CN106166239A - A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea and preparation processing method - Google Patents

A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea and preparation processing method Download PDF

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CN106166239A
CN106166239A CN201610234299.6A CN201610234299A CN106166239A CN 106166239 A CN106166239 A CN 106166239A CN 201610234299 A CN201610234299 A CN 201610234299A CN 106166239 A CN106166239 A CN 106166239A
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parts
radix
herba
vitis viniferae
herba dendrobii
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温从字
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Zhejiang Yu Chen Pharmaceutical Co Ltd
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Zhejiang Yu Chen Pharmaceutical Co Ltd
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    • A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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Abstract

The invention discloses a kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea of the present invention, be made up of the raw material of following weight portion: Radix Et Rhizoma Rhei 5 15 parts, Cortex Magnoliae Officinalis 5 12 parts, Fructus Aurantii Immaturus 39 parts, Fructus Crataegi 5 12 parts, Caulis Sargentodoxae 5 10 parts, Herba Patriniae 10 16 parts, Radix Aucklandiae (Radix Vladimiriae) 5 15 parts, Herba Taraxaci 6 15 parts, Radix Bupleuri 5 10 parts, Radix Scutellariae 5 10 parts, Herba Artemisiae Scopariae 5 10 parts, Haematitum 5 10 parts, Bin youth 5 10 parts, Caulis Bambusae In Taenia 5 10 parts.The invention have the advantage that inventive formulation Shugan Qingre, dampness removing purging FU-organs, heat-clearing and toxic substances removing, emesis, treat bowel dysfunction, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, the merit of resisting fatigue.

Description

A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea and preparation processing method
Technical field
The present invention relates to a kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, in particular, relate to a kind of dredging Liver and clearing heat dampness removing purging FU-organs treatment pancreatitis herb tea formula and preparation method thereof technical field.
Background technology
Pancreatitis is the disease that pancreas causes because of tryptic autodigestion effect.Pancreas has edema, hyperemia, or goes out Blood, necrosis.The symptoms such as stomachache, abdominal distention, Nausea and vomiting, heating occur clinically.In blood test and urine, amylase content raises Deng.Under normal circumstances, pancreatic juice is former containing inactive pancreatin in its gland tissue.Pancreatic juice is along pancreas pipeline constantly through gallbladder House steward's Oddi's sphincter flow into duodenum, due in duodenum with the presence of bile, add that duodenal wall mucosa is secreted A kind of enterokinase, under the effect of the two, pancreatin is former starts to transform to the digestive enzyme that activity is the strongest.If efferent tract is obstructed, row Let out not smooth, pancreatitis can be caused.
When Oddi's sphincter spasm or gallbladder overpressure raise, such as calculus, carcinomatous obstruction, bile reflux can enter ductus pancreaticus also Entering pancreatic tissue, now, lecithin contained in bile is decomposed into LYSOLECITHIN SUNLECITHIN A by A lecithinase contained in pancreatic juice, Pancreas can be produced toxic action.Or during biliary tract infection, antibacterial releasably goes out kinases and is activated by pancreatin, becomes energy loss equally Evil and the active substance of dissolving pancreatic tissue.These materials change into trypsin by former for pancreatin contained in pancreatic juice, and this enzyme disappears Change activity strong, infiltrate through pancreatic tissue and cause autodigestion, pancreatitis can be caused.
The most traditional beverage, only focuses on mouthfeel, is of low nutritive value, and does not have Shugan Qingre, dampness removing purging FU-organs, heat clearing away solution Poison, emesis, treatment bowel dysfunction, raising body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, fall three-hypers, preventing and treating sugar The sick function with aspects such as giving protection against cancer, anticancer of urine, it is impossible to release the sufferings of client, and traditional herbal tea is by Traditional medicine infusion, flavour of a drug Weight mouthfeel is poor, it is impossible to preserve for a long time.The most not yet occur a kind of in good taste, improve self and increase the wriggling of the intestines and stomach, control The sick beverage simultaneously strengthening body immunity.
Summary of the invention
The present invention is directed to the deficiency of existing product, and provide a kind of fresh juice beverage to regulate the effect of human physiological functions, This beverage have be easily absorbed by the human body, medicinal function is notable, delicious flavour, good mouthfeel, improve self and increase the wriggling of the intestines and stomach, Cure the disease and strengthen a kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea of the advantages such as body immunity simultaneously.
A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, is made up of the raw material of following weight portion: Radix Et Rhizoma Rhei 5-15 Part, Cortex Magnoliae Officinalis 5-12 part, Fructus Aurantii Immaturus 3-9 part, Fructus Crataegi 5-12 part, Caulis Sargentodoxae 5-10 part, Herba Patriniae 10-16 part, Radix Aucklandiae (Radix Vladimiriae) 5-15 part, Pu Herba Taraxaci 6-15 part, Radix Bupleuri 5-10 part, Radix Scutellariae 5-10 part, Herba Artemisiae Scopariae 5-10 part, Haematitum 5-10 part, Bin youth's 5-10 part, Caulis Bambusae In Taenia 5-10 Part, Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate.
The preparation processing method of described a kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, comprises the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, then take Go out to put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time The Chinese liquor of 52-60 DEG C, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, add the fresh bar of Herba Dendrobii The distilled water of weight 2-3 times, for the second time juice extractor time 10-15min, juice extractor rotating speed is 80～100r/s, stands 10min； After carry out third time squeeze the juice, add Herba Dendrobii fresh bar weight 3-5 times distilled water, time 20-30min, juice extractor rotating speed be 100～ 150r/s, separates fresh for Herba Dendrobii bar juice with fiber filter, makes the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, cell damage Rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；The warm water that new fresh grape is put into 50-60 DEG C again cleans dry After Jing, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 in tank Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, at 30-35 Seal at a temperature of DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；After extracting Matrix Solution It is the cellulase of 0.5-0.7% that Pericarpium Vitis viniferae and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10, Keep 35 DEG C, water soluble dietary fiber can be extracted further after 24h enzymolysis, water soluble dietary fiber is added Matrix Solution Obtain Matrix Solution II；
E, take mix homogeneously after Radix Et Rhizoma Rhei, Caulis Sargentodoxae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, every time 2 hours, merge 2 Radix Et Rhizoma Rhei, Caulis Sargentodoxae ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35, Prepare Radix Et Rhizoma Rhei, Caulis Sargentodoxae extract standby；
Herba Artemisiae Scopariae, Haematitum, Bin youth, Caulis Bambusae In Taenia being closed stirring and put into super micron mill, super micron mill heating keeps 80 degree of 5-6 of temperature Minute, carry out micronizing and obtain the ultra micro mixing fine powders of 300-400 mesh；
Taking Cortex Magnoliae Officinalis, Fructus Aurantii Immaturus, Fructus Crataegi, Herba Patriniae, Radix Aucklandiae (Radix Vladimiriae), Herba Taraxaci, Radix Bupleuri, Radix Scutellariae, Air Bladder pseudosciaenae seu Acipenser, mix homogeneously adds 30-60 DEG C After warm water soaking 10 minutes, put into reach in freezer ,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, by freezing medicine Block and ultra micro mixing fine powders boiling are extracted 3 times, add 1-2 times amount water for the first time, and temperature keeps 100-120 DEG C, carries out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10 times amount Water, temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, and is concentrated into the 1/2 of original volume, adds Radix Et Rhizoma Rhei, Caulis Sargentodoxae Extract, obtain Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is: Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial, Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
Further: step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute, Make Fructus Vitis viniferae freeze, after taking out nature defrosting, then carry out Fructus Vitis viniferae meat and Pericarpium Vitis viniferae detached job.
Further: step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, Oleum Vitis viniferae Weight proportion be 10:0.2～0.8:5～10:0.5.
Radix Et Rhizoma Rhei, bitter, cold.Return spleen, stomach, large intestine, liver, pericardium channel.Heat and toxic materials clearing away, clearing away heat-fire, removing pathogenic heat from blood and toxic substance from the body, removing blood stasis leads to Warp, dampness removing jaundice eliminating.
Cortex Magnoliae Officinalis, meridian distribution of property and flavor. bitter, pungent, temperature. return spleen, stomach, lung, large intestine channel, warming middle-JIAO, the therapeutic method to keep the adverse QI flowing downwards, dampness, expectorant. control chest and abdomen painful abdominal mass Full distending pain, regurgitation, vomiting, dyspepsia does not disappears, and phlegm retention is breathed heavily.
Fructus Aurantii Immaturus, bitter, pungent, sour, temperature.Return spleen, stomach, large intestine channel, stop in stagnant；Feeling of fullness distending pain；Constipation；After dysentery Weight；Blocked-up chest etc..
Fructus Crataegi, sour in the mouth is sweet. slightly warm in nature, and return taste Liver Channel, have promoting digestion and removing stagnation, effect of promoting blood circulation to remove blood stasis.
Caulis Sargentodoxae, bitter in the mouth, flat, nontoxic, return Liver Channel, large intestine channel, for promoting blood circulation to remove obstruction in the collateral, relieve internal heat dissipating blood stasis, wind dispelling insecticide.
Herba Patriniae, acrid in the mouth, hardship, for effects such as heat-clearing and toxic substances removing, removing blood stasis and expelling pus.
Radix Aucklandiae (Radix Vladimiriae), acrid in the mouth, hardship, warm in nature；Returning spleen, stomach, liver, large intestine channel, fragrance row dissipates, and can rise and can drop, and promoting the circulation of QI to relieve pain are used for Abdominal distention caused by stagnation of QI in spleen and stomach, lack of appetite vomiting.
Herba Taraxaci, heat-clearing and toxic substances removing, for heat toxin syndrome, especially it is apt to removing heat from the liver, treats liver-heat conjunctival congestion and swelling pain.
Radix Bupleuri, acrid in the mouth, hardship, cold nature.Reconciling superficies and interior, dispersing the stagnated live-QI to relieve the stagnation of QI, ascending up spleen-Qi and Yang, preventing the attack (or recurrence) of malaria of bringing down a fever, for cold, fever, Alternate attack of chill and fever, distending pain in the chest and hypochondrium.
Radix Scutellariae, has heat clearing and damp drying, and removing heat from blood is antiabortive, detoxicating functions.
Herba Artemisiae Scopariae, hepatoprotective effect, enriching yin and nourishing kidney, heat clearing away solution.
Haematitum, pancake lung, stomach two through inverse gas cease with preventing or arresting vomiting, Dingchuan, liver-fire drops clearly in lowering the adverse flow of QI, to excessive rising of liver-YANG it Card and liver-fire move blood.
Bin youth, expelling phlegm for arresting cough, the relieving alcoholic intoxication that helps digestion, the chest stuffiness relieving emesis, anthelmintic etc. act on.
Caulis Bambusae In Taenia, sweet in the mouth, cold nature, return lung, stomach, the heart, gallbladder meridian, removing heat-phlegm, relieving restlessness, preventing or arresting vomiting.
Fructus Vitis viniferae is the most delicious and tasty, and nutritive value is the highest, containing mineral calcium, potassium, phosphorus, ferrum and multiple in Fructus Vitis viniferae Vitamin B1, vitamin B2, vitamin B6, vitamin C and Citrin etc., possibly together with the aminoacid of multiple needed by human body, multiple Fruit acid contributes to digestion, suitably eats a little Fructus Vitis viniferae more, can be good for Pi stomach function regulating, and to neurasthenia, overfatigue is of great advantage and has.
The natural tradition medicinal and edible Chinese medicine above with multiple health care is share, Shugan Qingre, dampness removing purging FU-organs, clear Thermal detoxification, emesis, treat bowel dysfunction, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, resisting fatigue it Merit.The proportioning of each component is screened by great many of experiments, scientific and reasonable；And whole preparation technology is reasonable and extract drugs rate efficiency Height, can retain the effective ingredient in raw material well, does not bring any impurity, and sweet mouthfeel into, has no side effect.
The invention has the beneficial effects as follows:
1, the formula of the present invention, has promoting the production of body fluid to quench thirst, gastric acid secretion, helps digest, and health body-building has calm nerves and declines Weak, lessen fatigue, containing various trace elements such as calcium, ferrum, zinc, selenium, sodium etc., raising body immunity, defying age, toxin expelling are supported Face, nourish taste, three-hypers drops, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful, regulates human physiological functions.
2, the present invention is rich in anthocyanidin, it is possible to protection human body is from the damage of free radical, it is possible to strengthens blood vessel elasticity, relax Blood vessel, increases systemic blood circulation, has certain blood pressure reduction effect；Immune system ability can be strengthened, there is strong anti-oxidation, resist Suddenly change, alleviate the function such as hepatosis, protection cardiovascular；
3, add the Chinese herbal medicine such as Cortex Magnoliae Officinalis, Fructus Aurantii Immaturus, Fructus Crataegi, Herba Patriniae, Radix Aucklandiae (Radix Vladimiriae), Herba Taraxaci, Radix Bupleuri, Radix Scutellariae have soothing the liver clearly Heat, dampness removing purging FU-organs, heat-clearing and toxic substances removing, emesis, treat bowel dysfunction, improves body immunity, defying age, eliminating toxin and beautifying the skin, nourishing The function such as taste, resisting fatigue.
4, the products taste that the production technology of the present invention and preparation method draw is sour-sweet tasty and refreshing, rich in dendrobium polysaccharide, has The highest health care and medical value, long-term drink can with YIN nourishing skin care, change skin colour, defying age, life lengthening, and Carrying and drink conveniently, improve self and increase the wriggling of the intestines and stomach, cure the disease and strengthen the beverage of body immunity simultaneously, the shelf-life is up to 1- 2 years.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, in order to those skilled in the art knows more about The present invention, but and it is not so limited the present invention.
Embodiment 1
A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, is made up of the raw material of following weight portion: Radix Et Rhizoma Rhei 10 parts, Cortex Magnoliae Officinalis 10 parts, Fructus Aurantii Immaturus 8 parts, Fructus Crataegi 8 parts, Caulis Sargentodoxae 8 parts, Herba Patriniae 12 parts, Radix Aucklandiae (Radix Vladimiriae) 12 parts, Herba Taraxaci 12 parts, Radix Bupleuri 8 parts, Radix Scutellariae 8 Part, Herba Artemisiae Scopariae 8 parts, Haematitum 8 parts, Bin youth 8 parts, Caulis Bambusae In Taenia 8 parts, 8 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, Mel, water are fitted Amount.
The preparation processing method of a kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, described preparation method includes following Step；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
Fresh for the Herba Dendrobii cleaned up bar is put into microwave oven by B, keeps temperature 50-60 DEG C, carries out heating 10 minutes, further take out Put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content 52 of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time DEG C Chinese liquor, time 15min, the rotating speed of juice extractor is 30r/s；After standing 10 minutes, add the steaming of Herba Dendrobii fresh bar weight 2.5 times Distilled water, for the second time juice extractor time 15min, juice extractor rotating speed is 80r/s, stands 10min；After carry out third time squeeze the juice, add The distilled water of Herba Dendrobii fresh bar weight 3-5 times, time 30min, juice extractor rotating speed is 150r/s, by fresh for Herba Dendrobii bar juice and fiber mistake Filter separate, make the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, broken cell rate reaches more than 80%, obtain new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；Again new fresh grape is put into after the warm water of 55 DEG C cleans up, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated Stand-by；After new fresh grape cleans up, put into reach in freezer ,-10 ~-20 DEG C of freezings 10 minutes, make Fructus Vitis viniferae freeze, take out certainly After so thawing, then carry out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 120 in tank Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 6 times of weight, stirring is smashed to 100 mesh, 30-35 DEG C of temperature Degree lower seal preserves 24h, sterilizing, filters, puts into unglazed hermetically sealed can, obtain Matrix Solution standby；Extract the Fructus Vitis viniferae after Matrix Solution It is the cellulase of 0.5-0.7% that skin and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10, keeps 35 DEG C, water soluble dietary fiber can be extracted after 24h enzymolysis further, water soluble dietary fiber is added Matrix Solution and obtains Matrix Solution II；Rich in anthocyanidin in Pericarpium Vitis viniferae, it is possible to protection human body is from the damage of free radical, it is possible to enhancing blood vessel elasticity, Lax blood vessel, increases systemic blood circulation, has certain blood pressure reduction effect；Immune system ability can be strengthened, there is strong antioxygen Change, mutation, alleviate hepatosis, protection function, Pericarpium Vitis viniferae and the Herba Dendrobii fresh bar fiber such as cardiovascular together with stir smash through Anthocyanidin mentioned by hydromel, can protect the quality of anthocyanidin while farthest extracting anthocyanidin.By water solublity meals Food fiber adds Matrix Solution and obtains Matrix Solution II, can increase effect of the wriggling of the intestines and stomach, it is ensured that metabolic waste is normally discharged External；Adsorbing various metabolic waste, be allowed to normally excrete, the comprehensive utilization value improving Herba Dendrobii improves human body centering simultaneously The absorption of medicine composition.
E, take mix homogeneously after Radix Et Rhizoma Rhei, Caulis Sargentodoxae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, Each 2 hours, merge 2 Radix Et Rhizoma Rhei, Caulis Sargentodoxae ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15- 1.35, prepare Radix Et Rhizoma Rhei, Caulis Sargentodoxae extract standby；
Herba Artemisiae Scopariae, Haematitum, Bin youth, Caulis Bambusae In Taenia being closed stirring and put into super micron mill, super micron mill heating keeps 80 degree of 5-6 of temperature Minute, carry out micronizing and obtain the ultra micro mixing fine powders of 300-400 mesh；
Taking Cortex Magnoliae Officinalis, Fructus Aurantii Immaturus, Fructus Crataegi, Herba Patriniae, Radix Aucklandiae (Radix Vladimiriae), Herba Taraxaci, Radix Bupleuri, Radix Scutellariae, Air Bladder pseudosciaenae seu Acipenser, mix homogeneously adds 30-60 DEG C After warm water soaking 10 minutes, put into reach in freezer ,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, by freezing medicine Block and ultra micro mixing fine powders boiling are extracted 3 times, add 1-2 times amount water for the first time, and temperature keeps 100-120 DEG C, carries out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10 times amount Water, temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, and is concentrated into the 1/2 of original volume, adds Radix Et Rhizoma Rhei, Caulis Sargentodoxae Extract, obtain Matrix Solution III standby；
The hard to bear medicine boiled is pulverized and improves its extract drugs efficiency, make whole formula drug effect farthest be utilized.
F, take Matrix Solution I through instantaneous high-temperature 120 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is: Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；Supercritical extraction can be Extract under room temperature 37 DEG C and CO2 gas blanket, effectively prevent oxidation and the loss of heat-sensitive substance.Therefore, The effective ingredient of medicinal plants is remain in extract, and can be high boiling point, low volatility, the easy material being pyrolyzed the lowest Extract under its boiling temperature；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, and described material-compound tank endobasal-body solution I, matrix are molten Liquid II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae are 10:0.5:6:0.5.Sealing through bottle capper loads in vial, Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning, Carrying and drink conveniently, the shelf-life is up to 1-2.
Embodiment 2
A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, is made up of the raw material of following weight portion: Radix Et Rhizoma Rhei 5 parts, Cortex Magnoliae Officinalis 5 Part, Fructus Aurantii Immaturus 3 parts, Fructus Crataegi 5 parts, Caulis Sargentodoxae 5 parts, Herba Patriniae 10 parts, Radix Aucklandiae (Radix Vladimiriae) 5 parts, Herba Taraxaci 6 parts, Radix Bupleuri 5 parts, Radix Scutellariae 5 parts, Herba Artemisiae Scopariae 5 parts, Haematitum 5 parts, Bin youth 5 parts, Caulis Bambusae In Taenia 5 parts, 5 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are appropriate. Processing method is with embodiment 1.
Embodiment 3
A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, is made up of the raw material of following weight portion: Radix Et Rhizoma Rhei 15 parts, Cortex Magnoliae Officinalis 12 parts, Fructus Aurantii Immaturus 9 parts, Fructus Crataegi 12 parts, Caulis Sargentodoxae 10 parts, Herba Patriniae 16 parts, Radix Aucklandiae (Radix Vladimiriae) 15 parts, Herba Taraxaci 15 parts, Radix Bupleuri 10 parts, yellow A kind of reed mentioned in ancient books 10 parts, Herba Artemisiae Scopariae 10 parts, Haematitum 10 parts, Bin youth 10 parts, Caulis Bambusae In Taenia 10 parts, 10 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20 parts, Mel, water are appropriate.Processing method is with embodiment 1.
Clinical experiment divides three parts:
(1) animal acute toxicity and chronic toxicity experiment:
1, animal acute toxicity test
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 medicated tea add the medicated tea powder paste that rice flour is made.
Experimental animal: regular grade NIH mice, body weight 18g ± 2g, male and female half and half.
Method and result:
By three kinds of each 50g of medicated tea, add rice flour.Experiment mice is randomly divided into three groups of male and female half and half, respectively three kinds of medicated tea of feeding Powder is stuck with paste, volume 1ml/10g body weight, and close observation 8 hours is also noted down, and continues to observe 7 days；In 7 days, mice is without death, OK For vivaciously, food ration is as usual, and hair color light is without loose dirt, without fainting from fear addicted to saliva, and eye, mouth, nose, ear and crissum secretions without exception, Without the rotten toe that docks.5 execution of selection from three groups respectively, finding of naked eye: the important organs such as the heart, liver, lung, gastric and thymus, not See abnormal change, show that two kinds of these nutritive powders are all without acute toxicity.
2, long-term toxicity test for animals
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 gained medicated tea add the medicated tea powder paste that rice flour is made.
Animal: regular grade SD rat, body weight 200g ± 10g, male and female half and half.
Method and result:
The configuration that three kinds of medicated tea powder are stuck with paste: be divided into high, medium and low three dosage groups, respectively the 200 of edible for patients amount, 100, 50g；Experimental mouse is randomly divided into three groups, and the medicated tea powder that feeding modulates continuously respectively is stuck with paste, and continuous feeding 40 days observes animal General toxic reaction and the order of severity, place after death by rule of operation check each position, and carry out hematology, ALT, BUN and the heart, The pathological examination of the main organs such as liver, spleen, lung, kidney, stomach；
Through long-term feeding, all there is not toxic reaction in two groups of rats.Growth promoter is good.Macroscopic appearance and main organs have no Abnormal.Peripheral hemogram and Serum ALT, BUN compare with matched group without pathologic change.The pathological replacement heart, liver, spleen, lung, kidney, stomach Deng the most significant change, it is understood that through proved by pathology, three kinds of medicated tea powder are stuck with paste and showed animal without chronic toxicity.
By two above toxicity test, it was demonstrated that the medicated tea that the present invention is made by embodiment 1, embodiment 2 and embodiment 3 is Safety, have no side effect, can be used to clinical patients is carried out clinical trial.
3, the embodiment of the present invention drinks effect research:
(1) investigation method:
1. crowd is drunk: general population
2. Ganderwa: 45 days
3. number is drunk: 50 people
4. drinking method: 3 times for each person every day, each 300mL
5. index: after drinking, substantially the dampness-heat in the liver and gallbladder stasis of blood is stagnant, internal organs gas loses Jiao, vomiting, mental weariness, appetite in logical fall, damp and hot mutual resistance Depressed transference cure such as grade, and mouthfeel is the most sour-sweet for effective；Drink that the rear dampness-heat in the liver and gallbladder stasis of blood is stagnant, internal organs gas lose burnt in logical fall, damp and hot mutual resistance, The remissions such as vomiting, mental weariness, inappetence, and mouthfeel is the most sour-sweet, is designated as effectively.After drinking without obvious comfort then It is invalid to be designated as.
(2) survey result
Survey result is shown in Table 1.Be test result indicate that by table 1, embodiment 1,2,3 has the respondent of 98% to feel that the present invention is carried The beverage mouthfeel of confession is the most sour-sweet, and above-mentioned clinical symptom disappearance or be eased, the respondent of only 2% drink after without substantially Increase comfort.
The each embodiment of table 1 drinks effect research table
Group/effect Obvious effective rate (number) Effective percentage (number) Inefficiency (number)
Embodiment 1 44%(22) 54%(27) 2%(1)
Embodiment 2 42%(21) 56%(28) 2%(1)
Embodiment 3 42%(21) 56%(28) 2%(1)
Embodiment contrast groups A
Comparative example 4,5,6 is added without the nutrition such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae and becomes Point, according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing is traditional side of boiling Method；The investigation method of using method and using effect is with above.
Table 2 embodiment contrast groups A drinks effect research
Group/effect Obvious effective rate (number) Effective percentage (number) Inefficiency (number)
Comparative example 4 36%(18) 40%(20) 24%(12)
Comparative example 5 40%(20) 40%(20) 20%(10)
Comparative example 6 46%(23) 34%(17) 20%(10)
Embodiment contrast groups B
Comparative example 7,8,9 is added without the nutrition such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae and becomes Point, according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing uses in embodiment 1 The preparation processing method of step E；The investigation method of using method and using effect is with above.
Table 3 embodiment contrast groups B drinks effect research
Group/effect Obvious effective rate (number) Effective percentage (number) Inefficiency (number)
Comparative example 7 32%(16) 56%(28) 12%(6)
Comparative example 8 28%(14) 52%(31) 10%(5)
Comparative example 9 36%(18) 52%(26) 12%(6)
Embodiment contrast groups C
The processing method of comparative example 10,11,12 respectively corresponding embodiment 1,2,3 and formula, different be formula in Without Air Bladder pseudosciaenae seu Acipenser composition；The investigation method of using method and using effect is with above.
Table 4 embodiment contrast groups C drinks effect research
Group/effect Obvious effective rate (number) Effective percentage (number) Inefficiency (number)
Comparative example 10 44%(22) 46%(23) 10%(5)
Comparative example 11 38%(19) 50%(25) 12%(6)
Comparative example 12 40%(20) 48%(24) 12%(6)
Conclusion:
Contrasted by table 2 and table 1 and can be seen that
The inefficient number of embodiment contrast groups A is about 10 times of embodiment 1,2,3；This shows Chinese crude drug formula of the present invention And between the nutritional labeling such as water soluble dietary fiber and Oleum Vitis viniferae, creating the most collaborative pharmacological action, aqueous soluble dietary is fine Dimension increases effect of the wriggling of the intestines and stomach and promotes the human body absorption to ingredient, it is ensured that metabolic waste normally excretes, additionally The anthocyanidin that contains in Pericarpium Vitis viniferae, resveratrol, have strong anti-oxidation, mutation, alleviate hepatosis, protection cardiovascular etc. Function, strengthens immune system ability；Associate with Chinese medicine and improve assimilation effect and improve the mouthfeel of Chinese medicine, through the essence of the present invention simultaneously The extraction of heart configuration and at utmost ingredient, Chinese crude drug formula of the present invention and preparation method occur in that beat all technology Effect.
Table 2 and table 3 contrast can be seen that
About inefficient number is embodiment contrast groups B 2 times of embodiment contrast groups A, embodiment contrast groups B and traditional Embodiment contrast groups A of boiling method has compared significant raising at therapeutic effect, and this shows that Chinese crude drug of the present invention is through step The preparation processing method of rapid E has had significant raising than traditional boiling method, the extraction degree of active ingredient.
Table 1 is compared with table 4:
The formula of embodiment contrast groups C does not contains Air Bladder pseudosciaenae seu Acipenser, and the invalid number of embodiment contrast groups C is 5 times of left sides of embodiment 1,2,3 Right；And effective percentage number has and has declined；Show Air Bladder pseudosciaenae seu Acipenser serve in formula collaborative and priming return through effect, Air Bladder pseudosciaenae seu Acipenser should Unexpected technique effect is achieved by effect.
In sum, a kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea that the present invention provides, Shugan Qingre, dampness removing Purging FU-organs, heat-clearing and toxic substances removing, emesis, treat bowel dysfunction, has sour-sweet mouthfeel, and raising body immunity, defying age, toxin expelling are supported Face, nourish taste, three-hypers drops, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful.And all raw materials is all from medicine food two With natural plants, have no side effect.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For Yuan, under the premise without departing from the principles of the invention, it is also possible to make some improvements and modifications, these improvements and modifications also should It is considered as protection scope of the present invention.

Claims (7)

1. a Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, it is characterised in that be made up of the raw material of following weight portion: raw Radix Et Rhizoma Rhei 5-15 part, Cortex Magnoliae Officinalis 5-12 part, Fructus Aurantii Immaturus 3-9 part, Fructus Crataegi 5-12 part, Caulis Sargentodoxae 5-10 part, Herba Patriniae 10-16 part, Radix Aucklandiae (Radix Vladimiriae) 5-15 part, Herba Taraxaci 6-15 part, Radix Bupleuri 5-10 part, Radix Scutellariae 5-10 part, Herba Artemisiae Scopariae 5-10 part, Haematitum 5-10 part, Bin youth's 5-10 part, Caulis Bambusae In Taenia 5-10 part, Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate.
A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea the most according to claim 1, it is characterised in that by following The raw material of weight portion is made: Radix Et Rhizoma Rhei 10 parts, Cortex Magnoliae Officinalis 10 parts, Fructus Aurantii Immaturus 8 parts, Fructus Crataegi 8 parts, Caulis Sargentodoxae 8 parts, Herba Patriniae 12 parts, wide The Radix Aucklandiae 12 parts, Herba Taraxaci 12 parts, Radix Bupleuri 8 parts, Radix Scutellariae 8 parts, Herba Artemisiae Scopariae 8 parts, Haematitum 8 parts, Bin youth 8 parts, Caulis Bambusae In Taenia 8 parts, Air Bladder pseudosciaenae seu Acipenser 8 Part, new fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, Mel, water are appropriate.
A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea the most according to claim 1, it is characterised in that by following The raw material of weight portion is made: Radix Et Rhizoma Rhei 5 parts, Cortex Magnoliae Officinalis 5 parts, Fructus Aurantii Immaturus 3 parts, Fructus Crataegi 5 parts, Caulis Sargentodoxae 5 parts, Herba Patriniae 10 parts, extensively wood Fragrant 5 parts, Herba Taraxaci 6 parts, Radix Bupleuri 5 parts, Radix Scutellariae 5 parts, Herba Artemisiae Scopariae 5 parts, Haematitum 5 parts, Bin youth 5 parts, Caulis Bambusae In Taenia 5 parts, 5 parts of Air Bladder pseudosciaenae seu Acipenser, new Fresh Herba Dendrobii 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are appropriate.
A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea the most according to claim 1, it is characterised in that by following The raw material of weight portion is made: Radix Et Rhizoma Rhei 15 parts, Cortex Magnoliae Officinalis 12 parts, Fructus Aurantii Immaturus 9 parts, Fructus Crataegi 12 parts, Caulis Sargentodoxae 10 parts, Herba Patriniae 16 parts, Radix Aucklandiae (Radix Vladimiriae) 15 parts, Herba Taraxaci 15 parts, Radix Bupleuri 10 parts, Radix Scutellariae 10 parts, Herba Artemisiae Scopariae 10 parts, Haematitum 10 parts, Bin youth 10 parts, Caulis Bambusae In Taenia 10 Part, 10 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20 parts, Mel, water are appropriate.
5. the preparation processing method of a Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea, it is characterised in that include following step Suddenly；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, then take Go out to put into rotating centrifugal juice extractor, carry out three times and squeeze the juice, add the alcohol content of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time The Chinese liquor of 52-60 DEG C, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, add the fresh bar of Herba Dendrobii The distilled water of weight 2-3 times, for the second time juice extractor time 10-15min, juice extractor rotating speed is 80～100r/s, stands 10min； After carry out third time squeeze the juice, add Herba Dendrobii fresh bar weight 3-5 times distilled water, time 20-30min, juice extractor rotating speed be 100～ 150r/s, separates fresh for Herba Dendrobii bar juice with fiber filter, makes the fiber separation rate of the fresh bar of Herba Dendrobii reach more than 95%, cell damage Rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；The warm water that new fresh grape is put into 50-60 DEG C again cleans dry After Jing, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 in tank Degree, carries out infusion 10 minutes, obtains Matrix Solution I standby；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, in hermetically sealed can, add that to be equivalent to Herba Dendrobii fresh Bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, at 30-35 Seal at a temperature of DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；After extracting Matrix Solution It is the cellulase of 0.5-0.7% that Pericarpium Vitis viniferae and Herba Dendrobii fresh bar fiber add mass volume ratio, adds the water of the mass ratio of 1:10, Keep 35 DEG C, water soluble dietary fiber can be extracted further after 24h enzymolysis, water soluble dietary fiber is added Matrix Solution Obtain Matrix Solution II；
E, take mix homogeneously after Radix Et Rhizoma Rhei, Caulis Sargentodoxae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, every time 2 hours, merge 2 Radix Et Rhizoma Rhei, Caulis Sargentodoxae ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35, Prepare Radix Et Rhizoma Rhei, Caulis Sargentodoxae extract standby；
Herba Artemisiae Scopariae, Haematitum, Bin youth, Caulis Bambusae In Taenia being closed stirring and put into super micron mill, super micron mill heating keeps 80 degree of 5-6 of temperature Minute, carry out micronizing and obtain the ultra micro mixing fine powders of 300-400 mesh；
Taking Cortex Magnoliae Officinalis, Fructus Aurantii Immaturus, Fructus Crataegi, Herba Patriniae, Radix Aucklandiae (Radix Vladimiriae), Herba Taraxaci, Radix Bupleuri, Radix Scutellariae, Air Bladder pseudosciaenae seu Acipenser, mix homogeneously adds 30-60 DEG C After warm water soaking 10 minutes, put into reach in freezer ,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, by freezing medicine Block and ultra micro mixing fine powders boiling are extracted 3 times, add 1-2 times amount water for the first time, and temperature keeps 100-120 DEG C, carries out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10 times amount Water, temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, and is concentrated into the 1/2 of original volume, adds Radix Et Rhizoma Rhei, Caulis Sargentodoxae Extract, obtain Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II through mesh Number be 100 mesh fine filter filter after put into material-compound tank；Take Matrix Solution III again to put into after the fine filter filter that mesh number is 60 mesh In material-compound tank；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is: Extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial, Packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
The preparation processing method of a kind of Shugan Qingre dampness removing purging FU-organs the most according to claim 5 treatment pancreatitis medicated tea, its It is characterised by, step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute, make Fructus Vitis viniferae freezes, and after taking out nature defrosting, then carries out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
The preparation processing method of a kind of Shugan Qingre dampness removing purging FU-organs the most according to claim 5 treatment pancreatitis medicated tea, its Be characterised by, step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, the weight of Oleum Vitis viniferae Proportioning is 10:0.2～0.8:5～10:0.5.
CN201610234299.6A 2016-04-17 2016-04-17 A kind of Shugan Qingre dampness removing purging FU-organs treatment pancreatitis medicated tea and preparation processing method Pending CN106166239A (en)

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103300450A (en) * 2013-06-14 2013-09-18 浙江大学 Preparation method of raw dendrobium officinale pulp beverage

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103300450A (en) * 2013-06-14 2013-09-18 浙江大学 Preparation method of raw dendrobium officinale pulp beverage

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* Cited by examiner, † Cited by third party
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宋芳等: "超临界二氧化碳萃取葡萄籽油及其脂肪酸的分析", 《中国食品工业》 *
李文亮等: "《千家妙方（上册）》", 31 May 1999, 战士出版社 *

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