CN1778773A - Liquid fertilizer with pyroligneous liquor and oxalacetic liquor and production thereof - Google Patents
Liquid fertilizer with pyroligneous liquor and oxalacetic liquor and production thereof Download PDFInfo
- Publication number
- CN1778773A CN1778773A CN 200510061139 CN200510061139A CN1778773A CN 1778773 A CN1778773 A CN 1778773A CN 200510061139 CN200510061139 CN 200510061139 CN 200510061139 A CN200510061139 A CN 200510061139A CN 1778773 A CN1778773 A CN 1778773A
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- China
- Prior art keywords
- liquid
- liquid fertilizer
- pyroligneous
- drop
- contained
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- 239000007788 liquid Substances 0.000 title claims abstract description 120
- 239000003337 fertilizer Substances 0.000 title claims abstract description 58
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000000052 vinegar Substances 0.000 claims abstract description 91
- 235000021419 vinegar Nutrition 0.000 claims abstract description 91
- 239000002023 wood Substances 0.000 claims abstract description 33
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 claims abstract description 28
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims abstract description 28
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000004202 carbamide Substances 0.000 claims abstract description 14
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 14
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 14
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 14
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 14
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 14
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims abstract description 14
- 239000004323 potassium nitrate Substances 0.000 claims abstract description 14
- 235000010333 potassium nitrate Nutrition 0.000 claims abstract description 14
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 14
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 claims abstract description 14
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims abstract description 14
- 229910000368 zinc sulfate Inorganic materials 0.000 claims abstract description 14
- 229960001763 zinc sulfate Drugs 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 13
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000004327 boric acid Substances 0.000 claims abstract description 12
- 239000003375 plant hormone Substances 0.000 claims abstract description 10
- 239000002253 acid Substances 0.000 claims abstract description 7
- 235000018660 ammonium molybdate Nutrition 0.000 claims abstract description 7
- 239000011609 ammonium molybdate Substances 0.000 claims abstract description 7
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims abstract description 7
- 229940010552 ammonium molybdate Drugs 0.000 claims abstract description 7
- 229910052796 boron Inorganic materials 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 56
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 16
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 14
- 229910019142 PO4 Inorganic materials 0.000 claims description 13
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 13
- 229910000365 copper sulfate Inorganic materials 0.000 claims description 13
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 13
- 239000010452 phosphate Substances 0.000 claims description 13
- 239000011591 potassium Substances 0.000 claims description 13
- 229910052700 potassium Inorganic materials 0.000 claims description 13
- -1 rare earth nitrate Chemical class 0.000 claims description 13
- 229910021538 borax Inorganic materials 0.000 claims description 10
- 239000004328 sodium tetraborate Substances 0.000 claims description 10
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 10
- 229910002651 NO3 Inorganic materials 0.000 claims description 9
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 9
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- AXTGDCSMTYGJND-UHFFFAOYSA-N 1-dodecylazepan-2-one Chemical compound CCCCCCCCCCCCN1CCCCCC1=O AXTGDCSMTYGJND-UHFFFAOYSA-N 0.000 claims description 6
- 125000001931 aliphatic group Chemical group 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 239000004021 humic acid Substances 0.000 claims description 6
- 239000004615 ingredient Substances 0.000 claims description 6
- REZQBEBOWJAQKS-UHFFFAOYSA-N triacontan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO REZQBEBOWJAQKS-UHFFFAOYSA-N 0.000 claims description 6
- 239000005648 plant growth regulator Substances 0.000 claims description 5
- PRPINYUDVPFIRX-UHFFFAOYSA-N 1-naphthaleneacetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CC=CC2=C1 PRPINYUDVPFIRX-UHFFFAOYSA-N 0.000 claims description 4
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 4
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 4
- 229930191978 Gibberellin Natural products 0.000 claims description 4
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 4
- UHZZMRAGKVHANO-UHFFFAOYSA-M chlormequat chloride Chemical compound [Cl-].C[N+](C)(C)CCCl UHZZMRAGKVHANO-UHFFFAOYSA-M 0.000 claims description 4
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 4
- 239000003448 gibberellin Substances 0.000 claims description 4
- IXORZMNAPKEEDV-OBDJNFEBSA-N gibberellin A3 Chemical class C([C@@]1(O)C(=C)C[C@@]2(C1)[C@H]1C(O)=O)C[C@H]2[C@]2(C=C[C@@H]3O)[C@H]1[C@]3(C)C(=O)O2 IXORZMNAPKEEDV-OBDJNFEBSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 239000003352 sequestering agent Substances 0.000 claims description 4
- 239000011573 trace mineral Substances 0.000 claims description 4
- 235000013619 trace mineral Nutrition 0.000 claims description 4
- 239000011159 matrix material Substances 0.000 claims description 3
- YNWVFADWVLCOPU-MDWZMJQESA-N (1E)-1-(4-chlorophenyl)-4,4-dimethyl-2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol Chemical compound C1=NC=NN1/C(C(O)C(C)(C)C)=C/C1=CC=C(Cl)C=C1 YNWVFADWVLCOPU-MDWZMJQESA-N 0.000 claims description 2
- UDPGUMQDCGORJQ-UHFFFAOYSA-N (2-chloroethyl)phosphonic acid Chemical compound OP(O)(=O)CCCl UDPGUMQDCGORJQ-UHFFFAOYSA-N 0.000 claims description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 2
- PAMIQIKDUOTOBW-UHFFFAOYSA-N 1-methylpiperidine Chemical compound CN1CCCCC1 PAMIQIKDUOTOBW-UHFFFAOYSA-N 0.000 claims description 2
- LBLSRDDHGILUJH-UHFFFAOYSA-N 4-(1h-indol-2-yl)butanoic acid Chemical class C1=CC=C2NC(CCCC(=O)O)=CC2=C1 LBLSRDDHGILUJH-UHFFFAOYSA-N 0.000 claims description 2
- 229920001817 Agar Polymers 0.000 claims description 2
- IXVMHGVQKLDRKH-VRESXRICSA-N Brassinolide Natural products O=C1OC[C@@H]2[C@@H]3[C@@](C)([C@H]([C@@H]([C@@H](O)[C@H](O)[C@H](C(C)C)C)C)CC3)CC[C@@H]2[C@]2(C)[C@@H]1C[C@H](O)[C@H](O)C2 IXVMHGVQKLDRKH-VRESXRICSA-N 0.000 claims description 2
- 229920001353 Dextrin Polymers 0.000 claims description 2
- 239000004375 Dextrin Substances 0.000 claims description 2
- 102000018997 Growth Hormone Human genes 0.000 claims description 2
- 108010051696 Growth Hormone Proteins 0.000 claims description 2
- FAIXYKHYOGVFKA-UHFFFAOYSA-N Kinetin Natural products N=1C=NC=2N=CNC=2C=1N(C)C1=CC=CO1 FAIXYKHYOGVFKA-UHFFFAOYSA-N 0.000 claims description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 2
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- 239000008272 agar Substances 0.000 claims description 2
- IXVMHGVQKLDRKH-KNBKMWSGSA-N brassinolide Chemical compound C1OC(=O)[C@H]2C[C@H](O)[C@H](O)C[C@]2(C)[C@H]2CC[C@]3(C)[C@@H]([C@H](C)[C@@H](O)[C@H](O)[C@@H](C)C(C)C)CC[C@H]3[C@@H]21 IXVMHGVQKLDRKH-KNBKMWSGSA-N 0.000 claims description 2
- HCWYXKWQOMTBKY-UHFFFAOYSA-N calcium;dodecyl benzenesulfonate Chemical compound [Ca].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 HCWYXKWQOMTBKY-UHFFFAOYSA-N 0.000 claims description 2
- 235000019425 dextrin Nutrition 0.000 claims description 2
- 239000006196 drop Substances 0.000 claims description 2
- 239000003995 emulsifying agent Substances 0.000 claims description 2
- 239000000122 growth hormone Substances 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 2
- JTEDVYBZBROSJT-UHFFFAOYSA-N indole-3-butyric acid Chemical compound C1=CC=C2C(CCCC(=O)O)=CNC2=C1 JTEDVYBZBROSJT-UHFFFAOYSA-N 0.000 claims description 2
- QANMHLXAZMSUEX-UHFFFAOYSA-N kinetin Chemical compound N=1C=NC=2N=CNC=2C=1NCC1=CC=CO1 QANMHLXAZMSUEX-UHFFFAOYSA-N 0.000 claims description 2
- 229960001669 kinetin Drugs 0.000 claims description 2
- 229920001206 natural gum Polymers 0.000 claims description 2
- 229920000191 poly(N-vinyl pyrrolidone) Polymers 0.000 claims description 2
- 229920000136 polysorbate Polymers 0.000 claims description 2
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 230000008635 plant growth Effects 0.000 abstract description 6
- 241000894006 Bacteria Species 0.000 abstract description 3
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 abstract 2
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 abstract 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 abstract 1
- 229910000366 copper(II) sulfate Inorganic materials 0.000 abstract 1
- 239000003864 humus Substances 0.000 abstract 1
- 230000002401 inhibitory effect Effects 0.000 abstract 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 abstract 1
- 235000019341 magnesium sulphate Nutrition 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 abstract 1
- 229910000160 potassium phosphate Inorganic materials 0.000 abstract 1
- 235000011009 potassium phosphates Nutrition 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 239000004576 sand Substances 0.000 abstract 1
- 235000015393 sodium molybdate Nutrition 0.000 abstract 1
- 239000011684 sodium molybdate Substances 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 9
- 229910052799 carbon Inorganic materials 0.000 description 7
- 244000025254 Cannabis sativa Species 0.000 description 6
- 230000012010 growth Effects 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 240000008067 Cucumis sativus Species 0.000 description 5
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 5
- 230000000694 effects Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- 241000195940 Bryophyta Species 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000003415 peat Substances 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 230000000452 restraining effect Effects 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 206010039203 Road traffic accident Diseases 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 230000000507 anthelmentic effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000002361 compost Substances 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 238000009329 organic farming Methods 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Fertilizers (AREA)
Abstract
A liquid fertilizer containing wood vinegar liquid or oxalic vinegar liquid and its production are disclosed. The liquid fertilizer consists of urea 1-20.0%, potassium phosphate 1-20.0%, potassium nitrate 1-20.0%, lime nitrate 0.1-10.0%, magnesium sulfate 0.1-5.0%, ferrous sulfate 0.1-5.0%, manganous sulfate 0.1-5.0%, zinc sulfate 0.1-5.0%, cupric sulfate 0.1-5.0%, boron sand or boric acid 0.1-2.0%, sodium molybdate or ammonium molybdate 0.1-1.0%, plant hormone or plant regulator, rare earth element or humus acid or pesticide auxiliaries etc. The process is carried out by proportioning and mixing. It can improve bacterium inhibiting and plant growth regulating functions.
Description
Technical field
The invention belongs to technical field of fertilizers, be specifically related to liquid fertilizer of a kind of pyroligneous-contained or careless vinegar liquid and preparation method thereof.
Background technology
Wood vinegar is the by product that wood machining residues obtains through high temperature pyrolysis, and careless vinegar liquid stoste is meant the by product that herbaceous plant and crop stalk obtain through high temperature pyrolysis.Wood (grass) vinegar liquid stoste has a lot of positive effects in agricultural production process, therefore the peculiar property as antibiotic under in high density, promote microorganism active under lower concentration can be used as soil disinfectant, compost fermentation promotor and plant growth regulation.Widely used wood vinegar in the agriculture organic farming of developed country, still a kind of good inert ingredient and preservation agent.The problem of utilizing of herbaceous plant and crop stalk is the focus of research always, past, herbaceous plant is burned into plant ash with crop stalk in the field be restored to the field, yet, plant ash is to the active effects of farm crop and the improving effect of soil is not burnt till herbaceous plant and crop stalk the peat composed of rotten mosses return effective that the field uses, naturally burn herbaceous plant and crop stalk simultaneously in the field, polluted air can produce thick smoke, the dense smoke that burns generation in the highway both sides also influences driver's vision and causes traffic accident easily, therefore use industrialized method to seal one of focus of studying after the processing of burning carbon should be herbaceous plant and crop stalk, wherein the peat composed of rotten mosses can be applied to soil improvement, but the application of the careless vinegar liquid that produces in the process of making charcoal will be one of difficult problem of research.Though wood (grass) vinegar liquid can directly apply to farm-forestry crop, the nutrition and the biocidal efficacies of wood (grass) vinegar liquid are lower.
Summary of the invention
For overcoming problems of the prior art, the present invention aims to provide the technical scheme of liquid fertilizer of a kind of pyroligneous-contained or careless vinegar liquid that can supply with the required full nutrition of plant-growth, coordinate plant growth growth, bactericidal and disinfest and preparation method thereof.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that with wood vinegar or careless vinegar liquid be matrix, contains in this liquid fertilizer: urea 1～20.0%, potassium primary phosphate 1～20.0%, saltpetre 1～20.0%, nitrocalcite 0.1～10.0%, sal epsom 0.1～5.0%, ferrous sulfate 0.1～5.0%, manganous sulfate 0.1～5.0%, zinc sulfate 0.1～5.0%, copper sulfate 0.1～5.0%, borax or boric acid 0.1～2.0%, Sodium orthomolybdate or ammonium molybdate 0.1～1.0%.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid, it is characterized in that containing in this liquid fertilizer: urea 1～10.0%, potassium primary phosphate 1～10.0%, saltpetre 1～10.0%, nitrocalcite 0.1～5.0%, sal epsom 0.1～2.5%, ferrous sulfate 0.1～2.5%, manganous sulfate 0.1～2.5%, zinc sulfate 0.1～2.5%, copper sulfate 0.1～2.5%, borax or boric acid 0.1～1.0%, Sodium orthomolybdate or ammonium molybdate 0.1～0.5%.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid, it is characterized in that containing in this liquid fertilizer: urea 1～5.0%, potassium primary phosphate 1～5.0%, saltpetre 1～5.0%, nitrocalcite 0.1～2.5%, sal epsom 0.1～1.3%, ferrous sulfate 0.1～1.3%, manganous sulfate 0.1～1.3%, zinc sulfate 0.1～1.3%, copper sulfate 0.1～1.3%, borax or boric acid 0.1～0.5%, Sodium orthomolybdate or ammonium molybdate 0.1～0.3%.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that containing in this liquid fertilizer: rare earth nitrate or humic acids or humate 0.1～5.0% are preferably 0.1～2.5%, more preferably 0.1～1.3%.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that containing in this liquid fertilizer in following component and the content one or more:
Growth hormone 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Plant hormones regulators,gibberellins 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Ethrel 1～90.0% is preferably 1～45.0%, and more preferably 1～22.5%;
Phytokinin 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Kinetin 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Brassinolide 0.01～2.00% is preferably 0.01～1.00%, and more preferably 0.01～0.50%;
Choline dichloride 1～90.0% is preferably 1～45.0%, and more preferably 1～22.5%;
Indolebutyric acid or indolebutyric acid salt 0.01～5.00% are preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Naphthylacetic acid or naphthylacetic acid salt 0.01～5.00% are preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Methyl piperidine 0.01～15.00% is preferably 0.01～7.50%, and more preferably 0.01～3.75%;
Uniconazole 0.01～15.00% is preferably 0.01～7.50%, and more preferably 0.01～3.75%;
Triacontanol price quote 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%.
This group component materials is plant hormone or plant-growth regulator.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that containing in this liquid fertilizer: ethylenediamine tetraacetic acid (EDTA) or disodium ethylene diamine tetraacetate 1～20% are preferably 1～10%, more preferably 1～5%.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that containing in this liquid fertilizer in following component and the content one or more:
Tween series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Peregal series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
OP series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
NP series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Polyoxyethylenealkylphenol ether 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Polyoxyethylene aliphatic alcohol ether 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Aliphatic acid polyethenoxy ether 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Emulsifier EL 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Fast penetrant T 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Sodium lauryl sulphate 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Calcium dodecylbenzene sulphonate 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Azone 0.1～5.0% is preferably 0.1～2.5%, and more preferably 0.1～1.3%.
This group component materials is an inert ingredient.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that containing in this liquid fertilizer in following component and the content one or more:
Polyvinyl alcohol 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Polyoxyethylene glycol 0.1～30.0% is preferably 0.1～15.0%, and more preferably 0.1～7.5%;
Natural gum 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Agar 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Water soluble starch 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Dextrin 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%.
This group component materials is a membrane-forming agent.
The preparation method of the liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that may further comprise the steps:
A) in reactor, drop into wood vinegar or careless vinegar liquid, be heated to 30～100 ℃, the secondary element that slowly has high input, trace element during drop into the dissolving back, drop into rare earth element or humic acids or humate again, sequestrant is dropped in the dissolving back, cools to 30～50 ℃ behind the chelating gradually, drops into plant hormone or plant-growth regulator, drop into inert ingredient then, this process is finished in constantly stirring, and is cooled to normal temperature and obtains A, and is standby;
B) drop into wood vinegar or careless vinegar liquid in reactor, be heated to 50～100 ℃, slowly drop into membrane-forming agent, after dissolving disperses fully, stop heating, obtain B, this process is finished in constantly stirring;
C) standby composition A is slowly joined among the B, be stirred to fully evenly, obtain C, the liquid fertilizer of promptly described pyroligneous-contained or careless vinegar liquid.
The preparation method of the liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid is characterized in that may further comprise the steps:
A) in reactor, drop into wood vinegar or careless vinegar liquid, be heated to 30～100 ℃, slowly drop into membrane-forming agent, after dissolving disperses fully, stop heating, add normal temperature wood vinegar or careless vinegar liquid again, stir, obtain A;
B) in 20～50 ℃ A, secondary element slowly has high input, trace element during drop into the dissolving back, drop into rare earth element or humic acids or humate again, sequestrant is dropped in the dissolving back, drops into plant hormone or plant-growth regulator again, drops into inert ingredient then, this process is finished in constantly stirring, and is cooled to the liquid fertilizer that normal temperature gets described pyroligneous-contained or careless vinegar liquid.
Wood vinegar among the above-mentioned preparation method or careless vinegar liquid can be wood vinegar or careless vinegar liquid stoste, also can be wood vinegar or the careless vinegar liquid stoste that adds after suitable quantity of water is diluted.
The liquid fertilizer of described a kind of pyroligneous-contained or careless vinegar liquid, employing has the wood vinegar of coordinate plant growth and certain restraining and sterilizing bacteria and anthelminthic effect or careless vinegar liquid as matrix, cooperate the various nutritive elements that add, greatly increased the effect of restraining and sterilizing bacteria and coordinate plant growth, on the other hand, in the process of liquid fertilizer preparation, incorporated the film technique of wood vinegar or careless vinegar liquid, significantly reduced the waste when this liquid fertilizer uses.
Per-cent in the present specification all is weight percentage except that specifying.
Embodiment
Now describe specific embodiments of the invention in detail, and, further specify beneficial effect of the present invention in conjunction with experiment.
Embodiment 1:
In the 500L reactor, drop into wood vinegar 180L, be heated to 100 ℃, in heating, slowly drop into the 15kg polyvinyl alcohol, after in constantly stirring, dissolving fully, stop heating, continue to add the 120kg wood vinegar, after stirring and reaching 40 ℃ ± 5 ℃, slowly drop into 15kg urea, after the stirring and dissolving, slowly drop into the 35kg potassium primary phosphate, after the stirring and dissolving, slowly drop into saltpetre 45kg; Drop into 6kg nitrocalcite, 2kg sal epsom, 2kg ferrous sulfate, 2kg manganous sulfate, 1kg zinc sulfate, 0.5kg copper sulfate, 1.0kg Sodium orthomolybdate, 1kg borax after the dissolving respectively successively, the 2kg rare earth nitrate, after the stirring and dissolving, slowly drop into the 8kg ethylenediamine tetraacetic acid (EDTA), cool to 30 ℃ gradually after fully stirring chelating, drop into the 0.3kg fast penetrant T, stir, be cooled to normal temperature and obtain pyroligneous-contained liquid fertilizer.
Embodiment 2:
A) in the 500L reactor, drop into wood vinegar 300L, be heated to 40 ℃, slowly drop into 45kg urea, after the stirring and dissolving, slowly drop into the 25kg potassium primary phosphate, after the stirring and dissolving, slowly drop into saltpetre 35kg; Drop into 2kg nitrocalcite, 1kg sal epsom, 1kg ferrous sulfate, 1kg manganous sulfate, 1.2kg zinc sulfate, 1.8kg copper sulfate, 1kg boric acid, 4kg borax, 0.5kg Sodium orthomolybdate after the dissolving respectively successively, the 1kg rare earth nitrate, after the stirring and dissolving, slowly drop into the 6kg disodium ethylene diamine tetraacetate, cool to 30 ℃ gradually after fully stirring chelating, drop into 0.6kg Plant hormones regulators,gibberellins, the 1kg aliphatic acid polyethenoxy ether, 0.1kg azone stirs, and is cooled to normal temperature and obtains A, and is standby;
B) in the 500L reactor, drop into the 100kg wood vinegar, be heated to 85 ℃, slowly drop into the 10kg polyvinyl alcohol, after dissolving disperses fully in constantly stirring, stop heating, obtain B;
C) standby composition A is slowly joined among the B, be stirred to fully evenly, obtain C, i.e. the pyroligneous-contained liquid fertilizer of finished product.
Embodiment 3
In the 500L reactor, drop into careless vinegar liquid 180kg, be heated to 80 ℃, in heating, slowly drop into the 15kg polyvinyl alcohol, after dissolving disperses fully in constantly stirring, stop heating, continue to add 120kg grass vinegar liquid, after stirring and reaching 40 ℃ ± 5 ℃, slowly drop into 15kg urea, after the stirring and dissolving, slowly drop into the 35kg potassium primary phosphate, after the stirring and dissolving, slowly drop into saltpetre 45kg; Drop into 5kg nitrocalcite, 2kg sal epsom, 2kg ferrous sulfate, 2kg manganous sulfate, 1kg zinc sulfate, 0.5kg copper sulfate, 1.0kg Sodium orthomolybdate after the dissolving respectively successively, 2kg boric acid, the 2kg rare earth nitrate, after the stirring and dissolving, slowly drop into the 8kg ethylenediamine tetraacetic acid (EDTA), cool to 30 ℃ gradually after fully stirring chelating, drop into the 1kg aliphatic acid polyethenoxy ether, 0.1kg azone stirs, and is cooled to normal temperature and obtains the liquid fertilizer that finished product contains careless vinegar liquid.
Embodiment 4
A) in the 500L reactor, drop into careless vinegar liquid 300L, be heated to 30 ℃, slowly drop into 45kg urea, after the stirring and dissolving, slowly drop into the 25kg potassium primary phosphate, after the stirring and dissolving, slowly drop into saltpetre 35kg; Drop into 2kg nitrocalcite, 1kg sal epsom, 1kg ferrous sulfate, 1kg manganous sulfate, 1.2kg zinc sulfate, 1.8kg copper sulfate, 1kg boric acid, 4kg borax, 0.5kg Sodium orthomolybdate after the dissolving respectively successively, the 1kg rare earth nitrate, after the stirring and dissolving, slowly drop into the 6kg disodium ethylene diamine tetraacetate, cool to 30 ℃ gradually after fully stirring chelating, drop into 0.6kg Plant hormones regulators,gibberellins, the 1kg aliphatic acid polyethenoxy ether, 0.1kg azone stirs, and is cooled to normal temperature and obtains A, and is standby.
B) in the 500L reactor, drop into 100kg grass vinegar liquid, be heated to 85 ℃, slowly drop into the 8kg polyvinyl alcohol, after dissolving disperses fully in constantly stirring, stop heating, obtain B;
C) standby composition A is slowly joined among the B, be stirred to fully evenly, obtain C, promptly finished product contains the liquid fertilizer of careless vinegar liquid.
Embodiment 5
In the 500L reactor, drop into wood vinegar 180L, be heated to 90 ℃, in heating, slowly drop into the 15kg polyvinyl alcohol, after dissolving disperses fully in constantly stirring, stop heating, continue to add the 120L wood vinegar, after stirring and reaching 40 ℃ ± 5 ℃, slowly drop into 15kg urea, after the stirring and dissolving, slowly drop into the 35kg potassium primary phosphate, after the stirring and dissolving, slowly drop into saltpetre 45kg; Drop into 8kg nitrocalcite, 2kg sal epsom, 2kg ferrous sulfate, 2kg manganous sulfate, 1kg zinc sulfate, 0.5kg copper sulfate, 2kg borax, 1.0kg Sodium orthomolybdate after the dissolving respectively successively, the 2kg rare earth nitrate, after the stirring and dissolving, slowly drop into the 8kg ethylenediamine tetraacetic acid (EDTA), cool to 30 ℃ gradually after fully stirring chelating, drop into the 0.6kg triacontanol price quote, drop into the 1kg aliphatic acid polyethenoxy ether again after fully stirring, 0.1kg azone stirs, and is cooled to normal temperature and obtains the pyroligneous-contained liquid fertilizer of finished product.
Embodiment 6
In the 500L reactor, drop into wood vinegar 180L, be heated to 100 ℃, in heating, slowly drop into the 15kg polyvinyl alcohol, after dissolving disperses fully in constantly stirring, stop heating, continue to add the 120kg wood vinegar, after stirring and reaching 40 ℃ ± 5 ℃, slowly drop into 15kg urea, after the stirring and dissolving, slowly drop into the 35kg potassium primary phosphate, after the stirring and dissolving, slowly drop into saltpetre 45kg; Drop into 1kg nitrocalcite, 2kg sal epsom, 2kg ferrous sulfate, 2kg manganous sulfate, 1kg zinc sulfate, 0.5kg copper sulfate, 1kg boric acid, 1.0kg Sodium orthomolybdate after the dissolving respectively successively, the 2kg rare earth nitrate, after the stirring and dissolving, slowly drop into the 8kg ethylenediamine tetraacetic acid (EDTA), cool to 30 ℃ gradually after fully stirring chelating, drop into the 1.2kg choline dichloride, the 0.3kg fast penetrant T, stir, be cooled to normal temperature and obtain the pyroligneous-contained liquid fertilizer of finished product.
Embodiment 7
In the 500L reactor, drop into the careless vinegar liquid 180L of the processing of handling, be heated to 100 ℃, in heating, slowly drop into the 15kg polyvinyl alcohol, after dissolving disperses fully in constantly stirring, stop heating, continue to add 120L grass vinegar liquid, after stirring and reaching 40 ℃ ± 5 ℃, slowly drop into 15kg urea, after the stirring and dissolving, slowly drop into the 35kg potassium primary phosphate, after the stirring and dissolving, slowly drop into saltpetre 45kg; Drop into 1kg nitrocalcite, 2kg sal epsom, 2kg ferrous sulfate, 2kg manganous sulfate, 1kg zinc sulfate, 0.5kg copper sulfate, 1kg boric acid, 1.0kg Sodium orthomolybdate after the dissolving respectively successively, the 2kg rare earth nitrate, after the stirring and dissolving, slowly drop into the 8kg ethylenediamine tetraacetic acid (EDTA), cool to 30 ℃ gradually after fully stirring chelating, drop into the 1.2kg choline dichloride, the 0.3kg fast penetrant T, stir, be cooled to normal temperature and obtain the liquid fertilizer that finished product contains careless vinegar liquid.
Experimental technique, data and conclusion
Cucumber cotyledons expansion method
The cucumber seeds 5h that is soaked in water, cucumber is vernalization 2d under 28 ℃ of dark conditions, select 10 of cotyledons of the same size and put into the culture dish of the diameter 9cm that is covered with two layers of filter paper, the wood vinegar or the careless vinegar liquid 8ml that add the different concns gradient respectively, contrast adds 8mL distilled water, cultivates 4d with growth cabinet, cotyledon surface water droplet is removed in suction, measure the cotyledon fresh weight, repeat 3 times, and calculate its growth rate.
The influence of 1～4 pair of isolated cucumber cotyledon growth of table 1 embodiment
| Concentration (mg/L) | 200 | 100 | 50 | 20 | 10 | 5 | 2 | 1 |
| Former wood vinegar | -31.28 | -18.57 | -5.13 | -5.55 | 4.58 | 7.90 | 4.45 | 1.77 |
| Embodiment 1 | 3.42 | 27.42 | 13.37 | 4.15 | 36.53 | 12.46 | 32.80 | 29.20 |
| Embodiment 2 | -77.46 | -33.84 | 85.64 | 33.35 | 3.35 | 43.86 | 10.81 | 77.15 |
| Former careless vinegar liquid | -2.17 | -3.84 | -4.29 | 13.38 | 22.28 | 23.94 | 11.18 | 7.85 |
| Embodiment 3 | 74.89 | 79.80 | 78.39 | 69.55 | 69.89 | 35.95 | 79.89 | 45.12 |
| Embodiment 4 | -91.44 | -15.17 | 97.37 | 52.64 | 53.03 | 35.16 | 87.15 | 90.59 |
Embodiment 1～2 promotes the cucumber cotyledons growth respectively in the concentration range of 1-50mg/L, increasing maximum amplitude than the clear water contrast is 36.53% and 85.64%, also effective than wood vinegar stoste; Embodiment 3～4 suppresses growth under the situation of concentration greater than 100mg/L, in the concentration range of concentration range 1-50mg/L, increasing maximum amplitude than the clear water contrast is 79.89% and 87.15%, also effective than careless vinegar liquid stoste.
The Plantula Brassicae chinensis field plot trial of table 2 embodiment 1～4 (1000 times of sprayings of dilute with water)
| Prescription | Plant high cm | Increase % | The number of blade | Increase % | Petiole area cm2 | Increase % | Single-strain fresh weight | Increase % | Total dry weight | Increase % |
| Embodiment 1 | 11.8 | 15.7 | 3.9 | 0 | 7.9 | 12.9 | 9.2 | 15 | 1.9 | 18.8 |
| Embodiment 2 | 13.4 | 31.4 | 4.3 | 10.3 | 10.4 | 48.6 | 14.3 | 78.8 | 2.9 | 81.3 |
| Embodiment 3 | 11.5 | 12.7 | 4.1 | 5.13 | 8.7 | 24.3 | 9.8 | 22.5 | 2.0 | 25 |
| Embodiment 4 | 14.9 | 46.1 | 4.8 | 23.1 | 11.2 | 60.0 | 15.3 | 91.3 | 3.3 | 106 |
| Contrast | 10.2 | 3.9 | 7.0 | 8.0 | 1.6 |
Under embodiment 1～4 situation that spraying is used after diluting 1000 times respectively, the situation of the liquid fertilizer of pyroligneous-contained or careless vinegar liquid is not used in contrast, the high maximum of planting of Plantula Brassicae chinensis increases by 46.1%, the number of blade is maximum to increase by 23.1%, the petiole area is maximum to increase by 11.2%, blade area is maximum to increase by 60.0%, and single-strain fresh weight is maximum to increase by 91.3%, and total dry weight is maximum to increase by 106%.
Claims (10)
1. the liquid fertilizer of a pyroligneous-contained or careless vinegar liquid is characterized in that with wood vinegar or careless vinegar liquid be matrix, contains in this liquid fertilizer: urea 1～20.0%, potassium primary phosphate 1～20.0%, saltpetre 1～20.0%, nitrocalcite 0.1～10.0%, sal epsom 0.1～5.0%, ferrous sulfate 0.1～5.0%, manganous sulfate 0.1～5.0%, zinc sulfate 0.1～5.0%, copper sulfate 0.1～5.0%, borax or boric acid 0.1～2.0%, Sodium orthomolybdate or ammonium molybdate 0.1～1.0%.
2. the liquid fertilizer of a kind of pyroligneous-contained or careless vinegar liquid as claimed in claim 1, it is characterized in that containing in this liquid fertilizer: urea 1～10.0%, potassium primary phosphate 1～10.0%, saltpetre 1～10.0%, nitrocalcite 0.1～5.0%, sal epsom 0.1～2.5%, ferrous sulfate 0.1～2.5%, manganous sulfate 0.1～2.5%, zinc sulfate 0.1～2.5%, copper sulfate 0.1～2.5%, borax or boric acid 0.1～1.0%, Sodium orthomolybdate or ammonium molybdate 0.1～0.5%.
3. the liquid fertilizer of a kind of pyroligneous-contained or careless vinegar liquid as claimed in claim 1, it is characterized in that containing in this liquid fertilizer: urea 1～5.0%, potassium primary phosphate 1～5.0%, saltpetre 1～5.0%, nitrocalcite 0.1～2.5%, sal epsom 0.1～1.3%, ferrous sulfate 0.1～1.3%, manganous sulfate 0.1～1.3%, zinc sulfate 0.1～1.3%, copper sulfate 0.1～1.3%, borax or boric acid 0.1～0.5%, Sodium orthomolybdate or ammonium molybdate 0.1～0.3%.
4. as the liquid fertilizer of claim 1,2 or 3 described a kind of pyroligneous-contained or careless vinegar liquid, it is characterized in that containing in this liquid fertilizer: rare earth nitrate or humic acids or humate 0.1～5.0% are preferably 0.1～2.5%, more preferably 0.1～1.3%.
5. as the liquid fertilizer of claim 1,2 or 3 described a kind of pyroligneous-contained or careless vinegar liquid, it is characterized in that containing in this liquid fertilizer in following component and the content one or more:
Growth hormone 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Plant hormones regulators,gibberellins 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Ethrel 1～90.0% is preferably 1～45.0%, and more preferably 1～22.5%;
Phytokinin 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Kinetin 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Brassinolide 0.01～2.00% is preferably 0.01～1.00%, and more preferably 0.01～0.50%;
Choline dichloride 1～90.0% is preferably 1～45.0%, and more preferably 1～22.5%;
Indolebutyric acid or indolebutyric acid salt 0.01～5.00% are preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Naphthylacetic acid or naphthylacetic acid salt 0.01～5.00% are preferably 0.01～2.50%, and more preferably 0.01～1.25%;
Methyl piperidine 0.01～15.00% is preferably 0.01～7.50%, and more preferably 0.01～3.75%;
Uniconazole 0.01～15.00% is preferably 0.01～7.50%, and more preferably 0.01～3.75%;
Triacontanol price quote 0.01～5.00% is preferably 0.01～2.50%, and more preferably 0.01～1.25%.
6. as the liquid fertilizer of claim 1,2 or 3 described a kind of pyroligneous-contained or careless vinegar liquid, it is characterized in that containing in this liquid fertilizer: ethylenediamine tetraacetic acid (EDTA) or disodium ethylene diamine tetraacetate 1～20% are preferably 1～10%, more preferably 1～5%.
7. as the liquid fertilizer of claim 1,2 or 3 described a kind of pyroligneous-contained or careless vinegar liquid, it is characterized in that containing in this liquid fertilizer in following component and the content one or more:
Tween series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Peregal series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
OP series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
NP series 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Polyoxyethylenealkylphenol ether 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Polyoxyethylene aliphatic alcohol ether 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Aliphatic acid polyethenoxy ether 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Emulsifier EL 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Fast penetrant T 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Sodium lauryl sulphate 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Calcium dodecylbenzene sulphonate 0.1～10% is preferably 0.1～5%, and more preferably 0.1～2.5%;
Azone 0.1～5.0% is preferably 0.1～2.5%, and more preferably 0.1～1.3%.
8. as the liquid fertilizer of claim 1,2 or 3 described a kind of pyroligneous-contained or careless vinegar liquid, it is characterized in that containing in this liquid fertilizer in following component and the content one or more:
Polyvinyl alcohol 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Polyoxyethylene glycol 0.1～30.0% is preferably 0.1～15.0%, and more preferably 0.1～7.5%;
Natural gum 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Agar 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Water soluble starch 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%;
Dextrin 0.1～15.0% is preferably 0.1～7.5%, and more preferably 0.1～3.75%.
9. the preparation method of the liquid fertilizer of the described a kind of pyroligneous-contained or careless vinegar liquid of arbitrary claim in the claim 1～8 is characterized in that may further comprise the steps:
A) in reactor, drop into wood vinegar or careless vinegar liquid, be heated to 30～100 ℃, the secondary element that slowly has high input, trace element during drop into the dissolving back, drop into rare earth element or humic acids or humate again, sequestrant is dropped in the dissolving back, cools to 30～50 ℃ behind the chelating gradually, drops into plant hormone or plant-growth regulator, drop into inert ingredient then, this process is finished in constantly stirring, and is cooled to normal temperature and obtains A, and is standby;
B) drop into wood vinegar or careless vinegar liquid in reactor, be heated to 50～100 ℃, slowly drop into membrane-forming agent, after dissolving disperses fully, stop heating, obtain B, this process is finished in constantly stirring;
C) standby composition A is slowly joined among the B, be stirred to fully evenly, obtain C, the liquid fertilizer of promptly described pyroligneous-contained or careless vinegar liquid.
10. the preparation method of the liquid fertilizer of the described a kind of pyroligneous-contained or careless vinegar liquid of arbitrary claim in the claim 1～8 is characterized in that may further comprise the steps:
A) in reactor, drop into wood vinegar or careless vinegar liquid, be heated to 30～100 ℃, slowly drop into membrane-forming agent, after dissolving disperses fully, stop heating, add normal temperature wood vinegar or careless vinegar liquid again, stir, obtain A;
B) in 20～50 ℃ A, secondary element slowly has high input, trace element during drop into the dissolving back, drop into rare earth element or humic acids or humate again, sequestrant is dropped in the dissolving back, drops into plant hormone or plant-growth regulator again, drops into inert ingredient then, this process is finished in constantly stirring, and is cooled to the liquid fertilizer that normal temperature gets described pyroligneous-contained or careless vinegar liquid.
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| CNB2005100611398A CN100364934C (en) | 2005-10-17 | 2005-10-17 | Liquid fertilizer with pyroligneous liquor and oxalacetic liquor and production thereof |
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Family Cites Families (3)
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