DE15734579T1 - Fluorhaltige wasserabstossende zusammensetzung - Google Patents

Fluorhaltige wasserabstossende zusammensetzung Download PDF

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DE15734579T1
DE15734579T1 DE15734579.4T DE15734579T DE15734579T1 DE 15734579 T1 DE15734579 T1 DE 15734579T1 DE 15734579 T DE15734579 T DE 15734579T DE 15734579 T1 DE15734579 T1 DE 15734579T1
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isomers
weight
monomer
composition
substrate
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Waltraud GASAFI-MARTIN
Wolfgang Knaup
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Archroma IP GmbH
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Archroma IP GmbH
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Abstract

Zusammensetzung, aufweisend mindestens die Komponenten (A) und (B) und gegebenenfalls mindestens einer der Komponenten (C) bis (E): (A) Polyacrylat erhalten durch Polymerisation der Monomeren (M1) CH2=CR3COO-R1 (M2) CH2=CR3COO-R2 (M3) CH2=CR6COO-Y-RF und gegebenenfalls (M4) CH2=CR3-X-R4, (B) Wachs; (C) inaktiviertes Isocyanat; (D) organisches Polysiloxan; (E) Melaminharz; wobei R1 der Alkoholrest im (Meth)acrylatmonomer (M1) mit 1 bis 8 Kohlenstoffatome ist; R2 der Alkoholanteil im Methacrylatmonomer (M2) mit 9 bis 40 Kohlenstoffatome ist; RF-Y der Alkoholrest im Methacrylatmonomer (M3) ist, wobei Y -(CH2)m- ist, wobei m eine ganze Zahl im Bereich von 1 bis 10 ist; und RF CxF2x+1 ist, wobei x eine ganze Zahl im Bereich von 1 bis 12, vorzugsweise 1 bis 6, bevorzugter 4 bis 6 ist; R6 ausgewählt ist aus H, CH3, Cl oder F; R3 in Monomer (M1), (M2) und (M4) unabhängig ausgewählt ist aus H, CH3 oder C2H5; X in Monomer (M4) COO oder CONH ist; R4 Glycidyl oder CH2(CH2)n, OR5 ist, wobei n eine ganze Zahl im Bereich von 1 bis 10 und R5 H oder ein Rest mit 1 bis 6 Kohlenstoffatomen ist; und wobei die Zusammensetzung auf Wasser und/oder einem organischen Lösungsmittel basiert.

Claims (18)

  1. Zusammensetzung, aufweisend mindestens die Komponenten (A) und (B) und gegebenenfalls mindestens einer der Komponenten (C) bis (E): (A) Polyacrylat erhalten durch Polymerisation der Monomeren (M1) CH2=CR3COO-R1 (M2) CH2=CR3COO-R2 (M3) CH2=CR6COO-Y-RF und gegebenenfalls (M4) CH2=CR3-X-R4, (B) Wachs; (C) inaktiviertes Isocyanat; (D) organisches Polysiloxan; (E) Melaminharz; wobei R1 der Alkoholrest im (Meth)acrylatmonomer (M1) mit 1 bis 8 Kohlenstoffatome ist; R2 der Alkoholanteil im Methacrylatmonomer (M2) mit 9 bis 40 Kohlenstoffatome ist; RF-Y der Alkoholrest im Methacrylatmonomer (M3) ist, wobei Y -(CH2)m- ist, wobei m eine ganze Zahl im Bereich von 1 bis 10 ist; und RF CxF2x+1 ist, wobei x eine ganze Zahl im Bereich von 1 bis 12, vorzugsweise 1 bis 6, bevorzugter 4 bis 6 ist; R6 ausgewählt ist aus H, CH3, Cl oder F; R3 in Monomer (M1), (M2) und (M4) unabhängig ausgewählt ist aus H, CH3 oder C2H5; X in Monomer (M4) COO oder CONH ist; R4 Glycidyl oder CH2(CH2)n, OR5 ist, wobei n eine ganze Zahl im Bereich von 1 bis 10 und R5 H oder ein Rest mit 1 bis 6 Kohlenstoffatomen ist; und wobei die Zusammensetzung auf Wasser und/oder einem organischen Lösungsmittel basiert.
  2. Zusammensetzung nach Anspruch 1, wobei R1 1 bis 6 Kohlenstoffatome und R2 12 bis 40 Kohlenstoffatome enthält.
  3. Zusammensetzung nach Anspruch 1 oder 2, wobei R1 verzweigtes oder unverzweigtes oder zyklisches C1 bis C6-Alkyl und R2 verzweigtes oder unverzweigtes oder zyklisches C12 bis C40-Alkyl ist.
  4. Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei R1 ausgewählt ist aus einer oder mehreren der Gruppe bestehend aus Methyl, Ethyl, n-Propyl-, iso-Propyl, n-Butyl, iso-butyl, sec-Butyl, tert-Butyl, n-Pentyl und Isomere davon, n-Hexyl und Isomere davon, Cyclopropyl, Cyclobutyl, Cyclopentyl, Cyclohexyl; und R2 ausgewählt ist aus einer oder mehreren der Gruppe bestehend aus n-Dodecyl (lauryl) und Isomere davon, n-Tridecyl und Isomere davon, n-Tetradecyl (myristyl) und Isomere davon, n-Pentadecyl und Isomere davon, n-Hexadecyl (cetyl) und Isomere davon, n-Heptadecyl und Isomere davon, n-Octadecyl (stearyl) und Isomere davon, n-Nonadecyl und Isomere davon, n-Eicosyl und Isomere davon, n-Heneicosyl und Isomere davon, n-Docosyl (Behenyl) und Isomere davon, n-Tricosyl und Isomere davon, n-Tetracosyl und Isomere davon, n-Pentacosyl und Isomere davon, n-Hexacosyl (ceryl) und Isomere davon, n-Heptacosyl und Isomere davon, n-Octacosyl und Isomere davon, n-Nonacosyl und Isomere davon, n-Triacontyl (Myricyl) und Isomere davon.
  5. Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei (A) bei der Polymerisation von 5 bis 40 Gew.-% Monomer (M1); 30 bis 85 Gew.-% Monomer (M2); 1 bis 50 Gew.-% Monomer (M3); und optional 0,1 bis 20 Gew.-% Monomer (M4); bezogen auf die Gesamtmenge an (A) (= 100 Gew.-%), erhalten wird.
  6. Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei (A) bei der Polymerisation von 5 bis 30 Gew.-% Monomer (M1); 30 bis 70 Gew.-% Monomer (M2); 5 bis 40 Gew.-% Monomer (M3); und optional 0,1 bis 10 Gew.-% (M4); bezogen auf die Gesamtmenge an (A) (= 100 Gew.-%), erhalten wird.
  7. Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei das Wachs (B) einen Schmelzpunkt im Bereich von 50 bis 130°C aufweist.
  8. Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei das Wachs (B) einen Schmelzpunkt im Bereich von 60 bis 90°C aufweist.
  9. Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei das Wachs (B) ein Paraffinwachs ist.
  10. Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei die Zusammensetzung 5 bis 90 Gew.-% (A); 5 bis 90 Gew.-% (B); 0 bis 40 Gew.-% (C); 0 bis 40 Gew.-% (D); 0 bis 40 Gew.-% (E); 0,1–90 Gew.-% Wasser und/oder ein organisches Lösungsmittel bezogen auf die Gesamtmenge der Zusammensetzung (= 100 Gew.-%), aufweist.
  11. Verfahren zur Herstellung einer Zusammensetzung nach einem der vorhergehenden Ansprüche, aufweisend mindestens die Schritte (C1) bis (C2): (C1) Homogenisieren einer Mischung, die mindestens die Monomere (M1), (M2) und (M3) und ein Wachs (B) und Wasser und/oder ein organisches Lösungsmittel aufweist; (C2) Polymerisieren der in Schritt (C1) erhaltenen Mischung.
  12. Verfahren zur Behandlung eines Substrats, aufweisend mindestens Schritt (S1): (S1) Kontaktieren eines Substrats mit der in einem der Ansprüche 1 bis 10 definierten Zusammensetzung, oder in Kontakt bringen eines Substrats mit der Zusammensetzung, die gemäß des in Anspruch 11 definierten Verfahrens hergestellt ist.
  13. Substrat, aufweisend mindestens die Komponenten (A) und (B), wie in Anspruch 1 definiert.
  14. Substrat nach Anspruch 13, behandelt nach dem Verfahren nach Anspruch 12.
  15. Substrat nach Anspruch 13 oder 14, wobei das Substrat in Form einer linearen Formation wie einem Faden und Garn, in Form einer ebenen Formation, wie einem Gewebe, gestricktem Gewebe, geknotetem Gewebe, Vliesstoff, Filz oder in Form einer räumlichen Formation, wie einem Schlauch und Outwear für Frauen, Männer und Kinder vorliegt; oder wobei das Substrat ein Textil, Faser, Gewebe, Papier, Vlies, Leder oder eine Kombination von zwei oder mehreren davon ist.
  16. Verfahren nach Anspruch 12, wobei das Substrat in Form einer linearen Formation wie einem Faden und Garn, in Form einer ebenen Formation, wie Gewebe, gestricktes Gewebe, geknotetes Gewebe, Vliesstoff, Filz oder in Form einer räumlichen Formation, wie einem Schlauch und Outwear für Frauen, Männer und Kinder vorliegt; oder wobei das Substrat ein Textil, Faser, Gewebe, Papier, Vlies, Leder oder eine Kombination von zwei oder mehreren davon ist.
  17. Verwendung einer Zusammensetzung nach einem der Ansprüche 1 bis 10 oder einer Zusammensetzung hergestellt nach dem in Anspruch 11 definierten Verfahren, in oder als Veredelung für jegliches Textil in Form einer linearen Formation, wie einem Faden und Garn, in Form einer planaren Formation, wie einem Gewebe, gestricktem Gewebe, geknotetem Gewebe, Vliesstoff, Filz, oder in Form einer räumlichen Formation, wie einem Schlauch und Outwear für Frauen, Männer und Kinder.
  18. Verwendung eines Wachses, das ein n-Paraffin aufweist oder daraus besteht, in einer Menge von 75 bis 95 Gew.-% und einem oder mehreren Isoparaffinen, Cycloparaffinen oder einer aromatischen Verbindung in einer Menge von 5 bis 25 Gew.-%, bezogen auf die Gesamtmenge des Wachses, wobei das n-Paraffin 20 bis 60 Kohlenstoffatome aufweist, wobei vorzugsweise das n-Paraffin ein Molekulargewicht von 300 bis 600 aufweist in oder als Veredelung für jegliches Textil in Form einer linearen Formation, wie einem Faden und Garn, in Form einer ebenen Formation, wie einem Gewebe, gestricktem Gewebe, geknotetem Gewebe, Vliesstoff, Filz oder in Form einer räumlichen Formation wie einem Schlauch und Outwear für Frauen, Männer und Kinder.
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