WO2009060834A1 - 炭素繊維前駆体アクリル繊維用油剤組成物、炭素繊維前駆体アクリル繊維束及びその製造方法 - Google Patents

炭素繊維前駆体アクリル繊維用油剤組成物、炭素繊維前駆体アクリル繊維束及びその製造方法 Download PDF

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Publication number
WO2009060834A1
WO2009060834A1 PCT/JP2008/070055 JP2008070055W WO2009060834A1 WO 2009060834 A1 WO2009060834 A1 WO 2009060834A1 JP 2008070055 W JP2008070055 W JP 2008070055W WO 2009060834 A1 WO2009060834 A1 WO 2009060834A1
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Prior art keywords
agent composition
oil agent
carbon fiber
precursor acrylic
specific
Prior art date
Application number
PCT/JP2008/070055
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English (en)
French (fr)
Inventor
Hiromi Aso
Naoki Sugiura
Original Assignee
Mitsubishi Rayon Co., Ltd.
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Publication date
Application filed by Mitsubishi Rayon Co., Ltd. filed Critical Mitsubishi Rayon Co., Ltd.
Priority to US12/741,763 priority Critical patent/US8932711B2/en
Priority to MX2010005126A priority patent/MX2010005126A/es
Priority to CN2008801148776A priority patent/CN101849063B/zh
Priority to EP08846535.6A priority patent/EP2208821B1/en
Priority to JP2008554560A priority patent/JP4856724B2/ja
Publication of WO2009060834A1 publication Critical patent/WO2009060834A1/ja

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/647—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing polyether sequences
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M7/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made of other substances with subsequent freeing of the treated goods from the treating medium, e.g. swelling, e.g. polyolefins
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/14—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/109—Polyethers, i.e. containing di- or higher polyoxyalkylene groups esterified
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/045—Siloxanes with specific structure containing silicon-to-hydroxyl bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/046—Siloxanes with specific structure containing silicon-oxygen-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/047—Siloxanes with specific structure containing alkylene oxide groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/052—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
    • C10N2020/01—Physico-chemical properties
    • C10N2020/055—Particles related characteristics
    • C10N2020/06—Particles of special shape or size
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/24—Emulsion properties
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/46—Textile oils
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/26—Polymers or copolymers of unsaturated carboxylic acids or derivatives thereof
    • D06M2101/28—Acrylonitrile; Methacrylonitrile
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2929—Bicomponent, conjugate, composite or collateral fibers or filaments [i.e., coextruded sheath-core or side-by-side type]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2933—Coated or with bond, impregnation or core
    • Y10T428/2962—Silane, silicone or siloxane in coating

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Artificial Filaments (AREA)
  • Inorganic Fibers (AREA)
  • Chemical Treatment Of Fibers During Manufacturing Processes (AREA)

Abstract

　本発明は、シリコーン化合物を主成分として用いた油剤組成物を使用するときに発生する操業性低下や、非シリコーン系油剤組成物を使用するときに起きる炭素繊維束物性の低下を改善しうる油剤組成物の提供を目的とする。本発明の炭素繊維前駆体アクリル繊維用油剤組成物は、特定のアルキル鎖を含むユニットを有し、特定のポリエチレンオキサイド鎖を含むユニット、特定のポリグリセリン鎖を含むユニット及び特定のポリエーテル鎖を含むユニットうち少なくとも１つのユニットを有し、特定のポリジメチルシロキシアルキル鎖を含むユニットを任意で有する変性ポリジメチルシロキサンを１～１０ｗｔ％含有することを特徴とする。
PCT/JP2008/070055 2007-11-07 2008-11-04 炭素繊維前駆体アクリル繊維用油剤組成物、炭素繊維前駆体アクリル繊維束及びその製造方法 WO2009060834A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
US12/741,763 US8932711B2 (en) 2007-11-07 2008-11-04 Oil agent composition for acrylic precursor fibers for carbon fibers, acrylic precursor fiber bundle for carbon fibers, and method for producing the same
MX2010005126A MX2010005126A (es) 2007-11-07 2008-11-04 Composicion de agente de aceite para fibra acrilica precursora de fibra de carbon, manojo de fibra acrilica precursora de fibra de carbon y metodo para producir la misma.
CN2008801148776A CN101849063B (zh) 2007-11-07 2008-11-04 碳纤维前体丙烯腈纤维用油剂组合物、碳纤维前体丙烯腈纤维束及其制造方法
EP08846535.6A EP2208821B1 (en) 2007-11-07 2008-11-04 Oil agent composition for carbon fiber precursor acrylic fiber, carbon fiber precursor acrylic fiber bundle, and method for producing the same
JP2008554560A JP4856724B2 (ja) 2007-11-07 2008-11-04 炭素繊維前駆体アクリル繊維用油剤組成物、炭素繊維前駆体アクリル繊維束及びその製造方法

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
JP2007-289409 2007-11-07
JP2007289409 2007-11-07
JP2007318439 2007-12-10
JP2007318440 2007-12-10
JP2007-318439 2007-12-10
JP2007-318440 2007-12-10

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PCT/JP2008/070055 WO2009060834A1 (ja) 2007-11-07 2008-11-04 炭素繊維前駆体アクリル繊維用油剤組成物、炭素繊維前駆体アクリル繊維束及びその製造方法

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US (1) US8932711B2 (ja)
EP (1) EP2208821B1 (ja)
JP (1) JP4856724B2 (ja)
KR (1) KR101210081B1 (ja)
CN (1) CN101849063B (ja)
MX (1) MX2010005126A (ja)
PT (1) PT2208821E (ja)
TW (1) TWI397626B (ja)
WO (1) WO2009060834A1 (ja)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010140488A1 (ja) * 2009-06-04 2010-12-09 松本油脂製薬株式会社 炭素繊維製造用アクリル繊維油剤、炭素繊維製造用アクリル繊維および炭素繊維の製造方法
JP2011042916A (ja) * 2009-07-24 2011-03-03 Mitsubishi Rayon Co Ltd 炭素繊維前駆体アクリル繊維用油剤組成物、および炭素繊維前駆体アクリル繊維束とその製造方法
WO2012117514A1 (ja) * 2011-03-01 2012-09-07 三菱レイヨン株式会社 油剤組成物が付着した炭素繊維前駆体アクリル繊維束とその製造方法、および炭素繊維前駆体アクリル繊維用油剤組成物と炭素繊維前駆体アクリル繊維用油剤組成物分散液
JP2013513034A (ja) * 2009-12-04 2013-04-18 エスゲーエル カーボン ソシエタス ヨーロピア 複合材料を製造するための繊維
JP2014201851A (ja) * 2013-04-04 2014-10-27 三菱レイヨン株式会社 炭素繊維前駆体アクリル繊維用油剤組成物と炭素繊維前駆体アクリル繊維用油剤組成物分散液、および炭素繊維前駆体アクリル繊維束の製造方法
JP2015030931A (ja) * 2013-08-01 2015-02-16 三菱レイヨン株式会社 炭素繊維前駆体アクリル繊維用油剤組成物と炭素繊維前駆体アクリル繊維用油剤組成物分散液、および炭素繊維前駆体アクリル繊維束の製造方法
JP2021050428A (ja) * 2019-09-24 2021-04-01 東レ株式会社 炭素繊維前駆体繊維束および炭素繊維束の製造方法

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CN102454109B (zh) * 2010-10-21 2013-08-07 威海拓展纤维有限公司 一种处理碳纤维前驱体纤维的方法及其专用油剂
EP2719823B1 (en) * 2011-06-06 2017-11-08 Mitsubishi Chemical Corporation Oil agent for carbon fiber precursor acrylic fiber, processed-oil solution for carbon fiber precursor acrylic fibers, carbon fiber precursor acrylic fiber bundle, and method for producing carbon fiber bundle using carbon fiber precursor acrylic fiber bundle
CN103031621B (zh) * 2011-09-29 2014-12-10 中国石油化工股份有限公司 大丝束pan基碳纤维原丝的上油方法
CN103031734B (zh) * 2011-09-29 2015-06-10 中国石油化工股份有限公司 小丝束pan基碳纤维原丝油剂的制备方法
US8986647B2 (en) 2011-10-21 2015-03-24 Wacker Chemical Corporation Hydrophilic silicone copolymers useful in carbon fiber production
JP5309280B1 (ja) * 2012-03-02 2013-10-09 松本油脂製薬株式会社 炭素繊維製造用アクリル繊維処理剤、炭素繊維製造用アクリル繊維および炭素繊維の製造方法
CN104340764B (zh) * 2013-08-09 2017-09-01 中国石油天然气股份有限公司 碳纤维用聚丙烯腈原丝碳化时退丝的加湿处理方法及装置
CN106414841B (zh) * 2014-08-12 2018-08-28 松本油脂制药株式会社 丙烯酸纤维处理剂及其用途
JP6488104B2 (ja) * 2014-10-28 2019-03-20 松本油脂製薬株式会社 アクリル繊維処理剤及びその用途
CN104611787A (zh) * 2014-11-06 2015-05-13 江苏航科复合材料科技有限公司 一种聚丙烯腈基碳纤维原丝制造用油剂及其制造及使用方法
EP3337831B1 (en) 2015-08-21 2024-02-28 G&P Holding, Inc. Silver and copper itaconates and poly itaconates
TWI654240B (zh) 2017-11-22 2019-03-21 財團法人工業技術研究院 碳纖維前驅物組合物以及碳纖維前驅物之製備方法
JP7354840B2 (ja) * 2018-09-28 2023-10-03 東レ株式会社 耐炎化繊維束の製造方法および炭素繊維束の製造方法
JP6671698B1 (ja) * 2019-05-30 2020-03-25 竹本油脂株式会社 炭素繊維前駆体用処理剤及び炭素繊維前駆体
JP7491673B2 (ja) * 2019-08-30 2024-05-28 帝人株式会社 炭素繊維束の製造方法
CN110670350B (zh) * 2019-09-18 2022-01-25 江苏恒神股份有限公司 一种碳纤维原丝用无硅油剂
CN112746354A (zh) * 2020-12-29 2021-05-04 镇江市高等专科学校 一种碳纤维原丝用油剂乳液的制造方法
JP6973837B1 (ja) * 2021-06-04 2021-12-01 竹本油脂株式会社 炭素繊維前駆体用処理剤、及び炭素繊維前駆体
CN114232139A (zh) * 2021-12-16 2022-03-25 连云港神鹰复合材料科技有限公司 一种干喷湿纺原丝用碳纤维油剂的制备方法

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