CN106166240A - The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease and preparation processing method - Google Patents
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease and preparation processing method Download PDFInfo
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- CN106166240A CN106166240A CN201610234347.1A CN201610234347A CN106166240A CN 106166240 A CN106166240 A CN 106166240A CN 201610234347 A CN201610234347 A CN 201610234347A CN 106166240 A CN106166240 A CN 106166240A
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- herba
- vitis viniferae
- radix
- herba dendrobii
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Abstract
The invention discloses the medicated tea of a kind of activating blood and resolving stasis and treating purpura disease, be made up of the raw material of following weight portion: Caulis Spatholobi 10 30 parts, Cortex Moutan 5 15 parts, Radix Angelicae Sinensis 39 parts, Herba Ecliptae 5 12 parts, Radix Notoginseng 39 parts, Herba Agrimoniae 39 parts, Rhizoma Atractylodis 5 12 parts, Cortex Phellodendri 5 10 parts, Herba Taraxaci 10 30 parts, Folium Isatidis 5 10 parts, 10 16 parts of Talcum, Fructus Forsythiae 5 15 parts, Radix Isatidis 6 15 parts, Rhizoma Imperatae 5 10 parts, Radix Dipsaci 5 10 parts.The invention have the advantage that inventive formulation activating blood and resolving stasis and treating purpura disease, anorexia, middle gas do not save, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, the merit of resisting fatigue.
Description
Technical field
The present invention relates to the medicated tea of a kind of activating blood and resolving stasis and treating purpura disease, in particular, relate to a kind of blood circulation promoting and blood stasis dispelling
The herb tea formula for the treatment of purpura disease and preparation method thereof technical field.
Background technology
Purpura disease is a kind of immunity syndrome, is common hemorrhage.Feature is to there is anti-blood in blood circulation
Platelet antibodies, makes platelet destruction too much, causes purpura, show as congestion do not go, escape of blood from meridian, hypertension, cholecystitis, skin
Have trace of itching, damp and hot multiple abscess and skin, food stagnation not disappear, anorexia, the symptom such as middle gas not province.
The most traditional beverage, only focuses on mouthfeel, is of low nutritive value, and does not have blood circulation promoting and blood stasis dispelling, treatment purpura disease, raising people
Body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, drop three-hypers, prevent and treat diabetes and anti-cancer, the function of the aspect such as anticancer, nothing
Method releases the sufferings of client, and traditional herbal tea is by Traditional medicine infusion, and flavour of a drug weight mouthfeel is poor, it is impossible to preserve for a long time.Existing market
On not yet occur a kind of in good taste, improve self and increase the wriggling of the intestines and stomach, cure the disease and strengthen the beverage of body immunity simultaneously.
Summary of the invention
The present invention is directed to the deficiency of existing product, and provide a kind of fresh juice beverage to regulate the effect of human physiological functions,
This beverage have be easily absorbed by the human body, medicinal function is notable, delicious flavour, good mouthfeel, improve self and increase the wriggling of the intestines and stomach,
Cure the disease the medicated tea of a kind of activating blood and resolving stasis and treating purpura disease simultaneously strengthening the advantages such as body immunity.
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease, is made up of the raw material of following weight portion: Caulis Spatholobi 10-30 part, pellet
Skin 5-15 part, Radix Angelicae Sinensis 3-9 part, Herba Ecliptae 5-12 part, Radix Notoginseng 3-9 part, Herba Agrimoniae 3-9 part, Rhizoma Atractylodis 5-12 part, Cortex Phellodendri 5-10 part,
Herba Taraxaci 10-30 part, Folium Isatidis 5-10 part, Talcum 10-16 part, Fructus Forsythiae 5-15 part, Radix Isatidis 6-15 part, Rhizoma Imperatae 5-10 part, river
Disconnected 5-10 part, Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate.
The preparation processing method of the medicated tea of described a kind of activating blood and resolving stasis and treating purpura disease, comprises the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, then take
Go out to put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time
The Chinese liquor of 52-60 DEG C, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, add the fresh bar of Herba Dendrobii
The distilled water of weight 2-3 times, for the second time juice extractor time 10-15min, juice extractor rotating speed is 80～100r/s, stands 10min；
After carry out third time squeeze the juice, add Herba Dendrobii fresh bar weight 3-5 times distilled water, time 20-30min, juice extractor rotating speed be 100～
150r/s, separates fresh for Herba Dendrobii bar juice with fiber filter, makes the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, cell damage
Rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；The warm water that new fresh grape is put into 50-60 DEG C again cleans dry
After Jing, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 in tank
Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh
Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, at 30-35
Seal at a temperature of DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；After extracting Matrix Solution
It is the cellulase of 0.5-0.7% that Pericarpium Vitis viniferae and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10,
Keep 35 DEG C, water soluble dietary fiber can be extracted further after 24h enzymolysis, water soluble dietary fiber is added Matrix Solution
Obtain Matrix Solution II；
E, take mix homogeneously after Radix Angelicae Sinensis, Radix Notoginseng cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, each 2
Hour, merge 2 Radix Angelicae Sinensis, Radix Notoginseng ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35, system
Radix Angelicae Sinensis, Radix Notoginseng extract standby；
Talcum, Rhizoma Atractylodis mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing of 300-400 mesh carefully
Powder；
Take Caulis Spatholobi, Cortex Moutan, Herba Ecliptae, Herba Agrimoniae, Cortex Phellodendri, Herba Taraxaci, Folium Isatidis, Fructus Forsythiae, Radix Isatidis, Rhizoma Imperatae, Radix Dipsaci, fish
Fish glue, after mix homogeneously adds 30-60 DEG C of warm water soaking 10 minutes, puts into reach in freezer ,-10～-20 DEG C freezing 10-20 minute,
Forming freezing medicine block, freezing medicine block and ultra micro mixing fine powders boiling are extracted 3 times, add 1-2 times amount water for the first time, temperature is protected
Hold 100-120 DEG C, carry out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 points
Clock；Third time adds 6-10 times amount water, and temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, is concentrated into original volume
1/2, add Radix Angelicae Sinensis, the extract of Radix Notoginseng, obtain Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh
Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh
In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is:
Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial,
Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
Further: step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute,
Make Fructus Vitis viniferae freeze, after taking out nature defrosting, then carry out Fructus Vitis viniferae meat and Pericarpium Vitis viniferae detached job.
Further: step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, Oleum Vitis viniferae
Weight proportion be 10:0.2～0.8:5～10:0.5.
Caulis Spatholobi, relaxing muscles and tendons to promote blood circulation；Nourishing blood for regulating menstruation.Main numb hand and foot；Quadriplegia;Rheumatic arthralgia;Women has through uncomfortable;Bitterly
Warp;Amenorrhea.Enrich blood, invigorate blood circulation, dredging collateral.For menoxenia, blood deficiency and yellow complexion, paralysis and numbness, rheumatic arthralgia.
Cortex Moutan, pungent, bitter, be slightly cold.GUIXIN, liver, kidney channel.For the epidemic febrile disease pathogenic heat attacking blood system in febrile diseases, there is clearing away heat and cooling blood effect.
Radix Angelicae Sinensis, sweet, pungent, warm, return liver, the heart, spleen channel, enrich blood；Invigorate blood circulation；Menstruction regulating and pain relieving；Moisturize laxation.
Herba Ecliptae, sweet in the mouth acid, cool in nature, enter Liver and kidney two warp, nontoxic.Nourishing the liver and kidney, cooling blood for hemostasis, can control various haematemesis, intestinal
Hemorrhage disease such as grade.
Radix Notoginseng, enriches blood, invigorates blood circulation, for physical weakness, inappetence, neurasthenia, fatigue.
Herba Agrimoniae is bitter, cool.Return stomach, liver, spleen, lung, large intestine channel.Relieve internal heat anticancer, cooling blood for hemostasis, detumescent of healing the wounds.
Rhizoma Atractylodis are drying damp and strengthening spleen;Wind-damp dispelling;Improving eyesight.Main the spleen and stomach being stranded by dampness;Asthenia drowsiness;Born of the same parents' painful abdominal mass abdominal distention;Inappetence;Tell
Have loose bowels;Phlegm retention;Damp-edema;Exterior syndrome folder is wet.
Cortex Phellodendri, bitter, cold.Return kidney, bladder warp.Heat clearing and damp drying, pathogenic fire purging is except steaming, detoxification sore treatment.For damp-heat dysentery, jaundice,
Leukorrhagia, pyretic stranguria, tinea pedis, flaccidity { wards off }, hectic fever due to YIN-deficiency consumptive fever, night sweat, seminal emission, sore swollen toxin, eczema pruritus.
Herba Taraxaci, heat-clearing and toxic substances removing, for heat toxin syndrome, especially it is apt to removing heat from the liver, treats liver-heat conjunctival congestion and swelling pain.
Folium Isatidis, bitter in the mouth, cold in nature, return liver, the heart, stomach, spleen channel.Heat-clearing and toxic substances removing, blood cooling and ecchymoses removing.
Talcum, clearing away fire and eliminating phlegm, dampness removing is relieved summer heat, and restores menstrual flow and invigorates blood circulation, and antidiarrheal dysentery is vomitted, consumer edema fire-toxin.
Fructus Forsythiae, heat clearing away, removing toxic substances, eliminating stagnation, detumescence.
Radix Isatidis, heat-clearing and toxic substances removing, removing heat from blood;For warming heating, to send out speckle, anemopyretic cold, swelling throat rotten.
Rhizoma Imperatae, returns lung, stomach, bladder warp.Cooling blood for hemostasis, clearing away heat and promoting diuresis.
Radix Dipsaci, invigorating the liver and kidney, reuniting the fractured tendons and bones, blood circulation regulating.Control aching pain in waist and back.
The natural tradition medicinal and edible Chinese medicine above with multiple health care is share, blood circulation promoting and blood stasis dispelling, treats purpura disease,
Improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, the merit of resisting fatigue.Joining of each component is screened by great many of experiments
Ratio, scientific and reasonable；And whole preparation technology is rationally and extract drugs rate efficiency is high, the effective one-tenth in raw material can be retained well
Point, do not bring any impurity, and sweet mouthfeel into, have no side effect.
The invention has the beneficial effects as follows:
1, the formula of the present invention, has promoting the production of body fluid to quench thirst, gastric acid secretion, helps digest, and health body-building has calm nerves and declines
Weak, lessen fatigue, containing various trace elements such as calcium, ferrum, zinc, selenium, sodium etc., raising body immunity, defying age, toxin expelling are supported
Face, nourish taste, three-hypers drops, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful, regulates human physiological functions.
2, the present invention is rich in anthocyanidin, it is possible to protection human body is from the damage of free radical, it is possible to strengthens blood vessel elasticity, relax
Blood vessel, increases systemic blood circulation, has certain blood pressure reduction effect；Immune system ability can be strengthened, there is strong anti-oxidation, resist
Suddenly change, alleviate the function such as hepatosis, protection cardiovascular；
3, add the Chinese herbal medicine such as Caulis Spatholobi, Cortex Moutan, Herba Ecliptae, Herba Agrimoniae, Cortex Phellodendri, Herba Taraxaci, Folium Isatidis and there is blood circulation promoting and blood stasis dispelling, control
Treat purpura disease, improve the functions such as body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, resisting fatigue.
4, the products taste that the production technology of the present invention and preparation method draw is sour-sweet tasty and refreshing, rich in dendrobium polysaccharide, has
The highest health care and medical value, long-term drink can with YIN nourishing skin care, change skin colour, defying age, life lengthening, and
Carrying and drink conveniently, improve self and increase the wriggling of the intestines and stomach, cure the disease and strengthen the beverage of body immunity simultaneously, the shelf-life is up to 1-
2 years.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, in order to those skilled in the art knows more about
The present invention, but and it is not so limited the present invention.
Embodiment 1
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease, is made up of the raw material of following weight portion: Caulis Spatholobi 15 parts, Cortex Moutan 10 parts,
Radix Angelicae Sinensis 8 parts, Herba Ecliptae 10 parts, Radix Notoginseng 5 parts, Herba Agrimoniae 5 parts, Rhizoma Atractylodis 10 parts, Cortex Phellodendri 8 parts, Herba Taraxaci 15 parts, Folium Isatidis 8 parts, cunning
12 parts of stone, Fructus Forsythiae 12 parts, Radix Isatidis 12 parts, Rhizoma Imperatae 12 parts, Radix Dipsaci 8 parts, 8 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, honeybee
Honey, water are appropriate.
The preparation processing method of the medicated tea of a kind of activating blood and resolving stasis and treating purpura disease, described preparation method comprises the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
Fresh for the Herba Dendrobii cleaned up bar is put into microwave oven by B, keeps temperature 50-60 DEG C, carries out heating 10 minutes, further take out
Put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content 52 of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time
DEG C Chinese liquor, time 15min, the rotating speed of juice extractor is 30r/s；After standing 10 minutes, add the steaming of Herba Dendrobii fresh bar weight 2.5 times
Distilled water, for the second time juice extractor time 15min, juice extractor rotating speed is 80r/s, stands 10min；After carry out third time squeeze the juice, add
The distilled water of Herba Dendrobii fresh bar weight 3-5 times, time 30min, juice extractor rotating speed is 150r/s, by fresh for Herba Dendrobii bar juice and fiber mistake
Filter separate, make the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, broken cell rate reaches more than 80%, obtain new fresh Herba Dendrobii juice and
Herba Dendrobii fresh bar fiber；Again new fresh grape is put into after the warm water of 55 DEG C cleans up, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated
Stand-by；After new fresh grape cleans up, put into reach in freezer ,-10 ~-20 DEG C of freezings 10 minutes, make Fructus Vitis viniferae freeze, take out certainly
After so thawing, then carry out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 120 in tank
Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh
Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 6 times of weight, stirring is smashed to 100 mesh, 30-35 DEG C of temperature
Degree lower seal preserves 24h, sterilizing, filters, puts into unglazed hermetically sealed can, obtain Matrix Solution standby；Extract the Fructus Vitis viniferae after Matrix Solution
It is the cellulase of 0.5-0.7% that skin and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10, keeps
35 DEG C, water soluble dietary fiber can be extracted after 24h enzymolysis further, water soluble dietary fiber is added Matrix Solution and obtains
Matrix Solution II；；Rich in anthocyanidin in Pericarpium Vitis viniferae, it is possible to protection human body is from the damage of free radical, it is possible to enhancing blood vessel elasticity,
Lax blood vessel, increases systemic blood circulation, has certain blood pressure reduction effect；Immune system ability can be strengthened, there is strong antioxygen
Change, mutation, alleviate hepatosis, protection function, Pericarpium Vitis viniferae and the Herba Dendrobii fresh bar fiber such as cardiovascular together with stir smash through
Anthocyanidin mentioned by hydromel, can protect the quality of anthocyanidin while farthest extracting anthocyanidin.By water solublity meals
Food fiber adds Matrix Solution and obtains Matrix Solution II, can increase effect of the wriggling of the intestines and stomach, it is ensured that metabolic waste is normally discharged
External；Adsorb various metabolic waste, be allowed to normally excrete, improve the comprehensive utilization value of Herba Dendrobii.
E, take mix homogeneously after Radix Angelicae Sinensis, Radix Notoginseng cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, often
Secondary 2 hours, merge 2 Radix Angelicae Sinensis, Radix Notoginseng ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35,
Prepare Radix Angelicae Sinensis, Radix Notoginseng extract standby；
Talcum, Rhizoma Atractylodis mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing of 300-400 mesh carefully
Powder；
Take Caulis Spatholobi, Cortex Moutan, Herba Ecliptae, Herba Agrimoniae, Cortex Phellodendri, Herba Taraxaci, Folium Isatidis, Fructus Forsythiae, Radix Isatidis, Rhizoma Imperatae, Radix Dipsaci, fish
Fish glue, after mix homogeneously adds 30-60 DEG C of warm water soaking 10 minutes, puts into reach in freezer ,-10～-20 DEG C freezing 10-20 minute,
Forming freezing medicine block, freezing medicine block and ultra micro mixing fine powders boiling are extracted 3 times, add 1-2 times amount water for the first time, temperature is protected
Hold 100-120 DEG C, carry out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 points
Clock；Third time adds 6-10 times amount water, and temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, is concentrated into original volume
1/2, add Radix Angelicae Sinensis, the extract of Radix Notoginseng, obtain Matrix Solution III standby；
The hard to bear medicine boiled is pulverized and improves its extract drugs efficiency, make whole formula drug effect farthest be utilized.
F, take Matrix Solution I through instantaneous high-temperature 120 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh
Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh
In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is:
Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；Supercritical extraction can be
Extract under room temperature 37 DEG C and CO2 gas blanket, effectively prevent oxidation and the loss of heat-sensitive substance.Therefore,
The effective ingredient of medicinal plants is remain in extract, and can be high boiling point, low volatility, the easy material being pyrolyzed the lowest
Extract under its boiling temperature；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, and described material-compound tank endobasal-body solution I, matrix are molten
Liquid II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae are 10:0.5:6:0.5., seal through bottle capper and load vial
In, packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, dress
Case, carries and drinks conveniently, and the shelf-life is up to 1-2.
Embodiment 2
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease, is made up of the raw material of following weight portion: Caulis Spatholobi 10 parts, Cortex Moutan 5 parts, when
Return 3 parts, Herba Ecliptae 5 parts, Radix Notoginseng 3 parts, Herba Agrimoniae 3 parts, Rhizoma Atractylodis 5 parts, Cortex Phellodendri 5 parts, Herba Taraxaci 10 parts, Folium Isatidis 5 parts, Talcum 10
Part, Fructus Forsythiae 5 parts, Radix Isatidis 6 parts, Rhizoma Imperatae 5 parts, Radix Dipsaci 5 parts, 5 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are fitted
Amount.Processing method is with embodiment 1.
Embodiment 3
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease, is made up of the raw material of following weight portion: Caulis Spatholobi 30 parts, Cortex Moutan 15 parts,
Radix Angelicae Sinensis 9 parts, Herba Ecliptae 12 parts, Radix Notoginseng 9 parts, Herba Agrimoniae 9 parts, Rhizoma Atractylodis 12 parts, Cortex Phellodendri 10 parts, Herba Taraxaci 30 parts, Folium Isatidis 10 parts,
16 parts of Talcum, Fructus Forsythiae 15 parts, Radix Isatidis 15 parts, Rhizoma Imperatae 10 parts, Radix Dipsaci 10 parts, 10 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20
Part, Mel, water are appropriate.Processing method is with embodiment 1.
Clinical experiment divides three parts:
(1) animal acute toxicity and chronic toxicity experiment:
1, animal acute toxicity test
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 medicated tea add the medicated tea powder paste that rice flour is made.
Experimental animal: regular grade NIH mice, body weight 18g ± 2g, male and female half and half.
Method and result:
By three kinds of each 50g of medicated tea, add rice flour.Experiment mice is randomly divided into three groups of male and female half and half, respectively three kinds of medicated tea of feeding
Powder is stuck with paste, volume 1ml/10g body weight, and close observation 8 hours is also noted down, and continues to observe 7 days；In 7 days, mice is without death, OK
For vivaciously, food ration is as usual, and hair color light is without loose dirt, without fainting from fear addicted to saliva, and eye, mouth, nose, ear and crissum secretions without exception,
Without the rotten toe that docks.5 execution of selection from three groups respectively, finding of naked eye: the important organs such as the heart, liver, lung, gastric and thymus, not
See abnormal change, show that two kinds of these nutritive powders are all without acute toxicity.
2, long-term toxicity test for animals
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 gained medicated tea add the medicated tea powder paste that rice flour is made.
Animal: regular grade SD rat, body weight 200g ± 10g, male and female half and half.
Method and result:
The configuration that three kinds of medicated tea powder are stuck with paste: be divided into high, medium and low three dosage groups, respectively the 200 of edible for patients amount, 100,
50g；Experimental mouse is randomly divided into three groups, and the medicated tea powder that feeding modulates continuously respectively is stuck with paste, and continuous feeding 40 days observes animal
General toxic reaction and the order of severity, place after death by rule of operation check each position, and carry out hematology, ALT, BUN and the heart,
The pathological examination of the main organs such as liver, spleen, lung, kidney, stomach；
Through long-term feeding, all there is not toxic reaction in two groups of rats.Growth promoter is good.Macroscopic appearance and main organs have no
Abnormal.Peripheral hemogram and Serum ALT, BUN compare with matched group without pathologic change.The pathological replacement heart, liver, spleen, lung, kidney, stomach
Deng the most significant change, it is understood that through proved by pathology, three kinds of medicated tea powder are stuck with paste and showed animal without chronic toxicity.
By two above toxicity test, it was demonstrated that the medicated tea that the present invention is made by embodiment 1, embodiment 2 and embodiment 3 is
Safety, have no side effect, can be used to clinical patients is carried out clinical trial.
3, the embodiment of the present invention drinks effect research:
(1) investigation method:
1. crowd is drunk: general population
2. Ganderwa: 30 days
3. number is drunk: 50 people
4. drinking method: 3 times for each person every day, ante cibum each 500mL
5. index: after drinking, substantially sensation is the most tired, congestion does not go, escape of blood from meridian, hypertension, cholecystitis, skin have and itches
The transference cures such as trace, damp and hot multiple abscess and skin, food stagnation do not disappear, anorexia, middle gas not province, and mouthfeel is the most sour-sweet for effective；Drink
With rear sensation easily tired, congestion does not go, escape of blood from meridian, hypertension, cholecystitis, skin have trace of itching, damp and hot multiple abscess and skin, food
Long-pending do not disappear, anorexia, middle gas do not save remission, and mouthfeel is the most sour-sweet, is designated as effectively.After drinking without obvious comfort then
It is invalid to be designated as.
(2) survey result
Survey result is shown in Table 1.Be test result indicate that by table 1, embodiment 1,2,3 has the respondent of 98% to feel that the present invention is carried
The beverage mouthfeel of confession is the most sour-sweet, and above-mentioned clinical symptom disappearance or be eased, the respondent of only 2% drink after without substantially
Increase comfort.
The each embodiment of table 1 drinks effect research table
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Embodiment 1 | 44%(22) | 54%(27) | 2%(1) |
| Embodiment 2 | 42%(21) | 56%(28) | 2%(1) |
| Embodiment 3 | 42%(21) | 56%(28) | 2%(1) |
Embodiment contrast groups A
Comparative example 4,5,6 is added without the nutrition such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae and becomes
Point, according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing is traditional side of boiling
Method；The investigation method of using method and using effect is with above.
Table 2 embodiment contrast groups A drinks effect research
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 4 | 36%(18) | 40%(20) | 24%(12) |
| Comparative example 5 | 40%(20) | 40%(20) | 20%(10) |
| Comparative example 6 | 46%(23) | 34%(17) | 20%(10) |
Embodiment contrast groups B
Comparative example 7,8,9 is added without the nutrition such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae and becomes
Point, according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing uses in embodiment 1
The preparation processing method of step E；The investigation method of using method and using effect is with above.
Table 3 embodiment contrast groups B drinks effect research
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 7 | 32%(16) | 56%(28) | 12%(6) |
| Comparative example 8 | 28%(14) | 52%(31) | 10%(5) |
| Comparative example 9 | 36%(18) | 52%(26) | 12%(6) |
Embodiment contrast groups C
The processing method of comparative example 10,11,12 respectively corresponding embodiment 1,2,3 and formula, different be formula in
Without Air Bladder pseudosciaenae seu Acipenser composition；The investigation method of using method and using effect is with above.
Table 4 embodiment contrast groups C drinks effect research
| Group/effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 10 | 44%(22) | 46%(23) | 10%(5) |
| Comparative example 11 | 38%(19) | 50%(25) | 12%(6) |
| Comparative example 12 | 40%(20) | 48%(24) | 12%(6) |
Conclusion:
Contrasted by table 2 and table 1 and can be seen that
The inefficient number of embodiment contrast groups A is about 10 times of embodiment 1,2,3；This shows Chinese crude drug formula of the present invention
And between the nutritional labeling such as water soluble dietary fiber and Oleum Vitis viniferae, creating the most collaborative pharmacological action, aqueous soluble dietary is fine
Dimension increases effect of the wriggling of the intestines and stomach and promotes the human body absorption to ingredient, it is ensured that metabolic waste normally excretes, additionally
The anthocyanidin that contains in Pericarpium Vitis viniferae, resveratrol, have strong anti-oxidation, mutation, alleviate hepatosis, protection cardiovascular etc.
Function, strengthens immune system ability；Associate with Chinese medicine and improve assimilation effect and improve the mouthfeel of Chinese medicine, through the essence of the present invention simultaneously
The extraction of heart configuration and at utmost ingredient, Chinese crude drug formula of the present invention and preparation method occur in that beat all technology
Effect.
Table 2 and table 3 contrast can be seen that
About inefficient number is embodiment contrast groups B 2 times of embodiment contrast groups A, embodiment contrast groups B and traditional
Embodiment contrast groups A of boiling method has compared significant raising at therapeutic effect, and this shows that Chinese crude drug of the present invention is through step
The preparation processing method of rapid E has had significant raising than traditional boiling method, the extraction degree of active ingredient.
Table 1 is compared with table 4:
The formula of embodiment contrast groups C does not contains Air Bladder pseudosciaenae seu Acipenser, and the invalid number of embodiment contrast groups C is 5 times of left sides of embodiment 1,2,3
Right；And effective percentage number has and has declined；Air Bladder pseudosciaenae seu Acipenser can strengthen gastrointestinal digestive and absorptive functions, improves appetite, is conducive to anti-
Control the diseases such as inappetence, anorexia, dyspepsia, abdominal distention, constipation, show Air Bladder pseudosciaenae seu Acipenser serve in formula collaborative and priming return through
Effect, Air Bladder pseudosciaenae seu Acipenser application effect achieves unexpected technique effect.
In sum, the medicated tea of a kind of activating blood and resolving stasis and treating purpura disease that the present invention provides has sour-sweet mouthfeel, simultaneously
Have again treatment easily tired, congestion does not go, escape of blood from meridian, hypertension, cholecystitis, skin have trace of itching, damp and hot multiple abscess and skin,
The merit that food stagnation does not disappears, anorexia, middle gas do not save, improves body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, fall three
High, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful.And all raw materials is all from medicine-food two-purpose natural plants, nontoxic
Side effect.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For Yuan, under the premise without departing from the principles of the invention, it is also possible to make some improvements and modifications, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (7)
1. the medicated tea of an activating blood and resolving stasis and treating purpura disease, it is characterised in that be made up of the raw material of following weight portion: Caulis Spatholobi
10-30 part, Cortex Moutan 5-15 part, Radix Angelicae Sinensis 3-9 part, Herba Ecliptae 5-12 part, Radix Notoginseng 3-9 part, Herba Agrimoniae 3-9 part, Rhizoma Atractylodis 5-12 part, Huang
Cypress 5-10 part, Herba Taraxaci 10-30 part, Folium Isatidis 5-10 part, Talcum 10-16 part, Fructus Forsythiae 5-15 part, Radix Isatidis 6-15 part, Rhizoma Imperatae
5-10 part, Radix Dipsaci 5-10 part, Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate.
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease the most according to claim 1, it is characterised in that by following weight portion
Raw material make: Caulis Spatholobi 15 parts, Cortex Moutan 10 parts, Radix Angelicae Sinensis 8 parts, Herba Ecliptae 10 parts, Radix Notoginseng 5 parts, Herba Agrimoniae 5 parts, Rhizoma Atractylodis 10 parts,
Cortex Phellodendri 8 parts, Herba Taraxaci 15 parts, Folium Isatidis 8 parts, 12 parts of Talcum, Fructus Forsythiae 12 parts, Radix Isatidis 12 parts, Rhizoma Imperatae 12 parts, Radix Dipsaci 8 parts, fish
Fish glue 8 parts, new fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, Mel, water are appropriate.
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease the most according to claim 1, it is characterised in that by following weight portion
Raw material make: Caulis Spatholobi 10 parts, Cortex Moutan 5 parts, Radix Angelicae Sinensis 3 parts, Herba Ecliptae 5 parts, Radix Notoginseng 3 parts, Herba Agrimoniae 3 parts, Rhizoma Atractylodis 5 parts, yellow
Cypress 5 parts, Herba Taraxaci 10 parts, Folium Isatidis 5 parts, 10 parts of Talcum, Fructus Forsythiae 5 parts, Radix Isatidis 6 parts, Rhizoma Imperatae 5 parts, Radix Dipsaci 5 parts, Air Bladder pseudosciaenae seu Acipenser 5
Part, new fresh Herba Dendrobii 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are appropriate.
The medicated tea of a kind of activating blood and resolving stasis and treating purpura disease the most according to claim 1, it is characterised in that by following weight portion
Raw material make: Caulis Spatholobi 30 parts, Cortex Moutan 15 parts, Radix Angelicae Sinensis 9 parts, Herba Ecliptae 12 parts, Radix Notoginseng 9 parts, Herba Agrimoniae 9 parts, Rhizoma Atractylodis 12 parts,
Cortex Phellodendri 10 parts, Herba Taraxaci 30 parts, Folium Isatidis 10 parts, 16 parts of Talcum, Fructus Forsythiae 15 parts, Radix Isatidis 15 parts, Rhizoma Imperatae 10 parts, Radix Dipsaci 10
Part, 10 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20 parts, Mel, water are appropriate.
5. the preparation processing method of the medicated tea of an activating blood and resolving stasis and treating purpura disease, it is characterised in that comprise the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, then take
Go out to put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time
The Chinese liquor of 52-60 DEG C, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, add the fresh bar of Herba Dendrobii
The distilled water of weight 2-3 times, for the second time juice extractor time 10-15min, juice extractor rotating speed is 80～100r/s, stands 10min；
After carry out third time squeeze the juice, add Herba Dendrobii fresh bar weight 3-5 times distilled water, time 20-30min, juice extractor rotating speed be 100～
150r/s, separates fresh for Herba Dendrobii bar juice with fiber filter, makes the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, cell damage
Rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；The warm water that new fresh grape is put into 50-60 DEG C again cleans dry
After Jing, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 in tank
Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh
Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, at 30-35
Seal at a temperature of DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；After extracting Matrix Solution
It is the cellulase of 0.5-0.7% that Pericarpium Vitis viniferae and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10,
Keep 35 DEG C, water soluble dietary fiber can be extracted further after 24h enzymolysis, water soluble dietary fiber is added Matrix Solution
Obtain Matrix Solution II；
E, take mix homogeneously after Radix Angelicae Sinensis, Radix Notoginseng cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, each 2
Hour, merge 2 Radix Angelicae Sinensis, Radix Notoginseng ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35, system
Radix Angelicae Sinensis, Radix Notoginseng extract standby；
Talcum, Rhizoma Atractylodis mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing of 300-400 mesh carefully
Powder；
Take Caulis Spatholobi, Cortex Moutan, Herba Ecliptae, Herba Agrimoniae, Cortex Phellodendri, Herba Taraxaci, Folium Isatidis, Fructus Forsythiae, Radix Isatidis, Rhizoma Imperatae, Radix Dipsaci, fish
Fish glue, after mix homogeneously adds 30-60 DEG C of warm water soaking 10 minutes, puts into reach in freezer ,-10～-20 DEG C freezing 10-20 minute,
Forming freezing medicine block, freezing medicine block and ultra micro mixing fine powders boiling are extracted 3 times, add 1-2 times amount water for the first time, temperature is protected
Hold 100-120 DEG C, carry out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 points
Clock；Third time adds 6-10 times amount water, and temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, is concentrated into original volume
1/2, add Radix Angelicae Sinensis, the extract of Radix Notoginseng, obtain Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh
Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh
In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is:
Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial,
Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
The preparation processing method of the medicated tea of a kind of activating blood and resolving stasis and treating purpura disease the most according to claim 5, its feature exists
In, step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute, make grapevine knot
Ice, after taking out nature defrosting, then carries out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
The preparation processing method of the medicated tea of a kind of activating blood and resolving stasis and treating purpura disease the most according to claim 5, its feature exists
In, step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae be
10:0.2～0.8:5～10:0.5.
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| Title |
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| 宋芳等: "超临界二氧化碳萃取葡萄籽油及其脂肪酸的分析", 《中国食品工业》 * |
| 李文亮等: "《千家妙方（上册）》", 31 May 1999, 战士出版社 * |
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