JPH11505567A - 硬化性樹脂ゾル - Google Patents
硬化性樹脂ゾルInfo
- Publication number
- JPH11505567A JPH11505567A JP8534836A JP53483696A JPH11505567A JP H11505567 A JPH11505567 A JP H11505567A JP 8534836 A JP8534836 A JP 8534836A JP 53483696 A JP53483696 A JP 53483696A JP H11505567 A JPH11505567 A JP H11505567A
- Authority
- JP
- Japan
- Prior art keywords
- resin
- curable resin
- sol
- composition
- fine particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/06—Pretreated ingredients and ingredients covered by the main groups C08K3/00 - C08K7/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/02—Fibres or whiskers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
Abstract
Description
Claims (1)
- 【特許請求の範囲】 1.(a)硬化性樹脂中の実質的に球形で、実質的に無機の微粒子のコロイド 状分散を含む硬化性樹脂ゾルと、(b)強化繊維とを含む組成物。 2.前記組成物は本質的に揮発物を含有しない請求項1に記載の組成物。 3.前記硬化性樹脂はエポキシ樹脂、硬化性イミド樹脂、ビニルエステル樹脂 、アクリル樹脂、ビスベンゾシクロブタン樹脂、ポリシアネートエステル樹脂、 およびそれらの混合物から成る群から選択される樹脂を含み、前記微粒子はシリ カ、チタニア、アルミナ、ジルコニア、バナジア、クロミア、酸化鉄、酸化アン チモン、酸化スズ、またはそれらの混合物を含む請求項1に記載の組成物。 4.前記微粒子の平均粒子直径は約1nmから約1000nmの範囲であり、前記 微粒子は前記微粒子と前記樹脂を相溶化させるのに役立つ表面結合有機基を有す る請求項1に記載の組成物。 5.前記強化繊維は連続的であり、カーボン、ガラス、セラミック、ホウ素、 炭化ケイ素、ポリイミド、ポリアミド、ポリエチレンまたはそれらの組み合せを 含み、且つ個々の連続繊維の一方向配列、織布、メリヤス生地、糸、ロービング 、編組構造、または不織マットを含む請求項1に記載の組成物。 6.(a)硬化性樹脂中の実質的に球形で、実質的に無機の微粒子のコロイド 状分散を含む硬化性樹脂ゾルであって、前記微粒子はシリカを含み、前記硬化性 樹脂はエポキシ樹脂を含む硬化性樹脂ゾルと、(b)カーボンまたはガラスを含 む強化繊維とを含む組成物。 7.請求項1に記載の組成物を含むプレプレグ。 8.請求項1に記載の硬化した組成物を含む製品。 9.改良された樹脂支配的機械的特性を具有する請求項1に記載の繊維含有組 成物を作製する方法であって、(a)少なくとも1種の硬化性樹脂および少なく とも1種のオルガノゾルを含む混合物であって、前記オルガノゾルは揮発性液体 および実質的に球形で、実質的に無機の微粒子を含む混合物を形成する工程と、 (b)硬化性樹脂ゾルを形成するために、前記揮発性液体を前記混合物から除去 する工程と、(c)繊維含有組成物を形成するために、前記混合物または前記硬 化性樹脂ゾルを強化繊維と結合させる工程とを含む方法。 10.請求項9に記載の方法で作製されたプレプレグ。 11.請求項9に記載の方法で作製された複合材を含む製品。 12.本質的に揮発物を含まない、硬化性樹脂中の実質的に球形で、実質的に 無機の微粒子のコロイド状分散を含む硬化性樹脂ゾルであって、前記微粒子は、 前記微粒子を前記樹脂と相溶性にさせる表面結合有機基を有する硬化性樹脂ゾル 。 13.本質的に揮発物を含まない、硬化性樹脂中の実質的に球形で、実質的に 無機の微粒子のコロイド状分散を含む硬化性樹脂ゾルであって、前記微粒子はシ リカを含み、且つ前記微粒子を前記樹脂と相溶性にさせる表面結合有機基を有し 、前記樹脂はエポキシ樹脂を含む硬化性樹脂ゾル。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/442,026 | 1995-05-16 | ||
US08/442,026 US5648407A (en) | 1995-05-16 | 1995-05-16 | Curable resin sols and fiber-reinforced composites derived therefrom |
PCT/US1996/005438 WO1996036665A1 (en) | 1995-05-16 | 1996-04-19 | Curable resin sols |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2006248461A Division JP2006328425A (ja) | 1995-05-16 | 2006-09-13 | 硬化性樹脂ゾル及びその組成物 |
Publications (1)
Publication Number | Publication Date |
---|---|
JPH11505567A true JPH11505567A (ja) | 1999-05-21 |
Family
ID=23755229
Family Applications (4)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP8534836A Pending JPH11505567A (ja) | 1995-05-16 | 1996-04-19 | 硬化性樹脂ゾル |
JP2006248461A Withdrawn JP2006328425A (ja) | 1995-05-16 | 2006-09-13 | 硬化性樹脂ゾル及びその組成物 |
JP2008107121A Expired - Lifetime JP5107778B2 (ja) | 1995-05-16 | 2008-04-16 | 硬化性樹脂ゾル及びその組成物 |
JP2012064476A Expired - Lifetime JP5622119B2 (ja) | 1995-05-16 | 2012-03-21 | 硬化性樹脂ゾル及びその組成物 |
Family Applications After (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2006248461A Withdrawn JP2006328425A (ja) | 1995-05-16 | 2006-09-13 | 硬化性樹脂ゾル及びその組成物 |
JP2008107121A Expired - Lifetime JP5107778B2 (ja) | 1995-05-16 | 2008-04-16 | 硬化性樹脂ゾル及びその組成物 |
JP2012064476A Expired - Lifetime JP5622119B2 (ja) | 1995-05-16 | 2012-03-21 | 硬化性樹脂ゾル及びその組成物 |
Country Status (6)
Country | Link |
---|---|
US (1) | US5648407A (ja) |
EP (1) | EP0826017B1 (ja) |
JP (4) | JPH11505567A (ja) |
KR (1) | KR100389953B1 (ja) |
DE (1) | DE69632043D1 (ja) |
WO (1) | WO1996036665A1 (ja) |
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JP2011524444A (ja) * | 2008-06-12 | 2011-09-01 | スリーエム イノベイティブ プロパティズ カンパニー | ナノ粒子を樹脂と複合する方法 |
WO2011125396A1 (ja) * | 2010-04-05 | 2011-10-13 | 日東紡績株式会社 | シリカ微粒子保持ガラス繊維織物の製造方法、シリカ微粒子保持ガラス繊維織物及び繊維強化樹脂成形体 |
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JP2011524444A (ja) * | 2008-06-12 | 2011-09-01 | スリーエム イノベイティブ プロパティズ カンパニー | ナノ粒子を樹脂と複合する方法 |
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JP2016193963A (ja) * | 2015-03-31 | 2016-11-17 | 株式会社アドマテックス | フィラー強化複合材料及びプリプレグ |
Also Published As
Publication number | Publication date |
---|---|
WO1996036665A1 (en) | 1996-11-21 |
JP5622119B2 (ja) | 2014-11-12 |
KR100389953B1 (ko) | 2003-10-08 |
JP2008179835A (ja) | 2008-08-07 |
US5648407A (en) | 1997-07-15 |
JP5107778B2 (ja) | 2012-12-26 |
JP2006328425A (ja) | 2006-12-07 |
DE69632043D1 (de) | 2004-05-06 |
EP0826017A1 (en) | 1998-03-04 |
JP2012144736A (ja) | 2012-08-02 |
KR19990014780A (ko) | 1999-02-25 |
EP0826017B1 (en) | 2004-03-31 |
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