CN103998011B - 个人清洁组合物 - Google Patents
个人清洁组合物 Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
Abstract
本发明涉及液体个人清洁组合物。本发明人已经发现,所选二或三羧酸或其盐在与百里香酚或松油醇结合时以快速方式提供协同抗微生物作用并在极低的百里香酚和/或松油醇浓度下获得这样的效力。
Description
技术领域
本发明涉及液体个人清洁组合物。本发明更特别涉及提供协同抗微生物效力的个人清洁组合物。
发明背景
用于个人洗涤用途的液体组合物是已知的。这样的组合物包括通常从配有手压泵(其通过用手压致动)的瓶子中分配的洗手液。在公共场所,如机场、宾馆、餐馆和办公室的盥洗室中也配备这种类型的洗手液。其它个人清洁液包括洗脸液、沐浴液、洗发水和护发素。
这样的组合物不仅用于清洁身体表面以赋予消费者清除了灰尘、皮脂和汗液的感觉,还赋予消费者已将表面消毒以清除致病病菌的满足感。液体形式的此类组合物已知用于个人护理。此类组合物包括专门针对微生物,如细菌和病毒以杀死它们或使它们失活的抗微生物活性剂。
包含氯基抗微生物剂,如三氯生的消毒灭菌皂组合物是已知的。此类组合物需要相当长的接触时间以提供有效的抗微生物作用。在实践中,使用者,特别是儿童不会花费长时间进行清洁,因此,用此类组合物清洁不能提供充分预防表面或局部感染或充分预防疾病。尽管洗了手,但使用者的皮肤仍可能没有相对充分除菌并可能造成其它生命体表面和/或无生命表面的污染,这可能导致病原体传播和随之发生疾病。一般而言使用者,特别是儿童,他们在饭前用缓效(slow-acting)抗微生物组合物洗涤被污染的手相对短时间,仍具有接触疾病的危险。清洁动作的这些短时标(time scale)无法有效提供所需益处,因为此类产品中常用的大多数已知抗微生物剂需要数小时才能提供微生物的所需杀灭。
因此,本申请人实现了提供在清洁期相对更短(通常大约5分钟或更短,优选少于2分钟,在许多情况中少于1分钟或有时低至15秒或更短)时产生相对更有效的抗微生物作用的组合物的需要。它们在作为WO2010046238公开的在先专利申请中公开了百里香酚和松油醇的新型组合,它们协同相互作用以便能在少于大约15秒内实现快速抗微生物作用。本发明人已经发现,所选二或三羧酸或其盐在与百里香酚或松油醇结合时以快速方式提供类似的协同抗微生物作用,并在低得多的百里香酚和/或松油醇浓度下获得这样的效力。本发明的优点在于香精油活性剂如松油醇和百里香酚具有一些消费者不喜欢的强药味,在确保同样有效的抗微生物作用的同时包括更低浓度的百里香酚和松油醇是有利的。此外,通过本发明已经发现,所选阴离子表面活性剂的加入有助于进一步增强的抗微生物效力。
液体个人清洁组合物是已知的。
US2008045491(Fitchmun)公开了包含水混溶性醇、水、弱酸和多价阳离子(例如金属离子或金属化合物)的无毒抗微生物表面消毒剂。该组合物还可包括润肤剂、氧化剂、保湿剂、润滑剂、植物源烯、抗微生物组分或植物源香精油中的一种或多种,其可配制为用于消毒硬表面,如台面(countertop)和地板的溶液或施加到动物皮肤上的溶液/凝胶。
上述公开利用醇的公知抗微生物效力,这比大多数其它已知的抗微生物活性剂强得多。许多消费者不喜欢使用利用醇的产品,因为他们认为其刺激皮肤,因此希望开发在利用被认为对皮肤温和的活性剂的同时在快得多的时间范围内提供类似或更好的抗微生物效力的新型活性剂组合。
US2006093570(Reckitt Benckiser)描述了优选用于个人用途的表面处理组合物,其包含至少一种表面活性剂和至少两种不同的有机酸和/或有机酸盐,且其中所述有机酸和/或盐在该组合物中的总浓度为至少0.5%(w/v)。该发明进一步延伸至处理表面,优选头发或皮肤以除去污垢并除去或抑制微生物生长的方法。
上文引用的专利公开没有解决缓效抗微生物组合物的问题,也没有公开本发明中公开并要求保护的活性剂协同组合用于在人和/或动物的皮肤和/或其它角蛋白基底的清洁和消毒中的速效抗微生物作用。
本发明的一个目的是克服或改善现有技术的至少一个缺点或提供有用的替代方案。
本发明的另一目的是提供具有相对较快的抗微生物作用的液体个人护理清洁和消毒组合物。
发明概述
根据本发明的第一方面,提供包含少于1% C1至C3醇的具有4.5至7.5的pH的液体个人清洁组合物,其包含
(a) 0.25至2.5重量%二或三羧酸或其盐;
(b) 0.01至2重量%百里香酚;
(c) 0.01至2重量%松油醇;和
(d) 70至90重量%水。
根据本发明的另一方面,提供动物或人体的外表面的消毒方法,包括使所述表面与如前述权利要求任一项中所述的组合物接触的步骤,接着用水冲洗所述表面或擦拭所述表面以基本除去所述组合物的步骤。
发明详述
本领域普通技术人员在阅读下列详述和所附权利要求时容易看出这些和其它方面、特征和优点。为避免疑问,本发明的一个方面的任何特征可用在本发明的任何其它方面中。词语“包含”意在表示“包括”但不一定“由…构成”或“由…组成”。换言之,所列步骤或选项不需要是穷举的。要指出,下列描述中给出的实例旨在阐明本发明且无意将本发明限于这些实例本身。类似地,除非另行指明,所有百分比为重量/重量百分比。
除了在实施例和对比例中或另行明示之处外,本说明书中指示材料量或反应条件、材料物理性质和/或用途的所有数值应被理解为被词语“大约”修饰。除非另行规定,以格式“x至y”表示的数值范围被理解为包括x和y。当对于特定要素以格式“x至y”描述多个优选范围时,要理解的是,也考虑组合不同端点的所有范围。
本文所用的个人清洁组合物意在包括用于清洁和消毒局部区域,例如哺乳动物,尤其是人类的皮肤和/或头发的组合物。这样的组合物通常被分类为免洗型或冲洗型,并包括还为了改善外表、清洁、气味控制或一般美观而施加到人体上的任何产品。其更优选是冲洗型产品。液体形式的本发明的组合物可改为包括护肤液、霜、泡沫或凝胶或化妆水或用工具或经面膜、棉片或贴片施加。本文所用的“皮肤”意在包括面部和身体(例如颈、胸、背、手臂、腋下、手、腿、臀部和头皮)上的皮肤。本发明的组合物还可用在人体除皮肤外的任何其它角蛋白基质,例如头发上,在此可以以提供消毒和清洁为特定目的配制产品。
本发明的第一方面提供包含少于1% C1至C3醇的具有4.5至7.5的pH的液体个人清洁组合物,其包含二或三羧酸或其盐、百里香酚、松油醇和水。
该组合物具有4.5至7.5的pH。该组合物提供抗微生物效力,在该效力中甚至没有来自通常与水混溶的低分子量醇,即C1至C2醇,例如甲醇、乙醇、丙醇或异丙醇的任何贡献。如果存在,它们也可少于该组合物的1重量%,优选少于0.5%,更优选少于0.1%,并任选不存在于该组合物中。
该组合物包含占该组合物的按重量计0.25至2.5%,优选0.5至2%,更优选0.75至1.25%的二或三羧酸或其盐。
该二或三羧酸优选选自草酸、富马酸、邻苯二甲酸、马来酸、苹果酸、丙二酸或柠檬酸。该二或三羧酸最优选是苹果酸、丙二酸或柠檬酸。根据配制该组合物的pH,为制备本发明的组合物而添加的二或三羧酸的一部分可能作为二或三羧酸的盐存在。在这种情况下,该盐优选是碱金属或碱土金属盐,更优选碱金属盐,其中钠盐最优选。下面给出一些羧酸的盐的结构:
草酸钠 富马酸钠
邻苯二甲酸钠 马来酸钠
苹果酸钠 丙二酸钠
柠檬酸盐
。
据观察,在本发明的组合物中加入二或三羧酸提供所需抗微生物效力,而单羧酸没有表现出如此好的效力。
该组合物包含香精油抗微生物活性剂百里香酚和松油醇的组合,各活性剂为该组合物的0.01至2重量%。
百里香酚优选以该组合物的0.02至0.5%,更优选最多0.3重量%,再更优选最多0.2重量%存在。百里香酚可以以纯化形式添加到该抗微生物组合物中。或者,可以将包含百里香酚的百里香油或百里香提取物添加到该抗微生物组合物中,同时确保百里香酚以所需浓度存在于本发明的组合物中。百里香油或百里香提取物获自百里香植物。百里香植物是指属于百里香属的植物并包括但不限于下列物种:Thymus vulgaris、Thymus zygis、Thymus satureoides、Thymus mastichina、Thymus broussonetti、Thymus maroccanus、Thymus pallidus、Thymus algeriensis、Thymus serpyllum、Thymus pulegoide和Thymus citriodorus。
下面给出百里香酚及其异构体香芹酚的结构:
。
本发明的优选抗微生物组合物具有占该组合物的0.05至1%,更优选最多0.5重量%的松油醇。松油醇优选选自α-松油醇、β-松油醇、γ-松油醇或其混合物。松油醇特别优选是α-松油醇。松油醇可以以纯化形式添加到该抗微生物组合物中。或者,可以将包含松油醇的松树油添加到该抗微生物组合物中。
下面给出松油醇化合物的结构:
。
本发明的组合物包含水作为优选载体。水以该组合物的70至90重量%,优选85至90重量%存在。
本发明的组合物任选包含表面活性剂。优选的表面活性剂是阴离子表面活性剂。阴离子表面活性剂优选以该组合物的0.5至15重量%,更优选1至5重量%存在。特别优选的阴离子表面活性剂是甘氨酸盐、烷基硫酸盐或乙氧基化烷基硫酸盐。
该组合物还可包含本领域技术人员已知的各种附加成分。这样的附加成分包括但不限于:芳香剂、颜料、防腐剂、润肤剂、防晒剂、乳化剂、胶凝剂或增稠剂。
该抗微生物组合物可以是液体形式,但该液体组合物可进一步增稠成凝胶或膏。本发明的抗微生物组合物可用于人皮肤和头发的清洁和护理。
根据本发明的另一方面,提供人和/或动物的角蛋白基底的清洁和消毒方法,包括将本发明的组合物施加到所述表面,接着冲洗或擦拭所述表面以基本除去所述组合物的步骤。在表面上施加该组合物的步骤之前或期间,该组合物优选用水以1: 10至1: 40的重量比,优选以1:20至1:30的比率稀释。
该方法优选包括用合适的溶剂,优选水冲洗表面或用合适的擦布擦拭表面的步骤。
本发明人已经确定,本发明的组合物提供抗微生物作用,其中抗微生物活性剂与该表面的接触时间少,即大致小于5分钟,优选小于2分钟,再更优选小于1分钟,在许多情况下小于15秒。
现在通过下列非限制性实施例证实本发明。
实施例
实施例1至9
制备如表-1中所示的组合物并使用下列试验程序测试抗菌效力。
程序: 接触杀灭检测(15秒接触杀灭)
受试细菌E.coli ATCC 10536在TSB肉汤(Difco – 30gpl)中在37℃下培养整夜16小时。其中2毫升在40毫升新鲜TSB肉汤中传代培养(sub-cultured)并在37℃下继续培养4小时。该培养物随后如下加工:以2057g旋转5分钟、洗涤两次并收集细胞。在620 nm下调节细胞密度以得到108 cfu/ml (0.8 OD)的最终计数。制备如表-1中所示的组合物并保存3小时以便熟化。
将9毫升该组合物置于样品容器中并将1毫升加工过的培养物添加到其中。在15秒接触时间后,1毫升上述混合物立即在D/E肉汤(Difco - 39gpl)中中和。在D/E肉汤中进行连续稀释并一式双份铺在(plate)在TSA(Difco - 40gpl)的平板上。就对照物而言,将1毫升受试培养物添加到9毫升盐水中并连续稀释和铺在TSA的平板上。在固化后,将板在37℃下培养48小时。在培养48小时后计数剩余菌落并通过与对照物相比测定效力。数据概括在下表-1中。
表- 1
实施例 | 百里香酚(wt%) | 松油醇 wt% | 二/三羧酸 | 二/三羧酸(wt%) | pH | Log减少 |
实施例1 | 0.2 | 0.5 | - | - | 6.9 | 7.2 |
实施例2 | 0.025 | 0.0625 | - | - | 6.9 | 0 |
实施例3 | 0.025 | 0.0625 | 苹果酸 | 1.0 | 5.0 | 7.2 |
实施例4 | 0.025 | 0.0625 | 苹果酸 | 1.0 | 7.3 | 6.1 |
实施例5 | 0.025 | 0.0625 | 丙二酸 | 1.0 | 5.0 | 7.2 |
实施例6 | 0.025 | 0.0625 | 丙二酸 | 1.0 | 7.3 | 6.3 |
实施例7 | 0.025 | 0.0625 | 柠檬酸 | 1.0 | 5.0 | 7.2 |
实施例8 | 0.025 | 0.0625 | 柠檬酸 | 1.0 | 7.2 | 6.5 |
实施例9 | - | - | 丙二酸 | 1.0 | 5.0 | 0 |
实施例10 | - | - | 柠檬酸 | 1.0 | 5.0 | 0 |
表-1中的数据表明当二或三羧酸与低浓度的香精油活性剂(百里香酚和松油醇)结合时,它们与不属于本发明的组合物(实施例2、9和10)相比提供协同抗菌效力(实施例3至8)。
Claims (7)
1.包含少于1% C1至C3醇的具有4.5至7.5的pH的液体个人清洁组合物,其包含
(a) 0.25至2.5重量%二或三羧酸或其盐;
(b) 0.02至0.2重量%百里香酚;
(c) 0.05至0.5重量%松油醇;和
(d) 70至90重量%水。
2.如权利要求1中所述的组合物,其中所述二或三羧酸选自草酸、富马酸、邻苯二甲酸、马来酸、苹果酸、丙二酸或柠檬酸。
3.如权利要求2中所述的组合物,其中所述二或三羧酸选自苹果酸、丙二酸或柠檬酸。
4.如前述权利要求任一项中所述的组合物,其包含阴离子表面活性剂。
5.如权利要求4中所述的组合物,其中所述阴离子表面活性剂以所述组合物的0.5至15重量%的量存在。
6.如权利要求4中所述的组合物,其中所述阴离子表面活性剂选自甘氨酸盐、烷基硫酸盐或乙氧基化烷基硫酸盐。
7.动物或人体的外表面的非治疗消毒方法,包括使所述表面与如前述权利要求任一项中所述的组合物接触的步骤,接着用水冲洗所述表面或擦拭所述表面以除去所述组合物的步骤。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IN3096MU2011 | 2011-11-03 | ||
IN3096/MUM/2011 | 2011-11-03 | ||
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AT14444U1 (de) * | 2015-01-21 | 2015-11-15 | Andreas Maidler | Reiniger |
CN108289444B (zh) * | 2015-11-27 | 2021-08-27 | 联合利华知识产权控股有限公司 | 抗微生物组合物 |
CA3055449A1 (en) * | 2017-03-16 | 2018-09-20 | Unilever Plc | An antimicrobial composition comprising essential oil and antimicrobial lipid |
CN112153896A (zh) * | 2018-06-04 | 2020-12-29 | 荷兰联合利华有限公司 | 防腐组合物 |
BR112020022822A2 (pt) * | 2018-06-04 | 2021-02-02 | Unilever Nv | sistema de preservação antimicrobiana, substância de preservação, composição aquosa e método de preservação de composições |
EP3773921B1 (en) | 2018-06-04 | 2023-03-01 | Unilever IP Holdings B.V. | Preservation compositions |
CN109157426A (zh) * | 2018-10-15 | 2019-01-08 | 王杰 | 一种含有4-松油醇的皮肤护理剂及其制备方法 |
FR3116696B1 (fr) | 2020-11-28 | 2023-07-21 | Sergere Jean Christophe | Composition antimicrobienne |
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ZA201402431B (en) | 2016-01-27 |
US20140311515A1 (en) | 2014-10-23 |
BR112014009479B8 (pt) | 2019-01-29 |
IN2014MN00808A (zh) | 2015-09-04 |
EP2773315A2 (en) | 2014-09-10 |
BR112014009479A2 (pt) | 2017-05-09 |
BR112014009479B1 (pt) | 2018-08-07 |
EA024551B1 (ru) | 2016-09-30 |
WO2013064360A2 (en) | 2013-05-10 |
CN103998011A (zh) | 2014-08-20 |
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EP2773315B1 (en) | 2015-07-08 |
EA201400535A1 (ru) | 2014-08-29 |
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