CN107287603A - Soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid - Google Patents
Soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid Download PDFInfo
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- CN107287603A CN107287603A CN201710416030.4A CN201710416030A CN107287603A CN 107287603 A CN107287603 A CN 107287603A CN 201710416030 A CN201710416030 A CN 201710416030A CN 107287603 A CN107287603 A CN 107287603A
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- derusting
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/02—Cleaning or pickling metallic material with solutions or molten salts with acid solutions
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G1/00—Mixtures of fertilisers belonging individually to different subclasses of C05
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
Soil preparations and its waste water utilization method are gone the invention discloses a kind of multiple-effect derusting containing plant vinegar liquid.Belong to natural products field of deep.Formulation product is completely dissolved by refined plant vinegar liquid, emulsifying agent and organic acid by stirring to remove soil preparations as multiple-effect derusting；It is after 79, to distill all moisture, remaining dry, which just turns into organic and inorganic fertilizer or adds plant nutrient fertilizer, to be well mixed using the waste liquid after said preparation, adding NaOH or KOH adjustment pH values.Product of the present invention can replace traditional strong inorganic acid rust remover, can be not only used for metal-derusting, can also remove the dirt for degreasing and being formed by calcium ions and magnesium ions, and, the waste liquid formed after processing is completed, by processing method, organic and inorganic fertilizer material is converted into by waste liquid.
Description
Technical field
Soil preparations and its waste water utilization method are gone the present invention relates to a kind of multiple-effect derusting containing plant vinegar liquid, for refined plant
Vinegar liquid, belongs to natural rust remover field, and dirt preparation processing method and waste water utilization method are gone in specifically a kind of multiple-effect derusting.
Background technology
Traditional chemical derusting can chemically react usually using strong acid, acid with iron rust and metal oxide, and generation can
Dissolubility salt, so that the purpose of derusting is reached, while derusting, acid and can be reacted with underlying metal releasing hydrogen, Hydrogen Energy pair
The oxide skin of iron rust and indissoluble produces pressure, be conducive to they peeling and high price iron reduction, accelerate the process of pickling, but pass
There is also obvious defect for the acid solution processing method of system：The generation of a large amount of hydrogen can make steel produce hydrogen embrittlement i.e. in processing procedure
Phenomenon, causes the mechanical properties decrease of metal, the intensity of influence steel in itself；Acid mist is easily formed simultaneously, influence operating personnel's
Equipment and environment around health and corrosion；The consumption of acid solution is also larger, increases processing cost；This kind of acid can be formed to steel
Excessive erosion.In addition the residue largely produced, need to often be discharged, both heavy corrosion industrial pipeline, and contaminated soil and environment.
Plant biomass gasification liquid (abbreviation plant vinegar liquid) is to collect to obtain after vegetable material and its industrial wood waste pyrolysis
The brown liquid material that is condensed at normal temperatures of gas, what is be primarily present at present is bamboo vinegar, pyrolkigneous liquid and careless vinegar liquid.Mesh
Before, during bamboo and wood material and stalk are processed into corresponding plant charcoal, because the machine using modernization is efficiently produced,
The accessory substance produced in process of production-gasification of biomass liquid, never finds its purposes and turns into waste, many producers pair
It is not taken recycling and is directly discharged into air, and pollution is caused to environment, and easily forms local acid rain, and pollutes
Environment, therefore the technical barrier as modern production plant charcoal.
In a word, unpleasant sootiness taste, and active constituent content mistake are produced because plant vinegar liquid contains a certain amount of tar
It is low and cause that activity is not high, the reason for packed and transported cost is too high, prevent plant vinegar liquid from forming the large-tonnage consumer goods.Purport of the present invention
The market-oriented problem more than being solved with technological means.
The content of the invention
It is an object of the invention to overcome the defect that prior art is present, there is provided a kind of multiple-effect derusting decontamination containing plant vinegar liquid
Dirty preparation and its waste water utilization method, instead of traditional strong inorganic acid rust remover, can be not only used for metal-derusting, can also remove
Greasy dirt and the dirt formed by calcium ions and magnesium ions, moreover, the waste liquid formed after processing is completed, by distillation and concentration, addition or
Waste liquid is converted into organic and inorganic fertilizer material by person without the plant nutrient of needs.
Number is the number of weight in present specification.
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that contained
Refined 10-90 part of plant vinegar liquid, 2-10 part of emulsifying agent, 8-80 parts of organic acid, stir to be completely dissolved to become multiple-effect and derust and remove dirt
Preparation；Waste liquid after using said preparation, adds NaOH or KOH adjustment pH values after 7-9, to distill all moisture, remaining
Dry, which just turns into organic and inorganic fertilizer or adds plant nutrient fertilizer, to be well mixed.
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that described
The refined plant vinegar liquid of tar removing refer to that, by distillation or rectifying and the plant vinegar liquid after removing tar removing, tar content is less than 2%
Plant vinegar liquid.
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that described
Plant vinegar liquid include bamboo vinegar, pyrolkigneous liquid and careless vinegar liquid (also referred to as stalk vinegar liquid).
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that described
Emulsifying agent include DBSA, Tween-80, OP-10, APG (APG-0810, APG-1214, APG-0814)
One or more kinds of mixtures.
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that described
Organic acid be formic acid, acetic acid, propionic acid, one or more kinds of mixtures of citric acid.
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that described
Plant nutrient fertilizer include urea, potassium dihydrogen phosphate, potassium nitrate etc..
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that each
Component ratio is optimized for containing refined 40-60 parts of plant vinegar liquid, 5-8 parts of emulsifying agent, 27-55 parts of organic acid, and stirring is completely dissolved i.e.
Soil preparations are removed as multiple-effect derusting；It is distillation after 8 using the waste liquid after said preparation, adding NaOH or KOH adjustment pH values
Fall all moisture, remaining dry just turns into organic and inorganic fertilizer or adds the plant such as urea, potassium dihydrogen phosphate, potassium nitrate
Thing fertilizer is well mixed.
Soil preparations and its waste water utilization method are gone in a kind of described multiple-effect derusting containing plant vinegar liquid, it is characterised in that formula
Product is used for metal-derusting dirt, boiler tubing derusting dirt, family kitchen toilet derusting dirt, and waste liquid adds
Work is into organic and inorganic fertilizer material.
Embodiment
The present invention will be just further described by example below.
Example 1
10 kilograms of refined bamboo vinegars are put into enamel reaction still, emulsifying agent detergent alkylate is then slowly added to thereto
2 kilograms of stirrings of sulfonic acid are completely dissolved, and add 8 kilograms of formic acid, and stirring, which is completely dissolved, to be become multiple-effect derusting and remove soil preparations；
Using the waste liquid after said preparation, it is after 7, to distill all moisture, remaining dry just turns into that NaOH adjustment pH values have been lacked in addition
Organic and inorganic fertilizer.
Example 2
20 kilograms of acetum pyrolignosum rectificatum liquid are put into enamel reaction still, emulsifier tween -80 3 is then slowly added to thereto
Kilogram stirring is completely dissolved, and adds 20 kilograms of acetic acid, and stirring, which is completely dissolved, to be become multiple-effect derusting and remove soil preparations；Using
Waste liquid after said preparation, addition lacked KOH adjustment pH value be 7.5 after, distill all moisture, remaining dry adds urea
10 kilograms, stir, just turn into organic and inorganic fertilizer.
Example 3
30 kilograms of refined careless vinegar liquids are put into enamel reaction still, emulsifier op-10 4 are then slowly added to thereto public
Jin stirring is completely dissolved, and adds 30 kilograms of acetic acid, and stirring, which is completely dissolved, to be become multiple-effect derusting and remove soil preparations；Should using
Waste liquid after preparation, addition lacked KOH adjustment pH value be 8.0 after, distill all moisture, remaining dry adds di(2-ethylhexyl)phosphate
15 kilograms of hydrogen potassium, stirs, and just turns into organic and inorganic fertilizer.
Example 4
40 kilograms of refined careless vinegar liquids are put into enamel reaction still, emulsifying agent APG-0810 5 is then slowly added to thereto
Kilogram stirring is completely dissolved, and adds 40 kilograms of propionic acid, and stirring, which is completely dissolved, to be become multiple-effect derusting and remove soil preparations；Using
Waste liquid after said preparation, addition lacked KOH adjustment pH value be 8.0 after, distill all moisture, remaining dry adds phosphoric acid
15 kilograms of potassium dihydrogen, stirs, and just turns into organic and inorganic fertilizer.
Example 5
50 kilograms of acetum pyrolignosum rectificatum liquid are put into enamel reaction still, emulsifying agent APG-1214 6 is then slowly added to thereto
Kilogram stirring is completely dissolved, and adds 50 kilograms of citric acid, and stirring, which is completely dissolved, to be become multiple-effect derusting and remove soil preparations；Make
With the waste liquid after said preparation, it is after 8.5, to distill all moisture, remaining dry is added that NaOH adjustment pH values have been lacked in addition
20 kilograms of potassium nitrate, stirs, and just turns into organic and inorganic fertilizer.
Example 6
90 kilograms of refined bamboo vinegars are put into enamel reaction still, emulsifying agent APG-0814 is then slowly added to thereto
10 kilograms of stirrings are completely dissolved, and add 80 kilograms of formic acid, and stirring, which is completely dissolved, to be become multiple-effect derusting and remove soil preparations；Make
With the waste liquid after said preparation, it is after 9.0, to distill all moisture, remaining dry is added that NaOH adjustment pH values have been lacked in addition
30 kilograms of potassium nitrate, stirs, and just turns into organic and inorganic fertilizer.
Example 7
60 kilograms of refined plant vinegar liquids (refined careless each 20 kilograms of the vinegar liquid of bamboo and wood) are put into enamel reaction still, then thereto
It is slowly added to 9 kilograms of emulsifying agent (each 3 kilograms of DBSA, Tween-80, OP-10) stirring to be completely dissolved, has added
Sour 60 (each 20 kilograms of formic acid, acetic acid, the citric acids) kilogram of machine acid, stirring, which is completely dissolved, to be become multiple-effect derusting and removes soil preparations；
Using the waste liquid after said preparation, it is after 8.0, to distill all moisture, remaining dry is stirred that NaOH adjustment pH values have been lacked in addition
Mix uniform, just turn into organic and inorganic fertilizer.
Example 8
70 kilograms of refined plant vinegar liquids (refined each 35 kilograms of bamboo and wood vinegar liquid) are put into enamel reaction still, are then delayed thereto
Slow 6 kilograms of emulsifying agent of addition (each 2 kilograms of APG-0810, APG-1214, APG-0814) stirring is completely dissolved, and adds organic acid
Sour 70 kilograms (each 35 kilograms of formic acid, acetic acid), stirring, which is completely dissolved, to be become multiple-effect derusting and removes soil preparations；Using said preparation
Waste liquid afterwards, addition lacked NaOH adjustment pH value be 7.5 after, distill all moisture, remaining dry adds vegetable fertilizer
45 kilograms (each 15 kilograms of urea, potassium dihydrogen phosphate, potassium nitrate), stirs, and just turns into organic and inorganic fertilizer.
Example 9
80 kilograms of refined plant vinegar liquids (refined careless each 40 kilograms of the vinegar liquid of bamboo) are put into enamel reaction still, are then delayed thereto
Slow 9 kilograms of emulsifying agent of addition (each 4.5 kilograms of APG-0810, DBSA) stirring is completely dissolved, and adds organic acid
Sour 80 kilograms (each 20 kilograms of formic acid, acetic acid, propionic acid, citric acid), stirring, which is completely dissolved, to be become multiple-effect derusting and removes soil preparations；
Using the waste liquid after said preparation, it is after 7.0, to distill all moisture, remaining dry is again that NaOH adjustment pH values have been lacked in addition
50 kilograms of vegetable fertilizer (each 25 kilograms of potassium dihydrogen phosphate, potassium nitrate) is added, is stirred, just turns into organic and inorganic fertilizer.
Example 10
40 kilograms of refined plant vinegar liquids (refined careless each 20 kilograms of the vinegar liquid of wood) are put into enamel reaction still, are then delayed thereto
Slow 5 kilograms of the emulsifying agent (each 1 kilogram of Tween-80, OP-10, APG-0810, APG-1214, APG-0814) that adds stirs completely molten
Solution, adds sour 27 kilograms (each 9 kilograms of formic acid, acetic acid, the citric acid) of organic acid, and stirring, which is completely dissolved, becomes multiple-effect derusting
Soil preparations；Using the waste liquid after said preparation, it is after 7.0, to distill all moisture that NaOH adjustment pH values have been lacked in addition, remaining
Dry adds 30 kilograms of vegetable fertilizer (each 10 kilograms of urea, potassium dihydrogen phosphate, potassium nitrate), stirs, and just turning into has
Machine inorganic fertilizer.
Example 11
60 kilograms of refined plant vinegar liquid (25 kilograms of refined bamboo vinegar, 20 kilograms of pyrolkigneous liquid, careless vinegar are put into enamel reaction still
15 kilograms of liquid), emulsifying agent 8 kilograms of (DBSA, APG-0810, APG-1214, APG- are then slowly added to thereto
0814 each 2 kilograms) stirring is completely dissolved, and adds organic acid sour 55 kilograms of (25 kilograms of formic acid, 15 kilograms of acetic acid, citric acids 15
Kilogram), stirring be completely dissolved become multiple-effect derusting remove soil preparations；NaOH has been lacked in waste liquid after using said preparation, addition
Adjust pH value be 7.5 after, distill all moisture, remaining dry adds vegetable fertilizer 60 kilograms of (urea, biphosphates
Each 20 kilograms of potassium, potassium nitrate), stir, just turn into organic and inorganic fertilizer.
Example 12
50 kilograms of refined plant vinegar liquid (20 kilograms of refined bamboo vinegar, 15 kilograms of pyrolkigneous liquid, careless vinegar are put into enamel reaction still
15 kilograms of liquid), emulsifying agent 6 kilograms of (DBSA, Tween-80, OP-10, APG- are then slowly added to thereto
0810th, each 1 kilogram of APG-1214, APG-0814) stirring is completely dissolved, and adds organic acid sour 41 kilograms of (21 kilograms of formic acid, second
Sour 10 kilograms, 10 kilograms of citric acid), stirring, which is completely dissolved, to be become multiple-effect derusting and removes soil preparations；After using said preparation
Waste liquid, it is after 8.0, to distill all moisture, it is public that remaining dry adds vegetable fertilizer 90 that NaOH adjustment pH values have been lacked in addition
Jin (each 30 kilograms of urea, potassium dihydrogen phosphate, potassium nitrate), stirs, and just turns into organic and inorganic fertilizer.
Below by way of the effect of experiment explanation foregoing invention product.
The percentage of the natural 2 hours dirts that derust of the embodiment 1-12 of table 1.
(rust dirt area after before processing rust dirt area-processing)/before processing rust dirt area * 100%
The as shown by data of table 1, embodiment 1-12 has preferably to the percentage of the natural 2 hours dirts that derust of embodiment 1-12
Removal effect, wherein embodiment 1-9 effect gradually strengthen to more than 90%, and the effect for applying a 10-12 also basically reaches 80%
More than.
Claims (8)
1. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid, it is characterised in that contain refined plant vinegar
10-90 parts of liquid, 2-10 parts of emulsifying agent, 8-80 parts of organic acid, stirring be completely dissolved become multiple-effect derusting remove soil preparations；Make
With the waste liquid after said preparation, add after NaOH or KOH adjustment pH values are 7-9, distill all moisture, remaining dry just into
For organic and inorganic fertilizer or add plant nutrient fertilizer be well mixed.
2. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid according to claim 1, its
It is characterised by that the refined plant vinegar liquid of described tar removing refers to the plant vinegar liquid after tar removing is removed in distillation or rectifying, tar
Content is less than 2% plant vinegar liquid.
3. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid according to claim 1, its
It is characterised by that described plant vinegar liquid includes bamboo vinegar, pyrolkigneous liquid and careless vinegar liquid (also referred to as stalk vinegar liquid).
4. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid according to claim 1, its
It is characterised by that described emulsifying agent includes DBSA, Tween-80, OP-10, APG (APG-0810, APG-
1214th, APG-0814) one or more kinds of mixtures.
5. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid according to claim 1, its
It is formic acid, acetic acid, propionic acid, one or more kinds of mixtures of citric acid to be characterised by described organic acid.
6. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid according to claim 1, its
It is characterised by that described plant nutrient fertilizer includes urea, potassium dihydrogen phosphate, potassium nitrate etc..
7. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid according to claim 1, its
It is characterised by that each component ratio is optimized for, containing refined 40-60 parts of plant vinegar liquid, 5-8 parts of emulsifying agent, 27-55 parts of organic acid, stirring
Mix be completely dissolved become multiple-effect derusting remove soil preparations；Waste liquid after using said preparation, adds NaOH or KOH adjustment PH
It is worth after 8, to distill all moisture, remaining dry just turns into organic and inorganic fertilizer or adds urea, biphosphate
The vegetable fertilizers such as potassium, potassium nitrate are well mixed.
8. soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid according to claim 1, its
It is characterised by that formulation product is used for metal-derusting dirt, boiler tubing derusting dirt, the derusting decontamination of family kitchen toilet
Dirt, and waste liquid are processed into organic and inorganic fertilizer material.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710416030.4A CN107287603A (en) | 2017-06-01 | 2017-06-01 | Soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid |
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|---|---|---|---|
| CN201710416030.4A CN107287603A (en) | 2017-06-01 | 2017-06-01 | Soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid |
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| CN107287603A true CN107287603A (en) | 2017-10-24 |
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| CN201710416030.4A Pending CN107287603A (en) | 2017-06-01 | 2017-06-01 | Soil preparations and its waste water utilization method are gone in a kind of multiple-effect derusting containing plant vinegar liquid |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110607207A (en) * | 2019-10-09 | 2019-12-24 | 唐山进海新材料有限公司 | Wood vinegar liquid detergent composition with antibacterial effect and preparation method thereof |
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