CN106166232A - A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea and preparation processing method - Google Patents
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea and preparation processing method Download PDFInfo
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- A61K36/185—Magnoliopsida (dicotyledons)
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- A23F3/00—Tea; Tea substitutes; Preparations thereof
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Abstract
The invention discloses a kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea of the present invention, be made up of the raw material of following weight portion: Radix Angelicae Sinensis 5 15 parts, 5 15 parts of Radix Rehmanniae Preparata, the Cortex Eucommiae 5 12 parts, Cortex Cinnamomi 39 parts, Rhizoma Cimicifugae 5 12 parts, Herba Cistanches 5 10 parts, the Radix Paeoniae Alba 10 16 parts, RADIX PLATYCODI 5 15 parts, Lignum Aquilariae Resinatum 6 15 parts, Radix Codonopsis 5 10 parts, the Rhizoma Atractylodis Macrocephalae 5 10 parts, the Radix Astragali 5 10 parts, Pericarpium Citri Reticulatae 5 10 parts, 5 10 parts of Radix Glycyrrhizae, Rhizoma Corydalis 5 10 parts.The invention have the advantage that inventive formulation the kidney warming yang invigorating, adjust stomach invigorating the spleen and replenishing QI, treat chronic gastritis, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, the merit of resisting fatigue.
Description
Technical field
The present invention relates to a kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, in particular, relate to a kind of the kidney warming liter
Sun treatment prolapse of gastric mucosa herb tea formula and preparation method thereof technical field.
Background technology
Prolapse of gastric mucosa is to take off into 12 owing to the gastric mucosa of abnormal relaxation drives in the wrong direction for charging into esophagus or be advanced through pyloric canal
Duodenum 12 bulb, common with the latter clinically.Clinical symptoms is presented with stomachache, upper gastrointestinal hemorrhage, Nausea and vomiting, becomes thin, slightly
Anemia, epigastrium can have light tenderness, without rebound tenderness.Primary disease can be divided into primary and secondary two kinds, and the former sticks with the stomach of high activity
Film pleat is relevant with congenital gastric folds hypertrophy；The latter is secondary to gastritis, peptic ulcer and heart failure, hypoproteinemia more
Edema under the mucosa that disease causes.Primary disease is common in the adult of 30～60 years old, and male's sickness rate is higher, shows as flatulence pain, spleen
Insufficiency of kidney-YANG, gastric qi do not conform to, inappetence, feed relax etc. symptom
The most traditional beverage, only focuses on mouthfeel, is of low nutritive value, and does not have the kidney warming yang invigorating, adjusts stomach invigorating the spleen and replenishing QI, treats chronic
Gastritis, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, drop three-hypers, prevent and treat diabetes and anti-cancer, the side such as anticancer
The function in face, it is impossible to releasing the sufferings of client, and traditional herbal tea is by Traditional medicine infusion, flavour of a drug weight mouthfeel is poor, it is impossible to protect for a long time
Deposit.The most not yet occur a kind of in good taste, improve self and increase the wriggling of the intestines and stomach, cure the disease and strengthen body immunity simultaneously
Beverage.
Summary of the invention
The present invention is directed to the deficiency of existing product, and provide a kind of fresh juice beverage to regulate the effect of human physiological functions,
This beverage have be easily absorbed by the human body, medicinal function is notable, delicious flavour, good mouthfeel, improve self and increase the wriggling of the intestines and stomach,
Cure the disease and strengthen a kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea of the advantages such as body immunity simultaneously.
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, is made up of the raw material of following weight portion: Radix Angelicae Sinensis 5-15 part, Radix Rehmanniae Preparata
5-15 part, Cortex Eucommiae 5-12 part, Cortex Cinnamomi 3-9 part, Rhizoma Cimicifugae 5-12 part, Herba Cistanches 5-10 part, Radix Paeoniae Alba 10-16 part, RADIX PLATYCODI 5-15 part,
Lignum Aquilariae Resinatum 6-15 part, Radix Codonopsis 5-10 part, Rhizoma Atractylodis Macrocephalae 5-10 part, Radix Astragali 5-10 part, Pericarpium Citri Reticulatae 5-10 part, Radix Glycyrrhizae 5-10 part, Rhizoma Corydalis 5-10 part,
Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate.
The preparation processing method of described a kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, comprises the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, then take
Go out to put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time
The Chinese liquor of 52-60 DEG C, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, add the fresh bar of Herba Dendrobii
The distilled water of weight 2-3 times, for the second time juice extractor time 10-15min, juice extractor rotating speed is 80～100r/s, stands 10min；
After carry out third time squeeze the juice, add Herba Dendrobii fresh bar weight 3-5 times distilled water, time 20-30min, juice extractor rotating speed be 100～
150r/s, separates fresh for Herba Dendrobii bar juice with fiber filter, makes the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, cell damage
Rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；The warm water that new fresh grape is put into 50-60 DEG C again cleans dry
After Jing, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 in tank
Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh
Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, at 30-35
Seal at a temperature of DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；After extracting Matrix Solution
It is the cellulase of 0.5-0.7% that Pericarpium Vitis viniferae and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10,
Keep 35 DEG C, water soluble dietary fiber can be extracted further after 24h enzymolysis, water soluble dietary fiber is added Matrix Solution
Obtain Matrix Solution II；
E, take mix homogeneously after Radix Angelicae Sinensis, Radix Rehmanniae Preparata, Cortex Eucommiae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times,
Each 2 hours, merge 2 Radix Angelicae Sinensis, Radix Rehmanniae Preparata, Cortex Eucommiae ethanol extracts, receive alcohol and be evaporated to relative density at 40 DEG C and be
1.15-1.35, prepare Radix Angelicae Sinensis, Radix Rehmanniae Preparata, the Cortex Eucommiae extract standby；
Rhizoma Cimicifugae, Herba Cistanches mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing of 300-400 mesh carefully
Powder；
Taking Cortex Cinnamomi, the Radix Paeoniae Alba, RADIX PLATYCODI, Lignum Aquilariae Resinatum, Radix Codonopsis, the Rhizoma Atractylodis Macrocephalae, the Radix Astragali, Pericarpium Citri Reticulatae, Radix Glycyrrhizae, Rhizoma Corydalis, Air Bladder pseudosciaenae seu Acipenser, mix homogeneously adds 30-
60 DEG C of warm water soaking, after 10 minutes, put into reach in freezer ,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, by cold
Freezing medicine block and ultra micro mixing fine powders boiling is extracted 3 times, add 1-2 times amount water for the first time, temperature keeps 100-120 DEG C, carries out
Infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10
Times amount water, temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, is concentrated into the 1/2 of original volume, adds Radix Angelicae Sinensis, ripe
Ground, the extract of the Cortex Eucommiae, obtain Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh
Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh
In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is:
Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial,
Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
Further: step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute,
Make Fructus Vitis viniferae freeze, after taking out nature defrosting, then carry out Fructus Vitis viniferae meat and Pericarpium Vitis viniferae detached job.
Further: step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, Oleum Vitis viniferae
Weight proportion be 10:0.2～0.8:5～10:0.5.
Radix Angelicae Sinensis, sweet, pungent, warm, return liver, the heart, spleen channel, enrich blood；Invigorate blood circulation；Menstruction regulating and pain relieving；Moisturize laxation.
Radix Rehmanniae Preparata, sweet, tepor.Returning liver, kidney channel, yin nourishing of enriching blood, life essence-filling, marrow-benefitting, sweet Wen Zhirun, nourishing YIN benefit essence is with hemopoietic.
The Cortex Eucommiae, invigorating the liver and kidney, bone and muscle strengthening.
Cortex Cinnamomi, complement sun, warming the spleen and stomach, removing accumulated cold, promoting blood circulation.
Rhizoma Cimicifugae, pungent and cold medicine for relieving the exterior syndrome.Meridian distribution of property and flavor: sweet, pungent, be slightly cold.Return spleen, stomach, lung, large intestine channel.For delivering rash,
Heat-clearing and toxic substances removing, rises and lifts yang-energy.
Herba Cistanches, for impotence due to deficiency of the kidney, seminal emission premature ejaculation and chills and pain of the waist and kness, muscles and bones convulsion is weak.
The Radix Paeoniae Alba, suppressing the hyperactive liver pain relieving, nourishing blood for regulating menstruation, astringing YIN to stop sweating.For dizziness of having a headache, hypochondriac pain, stomachache, limb pain twin.
RADIX PLATYCODI, lung qi dispersing, sore-throat relieving, eliminate the phlegm, evacuation of pus.For cough with copious phlegm, uncomfortable in chest not smooth, pharyngalgia, hoarseness.
Lignum Aquilariae Resinatum, acrid in the mouth, hardship, warm in nature；Return spleen, stomach, kidney channel;Gas perfume (or spice) row dissipates, and drops and can rise；There is circulation of qi promoting warming middle-JIAO to send down the adverse QI, warm
Effect of kidney helping inspiration to relieve asthma.
Radix Codonopsis, sweet, flat.Invigorating the spleen and replenishing QI, stomach function regulating promotes the production of body fluid, expelling phlegm for arresting cough, for weakness of the spleen and stomach, deficiency of both QI and blood, fatigue and lack of strength,
Lack of appetite, thirsty.
The Rhizoma Atractylodis Macrocephalae, bitter in the mouth, sweet, warm in nature;Return spleen, stomach warp;Fragrance matter is soft, can rise and can drop, keep and do not walk to have invigorating the spleen and benefiting QI,
Dampness diuretic, strengthening superficial resistance to stop perspiration.
The Radix Astragali, returns lung, spleen, liver, kidney channel.Enhancing human body immunity function, protect the liver, diuresis, defying age, anti-stress, blood pressure lowering and
Wide antibacterial action.
Pericarpium Citri Reticulatae, bitter in the mouth, pungent, warm in nature.Return lung, spleen channel.Regulating qi-flowing for strengthening spleen, drying dampness to eliminate phlegm.
Radix Glycyrrhizae, and middle emergency, lung moistening, removing toxic substances, coordinating the actions of various ingredients in a prescription.
Rhizoma Corydalis, warm in nature, acrid in the mouth is bitter, enters the heart, spleen, liver, lung, is blood circulation promoting and blood stasis dispelling, promoting the circulation of QI to relieve pain.
Fructus Vitis viniferae is the most delicious and tasty, and nutritive value is the highest, containing mineral calcium, potassium, phosphorus, ferrum and multiple in Fructus Vitis viniferae
Vitamin B1, vitamin B2, vitamin B6, vitamin C and Citrin etc., possibly together with the aminoacid of multiple needed by human body, multiple
Fruit acid contributes to digestion, suitably eats a little Fructus Vitis viniferae more, can be good for Pi stomach function regulating, and to neurasthenia, overfatigue is of great advantage and has.
The natural tradition medicinal and edible Chinese medicine above with multiple health care is share, the kidney warming yang invigorating, tune stomach invigorating middle warmer benefit
Gas, treats chronic gastritis, improves body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, the merit of resisting fatigue.By a large amount of real
Test the proportioning screening each component, scientific and reasonable；And whole preparation technology is rationally and extract drugs rate efficiency is high, can protect well
Stay the effective ingredient in raw material, do not bring any impurity, and sweet mouthfeel into, have no side effect.
The invention has the beneficial effects as follows:
1, the formula of the present invention, has promoting the production of body fluid to quench thirst, gastric acid secretion, helps digest, and health body-building has calm nerves and declines
Weak, lessen fatigue, containing various trace elements such as calcium, ferrum, zinc, selenium, sodium etc., raising body immunity, defying age, toxin expelling are supported
Face, nourish taste, three-hypers drops, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful, regulates human physiological functions.
2, the present invention is rich in anthocyanidin, it is possible to protection human body is from the damage of free radical, it is possible to strengthens blood vessel elasticity, relax
Blood vessel, increases systemic blood circulation, has certain blood pressure reduction effect；Immune system ability can be strengthened, there is strong anti-oxidation, resist
Suddenly change, alleviate the function such as hepatosis, protection cardiovascular；
3, add the Chinese herbal medicine such as Cortex Cinnamomi, the Radix Paeoniae Alba, RADIX PLATYCODI, Lignum Aquilariae Resinatum, Radix Codonopsis, the Rhizoma Atractylodis Macrocephalae, the Radix Astragali, Pericarpium Citri Reticulatae, Radix Glycyrrhizae, Rhizoma Corydalis and there is the kidney warming
Yang invigorating, tune stomach invigorating the spleen and replenishing QI, treat chronic gastritis, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, resisting fatigue
Etc. function.
4, the products taste that the production technology of the present invention and preparation method draw is sour-sweet tasty and refreshing, rich in dendrobium polysaccharide, has
The highest health care and medical value, long-term drink can with YIN nourishing skin care, change skin colour, defying age, life lengthening, and
Carrying and drink conveniently, improve self and increase the wriggling of the intestines and stomach, cure the disease and strengthen the beverage of body immunity simultaneously, the shelf-life is up to 1-
2 years.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, in order to those skilled in the art knows more about
The present invention, but and it is not so limited the present invention.
Embodiment 1
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, is made up of the raw material of following weight portion: Radix Angelicae Sinensis 10 parts, 10 parts of Radix Rehmanniae Preparata,
The Cortex Eucommiae 10 parts, Cortex Cinnamomi 8 parts, Rhizoma Cimicifugae 10 parts, Herba Cistanches 8 parts, the Radix Paeoniae Alba 12 parts, RADIX PLATYCODI 12 parts, Lignum Aquilariae Resinatum 10 parts, Radix Codonopsis 8 parts, the Rhizoma Atractylodis Macrocephalae
8 parts, the Radix Astragali 8 parts, Pericarpium Citri Reticulatae 8 parts, 8 parts of Radix Glycyrrhizae, Rhizoma Corydalis 8 parts, 8 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, Mel, water fit
Amount.
The preparation processing method of a kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, described preparation method includes following step
Suddenly；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
Fresh for the Herba Dendrobii cleaned up bar is put into microwave oven by B, keeps temperature 50-60 DEG C, carries out heating 10 minutes, further take out
Put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content 52 of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time
DEG C Chinese liquor, time 15min, the rotating speed of juice extractor is 30r/s；After standing 10 minutes, add the steaming of Herba Dendrobii fresh bar weight 2.5 times
Distilled water, for the second time juice extractor time 15min, juice extractor rotating speed is 80r/s, stands 10min；After carry out third time squeeze the juice, add
The distilled water of Herba Dendrobii fresh bar weight 3-5 times, time 30min, juice extractor rotating speed is 150r/s, by fresh for Herba Dendrobii bar juice and fiber mistake
Filter separate, make the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, broken cell rate reaches more than 80%, obtain new fresh Herba Dendrobii juice and
Herba Dendrobii fresh bar fiber；Again new fresh grape is put into after the warm water of 55 DEG C cleans up, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated
Stand-by；After new fresh grape cleans up, put into reach in freezer ,-10 ~-20 DEG C of freezings 10 minutes, make Fructus Vitis viniferae freeze, take out certainly
After so thawing, then carry out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 120 in tank
Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh
Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 6 times of weight, stirring is smashed to 100 mesh, 30-35 DEG C of temperature
Degree lower seal preserves 24h, sterilizing, filters, puts into unglazed hermetically sealed can, obtain Matrix Solution standby；Extract the Fructus Vitis viniferae after Matrix Solution
It is the cellulase of 0.5-0.7% that skin and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10, keeps
35 DEG C, water soluble dietary fiber can be extracted after 24h enzymolysis further, water soluble dietary fiber is added Matrix Solution and obtains
Matrix Solution II；Rich in anthocyanidin in Pericarpium Vitis viniferae, it is possible to protection human body is from the damage of free radical, it is possible to enhancing blood vessel elasticity,
Lax blood vessel, increases systemic blood circulation, has certain blood pressure reduction effect；Immune system ability can be strengthened, there is strong antioxygen
Change, mutation, alleviate hepatosis, protection function, Pericarpium Vitis viniferae and the Herba Dendrobii fresh bar fiber such as cardiovascular together with stir smash through
Anthocyanidin mentioned by hydromel, can protect the quality of anthocyanidin while farthest extracting anthocyanidin.By water solublity meals
Food fiber adds Matrix Solution and obtains Matrix Solution II, can increase effect of the wriggling of the intestines and stomach, it is ensured that metabolic waste is normally discharged
External；Adsorbing various metabolic waste, be allowed to normally excrete, the comprehensive utilization value improving Herba Dendrobii improves human body centering simultaneously
The absorption of medicine composition.
E, take mix homogeneously after Radix Angelicae Sinensis, Radix Rehmanniae Preparata, Cortex Eucommiae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2
Secondary, each 2 hours, merge 2 Radix Angelicae Sinensis, Radix Rehmanniae Preparata, Cortex Eucommiae ethanol extracts, receive alcohol and be evaporated to relative density at 40 DEG C and be
1.15-1.35, prepare Radix Angelicae Sinensis, Radix Rehmanniae Preparata, the Cortex Eucommiae extract standby；
Rhizoma Cimicifugae, Herba Cistanches mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing of 300-400 mesh carefully
Powder；
Taking Cortex Cinnamomi, the Radix Paeoniae Alba, RADIX PLATYCODI, Lignum Aquilariae Resinatum, Radix Codonopsis, the Rhizoma Atractylodis Macrocephalae, the Radix Astragali, Pericarpium Citri Reticulatae, Radix Glycyrrhizae, Rhizoma Corydalis, Air Bladder pseudosciaenae seu Acipenser, mix homogeneously adds 30-
60 DEG C of warm water soaking, after 10 minutes, put into reach in freezer ,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, by cold
Freezing medicine block and ultra micro mixing fine powders boiling is extracted 3 times, add 1-2 times amount water for the first time, temperature keeps 100-120 DEG C, carries out
Infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10
Times amount water, temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, is concentrated into the 1/2 of original volume, adds Radix Angelicae Sinensis, ripe
Ground, the extract of the Cortex Eucommiae, obtain Matrix Solution III standby；
The hard to bear medicine boiled is pulverized and improves its extract drugs efficiency, make whole formula drug effect farthest be utilized.
F, take Matrix Solution I through instantaneous high-temperature 120 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh
Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh
In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is:
Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；Supercritical extraction can be
Extract under room temperature 37 DEG C and CO2 gas blanket, effectively prevent oxidation and the loss of heat-sensitive substance.Therefore,
The effective ingredient of medicinal plants is remain in extract, and can be high boiling point, low volatility, the easy material being pyrolyzed the lowest
Extract under its boiling temperature；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, and described material-compound tank endobasal-body solution I, matrix are molten
Liquid II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae are 10:0.5:6:0.5.Sealing through bottle capper loads in vial,
Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning,
Carrying and drink conveniently, the shelf-life is up to 1-2.
Embodiment 2
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, is made up of the raw material of following weight portion: Radix Angelicae Sinensis 5 parts, 5 parts of Radix Rehmanniae Preparata, Du
Secondary 5 parts, Cortex Cinnamomi 3 parts, Rhizoma Cimicifugae 5 parts, Herba Cistanches 5 parts, the Radix Paeoniae Alba 10 parts, RADIX PLATYCODI 5 parts, Lignum Aquilariae Resinatum 6 parts, Radix Codonopsis 5 parts, the Rhizoma Atractylodis Macrocephalae 5 parts, yellow
Stilbene 5 parts, Pericarpium Citri Reticulatae 5 parts, 5 parts of Radix Glycyrrhizae, Rhizoma Corydalis 5 parts, 5 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are appropriate.Processing
Method is with embodiment 1.
Embodiment 3
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, is made up of the raw material of following weight portion: Radix Angelicae Sinensis 15 parts, 15 parts of Radix Rehmanniae Preparata,
The Cortex Eucommiae 12 parts, Cortex Cinnamomi 9 parts, Rhizoma Cimicifugae 12 parts, Herba Cistanches 10 parts, the Radix Paeoniae Alba 16 parts, RADIX PLATYCODI 15 parts, Lignum Aquilariae Resinatum 15 parts, Radix Codonopsis 10 parts, white
Art 10 parts, the Radix Astragali 10 parts, Pericarpium Citri Reticulatae 10 parts, 10 parts of Radix Glycyrrhizae, Rhizoma Corydalis 10 parts, 10 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20 parts, honeybee
Honey, water are appropriate.Processing method is with embodiment 1.
Clinical experiment divides three parts:
(1) animal acute toxicity and chronic toxicity experiment:
1, animal acute toxicity test
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 medicated tea add the medicated tea powder paste that rice flour is made.
Experimental animal: regular grade NIH mice, body weight 18g ± 2g, male and female half and half.
Method and result:
By three kinds of each 50g of medicated tea, add rice flour.Experiment mice is randomly divided into three groups of male and female half and half, respectively three kinds of medicated tea of feeding
Powder is stuck with paste, volume 1ml/10g body weight, and close observation 8 hours is also noted down, and continues to observe 7 days；In 7 days, mice is without death, OK
For vivaciously, food ration is as usual, and hair color light is without loose dirt, without fainting from fear addicted to saliva, and eye, mouth, nose, ear and crissum secretions without exception,
Without the rotten toe that docks.5 execution of selection from three groups respectively, finding of naked eye: the important organs such as the heart, liver, lung, gastric and thymus, not
See abnormal change, show that two kinds of these nutritive powders are all without acute toxicity.
2, long-term toxicity test for animals
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 gained medicated tea add the medicated tea powder paste that rice flour is made.
Animal: regular grade SD rat, body weight 200g ± 10g, male and female half and half.
Method and result:
The configuration that three kinds of medicated tea powder are stuck with paste: be divided into high, medium and low three dosage groups, respectively the 200 of edible for patients amount, 100,
50g；Experimental mouse is randomly divided into three groups, and the medicated tea powder that feeding modulates continuously respectively is stuck with paste, and continuous feeding 40 days observes animal
General toxic reaction and the order of severity, place after death by rule of operation check each position, and carry out hematology, ALT, BUN and the heart,
The pathological examination of the main organs such as liver, spleen, lung, kidney, stomach；
Through long-term feeding, all there is not toxic reaction in two groups of rats.Growth promoter is good.Macroscopic appearance and main organs have no
Abnormal.Peripheral hemogram and Serum ALT, BUN compare with matched group without pathologic change.The pathological replacement heart, liver, spleen, lung, kidney, stomach
Deng the most significant change, it is understood that through proved by pathology, three kinds of medicated tea powder are stuck with paste and showed animal without chronic toxicity.
By two above toxicity test, it was demonstrated that the medicated tea that the present invention is made by embodiment 1, embodiment 2 and embodiment 3 is
Safety, have no side effect, can be used to clinical patients is carried out clinical trial.
3, the embodiment of the present invention drinks effect research:
(1) investigation method:
1. crowd is drunk: general population
2. Ganderwa: 30 days
3. number is drunk: 50 people
4. drinking method: 3 times for each person every day, ante cibum each 600mL
5. index: the transference cures such as after drinking, substantially flatulence pain, deficiency of spleen-YANG and kidneyYANG, gastric qi do not conform to, inappetence, feed are easypro, and
Mouthfeel is the most sour-sweet for effective；The remission such as drink rear flatulence pain, deficiency of spleen-YANG and kidneyYANG, gastric qi do not conform to, inappetence, feed are not relaxed,
And mouthfeel is the most sour-sweet, it is designated as effectively.It is invalid to be then designated as without obvious comfort after drinking.
(2) survey result
Survey result is shown in Table 1.Be test result indicate that by table 1, embodiment 1,2,3 has the respondent of 98% to feel that the present invention is carried
The beverage mouthfeel of confession is the most sour-sweet, and above-mentioned clinical symptom disappearance or be eased, the respondent of only 2% drink after without substantially
Increase comfort.
The each embodiment of table 1 drinks effect research table
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Embodiment 1 | 44%(22) | 54%(27) | 2%(1) |
| Embodiment 2 | 42%(21) | 56%(28) | 2%(1) |
| Embodiment 3 | 42%(21) | 56%(28) | 2%(1) |
Embodiment contrast groups A
Comparative example 4,5,6 is added without the nutrition such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae and becomes
Point, according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing is traditional side of boiling
Method；The investigation method of using method and using effect is with above.
Table 2 embodiment contrast groups A drinks effect research
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 4 | 36%(18) | 40%(20) | 24%(12) |
| Comparative example 5 | 40%(20) | 40%(20) | 20%(10) |
| Comparative example 6 | 46%(23) | 34%(17) | 20%(10) |
Embodiment contrast groups B
Comparative example 7,8,9 is added without the nutrition such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae and becomes
Point, according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing uses in embodiment 1
The preparation processing method of step E；The investigation method of using method and using effect is with above.
Table 3 embodiment contrast groups B drinks effect research
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 7 | 32%(16) | 56%(28) | 12%(6) |
| Comparative example 8 | 28%(14) | 52%(31) | 10%(5) |
| Comparative example 9 | 36%(18) | 52%(26) | 12%(6) |
Embodiment contrast groups C
The processing method of comparative example 10,11,12 respectively corresponding embodiment 1,2,3 and formula, different be formula in
Without Air Bladder pseudosciaenae seu Acipenser composition；The investigation method of using method and using effect is with above.
Table 4 embodiment contrast groups C drinks effect research
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 10 | 44%(22) | 46%(23) | 10%(5) |
| Comparative example 11 | 38%(19) | 50%(25) | 12%(6) |
| Comparative example 12 | 40%(20) | 48%(24) | 12%(6) |
Conclusion:
Contrasted by table 2 and table 1 and can be seen that
The inefficient number of embodiment contrast groups A is about 10 times of embodiment 1,2,3；This shows Chinese crude drug formula of the present invention
And between the nutritional labeling such as water soluble dietary fiber and Oleum Vitis viniferae, creating the most collaborative pharmacological action, aqueous soluble dietary is fine
Dimension increases effect of the wriggling of the intestines and stomach and promotes the human body absorption to ingredient, it is ensured that metabolic waste normally excretes, additionally
The anthocyanidin that contains in Pericarpium Vitis viniferae, resveratrol, have strong anti-oxidation, mutation, alleviate hepatosis, protection cardiovascular etc.
Function, strengthens immune system ability；Associate with Chinese medicine and improve assimilation effect and improve the mouthfeel of Chinese medicine, through the essence of the present invention simultaneously
The extraction of heart configuration and at utmost ingredient, Chinese crude drug formula of the present invention and preparation method occur in that beat all technology
Effect.
Table 2 and table 3 contrast can be seen that
About inefficient number is embodiment contrast groups B 2 times of embodiment contrast groups A, embodiment contrast groups B and traditional
Embodiment contrast groups A of boiling method has compared significant raising at therapeutic effect, and this shows that Chinese crude drug of the present invention is through step
The preparation processing method of rapid E has had significant raising than traditional boiling method, the extraction degree of active ingredient.
Table 1 is compared with table 4:
The formula of embodiment contrast groups C does not contains Air Bladder pseudosciaenae seu Acipenser, and the invalid number of embodiment contrast groups C is 5 times of left sides of embodiment 1,2,3
Right；And effective percentage number has and has declined；Show Air Bladder pseudosciaenae seu Acipenser serve in formula collaborative and priming return through effect, Air Bladder pseudosciaenae seu Acipenser should
Unexpected technique effect is achieved by effect.
In sum, a kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea that the present invention provides, warming spleen and stomach for dispelling cold, only regulate the flow of vital energy
Bitterly, treat chronic gastritis, there is sour-sweet mouthfeel, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, fall three
High, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful.And all raw materials is all from medicine-food two-purpose natural plants, nontoxic
Side effect.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For Yuan, under the premise without departing from the principles of the invention, it is also possible to make some improvements and modifications, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (7)
1. a kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, it is characterised in that be made up of the raw material of following weight portion: Radix Angelicae Sinensis 5-
15 parts, Radix Rehmanniae Preparata 5-15 part, Cortex Eucommiae 5-12 part, Cortex Cinnamomi 3-9 part, Rhizoma Cimicifugae 5-12 part, Herba Cistanches 5-10 part, Radix Paeoniae Alba 10-16 part, beautiful Fructus Citri tangerinae
Stalk 5-15 part, Lignum Aquilariae Resinatum 6-15 part, Radix Codonopsis 5-10 part, Rhizoma Atractylodis Macrocephalae 5-10 part, Radix Astragali 5-10 part, Pericarpium Citri Reticulatae 5-10 part, Radix Glycyrrhizae 5-10 part, unit
5-10 part, Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate recklessly.
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea the most according to claim 1, it is characterised in that by following weight
Part raw material make: Radix Angelicae Sinensis 10 parts, 10 parts of Radix Rehmanniae Preparata, the Cortex Eucommiae 10 parts, Cortex Cinnamomi 8 parts, Rhizoma Cimicifugae 10 parts, Herba Cistanches 8 parts, the Radix Paeoniae Alba 12 parts,
RADIX PLATYCODI 12 parts, Lignum Aquilariae Resinatum 10 parts, Radix Codonopsis 8 parts, the Rhizoma Atractylodis Macrocephalae 8 parts, the Radix Astragali 8 parts, Pericarpium Citri Reticulatae 8 parts, 8 parts of Radix Glycyrrhizae, Rhizoma Corydalis 8 parts, 8 parts of Air Bladder pseudosciaenae seu Acipenser,
New fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, Mel, water are appropriate.
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea the most according to claim 1, it is characterised in that by following weight
The raw material of part is made: Radix Angelicae Sinensis 5 parts, 5 parts of Radix Rehmanniae Preparata, the Cortex Eucommiae 5 parts, Cortex Cinnamomi 3 parts, Rhizoma Cimicifugae 5 parts, Herba Cistanches 5 parts, the Radix Paeoniae Alba 10 parts, beautiful Fructus Citri tangerinae
Obstruct 5 parts, Lignum Aquilariae Resinatum 6 parts, Radix Codonopsis 5 parts, the Rhizoma Atractylodis Macrocephalae 5 parts, the Radix Astragali 5 parts, Pericarpium Citri Reticulatae 5 parts, 5 parts of Radix Glycyrrhizae, Rhizoma Corydalis 5 parts, 5 parts of Air Bladder pseudosciaenae seu Acipenser, fresh stone
Dry measure used in former times 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are appropriate.
A kind of the kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea the most according to claim 1, it is characterised in that by following weight
Part raw material make: Radix Angelicae Sinensis 15 parts, 15 parts of Radix Rehmanniae Preparata, the Cortex Eucommiae 12 parts, Cortex Cinnamomi 9 parts, Rhizoma Cimicifugae 12 parts, Herba Cistanches 10 parts, the Radix Paeoniae Alba 16 parts,
RADIX PLATYCODI 15 parts, Lignum Aquilariae Resinatum 15 parts, Radix Codonopsis 10 parts, the Rhizoma Atractylodis Macrocephalae 10 parts, the Radix Astragali 10 parts, Pericarpium Citri Reticulatae 10 parts, 10 parts of Radix Glycyrrhizae, Rhizoma Corydalis 10 parts, fish
Fish glue 10 parts, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20 parts, Mel, water are appropriate.
5. the preparation processing method of a kidney warming yang invigorating treatment prolapse of gastric mucosa medicated tea, it is characterised in that comprise the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, then take
Go out to put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time
The Chinese liquor of 52-60 DEG C, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, add the fresh bar of Herba Dendrobii
The distilled water of weight 2-3 times, for the second time juice extractor time 10-15min, juice extractor rotating speed is 80～100r/s, stands 10min；
After carry out third time squeeze the juice, add Herba Dendrobii fresh bar weight 3-5 times distilled water, time 20-30min, juice extractor rotating speed be 100～
150r/s, separates fresh for Herba Dendrobii bar juice with fiber filter, makes the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, cell damage
Rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；The warm water that new fresh grape is put into 50-60 DEG C again cleans dry
After Jing, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 in tank
Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh
Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, at 30-35
Seal at a temperature of DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；After extracting Matrix Solution
It is the cellulase of 0.5-0.7% that Pericarpium Vitis viniferae and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10,
Keep 35 DEG C, water soluble dietary fiber can be extracted further after 24h enzymolysis, water soluble dietary fiber is added Matrix Solution
Obtain Matrix Solution II；
E, take mix homogeneously after Radix Angelicae Sinensis, Radix Rehmanniae Preparata, Cortex Eucommiae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times,
Each 2 hours, merge 2 Radix Angelicae Sinensis, Radix Rehmanniae Preparata, Cortex Eucommiae ethanol extracts, receive alcohol and be evaporated to relative density at 40 DEG C and be
1.15-1.35, prepare Radix Angelicae Sinensis, Radix Rehmanniae Preparata, the Cortex Eucommiae extract standby；
Rhizoma Cimicifugae, Herba Cistanches mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing of 300-400 mesh carefully
Powder；
Taking Cortex Cinnamomi, the Radix Paeoniae Alba, RADIX PLATYCODI, Lignum Aquilariae Resinatum, Radix Codonopsis, the Rhizoma Atractylodis Macrocephalae, the Radix Astragali, Pericarpium Citri Reticulatae, Radix Glycyrrhizae, Rhizoma Corydalis, Air Bladder pseudosciaenae seu Acipenser, mix homogeneously adds 30-
60 DEG C of warm water soaking, after 10 minutes, put into reach in freezer ,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, by cold
Freezing medicine block and ultra micro mixing fine powders boiling is extracted 3 times, add 1-2 times amount water for the first time, temperature keeps 100-120 DEG C, carries out
Infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10
Times amount water, temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, is concentrated into the 1/2 of original volume, adds Radix Angelicae Sinensis, ripe
Ground, the extract of the Cortex Eucommiae, obtain Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh
Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh
In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is:
Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial,
Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
The preparation processing method of a kind of the kidney warming yang invigorating the most according to claim 5 treatment prolapse of gastric mucosa medicated tea, its feature
It is, step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute, make Fructus Vitis viniferae
Freeze, after taking out nature defrosting, then carry out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
The preparation processing method of a kind of the kidney warming yang invigorating the most according to claim 5 treatment prolapse of gastric mucosa medicated tea, its feature
Be, step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae
It is 10:0.2～0.8:5～10:0.5.
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| CN103300450A (en) * | 2013-06-14 | 2013-09-18 | 浙江大学 | Preparation method of raw dendrobium officinale pulp beverage |
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| CN103300450A (en) * | 2013-06-14 | 2013-09-18 | 浙江大学 | Preparation method of raw dendrobium officinale pulp beverage |
Non-Patent Citations (2)
| Title |
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| 宋芳等: "超临界二氧化碳萃取葡萄籽油及其脂肪酸的分析", 《中国食品工业》 * |
| 李文亮等: "《千家妙方（上册）》", 31 May 1999, 战士出版社 * |
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