CN100550303C - 第ⅲ族氮化物晶体及其制备方法 - Google Patents

第ⅲ族氮化物晶体及其制备方法 Download PDF

Info

Publication number
CN100550303C
CN100550303C CNB2004100896735A CN200410089673A CN100550303C CN 100550303 C CN100550303 C CN 100550303C CN B2004100896735 A CNB2004100896735 A CN B2004100896735A CN 200410089673 A CN200410089673 A CN 200410089673A CN 100550303 C CN100550303 C CN 100550303C
Authority
CN
China
Prior art keywords
group iii
melt
iii nitride
crystal
nitrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB2004100896735A
Other languages
English (en)
Chinese (zh)
Other versions
CN1612295A (zh
Inventor
弘田龙
中畑成二
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Electric Industries Ltd
Original Assignee
Sumitomo Electric Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Electric Industries Ltd filed Critical Sumitomo Electric Industries Ltd
Publication of CN1612295A publication Critical patent/CN1612295A/zh
Application granted granted Critical
Publication of CN100550303C publication Critical patent/CN100550303C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10Inorganic compounds or compositions
    • C30B29/38Nitrides
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B9/00Single-crystal growth from melt solutions using molten solvents
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10Inorganic compounds or compositions
    • C30B29/40AIIIBV compounds wherein A is B, Al, Ga, In or Tl and B is N, P, As, Sb or Bi
    • C30B29/403AIII-nitrides
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10Inorganic compounds or compositions
    • C30B29/40AIIIBV compounds wherein A is B, Al, Ga, In or Tl and B is N, P, As, Sb or Bi
    • C30B29/403AIII-nitrides
    • C30B29/406Gallium nitride

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
CNB2004100896735A 2003-10-31 2004-10-29 第ⅲ族氮化物晶体及其制备方法 Expired - Fee Related CN100550303C (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2003373025 2003-10-31
JP2003373025 2003-10-31
JP2004195666 2004-07-01
JP2004195666A JP4534631B2 (ja) 2003-10-31 2004-07-01 Iii族窒化物結晶の製造方法

Publications (2)

Publication Number Publication Date
CN1612295A CN1612295A (zh) 2005-05-04
CN100550303C true CN100550303C (zh) 2009-10-14

Family

ID=34467811

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2004100896735A Expired - Fee Related CN100550303C (zh) 2003-10-31 2004-10-29 第ⅲ族氮化物晶体及其制备方法

Country Status (7)

Country Link
US (1) US20050098090A1 (enExample)
EP (2) EP1538241B1 (enExample)
JP (1) JP4534631B2 (enExample)
KR (5) KR20050041994A (enExample)
CN (1) CN100550303C (enExample)
DE (1) DE602004018452D1 (enExample)
TW (1) TWI399796B (enExample)

Families Citing this family (47)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005298269A (ja) * 2004-04-12 2005-10-27 Sumitomo Electric Ind Ltd Iii族窒化物結晶基板およびその製造方法ならびにiii族窒化物半導体デバイス
EP1930294A4 (en) * 2005-08-24 2012-12-26 Mitsubishi Chem Corp METHOD FOR PRODUCING GROUP 13 METAL NITRIDE CRYSTAL, METHOD FOR PRODUCING A SEMICONDUCTOR DEVICE, AND SOLUTION AND MELT USED THEREOF
JP4788524B2 (ja) * 2005-08-24 2011-10-05 三菱化学株式会社 第13族金属窒化物結晶の製造方法およびこれらの製造方法に用いる溶液と融液
EP1775356A3 (en) 2005-10-14 2009-12-16 Ricoh Company, Ltd. Crystal growth apparatus and manufacturing method of group III nitride crystal
JP4863264B2 (ja) * 2006-03-17 2012-01-25 豊田合成株式会社 半導体結晶の製造方法
WO2007057892A2 (en) * 2005-11-17 2007-05-24 Mosaic Crystals Ltd. Gan crystal sheet
WO2007108338A1 (ja) 2006-03-23 2007-09-27 Ngk Insulators, Ltd. 窒化物単結晶の製造方法および装置
CN101405438B (zh) 2006-03-23 2012-06-27 日本碍子株式会社 氮化物单晶的制造装置
JP5187848B2 (ja) 2006-03-23 2013-04-24 日本碍子株式会社 単結晶の製造方法
JP2007254201A (ja) * 2006-03-23 2007-10-04 Ngk Insulators Ltd 単結晶の製造方法
JP4827107B2 (ja) 2006-03-24 2011-11-30 日本碍子株式会社 窒化物単結晶の製造方法
JP4936310B2 (ja) * 2006-04-07 2012-05-23 豊田合成株式会社 Iii族窒化物系化合物半導体の製造装置
JP2007284267A (ja) * 2006-04-13 2007-11-01 Sumitomo Electric Ind Ltd GaN結晶の製造方法
JP4720672B2 (ja) * 2006-08-14 2011-07-13 住友金属工業株式会社 窒化アルミニウム単結晶の製造方法
JPWO2008117571A1 (ja) * 2007-03-26 2010-07-15 日本碍子株式会社 窒化物単結晶の製造方法
JP5235864B2 (ja) 2007-03-27 2013-07-10 日本碍子株式会社 窒化物単結晶の製造方法
JP4881496B2 (ja) * 2007-04-24 2012-02-22 豊田合成株式会社 Iii族窒化物系化合物半導体の製造方法
US8361222B2 (en) 2007-04-24 2013-01-29 Toyoda Gosei Co., Ltd. Method for producing group III nitride-based compound semiconductor
US9281438B2 (en) * 2007-09-28 2016-03-08 Ricoh Company, Ltd. Process for producing group III element nitride crystal and apparatus for producing group III element nitride crystal
JP4941448B2 (ja) * 2007-10-26 2012-05-30 豊田合成株式会社 Iii族窒化物半導体製造装置
JP2009114035A (ja) * 2007-11-08 2009-05-28 Toyoda Gosei Co Ltd Iii族窒化物半導体製造装置および製造方法
JP5560528B2 (ja) * 2008-01-28 2014-07-30 住友電気工業株式会社 Iii族窒化物単結晶インゴットの製造方法、及びiii族窒化物単結晶基板の製造方法
JP5229792B2 (ja) * 2008-03-25 2013-07-03 国立大学法人大阪大学 Iii族元素窒化物結晶の製造方法およびそれにより得られるiii族元素窒化物結晶
JP4886722B2 (ja) * 2008-03-25 2012-02-29 日本碍子株式会社 窒化物単結晶の製造方法
JP5056688B2 (ja) * 2008-09-15 2012-10-24 豊田合成株式会社 Iii族窒化物半導体結晶の製造方法
JP5310257B2 (ja) * 2009-05-21 2013-10-09 株式会社リコー 窒化物結晶製造方法
JP2010077022A (ja) * 2009-11-30 2010-04-08 Sumitomo Electric Ind Ltd Iii族窒化物結晶基板およびその製造方法ならびにiii族窒化物半導体デバイス
JP5729182B2 (ja) 2010-08-31 2015-06-03 株式会社リコー n型III族窒化物単結晶の製造方法、n型III族窒化物単結晶および結晶基板
CN102618920A (zh) * 2012-04-25 2012-08-01 浙江华友电子有限公司 一种单晶炉熔料过程中的热能控制方法
JP5522204B2 (ja) * 2012-06-14 2014-06-18 豊田合成株式会社 Iii族窒化物半導体結晶の製造方法
CN103603031A (zh) * 2013-12-06 2014-02-26 北京大学东莞光电研究院 一种通过调控釜体内部流场制备高质量单晶体材料的方法
CN106460228B (zh) * 2014-03-03 2019-04-26 国立大学法人大阪大学 Iii族氮化物结晶的制造方法及iii族氮化物结晶制造装置
JP6534030B2 (ja) * 2014-08-28 2019-06-26 国立大学法人名古屋大学 AlN単結晶の作製方法
CN104878451B (zh) * 2015-06-16 2017-07-28 北京大学东莞光电研究院 一种氮化物单晶生长装置
CN111052415B (zh) 2017-08-24 2023-02-28 日本碍子株式会社 13族元素氮化物层、自立基板以及功能元件
WO2019038892A1 (ja) 2017-08-24 2019-02-28 日本碍子株式会社 13族元素窒化物層、自立基板および機能素子
WO2019039189A1 (ja) * 2017-08-24 2019-02-28 日本碍子株式会社 13族元素窒化物層、自立基板および機能素子
JP6851486B2 (ja) * 2017-08-24 2021-03-31 日本碍子株式会社 13族元素窒化物層、自立基板および機能素子
US11309455B2 (en) 2017-08-24 2022-04-19 Ngk Insulators, Ltd. Group 13 element nitride layer, free-standing substrate and functional element
WO2019039208A1 (ja) * 2017-08-24 2019-02-28 日本碍子株式会社 13族元素窒化物層、自立基板および機能素子
CN111052413B (zh) * 2017-08-24 2023-08-15 日本碍子株式会社 13族元素氮化物层、自立基板以及功能元件
JP6851485B2 (ja) * 2017-08-24 2021-03-31 日本碍子株式会社 13族元素窒化物層、自立基板および機能素子
JP7051094B2 (ja) * 2018-05-01 2022-04-11 国立大学法人東北大学 窒化アルミニウム結晶の製造方法
CN109706524A (zh) * 2019-03-07 2019-05-03 中国电子科技集团公司第四十六研究所 一种降低氮化镓单晶氧原子浓度的方法
JP7063293B2 (ja) * 2019-03-18 2022-05-09 豊田合成株式会社 Iii族窒化物半導体の製造方法
US11280024B2 (en) * 2019-03-18 2022-03-22 Toyoda Gosei Co., Ltd. Method for producing a group III nitride semiconductor by controlling the oxygen concentration of the furnace internal atmosphere
JP7147644B2 (ja) * 2019-03-18 2022-10-05 豊田合成株式会社 Iii族窒化物半導体の製造方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4190630A (en) * 1978-01-03 1980-02-26 Vsesojuzny Nauchno-Isslekovatelsky Institut Monokristallov Stsintillyatsionnykh Materialov I Osobo Chistykh Khimicheskikh Veschestv Apparatus for pulling single crystals from melt
JPH07277897A (ja) * 1994-04-04 1995-10-24 Katsutoshi Yoneya 窒化アルミニウム単結晶の合成方法
US5868837A (en) 1997-01-17 1999-02-09 Cornell Research Foundation, Inc. Low temperature method of preparing GaN single crystals
US6270569B1 (en) * 1997-06-11 2001-08-07 Hitachi Cable Ltd. Method of fabricating nitride crystal, mixture, liquid phase growth method, nitride crystal, nitride crystal powders, and vapor phase growth method
TW428331B (en) * 1998-05-28 2001-04-01 Sumitomo Electric Industries Gallium nitride single crystal substrate and method of producing the same
US6562124B1 (en) * 1999-06-02 2003-05-13 Technologies And Devices International, Inc. Method of manufacturing GaN ingots
US6592663B1 (en) * 1999-06-09 2003-07-15 Ricoh Company Ltd. Production of a GaN bulk crystal substrate and a semiconductor device formed on a GaN bulk crystal substrate
JP4011828B2 (ja) 1999-06-09 2007-11-21 株式会社リコー Iii族窒化物結晶の結晶成長方法及びiii族窒化物結晶の製造方法
JP3929657B2 (ja) 1999-09-29 2007-06-13 株式会社リコー 結晶成長方法およびiii族窒化物結晶の製造方法
JP4094780B2 (ja) 1999-08-24 2008-06-04 株式会社リコー 結晶成長方法および結晶成長装置並びにiii族窒化物結晶の製造方法および結晶製造装置
JP2001128587A (ja) 1999-11-05 2001-05-15 Kochi Prefecture 付着性水産生物飼育装置およびこれを用いた飼育方法
JP2001338887A (ja) * 2000-05-26 2001-12-07 Sumitomo Electric Ind Ltd Iii−v族窒化物系半導体の成長方法及び成長装置
US20020148402A1 (en) * 2001-04-13 2002-10-17 Sindo Kou Growing of homogeneous crystals by bottom solid feeding
US7001457B2 (en) * 2001-05-01 2006-02-21 Ricoh Company, Ltd. Crystal growth method, crystal growth apparatus, group-III nitride crystal and group-III nitride semiconductor device
PL219109B1 (pl) * 2001-06-06 2015-03-31 Ammono Spółka Z Ograniczoną Odpowiedzialnością Sposób otrzymywania objętościowego monokrystalicznego azotku zawierającego gal oraz urządzenie do otrzymywania objętościowego monokrystalicznego azotku zawierającego gal
US6488767B1 (en) * 2001-06-08 2002-12-03 Advanced Technology Materials, Inc. High surface quality GaN wafer and method of fabricating same
JP2003137698A (ja) * 2001-10-26 2003-05-14 Ulvac Japan Ltd Iii−v族半導体材料
US6949140B2 (en) * 2001-12-05 2005-09-27 Ricoh Company, Ltd. Crystal growth method, crystal growth apparatus, group-III nitride crystal and group-III nitride semiconductor device
US7097707B2 (en) * 2001-12-31 2006-08-29 Cree, Inc. GaN boule grown from liquid melt using GaN seed wafers
US7063741B2 (en) * 2002-03-27 2006-06-20 General Electric Company High pressure high temperature growth of crystalline group III metal nitrides
JP4216612B2 (ja) * 2003-01-29 2009-01-28 株式会社リコー Iii族窒化物結晶の製造方法
JP4248276B2 (ja) * 2003-03-17 2009-04-02 株式会社リコー Iii族窒化物の結晶製造方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Conditions for seeded growth of GaN crystals bythe Na flux method. Masato Aoki, Hisanori Yamane, MasahikoShimada,SeijiSarayama, Francis J. DiSalvo.Materials Letters,Vol.56 No.5. 2002 *

Also Published As

Publication number Publication date
TW200515488A (en) 2005-05-01
EP1538241A3 (en) 2005-06-22
KR101075931B1 (ko) 2011-10-21
CN1612295A (zh) 2005-05-04
KR101117364B1 (ko) 2012-03-07
KR20050041994A (ko) 2005-05-04
KR20110043560A (ko) 2011-04-27
KR101187999B1 (ko) 2012-10-08
EP1538241A2 (en) 2005-06-08
EP1942211A1 (en) 2008-07-09
JP2005154254A (ja) 2005-06-16
JP4534631B2 (ja) 2010-09-01
EP1538241B1 (en) 2008-12-17
TWI399796B (zh) 2013-06-21
EP1942211B1 (en) 2011-09-14
KR20110043563A (ko) 2011-04-27
US20050098090A1 (en) 2005-05-12
KR20110043562A (ko) 2011-04-27
KR20110043561A (ko) 2011-04-27
DE602004018452D1 (de) 2009-01-29
KR101122327B1 (ko) 2012-03-23

Similar Documents

Publication Publication Date Title
CN100550303C (zh) 第ⅲ族氮化物晶体及其制备方法
US8461071B2 (en) Polycrystalline group III metal nitride with getter and method of making
CN101586253B (zh) N型ⅲ族氮化物基化合物半导体及其制造方法
CN102383181B (zh) 制备n-型Ⅲ族氮化物单晶的方法、所述单晶、和晶体基板
WO2010060034A1 (en) METHODS FOR PRODUCING GaN NUTRIENT FOR AMMONOTHERMAL GROWTH
US7294199B2 (en) Nitride single crystal and producing method thereof
CN104047054A (zh) 低碳的iii族元素氮化物晶体
JP5428706B2 (ja) SiC単結晶の製造方法
CN113818085B (zh) 助熔剂法均匀化生长氮化物单晶的系统及方法
JP5299213B2 (ja) Iii族窒化物結晶の製造方法
WO2018047844A1 (ja) 窒化ガリウム積層体の製造方法
CN101243011B (zh) 第13族金属氮化物结晶的制造方法、半导体器件的制造方法和这些制造方法中使用的溶液和熔融液
JP2004231467A (ja) 窒化物単結晶およびその製造方法
EP1612300B1 (en) Method for producing a single crystal of AlN.
CN119553363A (zh) 一种环境友好型的气相生长iii族氮化物晶体的方法
JP2014152066A (ja) 窒化ガリウム単結晶の成長方法
CN101346309A (zh) 多晶硅的制造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20091014

Termination date: 20171029