JP2010245518A - 低温でプラズマ励起原子膜の成膜によりシリコン酸化膜を成膜する方法 - Google Patents
低温でプラズマ励起原子膜の成膜によりシリコン酸化膜を成膜する方法 Download PDFInfo
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- 238000000034 method Methods 0.000 title claims abstract description 38
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 229910052814 silicon oxide Inorganic materials 0.000 title claims abstract description 20
- 238000000151 deposition Methods 0.000 title abstract description 28
- 238000000231 atomic layer deposition Methods 0.000 title abstract 2
- 230000008021 deposition Effects 0.000 claims abstract description 29
- 239000002243 precursor Substances 0.000 claims abstract description 23
- 239000000758 substrate Substances 0.000 claims abstract description 19
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 10
- 239000010703 silicon Substances 0.000 claims abstract description 10
- 230000008569 process Effects 0.000 claims abstract description 7
- 230000015572 biosynthetic process Effects 0.000 claims description 49
- 239000007789 gas Substances 0.000 claims description 29
- 238000010926 purge Methods 0.000 claims description 17
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 8
- 239000001301 oxygen Substances 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- 239000012495 reaction gas Substances 0.000 claims description 8
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical group [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 claims description 5
- 239000002826 coolant Substances 0.000 claims description 3
- 229910052756 noble gas Inorganic materials 0.000 claims description 2
- 239000010410 layer Substances 0.000 abstract 3
- 239000012044 organic layer Substances 0.000 abstract 1
- 239000000376 reactant Substances 0.000 abstract 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 28
- 125000006850 spacer group Chemical group 0.000 description 12
- 229920002120 photoresistant polymer Polymers 0.000 description 11
- 239000003507 refrigerant Substances 0.000 description 11
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 9
- 239000000463 material Substances 0.000 description 9
- 238000000059 patterning Methods 0.000 description 9
- 238000001816 cooling Methods 0.000 description 6
- 238000012886 linear function Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000008034 disappearance Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000001459 lithography Methods 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- JHPBZFOKBAGZBL-UHFFFAOYSA-N (3-hydroxy-2,2,4-trimethylpentyl) 2-methylprop-2-enoate Chemical compound CC(C)C(O)C(C)(C)COC(=O)C(C)=C JHPBZFOKBAGZBL-UHFFFAOYSA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000002528 anti-freeze Effects 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000001282 iso-butane Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 229910021420 polycrystalline silicon Inorganic materials 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000012686 silicon precursor Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
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- C23C16/45523—Pulsed gas flow or change of composition over time
- C23C16/45525—Atomic layer deposition [ALD]
- C23C16/45527—Atomic layer deposition [ALD] characterized by the ALD cycle, e.g. different flows or temperatures during half-reactions, unusual pulsing sequence, use of precursor mixtures or auxiliary reactants or activations
- C23C16/45536—Use of plasma, radiation or electromagnetic fields
- C23C16/45542—Plasma being used non-continuously during the ALD reactions
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- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
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Abstract
【解決手段】PEALDにより、基板に形成されたレジストパターン又はエッチされたライン上にシリコン酸化膜を成膜する方法が、レジストパターン又はエッチされたラインが形成された基板をPEALDリアクターに与える工程と、基板が配置されたサセプタの温度を成膜温度として50℃未満に制御する工程と、成膜温度を50℃未満の一定の温度に実質的に又はほぼ維持しながら、PEALDリアクターにシリコン含有前駆体及び酸素供給反応ガスを導入して、レジストパターン又はエッチされたラインにシリコン酸化原子膜を成膜する工程と、前記レジストパターン又は前記エッチされたラインにシリコン酸化原子膜を成膜するために、実質的に又はほぼ一定の温度で成膜サイクルを複数回繰り返す工程とを含む。
【選択図】なし
Description
y=−0.0005x+0.1397
ここで、yは成長速度(nm/cycle)で、xは成膜温度(℃)である。他の形態では、成長速度(nm/ cycle)がy+10%であってもよい。
成膜圧力 : 約400Pa
Si含有前駆体流量 : 300〜500sccm
酸素流量 : 100〜1000sccm
パージガス(例えばAr)流量 : 約1500sccm
基板の上に有機膜として、ArFレーザー用のフォトレジストであり、アクリル酸、またはメタクリル酸エステルの重合体及び共重合体のアルキル置換体を基本とした組成からなる構造を有した3種類のフォトレジストA、B、C(ライン幅40nm、厚み120nm)をそれぞれ形成し、その上にSiO2膜をPEALDにより成膜した。成膜の条件は以下の通りであった。
Si含有前駆体流量 :500sccn
Si含有前駆体パルス :0.5秒
酸素流量 :600sccm
Ar流量 :1.5sccm
RFパワー(13.56MHz) : 50W
RFパワーパルス :0.3秒
Si含有前駆体パルスとRFパワーパルスのインターバル(RFパワー印加前のパージ):0.3秒
RFパワーパルスとSi含有前駆体パルスのインターバル(RFパワー印加後のパージ):0.3秒
成膜圧力 :400Pa
一サイクルの長さ :1.5秒
Claims (18)
- プラズマ励起原子膜の成膜(PEALD)により、基板に形成されたレジストパターン又はエッチされたライン上にシリコン酸化膜を成膜する方法であって、
レジストパターン又はエッチされたラインが形成された基板をPEALDリアクターに与えられる工程と、
前記基板が配置されたサセプタの温度を成膜温度として50℃未満に制御する工程と、
前記成膜温度を50℃未満の一定の温度に維持しながら、PEALDリアクターにシリコン含有前駆体及び酸素供給反応ガスを導入し、これによりレジストパターン又はエッチされたラインにシリコン酸化原子膜を成膜する工程と、
前記レジストパターン又は前記エッチされたラインにシリコン酸化原子膜を成膜するために、一定の温度でサイクルを複数回繰り返す工程と、
を含む方法。 - 前記成膜温度が、40℃以下の一定の温度に制御する、請求項1に記載の方法。
- 前記成膜温度が、30℃以下の一定の温度に制御する、請求項2に記載の方法。
- サイクル中に、前記シリコン含有前駆体が、過剰なシリコン含有前駆体を除去するために、PEALDリアクターに導入される、請求項1に記載の方法。
- 前記シリコン含有前駆体が第一のパルス中に導入され、RFパワーが第二のパルス中に適用される、請求項1に記載の方法。
- 前記酸素供給反応ガスが一定に導入される、請求項5に記載の方法。
- サイクル中に、パージガスがPEALDリアクターに一定に導入される、請求項5に記載の方法。
- 前記シリコン含有前駆体がアミノシランガスである、請求項1に記載の方法。
- 前記アミノシランガスが、ビスジエチレルアミノシラン(BDEAS)、ビスエチルメチルアミノシラン(BEMAS)、トリスジメチルアミノシラン(3DMAS)、およびヘキサキスエチルアミノシラン(HEAD)からなるグループから選択される、請求項8に記載の方法。
- 前記酸素供給反応ガスがO2である、請求項1に記載の方法。
- 前記パージガスが希ガスである、請求項4に記載の方法。
- 成膜サイクルが約1.5秒から3.0秒の期間である、請求項1に記載の方法。
- 前記シリコン酸化膜の成長速度が約0.120nm/cycle以上である、請求項1に記載の方法。
- 請求項13に記載の方法であって、
サセプタの温度が以下の式に従ってセットされ、
y=−0.0005x+0.1397
ここで、yは成長速度(nm/cycle)で、xは成膜温度(℃)である、方法。 - 成膜温度が、サセプタ内に形成された導管に冷媒を通過させることにより調節される、請求項1に記載の方法。
- RFパワーが容量結合された平行な電極を使用して適用され、前記サセプタが下方電極として機能し、一枚の基板を保持する、請求項1に記載の方法。
- さらに、
基板がPEALDリアクターに与えられる前に、
シリコン酸化膜の成長速度と成膜温度との間の関係を定義する標準的な曲線を得る工程と、
一成膜サイクル中のシリコン酸化膜層の成長速度をセットする工程と、
前記標準的な曲線を使用して、セットされた成長速度に基づいて成膜温度を得る工程と、
を含む、請求項1に記載の方法。 - 標準的な曲線が、y=−0.0005x+0.1397であり、ここで、yは成長速度(nm/cycle)で、xは成膜温度(℃)である、請求項17に記載の方法。
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Also Published As
Publication number | Publication date |
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KR101680379B1 (ko) | 2016-11-28 |
KR20100109855A (ko) | 2010-10-11 |
US20100255218A1 (en) | 2010-10-07 |
US8197915B2 (en) | 2012-06-12 |
JP5679153B2 (ja) | 2015-03-04 |
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