CN101522752B - 热固性树脂组合物及用其形成的预浸料及层叠板 - Google Patents
热固性树脂组合物及用其形成的预浸料及层叠板 Download PDFInfo
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Abstract
Description
实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | 实施例6 | |
热固性树脂组合物(质量份) | ||||||
(A)成分 | ||||||
固化剂(A-1) | 40 | 40 | ||||
固化剂(A-2) | 40 | 40 | ||||
固化剂(A-3) | 40 | |||||
固化剂(A-4) | 40 | |||||
(B)成分 | ||||||
苯基胍胺 | 10 | 10 | 10 | 10 | 10 | 10 |
(C)成分 | ||||||
共聚树脂(C-1) | 10 | 10 | 10 | |||
共聚树脂(C-2) | 10 | |||||
共聚树脂(C-3) | 10 | |||||
共聚树脂(C-4) | 10 | |||||
(D)成分 | ||||||
苯酚酚醛清漆型环氧树脂(D-1) | 40 | 40 | 40 | 40 | ||
环戊二烯型环氧树脂(D-2) | 30 | 30 | ||||
(环氧固化剂) | ||||||
甲酚酚醛清漆型酚醛树脂 | 10 | 10 | ||||
(E)成分 | ||||||
粉碎二氧化硅(E-1) | 10 | 10 | 10 | 10 | 10 | 10 |
氢氧化铝(E-2) | 80 | 80 | 80 | 80 | 80 | 80 |
测定·评价结果 | ||||||
(1)对铜箔的胶粘性(铜箔剥离强度:kN/m) | 1.60 | 1.65 | 1.69 | 1.62 | 1.61 | 1.60 |
(2)玻璃化转变温度(Tg℃) | 230 | 225 | 228 | 230 | 230 | 235 |
(3)焊接耐热性 | 良好 | 良好 | 良好 | 良好 | 良好 | 良好 |
(4)附着到铜时的耐热性(T-288:min) | >60 | >60 | >60 | >60 | >60 | >60 |
(5)吸湿性(吸水率;%) | 0.5 | 0.5 | 0.5 | 0.5 | 0.6 | 0.5 |
(6)阻燃性 | V-0 | V-0 | V-0 | V-0 | V-0 | V-0 |
(7)介电常数(1GHz) | 4.0 | 3.9 | 4.0 | 4.0 | 4.1 | 4.0 |
(8)介质损耗角正切(1GHz) | 0.004 | 0.004 | 0.004 | 0.005 | 0.005 | 0.005 |
实施例7 | 实施例8 | 实施例9 | 实施例10 | |
热固性树脂组合物(质量份) | ||||
(A)成分 | ||||
固化剂(A-5) | 40 | |||
固化剂(A-6) | 40 | |||
固化剂(A-7) | 40 | |||
固化剂(A-8) | 40 | |||
(B)成分 | ||||
苯基胍胺 | 10 | 10 | 10 | 10 |
(C)成分 | ||||
共聚树脂(C-1) | 10 | |||
共聚树脂(C-2) | 10 | |||
共聚树脂(C-3) | 10 | |||
共聚树脂(C-4) | 10 | |||
(D)成分 | ||||
苯酚酚醛清漆型环氧树脂(D-1) | 40 | 40 | 40 | 40 |
环戊二烯型环氧树脂(D-2) | ||||
(环氧固化剂) | ||||
甲酚酚醛清漆型酚醛树脂 | ||||
(E)成分 | ||||
粉碎二氧化硅(E-1) | 10 | 10 | 10 | 10 |
氢氧化铝(E-2) | 80 | 80 | 80 | 80 |
测定·评价结果 | ||||
(1)对铜箔的胶粘性(铜箔剥离强度:kN/m) | 1.60 | 1.65 | 1.65 | 1.65 |
(2)玻璃化转变温度(Tg℃) | 240 | 235 | 225 | 245 |
(3)焊接耐热性 | 良好 | 良好 | 良好 | 良好 |
(4)附着到铜时的耐热性(T-288:min) | >60 | >60 | >60 | >60 |
(5)吸湿性(吸水率:%) | 0.5 | 0.5 | 0.5 | 0.5 |
(6)阻燃性 | V-0 | V-0 | V-0 | V-0 |
(7)介电常数(1GHz) | 4.1 | 3.8 | 3.7 | 4.1 |
(8)介质损耗角正切(1GHz) | 0.004 | 0.003 | 0.002 | 0.003 |
实施例11 | 实施例12 | 实施例13 | 实施例14 | 实施例15 | 实施例16 | |
热固性树脂组合物(质量份) | ||||||
(A)成分 | ||||||
固化剂(A-1) | 40 | 40 | ||||
固化剂(A-2) | 40 | 40 | ||||
固化剂(A-3) | 40 | |||||
固化剂(A-4) | 40 | |||||
(B)成分 | ||||||
双氰胺 | 10 | 10 | 10 | 10 | 10 | 10 |
(C)成分 | ||||||
共聚树脂(C-1) | 10 | 10 | 10 | |||
共聚树脂(C-2) | 10 | |||||
共聚树脂(C-3) | 10 | |||||
共聚树脂(C-4) | 10 | |||||
(D)成分 | ||||||
苯酚酚醛清漆型环氧树脂(D-1) | 40 | 40 | 40 | 40 | ||
双环戊二烯型环氧树脂(D-2) | 30 | 30 | ||||
(E)成分 | ||||||
粉碎二氧化硅(E-1) | 10 | 10 | 10 | 10 | 10 | 10 |
氢氧化铝(E-2) | 80 | 80 | 80 | 80 | 80 | 80 |
(环氧固化剂) | ||||||
甲酚酚醛清漆型酚醛树脂 | 10 | 10 | ||||
测定·评价结果 | ||||||
(1)对铜箔的胶粘性(铜箔剥离强度:kN/m) | 1.61 | 1.64 | 1.68 | 1.62 | 1.62 | 1.60 |
(2)玻璃化转变温度(Tg℃) | 231 | 226 | 229 | 230 | 231 | 236 |
(3)焊接耐热性 | 良好 | 良好 | 良好 | 良好 | 良好 | 良好 |
(4)附着到铜时的耐热性(T-288:min) | >60 | >60 | >60 | >60 | >60 | >60 |
(5)吸湿性(吸水率:%) | 0.6 | 0.5 | 0.5 | 0.5 | 0.6 | 0.6 |
(6)阻燃性 | V-0 | V-0 | V-0 | V-0 | V-0 | V-0 |
(7)介电常数(1GHz) | 4.1 | 3.9 | 4.0 | 4.0 | 4.2 | 4.1 |
(8)介质损耗角正切(1GHz) | 0.004 | 0.004 | 0.004 | 0.005 | 0.005 | 0.005 |
实施例17 | 实施例18 | 实施例19 | 实施例20 | |
热固性树脂组合物(质量份) | ||||
(A)成分 | ||||
固化剂(A-5) | 40 | |||
固化剂(A-6) | 40 | |||
固化剂(A-7) | 40 | |||
固化剂(A-8) | 40 | |||
(B)成分 | ||||
双氰胺 | 10 | 10 | 10 | 10 |
(C)成分 | ||||
共聚树脂(C-1) | 10 | |||
共聚树脂(C-2) | 10 | |||
共聚树脂(C-3) | 10 | |||
共聚树脂(C-4) | 10 | |||
(D)成分 | ||||
苯酚酚醛清漆型环氧树脂(D-1) | 40 | 40 | 40 | 40 |
双环戊二烯型环氧树脂(D-2) | ||||
(环氧固化剂) | ||||
甲酚酚醛清漆型酚醛树脂 | ||||
(E)成分 | ||||
粉碎二氧化硅(E-1) | 10 | 10 | 10 | 10 |
氢氧化铝(E-2) | 80 | 80 | 80 | 80 |
测定·评价结果 | ||||
(1)对铜箔的胶粘性(铜箔剥离强度:kN/m) | 1.60 | 1.64 | 1.63 | 1.64 |
(2)玻璃化转变温度(Tg℃) | 239 | 233 | 224 | 245 |
(3)焊接耐热性 | 良好 | 良好 | 良好 | 良好 |
(4)附着到铜时的耐热性(T-288:min) | >60 | >60 | >60 | >60 |
(5)吸湿性(吸水率:%) | 0.6 | 0.6 | 0.5 | 0.5 |
(6)阻燃性 | V-0 | V-0 | V-0 | V-0 |
(7)介电常数(1GHz) | 4.1 | 3.8 | 3.8 | 4.2 |
(8)介质损耗角正切(1GHz) | 0004 | 0.003 | 0.003 | 0.003 |
比较例1 | 比较例2 | 比较例3 | 比较例4 | 比较例5 | 比较例6 | |
热固性树脂组合物(质量份) | ||||||
(A)成分 | ||||||
固化剂(A-1) | 40 | 40 | ||||
固化剂(A-9) | 40 | 40 | 40 | |||
固化剂(A-10) | 40 | |||||
(B)成分 | ||||||
苯基胍胺 | 10 | 10 | 10 | 10 | ||
(C)成分 | ||||||
共聚树脂(C-3) | 10 | |||||
共聚树脂(C-4) | 10 | |||||
(D)成分 | ||||||
苯酚酚醛清漆型环氧树脂(D-1) | 40 | 40 | ||||
环戊二烯型环氧树脂(D-2) | 50 | 50 | 40 | 40 | ||
(环氧固化剂) | ||||||
甲酚酚醛清漆型酚醛树脂 | 10 | 10 | 10 | 10 | ||
(E)成分 | ||||||
粉碎二氧化硅(E-1) | 10 | 10 | 10 | 10 | 10 | 10 |
氢氧化铝(E-2) | 80 | 80 | 80 | 80 | 80 | 80 |
测定·评价结果 | ||||||
(1)对铜箔的胶粘性(铜箔剥离强度:kN/m) | 0.90 | 0.90 | 0.70 | 0.45 | - | - |
(2)玻璃化转变温度(Tg℃) | 140 | 150 | 130 | 120 | - | - |
(3)焊接耐热性 | 膨胀 | 膨胀 | 膨胀 | 膨胀 | - | - |
(4)附着到铜时的耐热性(T-288:min) | 1 | 1 | 1 | 0 | - | - |
(5)吸湿性(吸水率:%) | 1.1 | 1.1 | 0.8 | 1.1 | - | - |
(6)阻燃性 | V-0 | V-1 | V-1 | 燃烧 | - | - |
(7)介电常数(1GHz) | 49 | 49 | 5.1 | 5.1 | - | - |
(8)介质损耗角正切(1GHz) | 0.014 | 0.014 | 0.017 | 0.023 | - | - |
比较例7 | 比较例8 | |
热固性树脂组合物(质量份) | ||
(A)成分 | ||
固化剂(A-1) | ||
固化剂(A-5) | 40 | |
固化剂(A-6) | 40 | |
(B)成分 | ||
双氰胺 | 10 | 10 |
(C)成分 | ||
共聚树脂(C-3) | 10 | |
共聚树脂(C-4) | 10 | |
(D)成分 | ||
苯酚酚醛清漆型环氧树脂(D-1) | 40 | 40 |
双环戊二烯型环氧树脂(D-2) | ||
(E)成分 | ||
粉碎二氧化硅(E-1) | 10 | 10 |
氢氧化铝(E-2) | 80 | 80 |
(环氧固化剂) | ||
甲酚酚醛清漆型酚醛树脂 | ||
测定·评价结果 | ||
(1)对铜箔的胶粘性(铜箔剥离强度:kN/m) | 0.89 | 0.88 |
(2)玻璃化转变温度(Tg℃) | 140 | 150 |
(3)焊接耐热性 | 膨胀 | 膨胀 |
(4)附着到铜时的耐热性(T-288:min) | 1 | 1 |
(5)吸湿性(吸水率:%) | 1.1 | 1.1 |
(6)阻燃性 | V-0 | V-1 |
(7)介电常数(1GHz) | 4.9 | 4.9 |
(8)介质损耗角正切(1GHz) | 0.014 | 0.014 |
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- 2007-09-10 KR KR1020097006405A patent/KR101398731B1/ko active IP Right Grant
- 2007-09-10 WO PCT/JP2007/067596 patent/WO2008041453A1/ja active Application Filing
- 2007-09-10 SG SG2011088424A patent/SG177151A1/en unknown
- 2007-09-10 CN CN2011104448761A patent/CN102558505A/zh active Pending
- 2007-09-10 CN CN2007800362848A patent/CN101522752B/zh active Active
- 2007-09-28 TW TW96136368A patent/TWI434872B/zh active
-
2009
- 2009-11-27 HK HK09111078.3A patent/HK1131176A1/xx unknown
-
2017
- 2017-02-09 US US15/428,734 patent/US20170156207A1/en not_active Abandoned
Non-Patent Citations (3)
Title |
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JP平1-221413A 1989.09.04 |
JP昭57-028129A 1982.02.15 |
JP昭60-210685A 1985.10.23 |
Also Published As
Publication number | Publication date |
---|---|
KR101398731B1 (ko) | 2014-05-27 |
WO2008041453A1 (fr) | 2008-04-10 |
TW200837094A (en) | 2008-09-16 |
CN101522752A (zh) | 2009-09-02 |
CN102558505A (zh) | 2012-07-11 |
US20100143728A1 (en) | 2010-06-10 |
HK1131176A1 (en) | 2010-01-15 |
SG177151A1 (en) | 2012-01-30 |
US20170156207A1 (en) | 2017-06-01 |
KR20090074171A (ko) | 2009-07-06 |
TWI434872B (zh) | 2014-04-21 |
US9603244B2 (en) | 2017-03-21 |
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