CN103724128B - Preparation method of endotheliocyte leaf fertilizer - Google Patents
Preparation method of endotheliocyte leaf fertilizer Download PDFInfo
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- CN103724128B CN103724128B CN201310725448.5A CN201310725448A CN103724128B CN 103724128 B CN103724128 B CN 103724128B CN 201310725448 A CN201310725448 A CN 201310725448A CN 103724128 B CN103724128 B CN 103724128B
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Abstract
The invention belongs to the technical field of biomass chemical engineering and particularly relates to a preparation method of an endotheliocyte leaf fertilizer. The preparation method comprises the steps of sequentially carrying out oxidation, adsorption, ion exchange separation, reverse osmosis membrane concentration and the like on endotheliocyte, then adding humic acid, magnesium sulfate, urea, monopotassium phosphate, gibberellin, serine, betaine and other raw materials in certain proportions, and then mixing, drying and packaging to obtain the endotheliocyte leaf fertilizer. The preparation method is reasonable in design, simple to operate and low in cost; the concentration is carried out by adopting a membrane separation technology; the native state of the natural substances of the endotheliocyte is ensured through treatment at a relatively low temperature; the obtained endotheliocyte leaf fertilizer has the capabilities of improving the yield of crops by 20-30 percent, improving the quality of the crops and remarkably reducing the plant diseases and insect pests and has the control efficiency reaching 90 percent.
Description
Technical field
The invention belongs to technical field of biomass chemical engineering, be specifically related to a kind of preparation method of endotheliocyte leaf fertilizer.
Background technology
The acidity that the pyrolysis gas condensation that wood vinegar produces when being natural phant dry distillation charring obtains, reddish-brown or the dark-brown aqueous solution, containing 200 gas chromatographies such as alcohols, acids, phenols, aldehydes, ketones, be a kind of complicated components, diverse in function and metastable system material.In recent years, wood vinegar receives the concern of people as biomass application, and research shows that it has many reality and potentiality purposes at health care, food-processing and agricultural production.
Wood vinegar is also vegetable acid, agriculturally has plant growth regulation, improves the seed output and quality of crop.In addition, containing various active composition in wood vinegar, promotion meaning can be played in the growth of different aspect to plant.
Summary of the invention
For above problem, the invention provides a kind of preparation method of endotheliocyte leaf fertilizer with low cost, gained endotheliocyte leaf fertilizer can improve crop yield, improves crop, and significantly reduces disease and pest.
The present invention is achieved through the following technical solutions:
A preparation method for endotheliocyte leaf fertilizer, comprises the following steps:
(1) get wood vinegar stoste, add the hydrogen peroxide of its weight 1 ~ 2%, do not stop stirring 0.5 ~ 1 hour;
(2) continue the gac adding wood vinegar stoste weight 1 ~ 3%, stir 1 ~ 2 hour after being heated to 40 ~ 50 DEG C, filter, retain clear liquid; By gained clear liquid through being equipped with the resin column of ion exchange resin, after separation, obtain acetum pyrolignosum rectificatum liquid;
(3) by gained acetum pyrolignosum rectificatum liquid through reverse osmosis membrane separation system, making to obtain mass concentration is after the purifying wood vinegar of 50 ~ 70%, then adds the humic acid mixing and stirring of purifying wood vinegar weight 10 ~ 30%;
(4) by magnesium sulfate 5 ~ 7 weight part, urea 6 ~ 8 weight part, potassium primary phosphate 5 ~ 6 weight part, Plant hormones regulators,gibberellins 0.3 ~ 0.5 weight part, Serine 1 ~ 2 weight part, trimethyl-glycine 1 ~ 2 weight part mixing and stirring;
(5) step 3 gained liquid and step 4 gained powder are merged, mix and blend coating, the two weight ratio is 1:1.2 ~ 1.8, carries out successively drying, packing after coating, obtains endotheliocyte leaf fertilizer.
According to the preparation method of above-mentioned endotheliocyte leaf fertilizer, described hydrogen peroxide to be volumetric concentration be 30% the aqueous solution.
According to the preparation method of above-mentioned endotheliocyte leaf fertilizer, described ion exchange resin is macroporous adsorbent resin.
positive beneficial effect of the present invention:
Preparation method of the present invention is reasonable in design, simple to operate, with low cost, membrane separation technique is adopted to concentrate, process at a lower temperature ensure that the primordial condition of wood vinegar crude substance, gained endotheliocyte leaf fertilizer can improve crop yield 20 ~ 30%, improve crop, and significantly reduce disease and pest, prevent and treat efficiency and reach about 90% (see table 1).
Embodiment
Below in conjunction with specific embodiment, the present invention is described in more detail, but the invention is not restricted to these embodiments.
embodiment 1
The method of purification of the present embodiment biomass wood vinegar, comprises the following steps:
(1) in wood vinegar stoste, add the hydrogen peroxide of its weight 2%, do not stop stirring 40 minutes;
(2) continue the gac adding wood vinegar stoste weight 1%, stir 1 hour after being heated to 40 ~ 50 DEG C, filter, retain clear liquid; By gained clear liquid through being equipped with the resin column of ion exchange resin, after separation, obtain acetum pyrolignosum rectificatum liquid;
(3) gained acetum pyrolignosum rectificatum liquid is passed through reverse osmosis membrane separation system, obtaining mass concentration is after the purifying wood vinegar of 70%, then adds the humic acid mixing and stirring of its weight 10%;
(4) by magnesium sulfate 5 weight part, urea 8 weight part, potassium primary phosphate 5 weight part, Plant hormones regulators,gibberellins 0.5 weight part, Serine 1 weight part, trimethyl-glycine 2 weight part mixing and stirring;
(5) step 3 gained liquid and step 4 gained powder are merged, mix and blend coating, the two weight ratio is 1:1.2, carries out successively drying, packing after coating, obtains endotheliocyte leaf fertilizer.
Described hydrogen peroxide to be volumetric concentration be 30% the aqueous solution, described ion exchange resin is macroporous adsorbent resin.
embodiment 2
The method of purification of the present embodiment biomass wood vinegar, comprises the following steps:
(1) in wood vinegar stoste, add the hydrogen peroxide of its weight 1%, do not stop stirring 30 minutes;
(2) continue the gac adding wood vinegar stoste weight 2%, stir 1.5 hours after being heated to 40 ~ 50 DEG C, filter, retain clear liquid; By gained clear liquid through being equipped with the resin column of ion exchange resin, after separation, obtain acetum pyrolignosum rectificatum liquid;
(3) gained acetum pyrolignosum rectificatum liquid is passed through reverse osmosis membrane separation system, obtaining mass concentration is after the purifying wood vinegar of 60%, then adds the humic acid mixing and stirring of its weight 30%;
(4) by magnesium sulfate 7 weight part, urea 6 weight part, potassium primary phosphate 6 weight part, Plant hormones regulators,gibberellins 0.3 weight part, Serine 2 weight part, trimethyl-glycine 1 weight part mixing and stirring;
(5) step 3 gained liquid and step 4 gained powder are merged, mix and blend coating, the two weight ratio is 1:1.5, carries out successively drying, packing after coating, obtains endotheliocyte leaf fertilizer.
Described hydrogen peroxide to be volumetric concentration be 30% the aqueous solution, described ion exchange resin is macroporous adsorbent resin.
embodiment 3
The method of purification of the present embodiment biomass wood vinegar, comprises the following steps:
(1) in wood vinegar stoste, add the hydrogen peroxide of its weight 1.5%, do not stop stirring 1 hour;
(2) continue the gac adding wood vinegar stoste weight 3%, stir 2 hours after being heated to 40 ~ 50 DEG C, filter, retain clear liquid; By gained clear liquid through being equipped with the resin column of ion exchange resin, after separation, obtain acetum pyrolignosum rectificatum liquid;
(3) gained acetum pyrolignosum rectificatum liquid is passed through reverse osmosis membrane separation system, obtaining mass concentration is after the purifying wood vinegar of 50%, then adds the humic acid mixing and stirring of its weight 20%;
(4) by magnesium sulfate 6 weight part, urea 7 weight part, potassium primary phosphate 5.5 weight part, Plant hormones regulators,gibberellins 0.4 weight part, Serine 1.5 weight part, trimethyl-glycine 1.5 weight part mixing and stirring;
(5) step 3 gained liquid and step 4 gained powder are merged, mix and blend coating, the two weight ratio is 1:1.8, carries out successively drying, packing after coating, obtains endotheliocyte leaf fertilizer.
Described hydrogen peroxide to be volumetric concentration be 30% the aqueous solution, described ion exchange resin is macroporous adsorbent resin.
The prevention effect of table 1 embodiment 1 ~ 3 and output
| Process | Prevention effect | Cucumber yield/mu |
| Blank | 6232Kg | |
| Embodiment 1 | 91.8% | 7873Kg |
| Embodiment 2 | 87.6% | 7624Kg |
| Embodiment 3 | 89.3% | 7751Kg |
The present invention is not limited to above-mentioned embodiment, and those skilled in the art also can make multiple change accordingly, but to be anyly equal to the present invention or similar change all should be encompassed in the scope of the claims in the present invention.
Claims (3)
1. a preparation method for endotheliocyte leaf fertilizer, is characterized in that, comprises the following steps:
(1) get wood vinegar stoste, add the hydrogen peroxide of its weight 1 ~ 2%, do not stop stirring 0.5 ~ 1 hour;
(2) continue the gac adding wood vinegar stoste weight 1 ~ 3%, stir 1 ~ 2 hour after being heated to 40 ~ 50 DEG C, filter, retain clear liquid; By gained clear liquid through being equipped with the resin column of ion exchange resin, after separation, obtain acetum pyrolignosum rectificatum liquid;
(3) by gained acetum pyrolignosum rectificatum liquid through reverse osmosis membrane separation system, making to obtain mass concentration is after the purifying wood vinegar of 50 ~ 70%, then adds the humic acid mixing and stirring of purifying wood vinegar weight 10 ~ 30%;
(4) by magnesium sulfate 5 ~ 7 weight part, urea 6 ~ 8 weight part, potassium primary phosphate 5 ~ 6 weight part, Plant hormones regulators,gibberellins 0.3 ~ 0.5 weight part, Serine 1 ~ 2 weight part, trimethyl-glycine 1 ~ 2 weight part mixing and stirring;
(5) step 3 gained liquid and step 4 gained powder are merged, mix and blend coating, the two weight ratio is 1:1.2 ~ 1.8, carries out successively drying, packing after coating, obtains endotheliocyte leaf fertilizer.
2. the preparation method of endotheliocyte leaf fertilizer according to claim 1, is characterized in that: described hydrogen peroxide to be volumetric concentration be 30% the aqueous solution.
3. the preparation method of endotheliocyte leaf fertilizer according to claim 1, is characterized in that: described ion exchange resin is macroporous adsorbent resin.
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Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9604887B2 (en) | 2015-04-20 | 2017-03-28 | True Organic Products, Inc. | Betaine based organic fertilizer |
| US9850178B2 (en) | 2015-08-06 | 2017-12-26 | True Organic Products, Inc. | Betaine based organic fertilizer |
| US9815744B2 (en) | 2015-09-24 | 2017-11-14 | True Organic Products, Inc. | pH adjusted betaine based organic fertilizer |
| CN105647536A (en) * | 2015-12-29 | 2016-06-08 | 辛集市远翔环保能源科技有限公司 | Composition for removing pesticide residues in soil |
| CN105461455A (en) * | 2015-12-29 | 2016-04-06 | 辛集市远翔环保能源科技有限公司 | Foliar spray fertilizer |
| US10301226B2 (en) | 2016-04-13 | 2019-05-28 | True Organic Products, Inc. | Ph adjusted organic fertilizer from anaerobic digestate and grain by-products |
| CN106278525A (en) * | 2016-07-14 | 2017-01-04 | 北京澳佳生态农业股份有限公司 | A kind of activated humic acid, containing its chelating fertilizer and preparation method thereof |
| CN106495840A (en) * | 2016-10-11 | 2017-03-15 | 常州市鼎升环保科技有限公司 | A kind of preparation method of the lasting foliage fertilizer of fertilizer efficiency |
| CN109400399A (en) * | 2019-01-08 | 2019-03-01 | 北京三聚绿能科技有限公司 | A kind of wood vinegar organic fertilizer and its fertilizing method |
| US11155504B1 (en) | 2019-01-10 | 2021-10-26 | True Organic Products, Inc. | Combination fertilizer |
| CN110818456A (en) * | 2019-12-11 | 2020-02-21 | 武汉天颖环境工程股份有限公司 | Preparation method of pyroligneous foliar fertilizer |
| CN110746232A (en) * | 2019-12-11 | 2020-02-04 | 武汉天颖环境工程股份有限公司 | Preparation method of pyroligneous foliar fertilizer with lasting fertilizer effect |
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Effective date of registration: 20190729 Address after: 450000 No. 1 Shuguang Road, Mazhai Industrial Agglomeration Area, Erqi District, Zhengzhou City, Henan Province Patentee after: Henan golden land science and Technology Service Co., Ltd. Address before: 450000 Huacheng International Center, No. 80 University Road, Erqi District, Zhengzhou City, Henan Province, No. 18 Floor 9 Patentee before: ZHENGZHOU QIKE BIOTECHNOLOGY CO., LTD. |