DE69629845D1 - Rückgewinnung von Nickel und/oder Kobalt durch Auslaugen von hydroxidhaltigem Konzentrat mit einer Ammonium-Lösung - Google Patents

Rückgewinnung von Nickel und/oder Kobalt durch Auslaugen von hydroxidhaltigem Konzentrat mit einer Ammonium-Lösung

Info

Publication number
DE69629845D1
DE69629845D1 DE69629845T DE69629845T DE69629845D1 DE 69629845 D1 DE69629845 D1 DE 69629845D1 DE 69629845 T DE69629845 T DE 69629845T DE 69629845 T DE69629845 T DE 69629845T DE 69629845 D1 DE69629845 D1 DE 69629845D1
Authority
DE
Germany
Prior art keywords
leaching
cobalt
nickel
hydroxide
recovery
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69629845T
Other languages
English (en)
Other versions
DE69629845T2 (de
Inventor
David L Jones
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CESL Ltd
Original Assignee
CESL Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CESL Ltd filed Critical CESL Ltd
Publication of DE69629845D1 publication Critical patent/DE69629845D1/de
Application granted granted Critical
Publication of DE69629845T2 publication Critical patent/DE69629845T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/10—Hydrochloric acid, other halogenated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00—Obtaining noble metals
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00—Obtaining copper
    • C22B15/0063—Hydrometallurgy
    • C22B15/0065—Leaching or slurrying
    • C22B15/0067—Leaching or slurrying with acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00—Obtaining copper
    • C22B15/0063—Hydrometallurgy
    • C22B15/0065—Leaching or slurrying
    • C22B15/0067—Leaching or slurrying with acids or salts thereof
    • C22B15/0069—Leaching or slurrying with acids or salts thereof containing halogen
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00—Obtaining copper
    • C22B15/0063—Hydrometallurgy
    • C22B15/0065—Leaching or slurrying
    • C22B15/0067—Leaching or slurrying with acids or salts thereof
    • C22B15/0071—Leaching or slurrying with acids or salts thereof containing sulfur
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00—Obtaining copper
    • C22B15/0063—Hydrometallurgy
    • C22B15/0084—Treating solutions
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00—Obtaining copper
    • C22B15/0063—Hydrometallurgy
    • C22B15/0084—Treating solutions
    • C22B15/0089—Treating solutions by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B19/00—Obtaining zinc or zinc oxide
    • C22B19/20—Obtaining zinc otherwise than by distilling
    • C22B19/22—Obtaining zinc otherwise than by distilling with leaching with acids
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B19/00—Obtaining zinc or zinc oxide
    • C22B19/20—Obtaining zinc otherwise than by distilling
    • C22B19/26—Refining solutions containing zinc values, e.g. obtained by leaching zinc ores
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/0423—Halogenated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/043—Sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/08—Sulfuric acid, other sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
    • C22B3/384—Pentavalent phosphorus oxyacids, esters thereof
    • C22B3/3842—Phosphinic acid, e.g. H2P(O)(OH)
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Extraction Or Liquid Replacement (AREA)
DE1996629845 1995-06-07 1996-06-07 Rückgewinnung von Nickel und/oder Kobalt durch Auslaugen von hydroxidhaltigem Konzentrat mit einer Ammonium-Lösung Expired - Fee Related DE69629845T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US488128 1995-06-07
US08/488,128 US5650057A (en) 1993-07-29 1995-06-07 Chloride assisted hydrometallurgical extraction of metal

Publications (2)

Publication Number Publication Date
DE69629845D1 true DE69629845D1 (de) 2003-10-09
DE69629845T2 DE69629845T2 (de) 2004-07-08

Family

ID=23938434

Family Applications (5)

Application Number Title Priority Date Filing Date
DE1996610208 Expired - Lifetime DE69610208T2 (de) 1995-06-07 1996-01-04 Chloridunterstützte hydrometallurgische extraktion von nickel und kobalt
DE1996612617 Expired - Lifetime DE69612617T2 (de) 1995-06-07 1996-01-19 Chloridunterstützte hydrometallurgische metallextraktion
DE69626048T Expired - Lifetime DE69626048D1 (de) 1995-06-07 1996-06-07 Füssig-flüssig-Extraktion von Kobalt und Nickel aus einer magnesiumhaltigen Lösung
DE1996629845 Expired - Fee Related DE69629845T2 (de) 1995-06-07 1996-06-07 Rückgewinnung von Nickel und/oder Kobalt durch Auslaugen von hydroxidhaltigem Konzentrat mit einer Ammonium-Lösung
DE1996606036 Expired - Fee Related DE69606036T2 (de) 1995-06-07 1996-06-07 Chloridunterstützte hydrometallurgische extraktion von nickel und kobalt aus sulphiderzen

Family Applications Before (3)

Application Number Title Priority Date Filing Date
DE1996610208 Expired - Lifetime DE69610208T2 (de) 1995-06-07 1996-01-04 Chloridunterstützte hydrometallurgische extraktion von nickel und kobalt
DE1996612617 Expired - Lifetime DE69612617T2 (de) 1995-06-07 1996-01-19 Chloridunterstützte hydrometallurgische metallextraktion
DE69626048T Expired - Lifetime DE69626048D1 (de) 1995-06-07 1996-06-07 Füssig-flüssig-Extraktion von Kobalt und Nickel aus einer magnesiumhaltigen Lösung

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE1996606036 Expired - Fee Related DE69606036T2 (de) 1995-06-07 1996-06-07 Chloridunterstützte hydrometallurgische extraktion von nickel und kobalt aus sulphiderzen

Country Status (23)

Country Link
US (1) US5650057A (de)
EP (5) EP0832302B1 (de)
JP (3) JP4180655B2 (de)
KR (1) KR100426231B1 (de)
CN (3) CN1057344C (de)
AU (3) AU694960C (de)
BG (3) BG62178B1 (de)
BR (3) BR9608624A (de)
CA (6) CA2221930C (de)
DE (5) DE69610208T2 (de)
DK (3) DK0832302T3 (de)
ES (3) ES2153950T3 (de)
FI (2) FI116905B (de)
GT (2) GT199600014A (de)
NO (1) NO975707L (de)
OA (1) OA10643A (de)
PE (2) PE30096A1 (de)
PL (3) PL323593A1 (de)
RU (3) RU2178007C2 (de)
TR (5) TR199701570T1 (de)
TW (2) TW408186B (de)
WO (3) WO1996041026A1 (de)
ZA (1) ZA964866B (de)

Families Citing this family (62)

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US5976218A (en) * 1996-05-10 1999-11-02 Henkel Corporation Process for the recovery of nickel
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US6231823B1 (en) 2000-03-27 2001-05-15 Dynatec Corporation Solvent extraction process for the separation of cobalt from nickel in aqueous sulphate-containing solutions
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US6428604B1 (en) 2000-09-18 2002-08-06 Inco Limited Hydrometallurgical process for the recovery of nickel and cobalt values from a sulfidic flotation concentrate
US20050126923A1 (en) * 2001-07-25 2005-06-16 Phelps Dodge Corporation Process for recovery of copper from copper-bearing material using medium temperature pressure leaching, direct electrowinning and solvent/solution extraction
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CN100497680C (zh) * 2007-01-19 2009-06-10 昆明贵金属研究所 一种硫化镍精矿提取镍的新方法
MX2009000956A (es) * 2007-02-22 2009-03-09 Univ Autonoma Metropolitana Proceso para la recuperacion de valores que contienen metales a partir de minerales y menas.
US8003064B2 (en) 2007-09-17 2011-08-23 Freeport-Mcmoran Corporation Controlled copper leach recovery circuit
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FI122188B (fi) * 2010-03-18 2011-09-30 Outotec Oyj Hydrometallurginen menetelmä metallisen nikkelin valmistamiseksi
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CN102002586B (zh) * 2010-12-04 2012-09-26 金川集团有限公司 一种含镍高钴硫化物浸出工艺
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US9169533B2 (en) 2011-12-20 2015-10-27 Freeport Minerals Corporation System and method including multi-circuit solution extraction for recovery of metal values from metal-bearing materials
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CN105392907A (zh) * 2012-07-23 2016-03-09 淡水河谷公司 从硫化物矿石和精矿回收贱金属
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CN103205580A (zh) * 2013-04-19 2013-07-17 金川集团股份有限公司 一种贵金属富集过程中的脱硫方法
FI124954B (fi) * 2013-04-30 2015-04-15 Outotec Oyj Menetelmä kultaa sisältävän liuoksen valmistamiseksi ja prosessijärjestely kullan ja hopean talteenottamiseksi
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KR101399953B1 (ko) * 2013-11-20 2014-05-30 한국지질자원연구원 복합 구리광 선광방법
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CN107406906B (zh) * 2014-11-18 2020-07-21 联盟镁公司 在HCl回收回路中使用硫酸生产镁化合物和各种副产物的方法
JP6481542B2 (ja) * 2015-07-21 2019-03-13 住友金属鉱山株式会社 高純度硫酸ニッケル水溶液の製造方法
JP6428525B2 (ja) * 2015-08-04 2018-11-28 住友金属鉱山株式会社 酸化中和設備および酸化中和方法
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JP6448684B2 (ja) * 2017-03-03 2019-01-09 Ｊｘ金属株式会社 リチウム回収方法
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