CN106166268A - One treats qi depression to blood stasis pyloric obstruction medicated tea and preparation processing method - Google Patents
One treats qi depression to blood stasis pyloric obstruction medicated tea and preparation processing method Download PDFInfo
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- CN106166268A CN106166268A CN201610234323.6A CN201610234323A CN106166268A CN 106166268 A CN106166268 A CN 106166268A CN 201610234323 A CN201610234323 A CN 201610234323A CN 106166268 A CN106166268 A CN 106166268A
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Classifications
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Abstract
The one that the invention discloses the present invention treats qi depression to blood stasis pyloric obstruction medicated tea, is made up of the raw material of following weight portion: Pollen Typhae 5 15 parts, Oletum Trogopterori 5 15 parts, the Radix Paeoniae Alba 10 15 parts, Fructus Crataegi 5 12 parts, 5 15 parts of Poria, Pericarpium Citri Reticulatae 39 parts, Rhizoma dioscoreae 5 12 parts, Rhizoma Pinelliae Preparatum 5 10 parts, Fructus Amomi 5 10 parts, Radix Curcumae 10 16 parts, Radix Salviae Miltiorrhizae 5 15 parts, Fructus Citri Sarcodactylis 6 15 parts, Sword Jackbean Seed 5 10 parts, Concha Arcae 5 10 parts, 5 10 parts of Semen Armeniacae Amarum, Exocarpium Citri Rubrum 5 10 parts.The invention have the advantage that inventive formulation treats qi depression to blood stasis pyloric obstruction, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, the merit of resisting fatigue.
Description
Technical field
The present invention relates to one and treat qi depression to blood stasis pyloric obstruction medicated tea, in particular, relate to one and treat qi depression to blood stasis pyloric obstruction herb tea formula and preparation method thereof technical field.
Background technology
Pylorus is the position that digestive tract is the narrowest, normal diameter about 1.5cm, is therefore susceptible to block.Owing to pylorus is by obstacle, gastric content can not enter intestinal smoothly, and in a large amount of retention of gastric, causes coat of the stomach muscle layer plumpness, gastral cavity to expand and the inflammation of gastric mucosa layer, edema and erosion.Can not normally take food for a long time because of patient clinically, and vomit in a large number, cause serious malnutrition, hypoproteinemia and anemia, and have the water and rock-soil coupling such as serious dehydration, low potassium and alkalosis.
General patient has longer ulcer medical history, and with the progress of pathological changes, stomachache gradually increases the weight of, and has the symptom such as belch, regurgitation.Patient's often anorexia because of flatulence, antacid is the most invalid.Stomach is gradually expanded, epigastric fullness, and has mobility enclosed mass.Owing to vomiting number of times increases, dehydration is day by day serious, weight loss.Patient's headache, weak, thirsty, but sitophobia, severe one may occur in which collapse.Owing to gastric juice is lost too much, tetany can occur, even faint from fear.Urine volume day by day reduces, and finally can go into a coma.
The most traditional beverage, only focus on mouthfeel, it is of low nutritive value, not there is treatment qi depression to blood stasis pyloric obstruction medicated tea, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, drop three-hypers, prevent and treat diabetes and anti-cancer, the function of the aspect such as anticancer, the sufferings of client cannot be released, and traditional herbal tea is by Traditional medicine infusion, flavour of a drug weight mouthfeel is poor, it is impossible to preserve for a long time.The most not yet occur a kind of in good taste, improve self and increase the wriggling of the intestines and stomach, cure the disease and strengthen the beverage of body immunity simultaneously.
Summary of the invention
The present invention is directed to the deficiency of existing product, and provide a kind of fresh juice beverage to regulate the effect of human physiological functions, this beverage have be easily absorbed by the human body, medicinal function is notable, delicious flavour, good mouthfeel, improve self and increase the wriggling of the intestines and stomach, curing the disease strengthens the one of the advantages such as body immunity simultaneously and treats qi depression to blood stasis pyloric obstruction medicated tea.
One treats qi depression to blood stasis pyloric obstruction medicated tea, is made up of the raw material of following weight portion: Pollen Typhae 5-15 part, Oletum Trogopterori 5-15 part, Radix Paeoniae Alba 10-15 part, Fructus Crataegi 5-12 part, Poria 5-15 part, Pericarpium Citri Reticulatae 3-9 part, Rhizoma dioscoreae 5-12 part, Rhizoma Pinelliae Preparatum 5-10 part, Fructus Amomi 5-10 part, Radix Curcumae 10-16 part, Radix Salviae Miltiorrhizae 5-15 part, Fructus Citri Sarcodactylis 6-15 part, Sword Jackbean Seed 5-10 part, Concha Arcae 5-10 part, Semen Armeniacae Amarum 5-10 part, Exocarpium Citri Rubrum 5-10 part, Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate.
Described a kind of preparation processing method treating qi depression to blood stasis pyloric obstruction medicated tea, comprises the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, further take out and put into rotating centrifugal juice extractor, carry out three times to squeeze the juice, adding the Chinese liquor of alcohol content 52-60 DEG C of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, adding the distilled water of Herba Dendrobii fresh bar weight 2-3 times, juice extractor time 10-15min for the second time, juice extractor rotating speed is 80～100r/s, stands 10min；After carry out third time squeeze the juice, add the distilled water of Herba Dendrobii fresh bar weight 3-5 times, time 20-30min, juice extractor rotating speed is 100～150r/s, fresh for Herba Dendrobii bar juice is separated with fiber filter, the fiber separation rate making the fresh bar of Herba Dendrobii reaches more than 95%, and broken cell rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；Again new fresh grape is put into after the warm water of 50-60 DEG C cleans up, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 degree, carry out infusion 10 minutes, obtain Matrix Solution I standby in tank；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, add in hermetically sealed can and be equivalent to Herba Dendrobii fresh bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, seal at a temperature of 30-35 DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；Extract the Pericarpium Vitis viniferae after Matrix Solution and Herba Dendrobii fresh bar fiber addition mass volume ratio is the cellulase of 0.5-0.7%, add the water of the mass ratio of 1:10, keep 35 DEG C, water soluble dietary fiber can be extracted after 24h enzymolysis further, water soluble dietary fiber is added Matrix Solution and obtains Matrix Solution II；
E, take mix homogeneously after Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, Radix Curcumae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, each 2 hours, merge 2 Radix Salviae Miltiorrhizaes, Fructus Citri Sarcodactylis, Radix Curcumae ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35, prepare Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, Radix Curcumae extract standby；
Sword Jackbean Seed, Concha Arcae, Fructus Amomi mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing fine powders of 300-400 mesh；
Take Pollen Typhae, Oletum Trogopterori, the Radix Paeoniae Alba, Fructus Crataegi, Poria, Pericarpium Citri Reticulatae, Rhizoma dioscoreae, Rhizoma Pinelliae Preparatum, Semen Armeniacae Amarum, Exocarpium Citri Rubrum, Air Bladder pseudosciaenae seu Acipenser, after mix homogeneously adds 30-60 DEG C of warm water soaking 10 minutes, put into reach in freezer,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, freezing medicine block and ultra micro mixing fine powders boiling are extracted 3 times, adds 1-2 times amount water for the first time, temperature keeps 100-120 DEG C, carries out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10 times amount water, and temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, and is concentrated into the 1/2 of original volume, adds Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, the extract of Radix Curcumae, obtains Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II and put into material-compound tank after the fine filter filter that mesh number is 100 mesh；Take Matrix Solution III again and put into material-compound tank after the fine filter filter that mesh number is 60 mesh；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is: extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial, and packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
Further: step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute, make Fructus Vitis viniferae freeze, take out after nature thaws, then carry out Fructus Vitis viniferae meat and Pericarpium Vitis viniferae detached job.
Further: step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae be 10:0.2～0.8:5～10:0.5.
Pollen Typhae, returns liver, pericardium channel, hemostasis, and blood stasis dispelling is treating stranguria.
Oletum Trogopterori is sweet, temperature, and promoting blood circulation to remove blood stasis is had a pain for trusted subordinate's congestion.
The Radix Paeoniae Alba, suppressing the hyperactive liver pain relieving, nourishing blood for regulating menstruation, astringing YIN to stop sweating.For dizziness of having a headache, hypochondriac pain, stomachache, limb pain twin.
Fructus Crataegi, sour in the mouth is sweet. slightly warm in nature, and return taste Liver Channel, have promoting digestion and removing stagnation, effect of promoting blood circulation to remove blood stasis.
Poria, sweet in the mouth, light, property is put down, GUIXIN, lung, spleen, kidney channel, promoting diuresis to eliminate damp pathogen, spleen invigorating, mind calming.
Pericarpium Citri Reticulatae, bitter in the mouth, pungent, warm in nature.Return lung, spleen channel.Regulating qi-flowing for strengthening spleen, drying dampness to eliminate phlegm.
Rhizoma dioscoreae, nourishes strong, aid digestion, holds back sweating due to debility, effect of antidiarrheal.
Rhizoma Pinelliae Preparatum, returns spleen, stomach, lung meridian, drying dampness to eliminate phlegm, dry laryngopharynx, abundant expectoration cough with asthma, phlegm retention vertigo and palpitation, dizziness due to wind-phlegm, and syncope due to accumulation of phlegm is had a headache.
Fructus Amomi, removing dampness appetizing, warming spleen and stopping diarrha, for turbid damp obstructing in middle-JIAO, gastral cavity painful abdominal mass is the most hungry, Deficiency and coldness of spleen and stomach, and vomiting is had loose bowels.
Radix Curcumae, promoting blood circulation to relieve pain, promoting QI circulation for relieving depression, clear away heart-fire removing heat from blood, the effect of depressed liver-energy dispersing and function of gallbladder promoting, regulates immunity, improves blood circulation, effect of free radical resisting damage.
Radix Salviae Miltiorrhizae, has blood circulation promoting and blood stasis dispelling, inducing menstruation to relieve menalgia, and clear away heart-fire relieving restlessness, effect of removing heat from blood eliminating carbuncle.
Fructus Citri Sarcodactylis, activating QI to eliminate phlegm, preventing or arresting vomiting relieving distension, the liver soothing and the spleen invigorating, stomach function regulating.
Sword Jackbean Seed, sweet in the mouth, property is put down, nontoxic.Semen Canavaliae has that warming the middle warmer and descending qi, preventing or arresting vomiting be inverse, effect of kidney tonifying, can effectively treat after being ill and deficient cold type singultus, vomiting, abdominal distention and the diseases such as caused lumbago of suffering from a deficiency of the kidney.
Concha Arcae, sweet in the mouth;Salty;Property flat, expectorant blood stasis dispelling;Hard masses softening and resolving;Relieving gastric hyperacidity to alleviate stomachache.
Semen Armeniacae Amarum, bitter, tepor, relieving cough and asthma, loosening bowel to relieve constipation, return lung meridian, wind and cold is violated to the cough with asthma card of lung.
Exocarpium Citri Rubrum, gas fragrance, bitter in the mouth, micro-pungent, cold expelling, dampness, promoting the circulation of QI, expectorant.
Natural honey has He Yingwei, moistens internal organs, and logical three is burnt, adjusts effect of taste.
Fructus Vitis viniferae is the most delicious and tasty, and nutritive value is the highest, containing mineral calcium, potassium, phosphorus, ferrum and multivitamin B1, vitamin B2, vitamin B6, vitamin C and Citrin etc. in Fructus Vitis viniferae, aminoacid possibly together with multiple needed by human body, multiple fruit acid contributes to digestion, suitably eating a little Fructus Vitis viniferae more, can be good for Pi stomach function regulating, to neurasthenia, overfatigue is of great advantage and has.
The natural tradition medicinal and edible Chinese medicine above with multiple health care is share, treats qi depression to blood stasis pyloric obstruction medicated tea, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, the merit of resisting fatigue.The proportioning of each component is screened by great many of experiments, scientific and reasonable；And whole preparation technology is rationally and extract drugs rate efficiency is high, can retain the effective ingredient in raw material well, not bring any impurity, and sweet mouthfeel into, have no side effect.
The invention has the beneficial effects as follows:
1, the formula of the present invention, there is promoting the production of body fluid to quench thirst, gastric acid secretion, help digest, health body-building, there is calm nerves weak, lessen fatigue, containing various trace elements such as calcium, ferrum, zinc, selenium, sodium etc., to improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, three-hypers drops, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful, regulates human physiological functions.
2, the present invention is rich in anthocyanidin, it is possible to protection human body is from the damage of free radical, it is possible to strengthens blood vessel elasticity, lax blood vessel, increases systemic blood circulation, have certain blood pressure reduction effect；Immune system ability can be strengthened, there is strong anti-oxidation, mutation, alleviate the function such as hepatosis, protection cardiovascular；
3, add the Chinese herbal medicine such as Pollen Typhae, Oletum Trogopterori, the Radix Paeoniae Alba, Fructus Crataegi, Poria, Pericarpium Citri Reticulatae, Rhizoma dioscoreae, Rhizoma Pinelliae Preparatum, Semen Armeniacae Amarum, Exocarpium Citri Rubrum and there is treatment qi depression to blood stasis pyloric obstruction medicated tea, improve the functions such as body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, resisting fatigue.
4, the products taste that the production technology of the present invention and preparation method draw is sour-sweet tasty and refreshing, rich in dendrobium polysaccharide, there is the highest health care and medical value, long-term drink can be with YIN nourishing skin care, change skin colour, defying age, life lengthening, and carry and drink conveniently, improving self and increase the wriggling of the intestines and stomach, cure the disease and strengthen the beverage of body immunity simultaneously, the shelf-life is up to 1-2.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, in order to those skilled in the art knows more about the present invention, but and is not so limited the present invention.
Embodiment 1
One treats qi depression to blood stasis pyloric obstruction medicated tea, is made up of the raw material of following weight portion: Herba Plantaginis 10 parts, Spica Prunellae 10 parts, Radix Bupleuri 12 parts, the Radix Paeoniae Alba 10 parts, Fructus Aurantii Immaturus 10 parts, Fructus Crataegi 8 parts, Radix Curcumae 10 parts, Cortex Magnoliae Officinalis 8 parts, Mirabilitum crystallina 8 parts, 12 parts of Radix Glycyrrhizae, Pericarpium Citri Reticulatae 12 parts, Bulbus Lilii 12 parts, Caulis Spatholobi 8 parts, Radix Codonopsis 8 parts, the Rhizoma Atractylodis Macrocephalae 8 parts, 8 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, Mel, water are appropriate.
A kind of preparation processing method treating qi depression to blood stasis pyloric obstruction medicated tea, described preparation method comprises the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
Fresh for the Herba Dendrobii cleaned up bar is put into microwave oven by B, keep temperature 50-60 DEG C, carry out heating 10 minutes, further take out and put into rotating centrifugal juice extractor, carry out three times to squeeze the juice, adding the Chinese liquor of the alcohol content 52 DEG C of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time, time 15min, the rotating speed of juice extractor is 30r/s；After standing 10 minutes, adding the distilled water of Herba Dendrobii fresh bar weight 2.5 times, juice extractor time 15min for the second time, juice extractor rotating speed is 80r/s, stands 10min；After carry out third time squeeze the juice, add the distilled water of Herba Dendrobii fresh bar weight 3-5 times, time 30min, juice extractor rotating speed is 150r/s, fresh for Herba Dendrobii bar juice is separated with fiber filter, the fiber separation rate making the fresh bar of Herba Dendrobii reaches more than 95%, and broken cell rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；Again new fresh grape is put into after the warm water of 55 DEG C cleans up, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；After new fresh grape cleans up, put into reach in freezer ,-10 ~-20 DEG C of freezings 10 minutes, make Fructus Vitis viniferae freeze, after taking out nature defrosting, then carry out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 120 degree, carry out infusion 10 minutes, obtain Matrix Solution I standby in tank；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, add in hermetically sealed can and be equivalent to Herba Dendrobii fresh bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 6 times of weight, stirring is smashed to 100 mesh, seal at a temperature of 30-35 DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；Extract the Pericarpium Vitis viniferae after Matrix Solution and Herba Dendrobii fresh bar fiber addition mass volume ratio is the cellulase of 0.5-0.7%, add the water of the mass ratio of 1:10, keep 35 DEG C, water soluble dietary fiber can be extracted after 24h enzymolysis further, water soluble dietary fiber is added Matrix Solution and obtains Matrix Solution II；；Rich in anthocyanidin in Pericarpium Vitis viniferae, it is possible to protection human body is from the damage of free radical, it is possible to strengthen blood vessel elasticity, lax blood vessel, increase systemic blood circulation, there is certain blood pressure reduction effect；Immune system ability can be strengthened; there is strong anti-oxidation, mutation, alleviate the function such as hepatosis, protection cardiovascular; stir to smash together with Pericarpium Vitis viniferae bar fresh with Herba Dendrobii fiber and mention anthocyanidin through hydromel, while farthest extracting anthocyanidin, can protect the quality of anthocyanidin.Water soluble dietary fiber is added Matrix Solution and obtains Matrix Solution II, effect of the wriggling of the intestines and stomach can be increased, it is ensured that metabolic waste normally excretes；Adsorbing various metabolic waste, be allowed to normally excrete, the comprehensive utilization value improving Herba Dendrobii improves the human body absorption to Chinese medicine ingredients simultaneously.
E, take mix homogeneously after Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, Radix Curcumae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, each 2 hours, merge 2 Radix Salviae Miltiorrhizaes, Fructus Citri Sarcodactylis, Radix Curcumae ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35, prepare Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, Radix Curcumae extract standby；
Sword Jackbean Seed, Concha Arcae, Fructus Amomi mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing fine powders of 300-400 mesh；
Take Pollen Typhae, Oletum Trogopterori, the Radix Paeoniae Alba, Fructus Crataegi, Poria, Pericarpium Citri Reticulatae, Rhizoma dioscoreae, Rhizoma Pinelliae Preparatum, Semen Armeniacae Amarum, Exocarpium Citri Rubrum, Air Bladder pseudosciaenae seu Acipenser, after mix homogeneously adds 30-60 DEG C of warm water soaking 10 minutes, put into reach in freezer,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, freezing medicine block and ultra micro mixing fine powders boiling are extracted 3 times, adds 1-2 times amount water for the first time, temperature keeps 100-120 DEG C, carries out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10 times amount water, and temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, and is concentrated into the 1/2 of original volume, adds Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, the extract of Radix Curcumae, obtains Matrix Solution III standby；
The hard to bear medicine boiled is pulverized and improves its extract drugs efficiency, make whole formula drug effect farthest be utilized.
F, take Matrix Solution I through instantaneous high-temperature 120 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II and put into material-compound tank after the fine filter filter that mesh number is 100 mesh；Take Matrix Solution III again and put into material-compound tank after the fine filter filter that mesh number is 60 mesh；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is: extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；Supercritical extraction can extract under room temperature 37 DEG C and CO2 gas blanket, effectively prevent oxidation and the loss of heat-sensitive substance.Therefore, extract remains the effective ingredient of medicinal plants, and high boiling point, low volatility, the material of easily pyrolysis can be extracted under far below its boiling temperature；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, and described material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae are 10:0.5:6:0.5., sealing through bottle capper and load in vial, packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning, carries and drinks conveniently, and the shelf-life is up to 1-2.
Embodiment 2
One treats qi depression to blood stasis pyloric obstruction medicated tea, is made up of the raw material of following weight portion: Pollen Typhae 15 parts, Oletum Trogopterori 15 parts, the Radix Paeoniae Alba 15 parts, Fructus Crataegi 12 parts, 15 parts of Poria, Pericarpium Citri Reticulatae 9 parts, Rhizoma dioscoreae 12 parts, Rhizoma Pinelliae Preparatum 10 parts, Fructus Amomi 10 parts, Radix Curcumae 16 parts, Radix Salviae Miltiorrhizae 15 parts, Fructus Citri Sarcodactylis 15 parts, Sword Jackbean Seed 10 parts, Concha Arcae 10 parts, 10 parts of Semen Armeniacae Amarum, Exocarpium Citri Rubrum 10 parts, 5 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are appropriate.Processing method is with embodiment 1.
Embodiment 3
One treats qi depression to blood stasis pyloric obstruction medicated tea, is made up of the raw material of following weight portion: Pollen Typhae 5 parts, Oletum Trogopterori 5 parts, the Radix Paeoniae Alba 10 parts, Fructus Crataegi 5 parts, 5 parts of Poria, Pericarpium Citri Reticulatae 3 parts, Rhizoma dioscoreae 5 parts, Rhizoma Pinelliae Preparatum 5 parts, Fructus Amomi 5 parts, Radix Curcumae 10 parts, Radix Salviae Miltiorrhizae 5 parts, Fructus Citri Sarcodactylis 6 parts, Sword Jackbean Seed 5 parts, Concha Arcae 5 parts, 5 parts of Semen Armeniacae Amarum, Exocarpium Citri Rubrum 5 parts, 10 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20 parts, Mel, water are appropriate.Processing method is with embodiment 1.
Clinical experiment divides three parts:
(1) animal acute toxicity and chronic toxicity experiment:
1, animal acute toxicity test
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 medicated tea add the medicated tea powder paste that rice flour is made.
Experimental animal: regular grade NIH mice, body weight 18g ± 2g, male and female half and half.
Method and result:
By three kinds of each 50g of medicated tea, add rice flour.Experiment mice is randomly divided into three groups of male and female half and half, and three kinds of medicated tea powder of feeding are stuck with paste respectively, volume 1ml/10g
Body weight, close observation 8 hours is also noted down, and continues to observe 7 days；In 7 days, mice is without death, and behavior is active, and food ration is as usual, and hair color light is without loose dirt, and without fainting from fear addicted to saliva, eye, mouth, nose, ear and crissum secretions without exception, without the rotten toe that docks.Selecting 5 execution, finding of naked eye: the important organs such as the heart, liver, lung, gastric and thymus respectively from three groups, no abnormality seen changes, shows that two kinds of these nutritive powders are all without acute toxicity.
2, long-term toxicity test for animals
Medicine: the embodiment of the present invention 1, embodiment 2 and embodiment 3 gained medicated tea add the medicated tea powder paste that rice flour is made.
Animal: regular grade SD rat, body weight 200g ± 10g, male and female half and half.
Method and result:
The configuration that three kinds of medicated tea powder are stuck with paste: be divided into high, medium and low three dosage groups, respectively the 200 of edible for patients amount, 100,50g；Experimental mouse is randomly divided into three groups, the medicated tea powder that feeding modulates continuously respectively is stuck with paste, feeding 40 days continuously, observe animal general toxic reaction and the order of severity, place after death checks each position by rule of operation, and carries out the pathological examination of the main organs such as hematology, ALT, BUN and the heart, liver, spleen, lung, kidney, stomach；
Through long-term feeding, all there is not toxic reaction in two groups of rats.Growth promoter is good.Macroscopic appearance and main organs no abnormality seen.Peripheral hemogram and Serum ALT, BUN compare with matched group without pathologic change.The most significant changes such as the pathological replacement heart, liver, spleen, lung, kidney, stomach, it is understood that through proved by pathology, three kinds of medicated tea powder are stuck with paste and are showed animal without chronic toxicity.
By two above toxicity test, it was demonstrated that the medicated tea that the present invention is made by embodiment 1, embodiment 2 and embodiment 3 is safe, has no side effect, can be used to clinical patients is carried out clinical trial.
3, the embodiment of the present invention drinks effect research:
(1) investigation method:
1. crowd is drunk: general population
2. Ganderwa: 30 days
3. number is drunk: 50 people
4. drinking method: 3 times for each person every day, ante cibum each 500mL
5. index: after drinking substantially inappetence, vomiting, abdominal distention, qi depression to blood stasis, the bodily form become thin, the transference cure such as inappetence, and mouthfeel is the most sour-sweet for effective；Drink rear inappetence, the remission such as vomiting, abdominal distention, qi depression to blood stasis, the bodily form are become thin, inappetence, and mouthfeel is the most sour-sweet, is designated as effectively.It is invalid to be then designated as without obvious comfort after drinking.
(2) survey result
Survey result is shown in Table 1.Be test result indicate that by table 1, embodiment 1,2,3 have the respondent of 98% to feel beverage mouthfeel provided by the present invention is the most sour-sweet, and above-mentioned clinical symptom disappearance or be eased, the respondent of only 2% drink after without substantially increasing comfort.
The each embodiment of table 1 drinks effect research table
| Group/ Effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Embodiment 1 | 44%(22) | 54%(27) | 2%(1) |
| Embodiment 2 | 42%(21) | 56%(28) | 2%(1) |
| Embodiment 3 | 42%(21) | 56%(28) | 2%(1) |
Embodiment contrast groups A
Comparative example 4,5,6 is added without the nutritional labelings such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae, and according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing is traditional boiling method；The investigation method of using method and using effect is with above.
Table 2 embodiment contrast groups A drinks effect research
| Group/ Effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 4 | 36%(18) | 40%(20) | 24%(12) |
| Comparative example 5 | 40%(20) | 40%(20) | 20%(10) |
| Comparative example 6 | 46%(23) | 34%(17) | 20%(10) |
Embodiment contrast groups B
Comparative example 7,8,9 is added without the nutritional labelings such as new fresh Herba Dendrobii, Fructus Vitis viniferae, Mel, water soluble dietary fiber and Oleum Vitis viniferae, according to the raw material that the Chinese medicine part of embodiment 1,2,3 above is original, preparation for processing uses the preparation processing method of step E in embodiment 1；The investigation method of using method and using effect is with above.
Table 3 embodiment contrast groups B drinks effect research
| Group/ Effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 7 | 32%(16) | 56%(28) | 12%(6) |
| Comparative example 8 | 28%(14) | 52%(31) | 10%(5) |
| Comparative example 9 | 36%(18) | 52%(26) | 12%(6) |
Embodiment contrast groups C
The processing method of the most corresponding embodiment 1,2,3 of comparative example 10,11,12 and formula, different is that formula is interior without Air Bladder pseudosciaenae seu Acipenser composition；The investigation method of using method and using effect is with above.
Table 4 embodiment contrast groups C drinks effect research
| Group/ Effect | Obvious effective rate (number) | Effective percentage (number) | Inefficiency (number) |
| Comparative example 10 | 44%(22) | 46%(23) | 10%(5) |
| Comparative example 11 | 38%(19) | 50%(25) | 12%(6) |
| Comparative example 12 | 40%(20) | 48%(24) | 12%(6) |
Conclusion:
Contrasted by table 2 and table 1 and can be seen that
The inefficient number of embodiment contrast groups A is about 10 times of embodiment 1,2,3；This shows to create the most collaborative pharmacological action between Chinese crude drug formula of the present invention and the nutritional labeling such as water soluble dietary fiber and Oleum Vitis viniferae; water soluble dietary fiber increases effect of the wriggling of the intestines and stomach and promotes the human body absorption to ingredient; ensure that metabolic waste normally excretes; the anthocyanidin that additionally contains in Pericarpium Vitis viniferae, resveratrol; there is strong anti-oxidation, mutation, alleviate the function such as hepatosis, protection cardiovascular, strengthen immune system ability；Associating with Chinese medicine and improve assimilation effect and improve the mouthfeel of Chinese medicine simultaneously, through the configuration meticulously of the present invention and the extraction of at utmost ingredient, Chinese crude drug formula of the present invention and preparation method occur in that beat all technique effect.
Table 2 and table 3 contrast can be seen that
About inefficient number is embodiment contrast groups B 2 times of embodiment contrast groups A, embodiment contrast groups B has compared significant raising with embodiment contrast groups A of traditional boiling method at therapeutic effect, this shows that Chinese crude drug of the present invention has had significant raising through the preparation processing method of step E than traditional boiling method, the extraction degree of active ingredient.
Table 1 is compared with table 4:
The formula of embodiment contrast groups C does not contains Air Bladder pseudosciaenae seu Acipenser, and the invalid number of embodiment contrast groups C is about 5 times of embodiment 1,2,3；And effective percentage number has and has declined；Air Bladder pseudosciaenae seu Acipenser can strengthen gastrointestinal digestive and absorptive functions, improve appetite, be conducive to preventing and treating the diseases such as inappetence, anorexia, dyspepsia, abdominal distention, constipation, show Air Bladder pseudosciaenae seu Acipenser serve in formula collaborative and priming return through effect,, Air Bladder pseudosciaenae seu Acipenser application effect achieves unexpected technique effect.
In sum, the one that the present invention provides treats qi depression to blood stasis pyloric obstruction medicated tea, treatment qi depression to blood stasis pyloric obstruction medicated tea, has a sour-sweet mouthfeel, improve body immunity, defying age, eliminating toxin and beautifying the skin, nourishing taste, three-hypers drops, to prevent and treat diabetes and anti-cancer, the aspect such as anticancer the most powerful.And all raw materials is all from medicine-food two-purpose natural plants, have no side effect.
The above is only the preferred embodiment of the present invention; it should be pointed out that, for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications also should be regarded as protection scope of the present invention.
Claims (7)
1. a treatment qi depression to blood stasis pyloric obstruction medicated tea, it is characterized in that, be made up of the raw material of following weight portion: Pollen Typhae 5-15 part, Oletum Trogopterori 5-15 part, Radix Paeoniae Alba 10-15 part, Fructus Crataegi 5-12 part, Poria 5-15 part, Pericarpium Citri Reticulatae 3-9 part, Rhizoma dioscoreae 5-12 part, Rhizoma Pinelliae Preparatum 5-10 part, Fructus Amomi 5-10 part, Radix Curcumae 10-16 part, Radix Salviae Miltiorrhizae 5-15 part, Fructus Citri Sarcodactylis 6-15 part, Sword Jackbean Seed 5-10 part, Concha Arcae 5-10 part, Semen Armeniacae Amarum 5-10 part, Exocarpium Citri Rubrum 5-10 part, Air Bladder pseudosciaenae seu Acipenser 5-10 part, new fresh Herba Dendrobii 10-20 part, Fructus Vitis viniferae 10-20 part, Mel, water are appropriate.
One the most according to claim 1 treats qi depression to blood stasis pyloric obstruction medicated tea, it is characterized in that, be made up of the raw material of following weight portion: Pollen Typhae 10 parts, Oletum Trogopterori 10 parts, the Radix Paeoniae Alba 10 parts, Fructus Crataegi 8 parts, 8 parts of Poria, Pericarpium Citri Reticulatae 8 parts, Rhizoma dioscoreae 8 parts, Rhizoma Pinelliae Preparatum 6 parts, Fructus Amomi 8 parts, Radix Curcumae 12 parts, Radix Salviae Miltiorrhizae 12 parts, Fructus Citri Sarcodactylis 12 parts, Sword Jackbean Seed 8 parts, Concha Arcae 8 parts, 8 parts of Semen Armeniacae Amarum, Exocarpium Citri Rubrum 8 parts, 8 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 15 parts, Fructus Vitis viniferae 15 parts, Mel, water are appropriate.
One the most according to claim 1 treats qi depression to blood stasis pyloric obstruction medicated tea, it is characterized in that, be made up of the raw material of following weight portion: Pollen Typhae 5 parts, Oletum Trogopterori 5 parts, the Radix Paeoniae Alba 10 parts, Fructus Crataegi 5 parts, 5 parts of Poria, Pericarpium Citri Reticulatae 3 parts, Rhizoma dioscoreae 5 parts, Rhizoma Pinelliae Preparatum 5 parts, Fructus Amomi 5 parts, Radix Curcumae 10 parts, Radix Salviae Miltiorrhizae 5 parts, Fructus Citri Sarcodactylis 6 parts, Sword Jackbean Seed 5 parts, Concha Arcae 5 parts, 5 parts of Semen Armeniacae Amarum, Exocarpium Citri Rubrum 5 parts, 5 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 10 parts, Fructus Vitis viniferae 10 parts, Mel, water are appropriate.
One the most according to claim 1 treats qi depression to blood stasis pyloric obstruction medicated tea, it is characterized in that, be made up of the raw material of following weight portion: Pollen Typhae 15 parts, Oletum Trogopterori 15 parts, the Radix Paeoniae Alba 15 parts, Fructus Crataegi 12 parts, 15 parts of Poria, Pericarpium Citri Reticulatae 9 parts, Rhizoma dioscoreae 12 parts, Rhizoma Pinelliae Preparatum 10 parts, Fructus Amomi 10 parts, Radix Curcumae 16 parts, Radix Salviae Miltiorrhizae 15 parts, Fructus Citri Sarcodactylis 15 parts, Sword Jackbean Seed 10 parts, Concha Arcae 10 parts, 10 parts of Semen Armeniacae Amarum, Exocarpium Citri Rubrum 10 parts, 10 parts of Air Bladder pseudosciaenae seu Acipenser, new fresh Herba Dendrobii 20 parts, Fructus Vitis viniferae 20 parts, Mel, water are appropriate.
5. the preparation processing method treating qi depression to blood stasis pyloric obstruction medicated tea, it is characterised in that comprise the following steps；
A, fresh for Herba Dendrobii bar is put into service sink, remove surface clay stain, the fresh bar of screening high-quality Herba Dendrobii, dry standby；
B, fresh for the Herba Dendrobii cleaned up bar is put into microwave oven, keep temperature 50-60 DEG C, carry out heating 10 minutes, further take out and put into rotating centrifugal juice extractor, carry out three times to squeeze the juice, adding the Chinese liquor of alcohol content 52-60 DEG C of Herba Dendrobii fresh bar weight 0.1-0.5 times for the first time, time 10-15min, the rotating speed of juice extractor is 20～30r/s；After standing 10 minutes, adding the distilled water of Herba Dendrobii fresh bar weight 2-3 times, juice extractor time 10-15min for the second time, juice extractor rotating speed is 80～100r/s, stands 10min；After carry out third time squeeze the juice, add the distilled water of Herba Dendrobii fresh bar weight 3-5 times, time 20-30min, juice extractor rotating speed is 100～150r/s, fresh for Herba Dendrobii bar juice is separated with fiber filter, the fiber separation rate making the fresh bar of Herba Dendrobii reaches more than 95%, and broken cell rate reaches more than 80%, obtains new fresh Herba Dendrobii juice and Herba Dendrobii fresh bar fiber；Again new fresh grape is put into after the warm water of 50-60 DEG C cleans up, Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae are separated stand-by；
C, Herba Dendrobii fresh bar juice is put into and is put in pressure pan with Fructus Vitis viniferae meat, keeps pressure 0.5MP, temperature to keep 100-150 degree, carry out infusion 10 minutes, obtain Matrix Solution I standby in tank；
D, fresh for the Herba Dendrobii of separation bar fiber and Pericarpium Vitis viniferae are put into unglazed hermetically sealed can, add in hermetically sealed can and be equivalent to Herba Dendrobii fresh bar fiber and the Mel of Pericarpium Vitis viniferae gross weight 20-30% and the distilled water of 5-10 times of weight, stirring is smashed to 100 mesh, seal at a temperature of 30-35 DEG C and preserve 24h, sterilizing, filter, put into unglazed hermetically sealed can, obtain Matrix Solution standby；Extract the Pericarpium Vitis viniferae after Matrix Solution and Herba Dendrobii fresh bar fiber addition mass volume ratio is the cellulase of 0.5-0.7%, add the water of the mass ratio of 1:10, keep 35 DEG C, water soluble dietary fiber can be extracted after 24h enzymolysis further, water soluble dietary fiber is added Matrix Solution and obtains Matrix Solution II；
E, take mix homogeneously after Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, Radix Curcumae cleaning and sterilizing, respectively with 6 times of weight 85% mol ratio ethanol extractions 2 times, each 2 hours, merge 2 Radix Salviae Miltiorrhizaes, Fructus Citri Sarcodactylis, Radix Curcumae ethanol extracts, receive alcohol and to be evaporated to relative density at 40 DEG C be 1.15-1.35, prepare Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, Radix Curcumae extract standby；
Sword Jackbean Seed, Concha Arcae, Fructus Amomi mix and blend are put into super micron mill, carries out micronizing and obtain the ultra micro mixing fine powders of 300-400 mesh；
Take Pollen Typhae, Oletum Trogopterori, the Radix Paeoniae Alba, Fructus Crataegi, Poria, Pericarpium Citri Reticulatae, Rhizoma dioscoreae, Rhizoma Pinelliae Preparatum, Semen Armeniacae Amarum, Exocarpium Citri Rubrum, Air Bladder pseudosciaenae seu Acipenser, after mix homogeneously adds 30-60 DEG C of warm water soaking 10 minutes, put into reach in freezer,-10～-20 DEG C freezing 10-20 minute, form freezing medicine block, freezing medicine block and ultra micro mixing fine powders boiling are extracted 3 times, adds 1-2 times amount water for the first time, temperature keeps 100-120 DEG C, carries out infusion 10-20 minute；Second time adds 4-6 times amount water, and temperature keeps 80-100 DEG C, carries out infusion 10 minutes；Third time adds 6-10 times amount water, and temperature keeps 120-150 DEG C, carries out infusion 30 minutes, filters, and is concentrated into the 1/2 of original volume, adds Radix Salviae Miltiorrhizae, Fructus Citri Sarcodactylis, the extract of Radix Curcumae, obtains Matrix Solution III standby；
F, take Matrix Solution I through instantaneous high-temperature 110-130 DEG C, 1-2 minute, put into material-compound tank；Take Matrix Solution II and put into material-compound tank after the fine filter filter that mesh number is 100 mesh；Take Matrix Solution III again and put into material-compound tank after the fine filter filter that mesh number is 60 mesh；
G, by Semen Vitis viniferae through vacuum outgas, then use CO2 supercritical fluid extraction, the condition of CO2 supercritical fluid extraction is: extracting pressure 45MPa, extraction temperature 35-45 DEG C, extraction time 30min, isolated Oleum Vitis viniferae；
H, three kinds of Matrix Solutions are stirring evenly and then adding into Oleum Vitis viniferae at material-compound tank, seal through bottle capper and load in vial, and packaged vial puts into temperature 100～120 DEG C, 1.5MP, sterilization in 15～21 minutes steam ovens, packaging, vanning.
A kind of preparation processing method treating qi depression to blood stasis pyloric obstruction medicated tea the most according to claim 5, it is characterized in that, step B) in, after new fresh grape cleans up, put into reach in freezer ,-10～-20 DEG C freezing 5-10 minute, make Fructus Vitis viniferae freeze, after taking out nature defrosting, then carry out Fructus Vitis viniferae meat, Pericarpium Vitis viniferae, Semen Vitis viniferae detached job.
A kind of preparation processing method treating qi depression to blood stasis pyloric obstruction medicated tea the most according to claim 5, it is characterized in that, step H) described in material-compound tank endobasal-body solution I, Matrix Solution II, Matrix Solution III, the weight proportion of Oleum Vitis viniferae be 10:0.2～0.8:5～10:0.5.
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| 宋芳等: "超临界二氧化碳萃取葡萄籽油及其脂肪酸的分析", 《中国食品工业》 * |
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Application publication date: 20161130 |