KR850007367A - 과립의 제조방법 및 이의 장치 - Google Patents

과립의 제조방법 및 이의 장치 Download PDF

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Publication number
KR850007367A
KR850007367A KR1019850002309A KR850002309A KR850007367A KR 850007367 A KR850007367 A KR 850007367A KR 1019850002309 A KR1019850002309 A KR 1019850002309A KR 850002309 A KR850002309 A KR 850002309A KR 850007367 A KR850007367 A KR 850007367A
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fluidized bed
granules
classifier
countercurrent
zigzag
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KR1019850002309A
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KR920002748B1 (ko
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울레만 한스 (외 4)
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요아힘 그렘, 하인즈-게르트 뮐러
바이엘 아크티엔게젤샤프트
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Priority claimed from DE19843413200 external-priority patent/DE3413200A1/de
Priority claimed from DE19853507376 external-priority patent/DE3507376A1/de
Application filed by 요아힘 그렘, 하인즈-게르트 뮐러, 바이엘 아크티엔게젤샤프트 filed Critical 요아힘 그렘, 하인즈-게르트 뮐러
Publication of KR850007367A publication Critical patent/KR850007367A/ko
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/006—Separating solid material from the gas/liquid stream by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00539—Pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00761—Discharging
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S118/00—Coating apparatus
    • Y10S118/05—Fluidized bed

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Glanulating (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

내용 없음

Description

과립의 제조방법 및 이의 장치
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제 1도는 마멸을 고려하지 않고 과립성장과 핵형성간의 상호작용을 설명하기 위한 도해. 제 2도는 마멸을 고려하여 과립성장과 핵형성간의 상호작용을 설명하기 위한 도해. 제 3도는 미세재료의 내부반송을 나타내는 실시양태에서 본 발명에 따르는 전체 장치를 나타내는 개략도.

Claims (12)

  1. 과립화되는 제품을 액체형태로 유동층에 분무하고, 유동층에서 빠져나오는 배출가스중의 미세재료를 분리하여 과립을 형성하기 위한 핵으로서 유동층으로 반송하고, 유동층에서의 과립화공정은 분류가스로 크기를 미리 정한 과립이 형성되도록 분류가스류를 조정하는 것만으로 영향을 받게 하고, 완성된 과립은 유동층장치의 유출저에 끼워 넣어져 있는 하나 또는 몇개의 향류 비중분류기만으로 제거하며, 경우에 따라, 이렇게 수득한 과립에 열후처리를 행함을 특징으로하는 입자크기의 분포가 좁은 과립을 연속적으로 제조하는 방법.
  2. 제1항에 있어서, 과립화되는 제품이 하나 그 이상의 활성 성분을 함유하는 액체인 제조방법.
  3. 제2항에 있어서, 사용하는 활성성분이 농화학적으로 활성인 물질, 가정과 위생지역에서 해충을 박멸하기 위한 활성물질, 약리학적으로 활성인 물질, 영양소, 감미제, 염료 및 유기화합물 및/또는 무기화합물인 제조방법.
  4. 제1항에 있어서, 유동층에서 빠져나오는 미세재료를 사이클론 또는 분진여과기로 연속적으로 흡수하여 유동층으로 반송하거나, 또는 유동층위에 설치되어 있는 분진여과기로 미세재료를 내부로 반송하는 제조방법.
  5. 제1항에 있어서, 빗처럼 서로 연결되어 있으며, 단면이 지그재그형이고, 분류기의 축에 대하여 수직으로 미끄럼 가능한 비아로 단면과 갭의 길이를 조절할 수 있는 하나 또는 몇 개의 지그재그형 분류기로 배출을 행하는 제조방법.
  6. 제1항에 있어서, 몇개의 6각형 조각으로 나누어져 있고, 중심을 향하여 기울어져 있으며, 배출시 원형갭의 형태로 각각의 노즐을 둘러싸는 향류비중분류기 뿐만 아니라 노즐을 포함하는 유출저를 통하여 완성된 과립을 배출하는 제조방법.
  7. 분무 가능한 형태로 공급되는 제품을 분산시키기 위한 장치가 있고, 유동층에서 빠져나오는 미세재료를 반송하기에 적합한 시스템이 있으며, 하나 또는 몇 개의 향류비중 분류기가 이의 유출저에 부착되어 있는 유동층 반응기로 이루어짐을 특징으로 하는, 입자크기의 분포가 좁은 과립을 연속적으로 제조하기 위한 장치.
  8. 제 7항에 있어서, 사용하는 향류비중분류기가 지그재그형 분류기인 장치.
  9. 제 7항에 있어서, 사용하는 향류비중분류기가 빗처럼 서로 연결되어 있으며, 단면이 지그재그형이고, 분류기의 축에 대하여 수직으로 미끄럼 가능한 바아로 단면과 갭의 길이를 조절할 수 있는 지그재그형 분류기인 장치.
  10. 제 7항에 있어서, 과립화되는 제품을 2상재료노즐로 공급하고, 조자중에 노즐을 교환할 경우 외부의 공기가 과립제조기 안으로 침투하지 않고 제품이 과립제조기 밖으로 빠져나가지 않도록 미립화가스를 공급하는 장치.
  11. 제 7항에 있어서, 유출저가 몇 개의 6각형조각으로 나누어져 있고, 중심을 향하여 기울어져 있으며, 배출시 원형갭의 형태로 각각의 노즐을 둘러싸는 향류비중분류기 뿐만 아니라 노즐을 포함하는 장치.
  12. 활성성분 한가지 이상을 1내지 100중량%, 불활성 충진제 재료를 0내지 99중량% 분산제 및/또는 결합제를 0내지 40중량%, 및 임의로 첨가제를 함유하며, 평균입자크기가 0.1 내지이 3mm고최대, 입자의 직경과 최소입자의 직경이 평균입자크기의 1/2이내로 다르며, 형태가 균일하고 균질하게 구성되며, 조밀한 미공상 구조물이며, 물이나 기타의 용매에 자발적으로 분산될 수 있거나 용해될 수 있는 것을 특징으로 한 제 1항에 따르는 제조방법으로 수득할 수 있는 과립.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019850002309A 1984-04-07 1985-04-06 과립의 제조방법 및 이의 장치 KR920002748B1 (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DEP3413200.7 1984-04-07
DE19843413200 DE3413200A1 (de) 1984-04-07 1984-04-07 Vorrichtung zur herstellung von koernigem gut mit einstellbarer korngroesse aus fluessigen ausgangsprodukten
DE19853507376 DE3507376A1 (de) 1985-03-02 1985-03-02 Verfahren und vorrichtung zur herstellung von granulaten
DEP3507376.4 1985-03-02

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KR850007367A true KR850007367A (ko) 1985-12-04
KR920002748B1 KR920002748B1 (ko) 1992-04-02

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US (1) US4946654A (ko)
EP (1) EP0163836B1 (ko)
JP (1) JPH0817933B2 (ko)
KR (1) KR920002748B1 (ko)
AU (1) AU571959B2 (ko)
BR (1) BR8501554A (ko)
CA (1) CA1257534A (ko)
DE (1) DE3565475D1 (ko)
DK (1) DK159478C (ko)
ES (1) ES541983A0 (ko)
IL (1) IL74820A (ko)

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