wash clean and put into pot, add water, boil to completely mashed with little fire, add appropriate white sugar, lily band soup is eaten in the lump, this soup has the good moistening lung effect that clears away heart-fire, the most applicable lunger's dietotherapy.Lily decoction: get 30 grams of lilies, 9 grams of the tuber of dwarf lilyturfs, 12 grams, mulberry leaf, 9 grams, almond, 10 grams of sweet honey-fried FOLIUM ERIABOTRYAEs, add water and boil together, and the effect that have nourishing yin and relieving supperficies-syndrome, moistens the lung and relieve the cough can be used for treating the people of autumn because of cold cough, dry cough without phlegm, dry mouth and throat.Yiwei decoction: 10 grams of the root of straight ladybell, 15 grams of the tuber of dwarf lilyturfs, 10 grams, the dried rhizome of rehmannia, 5 grams of radix polygonati officinalis, 30 grams, rock sugar, decocting divides clothes three times, or works as beverage and take; For the dry cough of lung Tianjin damage, dry throat.Points for attention: the people of grippal cough and weakness of the spleen and the stomach easy diarrhoea does not take.
Shellfish pear syrup: 10 grams, Bulbus Fritillariae Cirrhosae powder, 1000 grams, snow pear juice, 500 grams, Donga glue, cook altogether.Each 10 grams, day take twice, can be nourishing Yin and moistening lung, control that chronic cough is not healed, blood-stained sputum, bleeding in the nose,epistaxis.
Eight Immortals cream: raw lotus root juice, ginger juice, pear juice, radish Juice, gingko juice, bamboo juice, sugar-cane juice, the each equal portions of honey, by each juice and even, cook rear with vial store, eat arbitrarily it; There is effect of promote the production of body fluid foster lung, clearing heat and eliminating phlegm.Pears congee: 2, pear, after wash clean, the chopping of gross weight band core, with 100 grams of polished rices, adds suitable quantity of water to cook congee.Carrot gruel: 250 grams, carrot, wash clean chopping, with 100 grams of polished rices, adds suitable quantity of water to cook congee.Chrysanthemum congee: 50 grams of chrysanthemums, 100 grams of polished rices, first decoct soup by chrysanthemum, then chrysanthemum soup is cooked into congee together with polished rice.Sesame gruel: 50 grams of sesames, 100 grams of polished rices, first fry sesame, and pulverization, after polished rice boils, is admixed sesame end with food.Chestnut porridge: 50 grams, chestnut, 100 grams of polished rices, add water and cook congee.
The Chinese medicine of moistening lung is also many, as Snakegourd Fruit, Chinese Drug Gualouzi, root of Chinese trichosanthes, lily, the tuber of dwarf lilyturf, asparagus fern, the root bark of white mulberry, loguat leaf, etc., have good moistening lung effect.
Chinese patent (number of patent application 201110382254.0) " eight-treasure peanut broth and preparation method thereof ", with peanut, lotus seeds, longan, seed of Job's tears, Semen Phaseoli Vulgaris, ginkgo (gingko), white fungus, lily, honey, cane suger is made, compared with prior art, the scientific formulation of this invention, raw material is easily obtained, the food of making has higher nutritive value, manufacture craft is simple, for finding, peanut utilizes outlet on the one hand, on the other hand, the food of making can meet the needs of people's life, products taste is good, product has anti-ageing, increase blood platelet, grow the effect of body complement, it is a kind of natural food that has very high medicinal health function.Another Chinese patent (number of patent application 95115524.5) " a kind of processing method of moistening lung fruit juice cold beverage ", comprising: after the foaming of white fungus water, add water and boil, picked up frozen water cooling for subsequent use; Choose fresh pawpaw, remove seed, be cut into fruit pulp for subsequent use; Pawpaw pulp is added to the white fungus, honey, condensed milk and the ice cube that boil, stir at food blending machine, white fungus, pulp and ice cube are smashed and battered down and stir, become the bland with frothy suspension; The fruit juice cold beverage outward appearance of this invention more attracts client, drinks and more has mouthfeel; And due to adopt many weeks the pawpaw with moistening lung effect, honey and white fungus, so there is the concept of moistening lung, more easily attract particular consumer.
Summary of the invention
The object of the present invention is to provide that one has invigorating spleen and reinforcing stomach, nourishing qi and blood, relaxes bowel, Yin-nourishing and body fluid promoting, clearing heat and moistening lung, lower gas help digestion, effect of eliminating phlegm moistening lung, removing toxic substances, lung are had to the health food that better moistens effect.
For achieving the above object, the technical measures that the present invention takes are a kind of moistening lung oil tea honey of invention, are to be prepared from by following raw material by weight:
The dry apple grunt 3-5 of tea seed 20-30 peanut 5-10
Pure tea oil 10-20 white fungus 5-10 grape berry 3-6
Bulbus Fritillariae Cirrhosae 5-10 lotus seeds 5-10 extra dry white wine radish 1-3
Adenophora tetraphylla 3-6 honey 10-20;
Its preparation method is as follows:
A, get the raw materials ready: get respectively tea seed, peanut, dry apple grunt, pure tea oil, white fungus, grape berry, Bulbus Fritillariae Cirrhosae, lotus seeds, extra dry white wine radish, adenophora tetraphylla, honey by above-mentioned weight portion, backup;
B, lotus seeds pretreatment:
A, by lotus seeds fragmentation for subsequent use, isolate embryo nelumbinis and Semen Nelumbinis, for subsequent use;
B, embryo nelumbinis for subsequent use is placed in to container, adds the yellow rice wine that 1-2 times of weight, weight concentration are 25-40%, soak 10-25min, filter; Again the embryo nelumbinis after filtering is washed 1-4 time with clear water again, obtain processing embryo nelumbinis, for subsequent use;
C, squeezing: tea seed for subsequent use, white fungus, peanut, processing embryo nelumbinis, Semen Nelumbinis are mixed, at 0-6 ℃, through low temperature cold squeezing, obtain the coarse tea oil after squeezing, for subsequent use;
D, alkali treatment: in coarse tea oil for subsequent use, add the aqueous alkali that equivalent weight, concentration are 0.1-1.2%, water temperature is controlled at 30-60 ℃, stir, and filters, and 3 times repeatedly, obtains alkali treatment coarse tea oil; Described aqueous alkali is sodium carbonate: the mixed base aqueous solution of sodium acetate=2:1;
E, initial filter: alkali treatment coarse tea oil for subsequent use is crossed to mixed column, and coutroi velocity is 10-50L/h; Then,, after mixing decolorizing column, coutroi velocity is 5-30L/h, obtains filtration coarse tea oil;
F, press filtration: filtration coarse tea oil for subsequent use, under 0.2-1.5MPa pressure, is filtered, obtains the tea oil I after press filtration, for subsequent use;
G, extraction: pure tea oil for subsequent use is dropped in vapor tight tank, heat to 40-75 ℃, then grape berry for subsequent use, dry apple grunt, extra dry white wine radish are dropped into, firing rate according to 5-10 ℃/min is heated to 100-150 ℃, be incubated again 10-50min, filter, obtain filtration tea oil;
H, mistake post: in filtration tea oil for subsequent use, add the aluminium oxide that accounts for its weight 5-14%, stir at normal temperatures 40-120min, filter, after D201 macroporous resin column, coutroi velocity 10-20L/h, obtained the tea oil II after post, for subsequent use;
I, adenophora tetraphylla pretreatment:
A, adenophora tetraphylla for subsequent use is cut into sheet, is placed in container, add the mature vinegar that accounts for adenophora tetraphylla weight 30-60%, soak 25-40min at 1-10 ℃ of lower seal, filter, dry, must process adenophora tetraphylla, for subsequent use;
B, processing adenophora tetraphylla for subsequent use is placed in to container, first adds the ethanol that 2-5 times of weight, volumetric concentration are 60-95%, at 30-60 ℃, soak 5-10 hour, then carry out diacolation, controlling diacolation flow velocity is 10-20L/h, collects adenophora tetraphylla diacolation ethanol, for subsequent use;
C, be the sodium-chloride water solution of 1-6% to adding weight concentration in adenophora tetraphylla diacolation ethanol for subsequent use, regulate concentration of alcohol to 45-65%, after sephadex column, in controls, column flow rate is 10-15L/h, and collection upper prop liquid is for subsequent use;
D, by upper prop liquid for subsequent use, at 45-70 ℃ of Vacuum Concentration, vacuum is 0.2-0.4MPa, is concentrated into without alcohol, obtains adenophora tetraphylla concentrate, for subsequent use;
J, Bulbus Fritillariae Cirrhosae pretreatment:
A, Bulbus Fritillariae Cirrhosae for subsequent use is placed in to container, adds 2-6 times of weight, extracted by the mixed solvent of low polar organic solvent: water=2-5:1, extracting temperature is 60-90 ℃, and the time is 1.5-2.0 hour, filters; In recrement, add the mixed solvent of same equimultiple to extract again, the time is 0.5-1.2 hour, filters, and merges twice filtrate, is down to after normal temperature, and just extract is for subsequent use to obtain Bulbus Fritillariae Cirrhosae; Described low polar organic solvent is one or more in ethyl acetate, benzinum, ether, n-hexane, No. six solvent naphthas, in the time being multiple, the ratio of each component is equal portions or other ratio;
B, by Bulbus Fritillariae Cirrhosae for subsequent use just extract drop in separator, carry out the separation of liquid liquid, collect low polar organic solvent liquid, for subsequent use;
C, by low polar organic solvent liquid for subsequent use 40-65 ℃ concentrated, be concentrated into without rudimentary property organic solvent, obtain Bulbus Fritillariae Cirrhosae concentrate, for subsequent use;
D, Bulbus Fritillariae Cirrhosae concentrate for subsequent use is sprayed dry, obtain dry powder, for subsequent use;
E, by dry powder for subsequent use, add the clear water of equivalent weight, stir, add the surfactant of the food-grade that accounts for dry powder weight 0.3-1.4% simultaneously, limit edged stirs, and to dissolving completely, till liquid clarification, obtains Bulbus Fritillariae Cirrhosae solution, for subsequent use; Described surfactant is one or more in sucrose ester, monoglyceride, betaine, Tweens, in the time being multiple, the ratio of each component is equal portions or other ratio;
K, mixing: tea oil I for subsequent use, tea oil II, honey, adenophora tetraphylla concentrate, Bulbus Fritillariae Cirrhosae solution are mixed, under 0.5-2.0MPa pressure, be filtered, then under same pressure, filter through microfiltration membranes device again, collect the liquid after filtering, obtain moistening lung oil tea honey.
Described white fungus is to clean through clear water, then adds 40-100 ℃ of emerge in worm water 30-80min of same weight, elimination moisture, then put into constant pressure and dry case and be dried to the white fungus raw material that moisture is less than 20%.
Described aluminium oxide is after using alcohol, hot water treatment, then is dried to the aluminium oxide that moisture is less than 2.0%.
Described D201 macroreticular resin is the resin after highly basic, ethanol, hot water treatment.
The technical scheme one of its optimization is to be prepared from by following raw material by weight:
The dry apple grunt 3 of tea seed 20 peanut 10
Pure tea oil 20 white fungus 10 grape berries 3
Bulbus Fritillariae Cirrhosae 5 lotus seeds 5 extra dry white wine radish 1
Adenophora tetraphylla 3 honey 20.
The technical scheme two of its optimization is to be prepared from by following raw material by weight:
The dry apple grunt 5 of tea seed 30 peanut 5
Pure tea oil 10 white fungus 5 grape berries 6
Bulbus Fritillariae Cirrhosae 10 lotus seeds 10 extra dry white wine radish 3
Adenophora tetraphylla 6 honey 10.
The technical scheme three of its optimization is to be prepared from by following raw material by weight:
The dry apple grunt 4 of tea seed 25 peanut 8
Pure tea oil 15 white fungus 7 grape berries 4
Bulbus Fritillariae Cirrhosae 8 lotus seeds 8 extra dry white wine radish 2
Adenophora tetraphylla 4 honey 15.
Moistening lung oil tea honey of the present invention, adopt tea-seed oil (Camellia oleifera Abel) and honey (Apis cerana Fabr or Apis mellifera L.) as primary raw material, auxiliary material includes peanut (Arachis hypogaea), dry apple grunt (Malus domestica), white fungus (Tremella fuciformis Berk.), grape berry [Vitis Vinifera LINN], lotus seeds (Nelumbo nucifere Gaertn.), extra dry white wine radish (White Radish), adenophora tetraphylla (Radix Adenophorae), Bulbus Fritillariae Cirrhosae (Fritillaria unibracteata Hsiao et K.C. Hsia or Fritillaria cirrhosa D. Don or Fritillaria delavayi Franch. or Fritillaria przewalskii Maxim.ex Batal or Fritillaria cirrhosa D.Don var. ecirrhosa Franch.).
Modern study shows, tea oil contains the compositions such as abundant oleic acid, linoleic acid, leukotrienes, vitamin E, tea saponin, squalene and trace element, and its nutrition and health care function even exceedes olive oil; Meanwhile, in tea oil, contain the active material that vitamin E, D, K and carrotene and camellin etc. are useful to human body, and there is certain sterilization, absorb ultraviolet effect.Honey flavour is sweet, property is flat, returns the spleen channel, stomach through, lung channel and large intestine channel, has harmonizing the spleen and stomach, relieving spasm to stop pain, moistens the lung and relieve the cough, relaxes bowel, the effect such as moisturizing myogenic, removing toxic substances.Peanut is flat, taste is sweet, enters spleen, lung channel, has invigorating spleen and reinforcing stomach, nourishing qi and blood, moistens the lung and relieve the cough, the function of defaecation laxation.Dry apple grunt is flat, sweet, the micro-acid of taste, have promote the production of body fluid to quench thirst, moistening lung relieving restlessness, invigorating spleen and reinforcing stomach, heart-nourishing and Qi-benefiting, ease constipation, antidiarrheal, relieving summer-heat, the effect such as sober up.White fungus slightly sweet flavor, property are flat, return lung, stomach, kidney channel, have that nourishing is promoted the production of body fluid, effect of moistening lung nourishing the stomach, cure mainly cough due to consumptive disease, blood-stained sputum, Tianjin few thirsty, body void, all diseases of shortness of breath and fatigue after being ill.Grape berry is flat, the sweet acid of taste; Enter lung, spleen, kidney channel, can invigorating qi and benefiting blood, Yin-nourishing and body fluid promoting, strengthening the muscles and bones, tonneau urine; Cure mainly deficient qi and blood, chronic cough of deficiency lung, the deficiency of liver-yin and kidney-yin, palpitation and night sweat, waist and leg ache, muscles and bones is unable, arthralgia due to wind-dampness, face limb edema, the illnesss such as difficult urination.Lotus seeds taste is sweet, puckery, and property is flat, and the thoughts of returning home, spleen, kidney, stomach, liver, urinary bladder channel, have the effects such as tonifying spleen antidiarrheal, supplementing the kidney to control the nocturnal, mental-tranquilization, cure mainly insufficiency of the spleenly rush down for a long time, rush down protracted dysentery, emission due to the kidney deficiency, lingering diarrhea, have no peace of mind, palpitation with fear, all diseases of egersis.Sweet pungent, the property of extra dry white wine radish taste is flat, returns lung, spleen two warps, has that lower gas helps digestion, eliminating phlegm moistening lung, removing toxic substances promote the production of body fluid and the effect such as middle cough-relieving, sharp stool and urine.Adenophora tetraphylla sweet and slightly bitter taste, cold nature, attach to the lung and stomach meridians, and has the effects such as replenishing the vital essence and removing heat, moistening lung for removing phlegm, reinforcing stomach reg fluid.Bulbus Fritillariae Cirrhosae taste is sweet, bitter, and cold nature is returned lung, the heart channel of Hang-Shaoyin, has clearing heat and moistening lung; Preventing phlegm from forming and stopping coughing; The effects such as mass dissipating and swelling eliminating.
Above-mentioned many raw materials share, and have invigorating spleen and reinforcing stomach, nourishing qi and blood, relax bowel, Yin-nourishing and body fluid promoting, clearing heat and moistening lung, lower gas help digestion, effect of eliminating phlegm moistening lung, removing toxic substances, and lung is had to the effect of moistening preferably;
Table 1 is below that the effective ingredient of moistening lung oil tea honey of the present invention detects data:
The effective ingredient of table 1 moistening lung oil tea of the present invention honey detects table (100 grams of content)
The traditional Chinese medical science is thought: the main the whole body flesh of lung table, the heresy of chill is the most easily violated lung, brings out or increases the weight of the respiratory diseases such as diseases caused by external factors, cough, asthma, or becoming the seed of trouble of other system disease.Therefore attention Changes in weather, increases and decreases clothes in time, suitably nourish, strengthen Abwehrkraft des Koepers, the outer evil impariment of the lung such as preventing common cold, avoids feeling stomach, is to want first of lungs health.It is first that lung is supported in autumn health care, lung happiness moisten and dislike dry, the dryness evil impariment of the lung.Autumn is dry, and air humidity is little, and especially, after the mid-autumn, wind is large, and people often have dry skin, dry nasal cavity dryness, swallow the diseases such as cough, constipation of itching, due to the dryness evil impariment of the lung.
Moistening lung oil tea honey of the present invention, once carried out therapeutic test to the cough causing because of the dryness evil impariment of the lung:
(1), definite principle of cough patient
(1), the age is between 40-60 year;
(2), life style is close with family's condition;
(3), fitness and health are close;
(4), all there is dry nasal cavity dryness, swallow the diseases such as cough, constipation of itching.
(2), physical data
According to mentioned above principle, determine cough patient 50 people, wherein: male 30 people, female 20 people, disease time 3-7 days.
(3), test method
At duration of test, take moistening lung oil tea honey of the present invention (technical scheme three) every day three times, each serving with 5.0 grams, within five days, be a course for the treatment of, observe the curative effect after three courses for the treatment of; Fasting maror and drinks etc. during this time.
(4), criterion
(1), recovery from illness: dry nasal cavity dryness, the pharynx symptoms such as cough, constipation of itching disappear completely;
(2), effective: dry nasal cavity dryness, the pharynx symptoms such as cough, constipation of itching make moderate progress;
(3), invalid: dry nasal cavity dryness, the pharynx symptoms such as cough, constipation of itching are not improved.
(5), result of the test
Through the test of three courses for the treatment of, according to statistics, this group case is treated cough patient 50 examples altogether, wherein: cure 38 examples, effective 6 examples, invalid 6 examples, total effective rate 88.0%.
Therefore, moistening lung oil tea honey of the present invention, has good result for the treatment of to the cough causing because of the dryness evil impariment of the lung, thereby, lung is had to the effect of moistening preferably.
The specific embodiment
Below in conjunction with embodiment, the present invention is further illustrated.Explanation is below the mode exemplifying, but protection scope of the present invention is not limited to this.
Embodiment mono-:
The preparation method of the moistening lung oil tea honey of the present embodiment is as follows:
A, get the raw materials ready: get respectively by weight 20 parts of tea seeds, 10 parts of peanuts, 3 parts of dry apple grunts, 20 parts of pure tea oil, white fungus (clean through clear water by this white fungus, add again 60 ℃ of emerge in worm water 45min of same weight, elimination moisture, then put into constant pressure and dry case and be dried to moisture and be less than 20% white fungus forming; Also can directly select clean white fungus or adopt conventional cleaning method to clean and dry white fungus) 10 parts, 3 parts of grape berries, 20 parts of honey, 5 parts, lotus seeds and 1 part of extra dry white wine radish, 5 parts of Bulbus Fritillariae Cirrhosaes, 3 parts of adenophora tetraphyllas, for subsequent use;
B, lotus seeds pretreatment:
A, by lotus seeds fragmentation for subsequent use, isolate embryo nelumbinis and Semen Nelumbinis, for subsequent use;
B, embryo nelumbinis for subsequent use is placed in to container, adds the yellow rice wine that 1.5 times of weight, weight concentration are 30%, soak 10min, filter; Again the embryo nelumbinis after filtering is washed 3 times with clear water again, obtain processing embryo nelumbinis, for subsequent use;
C, squeezing: tea seed for subsequent use, white fungus, peanut, processing embryo nelumbinis, Semen Nelumbinis are mixed, at 3 ℃, through low temperature cold squeezing, obtain the coarse tea oil after squeezing, for subsequent use;
D, alkali treatment: in coarse tea oil for subsequent use, add the aqueous alkali that equivalent weight, concentration are 0.8%, water temperature is controlled at 40 ℃, stir, and filters, and 3 times repeatedly, obtains alkali treatment coarse tea oil; This example aqueous alkali used is sodium carbonate: the mixed base aqueous solution of sodium acetate=2:1, also can adopt single sodium carbonate or the aqueous solution of sodium acetate;
E, initial filter: alkali treatment coarse tea oil for subsequent use is crossed to mixed column (this example adopts by D301 resin: the mixed column that alkaline polyamide=1.5:1 forms), and coutroi velocity is 20L/h; Then,, after mixing decolorizing column (this example adopts by slant acidity aluminium oxide: the ratio of slant acidity diatomite=1:0.6 forms), coutroi velocity is 16L/h, obtains filtration coarse tea oil;
F, press filtration: filtration coarse tea oil for subsequent use, under 1.5MPa pressure, is filtered through plate and frame pressurization oil filter (its model is STLY-50), obtain the tea oil I after press filtration, for subsequent use;
G, extraction: pure tea oil for subsequent use is dropped in vapor tight tank, heat to 65 ℃, then grape berry for subsequent use, dry apple grunt, extra dry white wine radish are dropped into, be heated to 125 ℃ according to the firing rate of 10 ℃/min, then be incubated 34min, filter, obtain filtration tea oil;
H, mistake post: in filtration tea oil for subsequent use, add the aluminium oxide that accounts for its weight 7.5%, stir at normal temperatures 50min, filter, after D201 macroporous resin column, coutroi velocity 14L/h, obtained the tea oil II after post, for subsequent use; This example aluminium oxide used is after using alcohol, hot water treatment, is dried to the aluminium oxide that moisture is less than 2.0% again, also can adopt the common aluminium oxide of food-grade; This example D201 macroreticular resin used is the resin after highly basic, ethanol, hot water treatment, also can adopt common D201 macroreticular resin;
I, adenophora tetraphylla pretreatment:
A, adenophora tetraphylla for subsequent use is cut into sheet, is placed in container, add the mature vinegar that accounts for adenophora tetraphylla weight 45%, soak 25min at 5 ℃ of lower seals, filter, dry, must process adenophora tetraphylla, for subsequent use;
B, processing adenophora tetraphylla for subsequent use is placed in to container, first adds the ethanol that 3.5 times of weight, volumetric concentration are 75%, soak 6 hours at 44 ℃, then carry out diacolation, controlling diacolation flow velocity is 10L/h, collects adenophora tetraphylla diacolation ethanol, for subsequent use;
C, be 2.5% sodium-chloride water solution to adding weight concentration in adenophora tetraphylla diacolation ethanol for subsequent use, regulate concentration of alcohol to 45%, after sephadex column (its model is LH-30), in controls, column flow rate is 15L/h, and collection upper prop liquid is for subsequent use;
D, by upper prop liquid for subsequent use, 70 ℃ of Vacuum Concentrations (its model is WZII-1500), vacuum is 0.4MPa, is concentrated into without alcohol, obtains adenophora tetraphylla concentrate, for subsequent use;
J, Bulbus Fritillariae Cirrhosae pretreatment:
A, Bulbus Fritillariae Cirrhosae for subsequent use is placed in to container, add 5 times of weight, by low polar organic solvent (this example adopts the low polar organic solvent being made up of ethyl acetate: benzinum=1:0.4): the mixed solvent of water=3:1 extracts, extracting temperature is 75 ℃, and the time is 1.5 hours, filters; In recrement, add the mixed solvent of same equimultiple to extract again, the time is 1.2 hours, filters, and merges twice filtrate, is down to after normal temperature, and just extract is for subsequent use to obtain Bulbus Fritillariae Cirrhosae;
B, by Bulbus Fritillariae Cirrhosae for subsequent use just extract drop in separator (its model is S-1500), carry out the separation of liquid liquid, collect rudimentary property organic solvent fluid, for subsequent use;
C, by rudimentary property organic solvent fluid for subsequent use 65 ℃ concentrated (its model is WZII-1500), be concentrated into without rudimentary property organic solvent, obtain Bulbus Fritillariae Cirrhosae concentrate, for subsequent use;
D, Bulbus Fritillariae Cirrhosae concentrate for subsequent use is sprayed dry, obtain dry powder, for subsequent use;
E, by dry powder for subsequent use, add the clear water of equivalent weight, stir, add the edible sucrose ester that accounts for dry powder weight 0.3% as surfactant simultaneously, limit edged stirs, and to dissolving completely, till liquid clarification, obtains Bulbus Fritillariae Cirrhosae solution, for subsequent use;
K, mixing: tea oil I for subsequent use, tea oil II, honey, adenophora tetraphylla concentrate, Bulbus Fritillariae Cirrhosae solution are mixed, under 2.0MPa pressure, filter through filter (this example adopts the hydraulic pressure one filter press that model is 800), then under same pressure, through microfiltration membranes device, (its model is UF-18m again
3/ h, membrane aperture is 12-20nm) filter, collect the liquid after filtering, obtain moistening lung oil tea honey.
Embodiment bis-:
The preparation method of the moistening lung oil tea honey of the present embodiment is as follows:
A, get the raw materials ready: get respectively by weight 30 parts of tea seeds, 5 parts of peanuts, 5 parts of dry apple grunts, 10 parts of pure tea oil, white fungus (clean through clear water by this white fungus, add again 40-100 ℃ of emerge in worm water 30-80min of same weight, elimination moisture, then put into constant pressure and dry case and be dried to moisture and be less than 20% white fungus forming; Also can directly select clean white fungus or adopt conventional cleaning method to clean and dry white fungus) 5 parts, 6 parts of grape berries, 10 parts of honey, 10 parts, lotus seeds and 3 parts of extra dry white wine radish, 10 parts of Bulbus Fritillariae Cirrhosaes, 6 parts of adenophora tetraphyllas, for subsequent use;
Other step is identical with embodiment mono-, repeats no more.
Embodiment tri-:
The preparation method of the moistening lung oil tea honey of the present embodiment is as follows:
A, get the raw materials ready: get respectively by weight 25 parts of tea seeds, 8 parts of peanuts, 4 parts of dry apple grunts, 15 parts of pure tea oil, white fungus (clean through clear water by this white fungus, add again 40-100 ℃ of emerge in worm water 30-80min of same weight, elimination moisture, then put into constant pressure and dry case and be dried to moisture and be less than 20% white fungus forming; Also can directly select clean white fungus or adopt conventional cleaning method to clean and dry white fungus) 7 parts, 4 parts of grape berries, 15 parts of honey, 8 parts, lotus seeds and 2 parts of extra dry white wine radish, 8 parts of Bulbus Fritillariae Cirrhosaes, 4 parts of adenophora tetraphyllas, for subsequent use;
Other step is identical with embodiment mono-, repeats no more.
Moistening lung oil tea honey of the present invention, both can be used for treatment because of the cough that the dryness evil impariment of the lung causes, also can be used for moistening lung and supported lung, avoided the dryness evil impariment of the lung; The men and women who is applicable to each ages takes.
Claims (7)
1. a moistening lung oil tea honey, it is characterized in that being prepared from by following raw material by weight:
The dry apple grunt 3-5 of tea seed 20-30 peanut 5-10
Pure tea oil 10-20 white fungus 5-10 grape berry 3-6
Bulbus Fritillariae Cirrhosae 5-10 lotus seeds 5-10 extra dry white wine radish 1-3
Adenophora tetraphylla 3-6 honey 10-20;
Its preparation method is as follows:
A, get the raw materials ready: get respectively tea seed, peanut, dry apple grunt, pure tea oil, white fungus, grape berry, Bulbus Fritillariae Cirrhosae, lotus seeds, extra dry white wine radish, adenophora tetraphylla, honey by above-mentioned weight portion, backup;
B, lotus seeds pretreatment:
A, by lotus seeds fragmentation for subsequent use, isolate embryo nelumbinis and Semen Nelumbinis, for subsequent use;
B, embryo nelumbinis for subsequent use is placed in to container, adds the yellow rice wine that 1-2 times of weight, weight concentration are 25-40%, soak 10-25min, filter; Again the embryo nelumbinis after filtering is washed 1-4 time with clear water again, obtain processing embryo nelumbinis, for subsequent use;
C, squeezing: tea seed for subsequent use, white fungus, peanut, processing embryo nelumbinis, Semen Nelumbinis are mixed, at 0-6 ℃, through low temperature cold squeezing, obtain the coarse tea oil after squeezing, for subsequent use;
D, alkali treatment: in coarse tea oil for subsequent use, add the aqueous alkali that equivalent weight, concentration are 0.1-1.2%, water temperature is controlled at 30-60 ℃, stir, and filters, and 3 times repeatedly, obtains alkali treatment coarse tea oil; Described aqueous alkali is sodium carbonate: the mixed base aqueous solution of sodium acetate=2:1;
E, initial filter: alkali treatment coarse tea oil for subsequent use is crossed to mixed column, and coutroi velocity is 10-50L/h; Then,, after mixing decolorizing column, coutroi velocity is 5-30L/h, obtains filtration coarse tea oil;
F, press filtration: filtration coarse tea oil for subsequent use, under 0.2-1.5MPa pressure, is filtered, obtains the tea oil I after press filtration, for subsequent use;
G, extraction: pure tea oil for subsequent use is dropped in vapor tight tank, heat to 40-75 ℃, then grape berry for subsequent use, dry apple grunt, extra dry white wine radish are dropped into, firing rate according to 5-10 ℃/min is heated to 100-150 ℃, be incubated again 10-50min, filter, obtain filtration tea oil;
H, mistake post: in filtration tea oil for subsequent use, add the aluminium oxide that accounts for its weight 5-14%, stir at normal temperatures 40-120min, filter, after D201 macroporous resin column, coutroi velocity 10-20L/h, obtained the tea oil II after post, for subsequent use;
I, adenophora tetraphylla pretreatment:
A, adenophora tetraphylla for subsequent use is cut into sheet, is placed in container, add the mature vinegar that accounts for adenophora tetraphylla weight 30-60%, soak 25-40min at 1-10 ℃ of lower seal, filter, dry, must process adenophora tetraphylla, for subsequent use;
B, processing adenophora tetraphylla for subsequent use is placed in to container, first adds the ethanol that 2-5 times of weight, volumetric concentration are 60-95%, at 30-60 ℃, soak 5-10 hour, then carry out diacolation, controlling diacolation flow velocity is 10-20L/h, collects adenophora tetraphylla diacolation ethanol, for subsequent use;
C, be the sodium-chloride water solution of 1-6% to adding weight concentration in adenophora tetraphylla diacolation ethanol for subsequent use, regulate concentration of alcohol to 45-65%, after sephadex column, in controls, column flow rate is 10-15L/h, and collection upper prop liquid is for subsequent use;
D, by upper prop liquid for subsequent use, at 45-70 ℃ of Vacuum Concentration, vacuum is 0.2-0.4MPa, is concentrated into without alcohol, obtains adenophora tetraphylla concentrate, for subsequent use;
J, Bulbus Fritillariae Cirrhosae pretreatment:
A, Bulbus Fritillariae Cirrhosae for subsequent use is placed in to container, adds 2-6 times of weight, extracted by the mixed solvent of low polar organic solvent: water=2-5:1, extracting temperature is 60-90 ℃, and the time is 1.5-2.0 hour, filters; In recrement, add the mixed solvent of same equimultiple to extract again, the time is 0.5-1.2 hour, filters, and merges twice filtrate, is down to after normal temperature, obtains just extract of Bulbus Fritillariae Cirrhosae, for subsequent use;
B, by Bulbus Fritillariae Cirrhosae for subsequent use just extract drop in knockout drum, carry out the separation of liquid liquid, collect low polar organic solvent liquid, for subsequent use;
C, by low polar organic solvent liquid for subsequent use 40-65 ℃ concentrated, be concentrated into without rudimentary property organic solvent, obtain Bulbus Fritillariae Cirrhosae concentrate, for subsequent use;
D, Bulbus Fritillariae Cirrhosae concentrate for subsequent use is sprayed dry, obtain dry powder, for subsequent use;
E, by dry powder for subsequent use, add the clear water of equivalent weight, stir, add the surfactant of the food-grade that accounts for dry powder weight 0.3-1.4% simultaneously, limit edged stirs, and to dissolving completely, till liquid clarification, obtains Bulbus Fritillariae Cirrhosae solution, for subsequent use;
K, mixing: tea oil I for subsequent use, tea oil II, honey, adenophora tetraphylla concentrate, Bulbus Fritillariae Cirrhosae solution are mixed, under 0.5-2.0MPa pressure, be filtered, then under same pressure, filter through microfiltration membranes device again, collect the liquid after filtering, obtain moistening lung oil tea honey.
2. moistening lung oil tea honey according to claim 1, it is characterized in that: described white fungus is to clean through clear water, add again 40-100 ℃ of emerge in worm water 30-80min of same weight, elimination moisture, then put into constant pressure and dry case and be dried to the white fungus raw material that moisture is less than 20%.
3. according to moistening lung oil tea honey described in claim 1 or 2, it is characterized in that: described aluminium oxide is after using alcohol, hot water treatment, then is dried to the aluminium oxide that moisture is less than 2.0%.
4. moistening lung oil tea honey according to claim 3, is characterized in that: described D201 macroreticular resin is the resin after highly basic, ethanol, hot water treatment.
5. moistening lung oil tea honey according to claim 4, it is characterized in that being prepared from by following raw material by weight:
The dry apple grunt 3 of tea seed 20 peanut 10
Pure tea oil 20 white fungus 10 grape berries 3
Bulbus Fritillariae Cirrhosae 5 lotus seeds 5 extra dry white wine radish 1
Adenophora tetraphylla 3 honey 20.
6. moistening lung oil tea honey according to claim 4, it is characterized in that being prepared from by following raw material by weight:
The dry apple grunt 5 of tea seed 30 peanut 5
Pure tea oil 10 white fungus 5 grape berries 6
Bulbus Fritillariae Cirrhosae 10 lotus seeds 10 extra dry white wine radish 3
Adenophora tetraphylla 6 honey 10.
7. moistening lung oil tea honey according to claim 4, it is characterized in that being prepared from by following raw material by weight:
The dry apple grunt 4 of tea seed 25 peanut 8
Pure tea oil 15 white fungus 7 grape berries 4
Bulbus Fritillariae Cirrhosae 8 lotus seeds 8 extra dry white wine radish 2
Adenophora tetraphylla 4 honey 15.
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CN101843307A (en) * | 2010-06-07 | 2010-09-29 | 杭州天厨蜜源保健品有限公司 | American ginseng-royal jelly soft capsules and preparation method thereof |
CN102987193A (en) * | 2012-08-15 | 2013-03-27 | 明光市昊昊蜂业有限公司 | Preparation method of Indian rorippa herb honey cough-relieving health-care extract and health-care extract prepared by same |
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