CN203128526U - Distillation-free biodiesel production system - Google Patents
Distillation-free biodiesel production system Download PDFInfo
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- CN203128526U CN203128526U CN2013200551772U CN201320055177U CN203128526U CN 203128526 U CN203128526 U CN 203128526U CN 2013200551772 U CN2013200551772 U CN 2013200551772U CN 201320055177 U CN201320055177 U CN 201320055177U CN 203128526 U CN203128526 U CN 203128526U
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 27
- 239000003225 biodiesel Substances 0.000 title claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 73
- 239000007788 liquid Substances 0.000 claims abstract description 62
- 238000000926 separation method Methods 0.000 claims abstract description 48
- 239000000084 colloidal system Substances 0.000 claims abstract description 28
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000012075 bio-oil Substances 0.000 claims description 56
- 239000004519 grease Substances 0.000 claims description 50
- 239000003921 oil Substances 0.000 claims description 49
- 238000000034 method Methods 0.000 claims description 26
- 239000002551 biofuel Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 15
- 238000004821 distillation Methods 0.000 claims description 11
- 241000883990 Flabellum Species 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 6
- 150000002500 ions Chemical class 0.000 claims description 6
- 238000006385 ozonation reaction Methods 0.000 claims description 5
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- 238000007599 discharging Methods 0.000 claims 1
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- 239000010806 kitchen waste Substances 0.000 abstract 1
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- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
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- 150000003509 tertiary alcohols Chemical class 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000002918 waste heat Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B5/00—Operations not covered by a single other subclass or by a single other group in this subclass
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
- C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L5/00—Solid fuels
- C10L5/40—Solid fuels essentially based on materials of non-mineral origin
- C10L5/48—Solid fuels essentially based on materials of non-mineral origin on industrial residues and waste materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W10/00—Technologies for wastewater treatment
- Y02W10/30—Wastewater or sewage treatment systems using renewable energies
- Y02W10/37—Wastewater or sewage treatment systems using renewable energies using solar energy
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Environmental & Geological Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Processing Of Solid Wastes (AREA)
- Fats And Perfumes (AREA)
- Drying Of Solid Materials (AREA)
- Liquid Carbonaceous Fuels (AREA)
- Treatment Of Water By Oxidation Or Reduction (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Treating Waste Gases (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Crushing And Pulverization Processes (AREA)
- Treatment Of Sludge (AREA)
- Combined Means For Separation Of Solids (AREA)
- Catalysts (AREA)
Abstract
The utility model discloses a distillation-free biodiesel production system for treating kitchen waste. The system comprises a horizontal spiral ribbon solid-liquid separation device, an oil-water separation tower, an oil storage container, an oil colloid removing device, a biodiesel normal temperature exchange device, a liquid separation device and a filtering device. The outlet of the horizontal spiral ribbon solid-liquid separation device is connected to the middle lower end of the oil-water separation tower through a pipeline, the oil storage container is communicated with the oil colloid removing device through a pipeline, and the oil outlet is communicated to a strong gas-liquid mixer through a pipeline. The oil mixed with ozone gas enters into an ozone treatment reactor. The oil after ozone treatment is output to the biodiesel normal temperature exchange device through the lower outlet of the oil reactor. The bottom of the biodiesel normal temperature exchange device is communicated with the liquid separation device through a pipeline. The bottom of the liquid separation device is connected to the filtering device through an oil pipeline. The filtering device outputs the biodiesel. The system provided by the utility model is simple in device structure, energy-saving and low in production cost.
Description
Technical field
The utility model discloses a kind of changing food waste treatment unit, more specifically relates to a kind of distillation method production of biodiesel system that exempts from for the changing food waste processing.
Background technology
The science and technology of utilization of waste as resource; through using for a long time; proved a reason; if be exactly the single application of resource treatment technique of waste; its consequence will be brought bigger crisis to environment for human survival; especially the serious problems that produce secondary pollution are difficult to control, so the comprehensive treating process of waste has become the trend of current development.The composition of changing food waste is extremely complicated, wherein comprises materials such as sewage, plastics bag, Plastic Bottle, useless cloth, putrefactive organism, paper, metal Bottle ﹠ Can, broken glass, broken ceramic plate, animal grease, Vegetable oil lipoprotein, primary bacterial body.At present the changing food waste into resources treatment technology at home and abroad method and technology in present " a hundred flowers blossom " situation, but substantially all be simple single-item handling, the international environmental protection treatment trend and direction that does not have trend to turn to comprehensive treating process, utilize and dispose from simple processing, may cause inevitable dirt settling in the changing food waste to shift and disorderly fill out and leave about, cause water and soil to pollute, or shift, not only stop up the urban sewage pipeline, distribute foul odour, cause serious secondary pollution.The single treatment process of changing food waste is worth to consider it is feasible from recycling, but considers from the environment of preserving our planet for a long time, the people's comprehensive angle livable, the protection atmospheric environment, still may be more harm than good.At present, in the treating processes of changing food waste, usually all be to extract wherein solid matter as feed, and waste water and grease all mix discharge, still can cause secondary pollution to environment, though the current technology that has the grease that adopts in the changing food waste to make biofuel, but it only is that the grease in the changing food waste is carried out bulk processing, and range of application is less, can not be widely used in the life, and its production unit is huge, complex manufacturing, processing cost are higher.
Summary of the invention
Handle shortcomings such as making the oil equipment complex structure at the above-mentioned changing food waste of mentioning of the prior art, the utility model provides a kind of new distillation method production of biodiesel system that exempts from, its by solid-liquid separation, oily water separation, grease colloid remove, steps such as ozonize reaction, the exchange of ultrasonic wave normal temperature fat convert the grease that contains in the changing food waste to biofuel, further utilize.
The technical scheme that its technical problem that solves the utility model adopts is: a kind of distillation method production of biodiesel system that exempts from, this system comprises horizontal ribbon solid-liquid separating equipment, the oily water separation tower, oil pot, the grease colloid removes equipment, bio oil normal temperature fat switching equipment, separatory equipment and filter plant, the outlet of horizontal ribbon solid-liquid separating equipment is by pipe connection lower end to the oily water separation tower, be provided with water back in the oily water separation tower, water back stretches to oily water separation tower inside from oily water separation tower bottom, export the oily water separation tower outside again to from oily water separation tower middle and upper part, the oily water separation top of tower is provided with oil wiper, the oily water separation tower is connected with oil pot by flowline, the flowline entrance is corresponding to the oil wiper setting, oil pot removes equipment by pipeline with the grease colloid and is communicated with, the grease colloid removes device interior and is provided with and is set with the hole crash panel, the both sides correspondence position of crash panel is separately installed with rotary propeller type waterpower pusher, the water screw flabellum of rotary propeller type waterpower pusher is arranged on the grease colloid and removes in the equipment, motor is arranged on the grease colloid and removes the equipment outside, electric motor driving water screw flabellum rotates, the grease colloid removes the equipment bottom and is provided with the grease outlet, the grease outlet is communicated to powerful gas by pipeline, liquid mixer with enter reactor after ozone mixes and carry out oxidation, except impurity in the degrease, pigment, stink, protein etc., in the regrowth oil normal temperature fat switching equipment, be provided with more than one ultrasonic generator in the bio oil normal temperature fat switching equipment, bio oil normal temperature fat switching equipment top has dog-house, bio oil normal temperature fat switching equipment bottom is communicated to separatory equipment by pipeline, the separatory device bottom is connected to filter plant by oil pipeline, filter plant output biofuel.
The technical scheme that its technical problem that solves the utility model adopts further comprises:
Described horizontal ribbon solid-liquid separating equipment includes a horizontal cylindrical housing, be provided with filter screen in the shell, the filter screen internal fixation is provided with the conveying ribbon, the ribbon drive-motor cooperates variator to drive filter screen and ribbon rotates, and horizontal ribbon solid-liquid separating equipment bottom is provided with oil, water mixture output channel.
Infrared rays water body liquid level orientator is equipped with at the top of described oily water separation tower.
Described flowline is provided with motorized valve.
Described ozone gas is provided by ozonizer.
Described ultrasonic generator periphery is equipped with sleeve pipe respectively, has the internal thread fluid orifice around the sleeve pipe, and the material of sleeve pipe is to discharge cationic acid and alkali-resistance plastics.
Described sleeve pipe upper fixed is provided with fastener, by fastener ultrasonic generator is installed in bio oil normal temperature fat switching equipment inside.
In the described bio oil normal temperature fat switching equipment liquid guide flow pipe is housed, liquid guide flow Guan Yiduan is connected bio oil normal temperature fat switching equipment top, and the other end is connected bio oil normal temperature fat switching equipment bottom, is connected with the pump tool on the liquid guide flow pipe.
Described bio oil normal temperature fat switching equipment bottom is provided with aspiration tube, and an end of aspiration tube connects air compressor.
The beneficial effects of the utility model are: the utility model can be automatically separates the solid that comprises in the changing food waste, moisture etc., further contained grease being converted to biofuel then uses, device structure is simple, treating processes, and save energy, production cost are low.
Below in conjunction with the drawings and specific embodiments the utility model is described further.
Description of drawings
Fig. 1 is the utility model Zhong Shui, oil, solid separation device structural representation.
Fig. 2 is production of biodiesel apparatus structure synoptic diagram in the utility model.
Fig. 3 is bio oil normal temperature fat switching equipment tangent plane structural representation in the utility model.
Fig. 4 is ultrasonic transducer tangent plane structural representation in the utility model.
Among the figure, 1-oil pot, 2-profit mixing pit, the horizontal ribbon solid-liquid separating equipment of 3-, 4-oily water separation tower, 5-water back, 6-infrared rays water body liquid level orientator, 7-oil wiper, 8-flowline, the 9-motorized valve, the 10-oil inlet pipe, 11-grease colloid removes equipment, 12-hole crash panel, 13-doser, 14-rotary propeller type waterpower pusher, the 15-water outlet, 16-bio oil normal temperature fat switching equipment, 17-ultrasonic transducer, the 18-sleeve pipe, 19-internal thread fluid orifice, 20-fastener, 21-liquid guide flow pipe, 22-pump tool, 23-top cover, the 24-dog-house, 25-pressurized air is agitated pipe, 26-separatory equipment, the 27-filter plant, 28-ozonization device, 28A-ozonizer, the anti-recoil valve of 29-, the powerful gas of 30-, liquid mixer, the 31-liquid-level controller, 32-ozone residual air is destroyed device, 33-theorem feeder, the 34-recycle pump, the pneumatic landing device of 35-.
Embodiment
Present embodiment is the utility model preferred implementation, and other all its principles are identical with present embodiment or approximate with basic structure, all within the utility model protection domain.
The utility model is that oil, water, solid mixture that each workshop section in the changing food waste treating processes produces are handled, and makes the system of biofuel with it.
Please referring to accompanying drawing 1, biofuel manufacturing system front end in the utility model is provided with profit mixing pit 2, each workshop section produces in the changing food waste treating processes oil, water, solid mixture are delivered in the profit mixing pit 2 by outlet conduit, and profit mixing pit 2 is arranged on the outlet conduit tail end.Profit mixing pit 2 rear ends are provided with a horizontal ribbon solid-liquid separating equipment 3, be used for the solid of oil, water, solid mixture is deviate from, in the present embodiment, horizontal ribbon solid-liquid separating equipment 3 includes a horizontal cylindrical housing, be provided with filter screen in the shell, the filter screen internal fixation is provided with the conveying ribbon, and motor cooperates variator to drive filter screen and ribbon rotates, and horizontal ribbon solid-liquid separating equipment 3 bottoms are provided with oil, water mixture transport pipe.Oil, water, solid mixture are imported in the horizontal ribbon solid-liquid separating equipment 3 by pipeline by the pump tool, and after horizontal ribbon solid-liquid separating equipment 3 carried out liquid-solid separation, oil, water mixture were imported next treatment unit by transport pipe, and solid is discharged.The liquid of horizontal ribbon solid-liquid separating equipment 3 is discharged the rear end and is connected oily water separation tower 4, process is taken off the oil behind the solid, the water mixture is transported in the oily water separation tower 4, in the present embodiment, oily water separation tower 4 is vertical and cylindrical, its opening for feed is arranged on the middle and lower part, side, oily water separation tower 4 inside are provided with water back 5, water back 5 stretches to oily water separation tower 4 inside from oily water separation tower 4 bottoms, export oily water separation tower 4 outsides to from oily water separation tower 4 middle and upper parts again, in the present embodiment, the thermal source that water back 5 adopts is the waste heat of heat-conducting oil furnace, but the use of save energy, during concrete enforcement, also can be provided with thermal source separately.Infrared rays water body liquid level orientator 6 is equipped with at the top of oily water separation tower 4, the location of the profit mixture height when being used for oily water separation, and control the inlet of oil-water mixture automatically with this.Oily water separation tower 4 is equipped with oil wiper 7 and flowline 8 near a side on top, in the present embodiment, it is tabular that oil wiper 7 is bar shaped, rotated by the driven by motor that is arranged on oily water separation tower 4 tops, oil in the profit mixture is scraped in the oil groove, and by flowline 8 outputs.In the present embodiment, be provided with motorized valve 9 at flowline 8, enter oil pot 1 by motorized valve 9 control bio-oil materials from flowline 8.
Please in conjunction with referring to accompanying drawing 2, in the utility model, utilize the grease of deviating from the changing food waste to carry out the production of biofuel, production of biodiesel device front end removes equipment 11 for the grease colloid, in the present embodiment, the grease colloid removes equipment 11 and is rectangle, the grease colloid removes equipment 11 center fixed and is provided with hole crash panel 12, have hole on the crash panel 12, hole diameter is 0.5-1mm, pitch-row is 50-80mm, and the two sides of crash panel 12 is separately installed with rotary propeller type waterpower pusher 14 to open position, and the rotating plasma flabellum back side removes apparatus casing inwall 150-200mm apart from the grease colloid.In the present embodiment, rotary propeller type waterpower pusher 14 includes and is arranged on the grease colloid and removes the water screw flabellum of equipment 11 inside and be arranged on the motor that the grease colloid removes equipment 11 outsides, driven by motor water screw flabellum rotates, and rotating speed is 500-700 commentaries on classics/min, is controlled by the frequency transformer adjustment.When needs production biofuel, by special-purpose oil pump bio-oil materials being inputed to the grease colloid from oil pot 1 removes in the equipment 11, remove phosphide, sugar, protein and other impurity in the grease effectively, prevent that colloid from hiding the grease fine particle in one workshop section of back, and the contacting of obstacle grease and catalyzer.In the present embodiment, the ozone Oxidation Treatment device is by ozonizer 28A, anti-liquid recoil valve 29, powerful gas, liquid mixer 30, reactor 28, recycle pump 34, inflow pipeline A1, oil outlet A2, liquid-level controller 31 and ozone residual air are ruined device 32 compositions, and ozonizer 28A is by anti-liquid recoil valve 29 and powerful gas, liquid mixer 30 connects powerful gas, liquid mixer 30 removes equipment 11 by inflow pipeline A1 with the grease colloid and is connected, powerful gas, liquid mixer 30 is connected with reactor 28 by pipeline, be connected with recycle pump 34 on the reactor 28, reactor 28 bottoms are oil outlet A2, and oil outlet A2 is connected with bio oil normal temperature fat switching equipment 16 by pipeline, liquid-level controller 31 is installed in the reactor 28, and reactor 28 tops are equipped with ozone residual air and ruin device 32.Reactor 28 tops also are equipped with doser 33.Can remove impurity in the degrease, pigment, stink, protein etc. to grease by the ozone Oxidation Treatment device.The production of biodiesel apparatus main body is bio oil normal temperature fat switching equipment 16, in the present embodiment, bio oil normal temperature fat switching equipment 16 is round shape awl end reactor, the ultrasonic transducer 17 more than one is equipped with in bio oil normal temperature fat switching equipment 16 inside, in the present embodiment, be provided with four, each ultrasonic transducer 17 periphery is equipped with sleeve pipe 18 respectively, have internal thread fluid orifice 19 around the sleeve pipe 18, sleeve pipe 18 upper fixed are provided with fastener 20, fastener 20 tops are connected with pneumatic landing device 35, act on control sleeve pipe 18 and ultrasonic transducer 17 and in bio oil normal temperature fat switching equipment, go into the liquid degree of depth, by fastener 20 ultrasonic transducer 17 is fixed on the inside pipe casing center.In the bio oil normal temperature fat switching equipment 16 liquid guide flow pipe 21 is housed, liquid guide flow pipe 21 1 ends are connected bio oil normal temperature fat switching equipment 16 tops, and enter the inner chamber of sleeve pipe 18, and the other end is connected bio oil normal temperature fat switching equipment 16 bottoms, and the pump tool is connected on the liquid guide flow pipe 18.Top cover 23 is equipped with at bio oil normal temperature fat switching equipment 16 tops, and top cover 23 is provided with dog-house 24, and form A3 is equipped with in bio oil normal temperature fat switching equipment 16 sides.In the present embodiment, be provided with aspiration tube 25 in bio oil normal temperature fat switching equipment 16 bottoms, an end of aspiration tube 25 connects air compressor.Behind bio-oil input bio oil normal temperature fat switching equipment 16, add methyl alcohol and cosolvent from dog-house 24 again, in the present embodiment, cosolvent should selection can strengthen the liquid agent of the mutual solubility of grease and methyl alcohol, and after adding the solid negatively charged ion metal base catalyzer of reproducible utilization, ultrasonic transducer 17 enters in the bio oil by pneumatic or hydraulictool 35 by bio oil normal temperature fat switching equipment 16 top covers 23 places from top to down, simultaneously, pressurized air begins air-blowing from bio oil normal temperature fat switching equipment 16 bottoms, thereby it is molten altogether to promote bio oil and methyl alcohol to accelerate, and the bio-oil mixture is input to the inner chamber top of sleeve pipe 18 by oil pump 22, from top to bottom flow into supersound process, ultrasonic frequency progressively is strengthened to 30KHz by 25KHz, and the time is 20---60min.Bio oil normal temperature fat switching equipment 16 bottom discharge ports are connected with separatory equipment 26, in the present embodiment, separatory equipment 26 is vertical tubular, separatory equipment 26 rear ends are provided with filter plant 27, mixing liquid input separatory equipment 26 after ultrasonication finishes, obtained coarse biodiesel is obtained biofuel by filter plant 27.
In the utility model, the manufacture method of biofuel, namely the How It Works of said apparatus comprises the steps:
(1), the oil with producing in the changing food waste production process, water, solid mixture takes off solid processing, obtains oil-water mixture;
(2), oil-water mixture is delivered to oily water separation tower 4, carry out oily water separation, in the present embodiment, during oily water separation, utilize residual heat of heat-conducting oil furnace that the oil-water mixture in the oily water separation tower 4 is heated to 60 ℃---85 ℃, treat the layering of biological grease come-up back realization profit, the water body of lower floor is delivered to Sewage treatment systems by transport pipe, the bio-oil on upper strata is scraped by oil wiper 7, and sends in the oil pot by flowline 8;
(3), when needs during to bio-oil during the row processing treatment, after by instruments such as transferpumps bio-oil being sent to the grease colloid and removed in the equipment 11, start rotating plasma waterpower pusher 14, and add as phosphoric acid, the ratio of phosphoric acid and bio-oil is to be no more than 1% of grease total amount---1.2%, the liquid that the rotating plasma thrust of utilizing the grease colloid to remove equipment 11 two ends makes the grease colloid remove equipment 11 inside produces bump in opposite directions, collision time is based upon in the required time scope of processing condition of setting, in the present embodiment, the head-on collision time is 10 min---15min, after the collision time in opposite directions of liquid finishes, add weak brine at once, water, the weight ratio of salt is between the 95:5 to 90:10, the part by weight of bio-oil and weak brine is between the 90:10 to 80:20, adding weak brine is to act on the effect that utilizes electrolytic salt, and flocculation is accelerated, and the micelle of formation is more stable;
(4), continue to start rotating plasma waterpower pusher 14, the time is 10 min---20min;
(5), finish when above-mentioned Degumming Procedures, the grease mixture stops 60min---120min in equipment;
(6), the water body that will have micelle is discharged otherwise processed, the bio-oil of the matter of coming unstuck is input into powerful gas, liquid mixer 30, after the gas of ozonized gas generator 28A output mixes, enter in the ozonation treatment reactor 28, in the present embodiment, ozone concn is 13.5g/L, and the ozone flow velocity is 6.5L/min, during concrete enforcement, can suitably adjust according to practical situation.Add the normal heptane that accounts for grease gross weight 2% in the mixture in ozonization device 28 again, utilization is located at the outer circulating line 34 of reactor under the effect of oil pump, gas, liquid mixture are made cyclic motion, with this as reaction process, reaction times is 30min, and after the reaction times finished, the viscosity of waste oil reduced, peculiar smell is removed in the oil, and colourity descends obviously.
(7), the grease after ozonation treatment has finished is input into bio oil normal temperature fat switching equipment 16;
(8), when the liquid level of the input of the grease in the bio oil normal temperature fat switching equipment 16 reaches the liquid level of production technique setting, stop input, begin to start the aspiration tube 25 of bio oil normal temperature fat switching equipment 16 bottoms, powerful rolling is unsteady rapidly to make liquid level, at this moment, open dog-house 24, add solid catalyst and methyl alcohol, catalyst levels is 1.5% of biological oil quality---3.5%, methanol usage is 13% of biological oil quality---38%, after adding methyl alcohol, add cosolvent again, strengthen the cosolvency energy of bio-oil and methyl alcohol, form homogeneous system, cosolvent be chosen as methylethylketone, the add-on of cosolvent is 0.5% of bio-oil quality---2%, and in the present embodiment, cosolvent also includes 0.5% the fourth tertiary alcohol that add-on is the bio-oil quality;
(9), utilize high-pressure air to agitate continuously in fat switching equipment bottom and stir 10 min---15min thereafter, add solid negatively charged ion metal base catalyzer (model of producing for south China renewable resource (middle mountain) company limited that adopts in the present embodiment is the catalyzer of south China 713#) again, add-on is 3% of biological oil quality---4.5%, the feature of this solid catalyst is with agent of activity carbon and aluminium, sodium, iron, the nano particle of the ring texture silicate minerals of magnesium and lithium (it is a kind of tourmalinite) is base nuclear, at first recording base nuclear, self to discharge the above negative ion of 12000/cm3 be salable product, then base nuclear is immersed in the mixing liquid of alkaline silica sol and aluminium colloidal sol and lithium hydride, the blending ratio of its three kinds of materials is 1:1:0.5, take out the back under 650-720 ℃ temperature condition, constant temperature one hour, after the cooling through the screening refinement, make a kind of outer silicon of wrapping up in, aluminium, lithium mesh skeleton medium, and the band polarity the hybrid charge carrier, again with this carrier impregnation in KNO
3Solution in, take out back drying in 110 ℃ of drying plants and make and be loaded with 15%---25% KNO
3Basic catalyst.
(10), after adding needed auxiliary agent, close batching hole 21, open material circulation transferpump, and unlatching ultrasonic transducer 17, the original frequency of ultrasonic wave parallel operation device 17 is 25KHZ, and the time is 1min, progressively increases to 30KHZ subsequently, time is 30 min---40min, and temperature of reaction is 25---35 ℃.
(11), when grease is finished fat exchange in bio oil normal temperature fat switching equipment 16 after, with bio-oil mixture input separatory equipment 26 standing demix, the upper strata is methyl alcohol and glycerine mixing liquid, lower floor is rough biofuel;
(12), at first separatory equipment is located at the bottom leakage fluid dram and is opened, allow rough biofuel deliver into filter plant 27, obtain refining biodiesel after the filtration and reclaim solid catalyst, waiting to regenerate, the back is capable of circulation uses again.And biofuel is transfused to into and treats further refiningly in the storage vessel, and methyl alcohol and glycerine mixed solution are done his in addition and used.
The utility model can be automatically separates the solid that comprises in the changing food waste, moisture etc., further contained grease is converted to biofuel then and uses, and device structure is simple, treating processes, and save energy, production cost are low.
Claims (7)
1. exempt from distillation method production of biodiesel system for one kind, it is characterized in that: described system comprises horizontal ribbon solid-liquid separating equipment (3), oily water separation tower (4), oil pot (1), the grease colloid removes equipment (11), bio oil normal temperature fat switching equipment (16), separatory equipment (26) and filter plant (27), the outlet of horizontal ribbon solid-liquid separating equipment (3) is by pipe connection lower end to the oily water separation tower (4), be provided with water back (5) in the oily water separation tower (4), water back (5) stretches to oily water separation tower (4) inside from oily water separation tower (4) bottom, export oily water separation tower (4) outside again to from oily water separation tower (4) middle and upper part, oily water separation tower (4) top is provided with oil wiper (7), oily water separation tower (4) is connected with oil pot (1) by flowline (8), flowline (8) entrance arranges corresponding to oil wiper (7), oil pot (1) removes equipment (10) by pipeline (10) and grease colloid and is communicated with, the grease colloid removes equipment (11) inside and is provided with and is set with hole crash panel (12), the both sides correspondence position of crash panel (12) is separately installed with rotary propeller type waterpower pusher (14), the water screw flabellum of rotary propeller type waterpower pusher (14) is arranged on the grease colloid and removes in the equipment (11), motor is arranged on the grease colloid and removes equipment (11) outside, electric motor driving water screw flabellum rotates, the grease colloid removes equipment (11) bottom and is provided with the grease outlet, the grease outlet is communicated to powerful gas by pipeline, liquid mixer (30), after ozone gas mixes, enter in the ozonize reactor (28), grease through ozonation treatment is transported in the bio oil normal temperature fat switching equipment (16) by the lower part outlet of reactor, be provided with more than one ultrasonic transducer (17) in the bio oil normal temperature fat switching equipment (16), bio oil normal temperature fat switching equipment (16) top has dog-house (24), bio oil normal temperature fat switching equipment (16) bottom is communicated to separatory equipment (26) by pipeline, separatory equipment (26) bottom is connected to filter plant (27) by oil pipeline, filter plant (27) output biofuel.
2. the distillation method production of biodiesel system that exempts from according to claim 1, it is characterized in that: described horizontal ribbon solid-liquid separating equipment (3) includes a horizontal cylindrical housing, be provided with filter screen in the shell, the filter screen internal fixation is provided with the conveying ribbon, the ribbon drive-motor cooperates variator to drive filter screen and ribbon rotates, and horizontal ribbon solid-liquid separating equipment (3) bottom is provided with oil, water mixture output channel.
3. the distillation method production of biodiesel system that exempts from according to claim 1, it is characterized in that: infrared rays water body liquid level orientator (6) is equipped with at the top of described oily water separation tower (4).
4. the distillation method production of biodiesel system that exempts from according to claim 1, it is characterized in that: described ultrasonic transducer (17) periphery is equipped with sleeve pipe (18) respectively, sleeve pipe (18) has internal thread fluid orifice (19) all around, sleeve pipe (15) upper fixed is provided with fastener (20), by fastener (20) ultrasonic transducer (17) is fixed on sleeve pipe (18) inside center, sleeve pipe (18) and ultrasonic transducer (17) fall device (35) and control it and penetrate with the inner height of bio oil normal temperature fat switching equipment (16) by being located at pneumatic outside fat switching equipment (16) top or surging to carry.
5. the distillation method production of biodiesel system that exempts from according to claim 1, it is characterized in that: liquid guide flow pipe (21) is housed in the described bio oil normal temperature fat switching equipment (16), liquid guide flow pipe (21) one ends are connected bio oil normal temperature fat switching equipment (16) top, and entered the inner chamber top of sleeve pipe (18) by liquid outlet, the other end is connected bio oil normal temperature fat switching equipment (16) bottom, is connected with pump tool (22) on the liquid guide flow pipe (21).
6. the distillation method production of biodiesel system that exempts from according to claim 1 is characterized in that: be provided with aspiration tube (25) bottom the described bio oil normal temperature fat switching equipment (16), the end connection air compressor of aspiration tube (25).
7. the distillation method production of biodiesel system that exempts from according to claim 4, it is characterized in that: described sleeve pipe material is for discharging acid and alkali-resistance plastics or the pottery of negatively charged ion, the negatively charged ion burst size is more than 10000/cm2, described internal thread fluid orifice is a turriform hollow, in screw thread is arranged, and have and can discharge naturally more than 15000/energy of cm2 negatively charged ion.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013200551772U CN203128526U (en) | 2012-11-23 | 2013-01-31 | Distillation-free biodiesel production system |
| HK13108026A HK1180890A2 (en) | 2013-01-31 | 2013-07-09 | A biodiesel production system without distillation |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210481274.8 | 2012-11-23 | ||
| CN201210481274 | 2012-11-23 | ||
| CN2013200551772U CN203128526U (en) | 2012-11-23 | 2013-01-31 | Distillation-free biodiesel production system |
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| CN203128526U true CN203128526U (en) | 2013-08-14 |
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| CN201310038171.9A Expired - Fee Related CN103084049B (en) | 2012-11-23 | 2013-01-31 | Plasma photocatalyst anion air deodorization, sterilizing unit |
| CN2013200551772U Expired - Fee Related CN203128526U (en) | 2012-11-23 | 2013-01-31 | Distillation-free biodiesel production system |
| CN201310038186.5A Expired - Fee Related CN103056152B (en) | 2012-11-23 | 2013-01-31 | biochemical fermentation method and device |
| CN201310037324.8A Expired - Fee Related CN103072726B (en) | 2012-11-23 | 2013-01-31 | Plastic bag segmenting and lacerating device for holding kitchen wastes |
| CN201310038136.7A Expired - Fee Related CN103115477B (en) | 2012-11-23 | 2013-01-31 | Automatic discharging multi-stage drying device |
| CN201320054411XU Withdrawn - After Issue CN203316248U (en) | 2012-11-23 | 2013-01-31 | Combined screening system for kitchen waste |
| CN2013200552991U Withdrawn - After Issue CN203124395U (en) | 2012-11-23 | 2013-01-31 | Oxidization, deodorization, inactivation, cleaning and desaltation device for kitchen waste |
| CN2013200551166U Withdrawn - After Issue CN203124393U (en) | 2012-11-23 | 2013-01-31 | Biochemical fermentation device |
| CN2013200542519U Withdrawn - After Issue CN203124392U (en) | 2012-11-23 | 2013-01-31 | Integrated equipment for comprehensive treatment of kitchen waste |
| CN201310038252.9A Expired - Fee Related CN103071666B (en) | 2012-11-23 | 2013-01-31 | Integrated equipment for omnibearing treatment of kitchen garbage and production method of products |
| CN201310038156.4A Expired - Fee Related CN103074131B (en) | 2012-11-23 | 2013-01-31 | Preparation method and device of oxygen-enriched microemulsion mixed biodiesel |
| CN2013200551768U Expired - Fee Related CN203124394U (en) | 2012-11-23 | 2013-01-31 | Material selecting device |
| CN201310037944.1A Expired - Fee Related CN103056022B (en) | 2012-11-23 | 2013-01-31 | Combined screening system of kitchen wastes |
| CN201310038148.XA Expired - Fee Related CN103056151B (en) | 2012-11-23 | 2013-01-31 | Kitchen waste oxidizing, deodorizing, inactivating, washing and salt-reducing device |
| CN2013200551753U Withdrawn - After Issue CN203323492U (en) | 2012-11-23 | 2013-01-31 | Automatic discharge multi-stage drying device |
| CN201310038212.4A Expired - Fee Related CN103060100B (en) | 2012-11-23 | 2013-01-31 | Distillation-free biodiesel production method and system |
| CN201310038166.8A Expired - Fee Related CN103055650B (en) | 2012-11-23 | 2013-01-31 | Exhaust treatment system |
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| CN201310038171.9A Expired - Fee Related CN103084049B (en) | 2012-11-23 | 2013-01-31 | Plasma photocatalyst anion air deodorization, sterilizing unit |
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| CN201310038186.5A Expired - Fee Related CN103056152B (en) | 2012-11-23 | 2013-01-31 | biochemical fermentation method and device |
| CN201310037324.8A Expired - Fee Related CN103072726B (en) | 2012-11-23 | 2013-01-31 | Plastic bag segmenting and lacerating device for holding kitchen wastes |
| CN201310038136.7A Expired - Fee Related CN103115477B (en) | 2012-11-23 | 2013-01-31 | Automatic discharging multi-stage drying device |
| CN201320054411XU Withdrawn - After Issue CN203316248U (en) | 2012-11-23 | 2013-01-31 | Combined screening system for kitchen waste |
| CN2013200552991U Withdrawn - After Issue CN203124395U (en) | 2012-11-23 | 2013-01-31 | Oxidization, deodorization, inactivation, cleaning and desaltation device for kitchen waste |
| CN2013200551166U Withdrawn - After Issue CN203124393U (en) | 2012-11-23 | 2013-01-31 | Biochemical fermentation device |
| CN2013200542519U Withdrawn - After Issue CN203124392U (en) | 2012-11-23 | 2013-01-31 | Integrated equipment for comprehensive treatment of kitchen waste |
| CN201310038252.9A Expired - Fee Related CN103071666B (en) | 2012-11-23 | 2013-01-31 | Integrated equipment for omnibearing treatment of kitchen garbage and production method of products |
| CN201310038156.4A Expired - Fee Related CN103074131B (en) | 2012-11-23 | 2013-01-31 | Preparation method and device of oxygen-enriched microemulsion mixed biodiesel |
| CN2013200551768U Expired - Fee Related CN203124394U (en) | 2012-11-23 | 2013-01-31 | Material selecting device |
| CN201310037944.1A Expired - Fee Related CN103056022B (en) | 2012-11-23 | 2013-01-31 | Combined screening system of kitchen wastes |
| CN201310038148.XA Expired - Fee Related CN103056151B (en) | 2012-11-23 | 2013-01-31 | Kitchen waste oxidizing, deodorizing, inactivating, washing and salt-reducing device |
| CN2013200551753U Withdrawn - After Issue CN203323492U (en) | 2012-11-23 | 2013-01-31 | Automatic discharge multi-stage drying device |
| CN201310038212.4A Expired - Fee Related CN103060100B (en) | 2012-11-23 | 2013-01-31 | Distillation-free biodiesel production method and system |
| CN201310038166.8A Expired - Fee Related CN103055650B (en) | 2012-11-23 | 2013-01-31 | Exhaust treatment system |
Country Status (6)
| Country | Link |
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| KR (1) | KR20150105299A (en) |
| CN (17) | CN103084049B (en) |
| HK (9) | HK1180657A1 (en) |
| RU (1) | RU2015123832A (en) |
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| CN103060100A (en) * | 2012-11-23 | 2013-04-24 | 华南再生资源（中山）有限公司 | Distillation-free biodiesel production method and system |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103060100A (en) * | 2012-11-23 | 2013-04-24 | 华南再生资源（中山）有限公司 | Distillation-free biodiesel production method and system |
| CN103060100B (en) * | 2012-11-23 | 2014-07-09 | 华南再生资源（中山）有限公司 | Distillation-free biodiesel production method and system |
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