WO2004047158A1 - プラズマ処理装置およびプラズマ処理方法 - Google Patents
プラズマ処理装置およびプラズマ処理方法 Download PDFInfo
- Publication number
- WO2004047158A1 WO2004047158A1 PCT/JP2003/014850 JP0314850W WO2004047158A1 WO 2004047158 A1 WO2004047158 A1 WO 2004047158A1 JP 0314850 W JP0314850 W JP 0314850W WO 2004047158 A1 WO2004047158 A1 WO 2004047158A1
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- WO
- WIPO (PCT)
- Prior art keywords
- plasma processing
- plasma
- processing chamber
- processing apparatus
- oxide film
- Prior art date
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Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32192—Microwave generated discharge
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/4401—Means for minimising impurities, e.g. dust, moisture or residual gas, in the reaction chamber
- C23C16/4404—Coatings or surface treatment on the inside of the reaction chamber or on parts thereof
Definitions
- the present invention relates to a plasma processing apparatus and a plasma processing method that can be suitably used when performing various plasma processes on an object to be processed in order to manufacture an electronic device or the like.
- the plasma processing apparatus of the present invention can be widely applied to plasma processing in general, including the manufacture of electronic devices such as semiconductors, semiconductor devices, and liquid crystal devices.
- the background art will be described as an example.
- a plasma processing apparatus is often used for such various kinds of processing. This is because when a plasma processing apparatus is used, there is an advantage of low-temperature processing.
- a plasma processing chamber in which an object to be processed is to be subjected to plasma processing is usually configured using metal walls.
- the plasma processing chamber is included in plasma generated in the plasma processing chamber.
- the metal on the inner wall may be sputtered and / or etched to cause contaminants on the object to be processed.
- the inner wall of the plasma processing chamber is subjected to alumite treatment (that is, an oxide film is formed on the aluminum surface) or the inner wall is formed. Ceramic coating has been done.
- An object of the present invention is to provide a plasma processing apparatus and a plasma processing method which solve the above-mentioned disadvantages of the prior art.
- Another object of the present invention is to suppress spattering and etching of a plasma processing chamber inner wall while suppressing contamination of an object to be processed. It is an object of the present invention to provide a plasma processing apparatus and a plasma processing method that can effectively prevent the occurrence of a plasma.
- the present inventor has found that the plasma processing chamber inner wall (and / or the plasma processing chamber inner wall) is not used separately as in the conventional case, but by using the plasma processing itself instead of separately performing alumite processing or ceramic coating processing. It has been found that forming an oxide film on parts that should form the inner wall, etc.) is extremely effective in achieving the above object.
- the plasma processing apparatus of the present invention is based on the above findings, and more specifically, a plasma processing chamber for performing plasma processing on a processing target; and a plasma processing chamber for disposing the processing target in the plasma processing chamber.
- a plasma processing apparatus comprising: at least a target object holding means; and a plasma generation means for generating plasma in the plasma processing chamber; It is characterized by being covered with an oxide film based on processing plasma.
- a plasma processing chamber for performing plasma processing on the processing object; a processing object holding unit for arranging the processing object in the plasma processing chamber;
- a plasma processing apparatus including at least plasma generating means for generating plasma in the plasma processing chamber; when a reference target object is processed in the plasma processing chamber with plasma based on an oxygen-containing gas, the total number of atoms of the target object to your Keru a l, C u, N a and F e the later, 2 x 1 0 1.
- the number is not more than the number.
- a plasma processing chamber for performing plasma processing on the processing object; a processing object holding unit for arranging the processing object in the plasma processing chamber;
- a plasma processing apparatus including at least plasma generating means for generating plasma in the plasma processing apparatus;
- a plasma processing method is provided in which an oxide film is formed on at least a part of the inner wall of the plasma processing chamber by generating the plasma processing chamber.
- the contamination metal itself present in the plasma is not only removed by sputtering based on the plasma treatment for cleaning, but also a predetermined thickness (for example, 10 nm or more) is formed on the surface of the plasma processing chamber inner wall. Since an oxide film having a thickness of about 100 nm is formed, generation of contamination can be effectively suppressed in the subsequent plasma treatment.
- the oxide film on the inner wall of the plasma processing chamber formed based on the plasma processing for cleaning is sufficiently resistant to ion irradiation based on the plasma processing (because the oxide film itself is an oxide film formed by the plasma processing). It is.
- FIG. 1 is a schematic sectional view showing a preferred embodiment of the plasma processing apparatus of the present invention.
- FIG. 2 is a schematic sectional view showing another embodiment of the plasma processing apparatus of the present invention.
- FIG. 3 is a schematic sectional view showing an observation position after an oxide film is formed on the inner wall of the plasma processing apparatus of FIG.
- FIG. 4 is a photograph showing an SEM observation result of an oxide film on the inner wall (aluminum member) of the plasma processing apparatus of FIG.
- FIG. 5 is a photograph showing the result of Auger analysis on the inner wall (aluminum member) of the plasma processing apparatus of FIG.
- Figure 6 is a photograph showing the SEM observation results of the oxide and nitride films on the aluminum test piece placed in the plasma processing apparatus of Figure 2. is there.
- FIG. 7 is a graph showing the measurement results of metal contamination obtained in Example 5.
- FIG. 8 is a graph showing the results of measurement of metal contamination obtained in Example 5.
- a plasma processing chamber for performing plasma processing on the object to be processed; and an object holding means for arranging the object to be processed at a predetermined position in the plasma processing chamber; And a plasma generating means for generating plasma in the plasma processing chamber.
- This plasma processing apparatus is characterized in that at least a part of the inner wall of the plasma processing chamber is covered with an oxide film based on pretreatment plasma.
- the formation of the oxide film may be performed on the inner wall after the plasma processing apparatus is assembled, or may be performed on a part having a part to constitute the inner wall. Accordingly, the formation of the oxide film before and after the assembly may be combined.
- the total area of the inner wall of the plasma processing chamber is 5
- 0% or more is covered with an oxide film having a thickness of at least 1 O nm.
- the proportion of the area covered by the oxide film having a thickness of at least 20 nm is more preferably 60% or more, particularly preferably 80% or more.
- the average thickness of the above oxide film is preferably 20 nm, more preferably 30 nm.
- the thickness of the oxide film, the average film thickness, and the “ratio of the area covered by the oxide film having a thickness of at least 10 nm” are preferably determined by the following measurement methods. Can be measured.
- the object to be processed which is a reference for the contamination
- a 1, Cu, Na, and Fe in the object to be treated after the treatment (hereinafter, these four kinds of metal elements may be collectively referred to as “contamination metal”).
- the total number of atoms 2 X 1 0 1. It is preferable that the number is not more than the number.
- the A l, C u, the total number of atoms of N a and F e are especially 1 X 1 0 1. It is preferable that the number is not more than the number. This is because these four types of contaminant metals have a particularly significant adverse effect on the characteristics of the object (eg, semiconductor device characteristics) when attached or incorporated into the object.
- sample silicon wafer sample wafer, diameter: 20 cm
- plasma treatment is performed by arranging it as an object to be processed, and the total number of atoms of contamination metals in a wafer obtained after the plasma treatment is measured.
- a plasma processing chamber for performing plasma processing on a processing target, and a processing target for disposing the processing target at a predetermined position in the plasma processing chamber.
- a plasma processing apparatus including at least a holding unit and an antenna unit for guiding a microwave to the plasma processing chamber is used.
- plasma based on an oxygen-containing gas is generated in the plasma processing chamber, and an oxide film is formed on an inner wall of the plasma processing chamber.
- another object to be processed for example, a component or a component of a plasma processing apparatus
- the surface of the component or the like is placed on the surface of the component.
- An oxide film may be formed.
- an oxygen-containing gas can be suitably used.
- This "oxygen-containing gas” is such that at least one component of the gas itself (when the gas is a single substance) or the gas (when the gas is a mixture) contains at least oxygen. Just do it.
- Examples of the “oxygen-containing gas” include the following.
- the following gases can be particularly preferably used from the viewpoint of low cost and safety.
- pretreatment plasma conditions can be particularly preferably used. That is, the “pre-treatment plasma” condition is different from the normal plasma condition described below in terms of the treatment speed.
- the present invention it is possible to use ordinary plasma processing conditions for the object to be processed (for example, a substrate for an electronic device such as a semiconductor wafer).
- the degree of oxidation in the plasma processing chamber by the above-described pretreatment plasma is determined, for example, by using a standard sample wafer (or monitor wafer) as the wafer W in FIG.
- the degree of oxidation of the sample wafer can be measured by monitoring the film thickness measurement.
- the oxide film coating in the plasma processing chamber by the pretreatment plasma described above is effective by itself, but the effect is further enhanced by combining with the wet cleaning in advance of the plasma processing chamber. (Wet cleaning)
- wet cleaning in this case preferably includes acid cleaning.
- the type, material, shape, size, manufacturing method, and the like are not particularly limited as long as formation of an oxide film thereon is useful.
- it may be the above-described sample wafer, may be a component or a part of a plasma processing apparatus, or may be various substrates for electronic devices (for example, substrates for various semiconductor devices such as silicon). Material).
- the type, material, shape, size, manufacturing method, and the like are not particularly limited as long as formation of an oxide film thereon is useful.
- the plasma processing chamber may be metal (eg, aluminum, SuS, Si, etc.) or other material (eg, ceramic).
- the type, material, shape, size, manufacturing method, and the like are not particularly limited as long as the object to be processed can be held thereon for a predetermined time.
- a known object holding means such as a chuck and an electrostatic holding means can be suitably used.
- a predetermined plasma for example, a plasma for processing a pretreatment plasma or another object to be processed
- a plasma processing chamber for example, a plasma for processing a pretreatment plasma or another object to be processed
- this plasma generation means may be an antenna means for guiding the microwave into the processing chamber. I like it.
- the antenna means is preferably a planar antenna (RLSA) member having a plurality of slots.
- FIG. 1 is a schematic sectional view showing an example of a plasma processing apparatus according to the present invention.
- FIG. 1 in this embodiment, a case will be described in which the plasma processing apparatus is applied to plasma CVD (Chemical Vapor Deposition) processing.
- the embodiment of FIG. 1 is an example in which a planar antenna member is used as an antenna member.
- the plasma processing apparatus 30 has a plasma processing chamber 32 in which the side walls and the bottom are made of a conductor such as aluminum, and the whole is formed in a cylindrical shape.
- the inside is configured as a closed processing space S.
- a mounting table 34 for mounting an object to be processed (for example, a semiconductor wafer W) on its upper surface is accommodated.
- the mounting table 34 is formed in a substantially columnar shape which is made convex and flat by, for example, anodized aluminum or the like.
- the lower part of the mounting table 34 is also a columnar shape made of aluminum or the like.
- the support base 36 is provided at the bottom of the plasma processing chamber 32 via an insulating material 38.
- An electrostatic chuck or a clamp mechanism (not shown) for holding the wafer is provided on the upper surface of the mounting table 34 described above. Further, the mounting table 34 is connected to a matching box 42 and a high-frequency power source for bias (for example, for 1.3.6 MHz) 44 via a feeder line 40. In the case of CVD, the high-frequency bias power supply 44 need not be provided.
- the support 36 supporting the mounting table 34 is provided with a cooling jacket 46 for flowing cooling water or the like for cooling the wafer W during the plasma processing. Note that a heater for heating may be provided in the mounting table 34 as necessary.
- a plasma gas supply nozzle 48 made of quartz pipe for supplying a plasma gas, for example, an argon gas into the container, or a processing gas, for example,
- a processing gas supply nozzle 50 made of, for example, a quartz pipe for introducing a deposition gas is provided.
- These nozzles 48 and 50 are connected to the gas supply paths 52 and 54, respectively, via the mass flow controllers 56 and 58 and the opening and closing valves 60 and 62, respectively, to generate the plasma gas source 64 and 50, respectively.
- the processing gas source 6 6.
- a deposition gas as a processing gas SiH 4 , O 2 , N 2 gas, or the like can be used.
- a gate valve 68 that opens and closes when loading / unloading the wafer W into / from the plasma processing chamber 32 is provided outside the side wall of the plasma processing chamber 32, and a cooling jacket that cools the side wall. G 69 is provided. Further, an exhaust port 70 is provided at the bottom of the container, and an exhaust path 72 to which a vacuum pump (not shown) is connected is connected to the exhaust port 70, and a plasma processing chamber is provided as necessary. It is designed to evacuate the interior of 32 to a specified pressure.
- the ceiling of the plasma processing chamber 32 is opened, and is made of a ceramic material such as A1N, for example, and has an insulating plate 74 (for example, a thick plate) that transmits microwaves. (About 20 mm) is provided in an airtight manner via a sealing member 76 such as an O-ring.
- a disk-shaped planar antenna member 78 and a slow-wave member 80 having high dielectric constant characteristics are provided on the upper surface of the insulating plate 74.
- the planar antenna member 78 is formed integrally with the plasma processing chamber 32. It is configured as a bottom plate of a waveguide box 82 formed of a hollow cylindrical container, and is provided to face the mounting table 34 in the plasma processing chamber 32.
- the waveguide box 82 and the plasma processing chamber 32 are both grounded, and an outer tube 84 A of a coaxial waveguide 84 is connected to the center of the upper part of the waveguide box 82,
- the internal cable 84B is connected to the center of the planar antenna member 78 through a through hole 86 at the center of the slow wave member 80.
- the coaxial waveguide 84 is connected to, for example, a 2.45 GHz microwave generator 92 via a mode converter 88 and a waveguide 90. Microwaves are propagated to antenna members 78. This frequency is not limited to 2.45 GHz, and another frequency, for example, 8.35 GHz may be used.
- a waveguide having a circular or rectangular cross section or a coaxial waveguide can be used.
- a ceiling cooling jacket 96 in which a cooling water flow passage 94 for flowing cooling water is formed is provided to cool the slow wave material 80 and the like. It has become.
- the slow wave material 80 having the above-mentioned high dielectric constant is provided, and by this wavelength shortening effect, the micro wave is reduced. The tube wavelength has been shortened.
- the slow wave material 80 for example, aluminum nitride or the like can be used.
- planar antenna member 78 corresponds to an 8-inch wafer W
- a conductive material having a diameter of 300 to 400 mm and a thickness of 1 to several mm (for example, 5 mm) is used.
- a disk made of, for example, a copper plate or an aluminum plate whose surface is coated with silver, has a large number of microwave radiation holes 98 made of, for example, circular through holes, and an antenna member 78 Are provided substantially uniformly.
- the arrangement of the microphone mouth-wave radiation holes 98 is not particularly limited. It may be arranged spirally or radially.
- the shape of the microwave radiation holes 98 is not limited to a circular shape, and may be, for example, a slit shape of a long groove, and the slit-shaped radiation holes may be represented by “C”. They may be arranged in a pattern.
- the semiconductor wafer WW is accommodated in the plasma processing chamber 32 by the transfer arm (not shown) via the gate valve 68, and the lifter pin (not shown) is moved up and down.
- the wafer WW is mounted on the mounting surface of the mounting table 3 4.
- the plasma gas supply nozzle 48 supplies, for example, argon gas while controlling the flow rate.
- a deposition gas such as SiH 4 , O 2 , and N 2 is supplied while controlling the flow rate.
- the microwave from the microwave mouthpiece generator 92 is supplied to the planar antenna member 78 via the waveguide 90 and the coaxial waveguide 84, and is supplied to the processing space S and the slow wave material 8 Microwaves whose wavelength is shortened by 0 are introduced, thereby generating plasma and performing predetermined plasma processing, for example, film forming processing by plasma CVD.
- the object to be processed is not limited to the semiconductor wafer W, but can be applied to a glass substrate, an LCD (liquid crystal device) substrate, and the like.
- the above-described sample wafer, monitor wafer, or wafer for performing ordinary plasma processing is generally subjected to the following cleaning processing.
- Substrate A 20 cm (8 inch) P-type silicon substrate was used as the substrate, with a specific resistance of l Qcm and a plane orientation of (100).
- IPA isopropyl alcohol, 220 ° C
- an oxide film was coated in the plasma processing chamber by using the silicon wafer (sample / wafer) W after the cleaning treatment as in the first embodiment.
- Plasma output 2500 W Temperature: 400 ° C
- the aluminum-test piece was oxidized under the following plasma processing conditions using a plasma processing apparatus on which an oxide film forming process according to Example 2 was performed.
- Plasma power 350 W
- Plasma power 350 W
- plasma is generated in the plasma processing chamber by using the silicon wafer (sample wafer) W that has been subjected to the cleaning process as in Example 1 in the following manner.
- the metal contamination at was measured.
- a plasma processing apparatus and a plasma processing method that effectively prevent sputtering and etching of the inner wall of a plasma processing chamber while suppressing contamination of an object to be processed.
- a plasma processing method is provided.
Abstract
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Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/535,856 US7754995B2 (en) | 2002-11-20 | 2003-11-20 | Plasma processing apparatus and plasma processing method |
AU2003284605A AU2003284605A1 (en) | 2002-11-20 | 2003-11-20 | Plasma processing apparatus and plasma processing method |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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JP2002336837A JP3946130B2 (ja) | 2002-11-20 | 2002-11-20 | プラズマ処理装置およびプラズマ処理方法 |
JP2002-336837 | 2002-11-20 |
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WO2004047158A1 true WO2004047158A1 (ja) | 2004-06-03 |
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PCT/JP2003/014850 WO2004047158A1 (ja) | 2002-11-20 | 2003-11-20 | プラズマ処理装置およびプラズマ処理方法 |
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US (1) | US7754995B2 (ja) |
JP (1) | JP3946130B2 (ja) |
AU (1) | AU2003284605A1 (ja) |
TW (1) | TWI256069B (ja) |
WO (1) | WO2004047158A1 (ja) |
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JP2004172397A (ja) | 2004-06-17 |
AU2003284605A1 (en) | 2004-06-15 |
TW200415685A (en) | 2004-08-16 |
US7754995B2 (en) | 2010-07-13 |
JP3946130B2 (ja) | 2007-07-18 |
TWI256069B (en) | 2006-06-01 |
US20060108331A1 (en) | 2006-05-25 |
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