JP2021526151A - 透明な洗浄組成物 - Google Patents
透明な洗浄組成物 Download PDFInfo
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- JP2021526151A JP2021526151A JP2020567228A JP2020567228A JP2021526151A JP 2021526151 A JP2021526151 A JP 2021526151A JP 2020567228 A JP2020567228 A JP 2020567228A JP 2020567228 A JP2020567228 A JP 2020567228A JP 2021526151 A JP2021526151 A JP 2021526151A
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- 239000003380 propellant Substances 0.000 description 1
- WHMDPDGBKYUEMW-UHFFFAOYSA-N pyridine-2-thiol Chemical class SC1=CC=CC=N1 WHMDPDGBKYUEMW-UHFFFAOYSA-N 0.000 description 1
- FGVVTMRZYROCTH-UHFFFAOYSA-N pyridine-2-thiol N-oxide Chemical compound [O-][N+]1=CC=CC=C1S FGVVTMRZYROCTH-UHFFFAOYSA-N 0.000 description 1
- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 description 1
- 229960002026 pyrithione Drugs 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- ARIWANIATODDMH-UHFFFAOYSA-N rac-1-monolauroylglycerol Chemical compound CCCCCCCCCCCC(=O)OCC(O)CO ARIWANIATODDMH-UHFFFAOYSA-N 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 description 1
- 229960003656 ricinoleic acid Drugs 0.000 description 1
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000010979 ruby Substances 0.000 description 1
- 229910001750 ruby Inorganic materials 0.000 description 1
- 229940071089 sarcosinate Drugs 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- VIDTVPHHDGRGAF-UHFFFAOYSA-N selenium sulfide Chemical compound [Se]=S VIDTVPHHDGRGAF-UHFFFAOYSA-N 0.000 description 1
- 229960005265 selenium sulfide Drugs 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 230000021148 sequestering of metal ion Effects 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 231100000051 skin sensitiser Toxicity 0.000 description 1
- 238000001464 small-angle X-ray scattering data Methods 0.000 description 1
- WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 description 1
- 229910000342 sodium bisulfate Inorganic materials 0.000 description 1
- 229940079781 sodium cocoyl glutamate Drugs 0.000 description 1
- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical compound [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 description 1
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 1
- 229940045998 sodium isethionate Drugs 0.000 description 1
- 239000001540 sodium lactate Substances 0.000 description 1
- 229940005581 sodium lactate Drugs 0.000 description 1
- 235000011088 sodium lactate Nutrition 0.000 description 1
- 229940045944 sodium lauroyl glutamate Drugs 0.000 description 1
- 229940079862 sodium lauryl sarcosinate Drugs 0.000 description 1
- 229940075560 sodium lauryl sulfoacetate Drugs 0.000 description 1
- 229940048109 sodium methyl cocoyl taurate Drugs 0.000 description 1
- 229940077092 sodium myristoyl glutamate Drugs 0.000 description 1
- 229940045898 sodium stearoyl glutamate Drugs 0.000 description 1
- FCBUGCHAVCFTHW-NTISSMGPSA-N sodium;(2s)-2-(tetradecanoylamino)pentanedioic acid Chemical compound [Na].CCCCCCCCCCCCCC(=O)N[C@H](C(O)=O)CCC(O)=O FCBUGCHAVCFTHW-NTISSMGPSA-N 0.000 description 1
- KLIFRVSZGDONER-FERBBOLQSA-M sodium;(4s)-4-(hexadecanoylamino)-5-hydroxy-5-oxopentanoate Chemical compound [H+].[Na+].CCCCCCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC([O-])=O KLIFRVSZGDONER-FERBBOLQSA-M 0.000 description 1
- KDHFCTLPQJQDQI-BDQAORGHSA-M sodium;(4s)-4-amino-5-octadecanoyloxy-5-oxopentanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC(=O)OC(=O)[C@@H](N)CCC([O-])=O KDHFCTLPQJQDQI-BDQAORGHSA-M 0.000 description 1
- NTYZDAJPNNBYED-UHFFFAOYSA-M sodium;2-(2-dodecanoyloxypropanoyloxy)propanoate Chemical compound [Na+].CCCCCCCCCCCC(=O)OC(C)C(=O)OC(C)C([O-])=O NTYZDAJPNNBYED-UHFFFAOYSA-M 0.000 description 1
- CAVXVRQDZKMZDB-UHFFFAOYSA-M sodium;2-[dodecanoyl(methyl)amino]ethanesulfonate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CCS([O-])(=O)=O CAVXVRQDZKMZDB-UHFFFAOYSA-M 0.000 description 1
- ADWNFGORSPBALY-UHFFFAOYSA-M sodium;2-[dodecyl(methyl)amino]acetate Chemical compound [Na+].CCCCCCCCCCCCN(C)CC([O-])=O ADWNFGORSPBALY-UHFFFAOYSA-M 0.000 description 1
- IZWPGJFSBABFGL-GMFCBQQYSA-M sodium;2-[methyl-[(z)-octadec-9-enoyl]amino]ethanesulfonate Chemical compound [Na+].CCCCCCCC\C=C/CCCCCCCC(=O)N(C)CCS([O-])(=O)=O IZWPGJFSBABFGL-GMFCBQQYSA-M 0.000 description 1
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 description 1
- LADXKQRVAFSPTR-UHFFFAOYSA-M sodium;2-hydroxyethanesulfonate Chemical compound [Na+].OCCS([O-])(=O)=O LADXKQRVAFSPTR-UHFFFAOYSA-M 0.000 description 1
- IWMMSZLFZZPTJY-UHFFFAOYSA-M sodium;3-(dodecylamino)propane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCNCCCS([O-])(=O)=O IWMMSZLFZZPTJY-UHFFFAOYSA-M 0.000 description 1
- HWCHICTXVOMIIF-UHFFFAOYSA-M sodium;3-(dodecylamino)propanoate Chemical compound [Na+].CCCCCCCCCCCCNCCC([O-])=O HWCHICTXVOMIIF-UHFFFAOYSA-M 0.000 description 1
- DUXXGJTXFHUORE-UHFFFAOYSA-M sodium;4-tridecylbenzenesulfonate Chemical compound [Na+].CCCCCCCCCCCCCC1=CC=C(S([O-])(=O)=O)C=C1 DUXXGJTXFHUORE-UHFFFAOYSA-M 0.000 description 1
- HSFQBFMEWSTNOW-UHFFFAOYSA-N sodium;carbanide Chemical group [CH3-].[Na+] HSFQBFMEWSTNOW-UHFFFAOYSA-N 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 229940117986 sulfobetaine Drugs 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 230000000475 sunscreen effect Effects 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 238000004808 supercritical fluid chromatography Methods 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 229940104261 taurate Drugs 0.000 description 1
- RJSZFSOFYVMDIC-UHFFFAOYSA-N tert-butyl n,n-dimethylcarbamate Chemical compound CN(C)C(=O)OC(C)(C)C RJSZFSOFYVMDIC-UHFFFAOYSA-N 0.000 description 1
- 229940124597 therapeutic agent Drugs 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 229940048912 triethanolamine cocoyl glutamate Drugs 0.000 description 1
- HTJNEBVCZXHBNJ-XCTPRCOBSA-H trimagnesium;(2r)-2-[(1s)-1,2-dihydroxyethyl]-3,4-dihydroxy-2h-furan-5-one;diphosphate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.OC[C@H](O)[C@H]1OC(=O)C(O)=C1O HTJNEBVCZXHBNJ-XCTPRCOBSA-H 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
- OBYIEPMKXIBQEV-UHFFFAOYSA-N undecyl hydrogen sulfate Chemical compound CCCCCCCCCCCOS(O)(=O)=O OBYIEPMKXIBQEV-UHFFFAOYSA-N 0.000 description 1
- 239000004034 viscosity adjusting agent Substances 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000010374 vitamin B1 Nutrition 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940011671 vitamin b6 Drugs 0.000 description 1
- 229940046008 vitamin d Drugs 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 229940118846 witch hazel Drugs 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
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Abstract
Description
洗浄組成物は、洗浄性界面活性剤と、水性キャリアと、離散粒子と、を含む。離散粒子は、(例えば、無水粒子を洗浄性界面活性剤及び水相に添加してシャンプー製品を形成するとき)水相の存在下で膨潤した無水粒子である。無水粒子は、脂肪両親媒性物質と、少なくとも1つの二次界面活性剤と、低レベルの水相と、を含む。無水粒子の形成中に使用される低レベルの水相は、無水粒子の約0重量%〜無水粒子の約30重量%である。シャンプー組成物は実質的に透明であってよく、75%以上、あるいは約75%〜約99%の透過率を有する。
洗浄組成物は、無水粒子及び水相を含む離散粒子を含む。無水粒子は、1種以上の脂肪両親媒性物質及び1種以上の二次界面活性剤を同時に融解させ、次いで、冷却して凝固させることによって調製される。このような無水粒子の粒径を制御するために、様々な方法を使用することができる。次いで、無水粒子を、洗浄性界面活性剤を含有する水相に添加する。その結果、当該粒子が膨張して、離散粒子に転換される。離散粒子は、ゲルネットワークであり得る。
無水粒子は、少なくとも1つの脂肪両親媒性物質を含む。本明細書で使用するとき、「脂肪両親媒性物質」は、疎水性尾部基と、化合物を水溶性にしない親水性頭部基とを有する化合物であって、洗浄組成物のpHにおいて正味の中性電荷も有する化合物を指す。
無水粒子はまた、1種以上の二次界面活性剤を含んでいてもよい。脂肪両親媒性物質と組み合わされて無水粒子を形成するこの二次界面活性剤を同時に融解させ、混合し、次いで、冷却して、無水粒子を生成する。無水粒子を調製するために使用される二次界面活性剤は、洗浄組成物の洗浄性界面活性剤成分から分離され、当該成分に加えられる。しかし、この二次界面活性剤は、上記の洗浄性界面活性剤成分のために選択されるものと同一又は異なる種類の界面活性剤(単数又は複数)であってよい。
無水粒子は、無水粒子の約0重量%〜約30重量%、あるいは約1重量%〜約20重量%、あるいは約0重量%〜約5重量%、あるいは約1重量%〜約10重量%の水又は好適な溶媒を更に含んでいてもよい。本明細書で使用するとき、用語「好適な溶媒」とは、水の代わりに又は水と組み合わせて使用することができる任意の溶媒を指す。
次いで、離散粒子を洗浄組成物ベース(シャンプーベースなど)に添加する。シャンプーベースは、カチオン性付着ポリマー、界面活性剤、共界面活性剤、水性キャリア、及びシリコーンなどの追加成分を含み得る。
洗浄組成物は、カチオン性付着ポリマーを含んでいてよい。洗浄組成物中のカチオン性付着ポリマーの濃度は、洗浄組成物の約0.05重量%〜約5重量%、あるいは約0.075重量%〜約2.5重量%、あるいは約0.1重量%〜約1.0重量%、あるいは約0.5重量%〜約1.0重量%であってよい。
洗浄組成物は、洗浄ベース中に1種以上の洗浄性界面活性剤を含む。洗浄性界面活性剤の成分は、洗浄性能を提供するために洗浄組成物中に含まれる。洗浄性界面活性剤は、アニオン性洗浄性界面活性剤、双極イオン性又は両性洗浄性界面活性剤、あるいはこれらの組み合わせから選択されてよい。このような界面活性剤は、本明細書に記載される必須成分と物理的及び化学的に適合すべきである、又はさもなければ過度に製品の安定性、審美性、若しくは性能を損なうべきではない。n=1であるラウレス−n−硫酸ナトリウムが、本明細書において特に好適である(「SLE1S」)。SLE1Sは、より高いモルエトキシレート当量と比較したとき、特に、高レベルのコンディショニング活性物質を含有する洗浄組成物において、より効率的な泡立ち及び洗浄を可能にする。
共界面活性剤は、泡立ち体積の向上及び/又は起泡質感を変えるために、硫酸ウンデシル界面活性剤及び所望によりアニオン性界面活性剤と組み合わされる物質である。典型的には、これらの物質は、限定されないが、両性、双極性、カチオン性、及び非イオン性を含む構造の様々な群から選択され得る。それらは、典型的には1:20〜1:4の重量比、あるいは1:12〜1:7の重量比でアニオン性界面活性剤と共に使用される。
洗浄組成物は、水性キャリアを含んでいてもよい。典型的に、組成物は、注入可能な液体の形態である(周囲条件下で)。そのため組成物は、組成物の少なくとも約、あるいは約20重量%〜約95重量%、あるいは約60重量%〜約85重量%の濃度で水性キャリアを含む。水性キャリアは、水、又は水と有機溶媒との混和性混合物を含んでもよい。水性キャリアは、また、他の構成成分の微量成分として組成物中に別に付随的に組み込む場合を除き、最小限の有機溶媒を含むか、又は有意の濃度の有機溶媒を含まない水を含んでもよい。
洗浄組成物は、任意成分が本明細書に記載の成分と物理的及び化学的に適合性であるか、又はそうでなければ製品の安定性、審美性、若しくは性能を過度に損なわない限り、ヘアケア製品又はパーソナルケア製品で使用することが知られている1種以上の任意成分を更に含んでいてもよい。このような任意成分の個々の濃度は、組成物の約0.001重量%〜約10重量%の範囲であってもよい。
組成物は、分散粒子を含んでいてよい。有用な粒子は、元来、無機、合成又は半合成であってよい。存在する場合、分散粒子は、組成物の約0.025重量%〜約20重量%、あるいは約0.05重量%〜約10重量%、あるいは約0.1重量%〜約5重量%、あるいは約0.25重量%〜約3重量%、あるいは約0.5重量%〜約2重量%の量で組み込まれる。
約1000を超える分子量を有するポリアルキレングリコールが、本明細書において有用である。以下の一般式を有するものが有用である:
組成物はまた、離散粒子によってもたらされるコンディショニングに加えて、1種以上のコンディショニング剤を含んでいてもよい。コンディショニング剤としては、毛髪及び/又は皮膚に特別なコンディショニング効果を与えるために用いられる物質が挙げられる。組成物において有用なコンディショニング剤は、典型的には、乳化液体粒子を形成する水不溶性で水分散性の不揮発性液体を含む。本組成物で使用するのに好適なコンディショニング剤は、一般にシリコーン(例えば、シリコーンオイル、カチオン性シリコーン、シリコーンゴム、高屈折率シリコーン、及びシリコーン樹脂)、有機コンディショニングオイル(例えば、炭化水素油、ポリオレフィン、及び脂肪酸エステル)又はこれらの組み合わせとして特徴付けられるコンディショニング剤、あるいはさもなければ水性界面活性剤マトリックス中に液状の分散粒子を形成するコンディショニング剤である。
組成物はまた、フケ防止活性物質を含有していてもよい。フケ防止活性物質の好適な非限定的な例としては、ピリジンチオン塩、アゾール、硫化セレン、粒子状硫黄、角質溶解剤、ピロクトンオラミン、及びこれらの混合物が挙げられる。このようなフケ防止活性物質は、組成物の構成成分と物理的及び化学的に適合すべきであり、その他の点では、過度に製品の安定性、審美性、又は性能を損なうものであってはならない。
組成物は、保湿剤を含有し得る。本明細書における保湿剤は、多価アルコール、水溶性アルコキシル化非イオン性ポリマー、及びこれらの混合物からなる群から選択される。本明細書で用いられる場合、保湿剤は、組成物の約0.1重量%〜約20重量%、あるいは約0.5重量%〜約5重量%の量で存在してもよい。
組成物は、組成物中に非水溶性物質を分散した形態で懸濁させるか又は組成物の粘度を変化させるのに有効な濃度で、構造化剤又は懸濁化剤を更に含んでいてもよい。こうした濃度は、組成物の約0.02重量%〜約10重量%、あるいは約0.02重量%〜約5.0重量%、あるいは約0.02重量%〜約1.5重量%の範囲である。
組成物は、他の任意成分を含有していてもよい。任意成分は、分散ゲルネットワーク相に存在していてもよく、又は別個の成分として最終洗浄組成物に添加されてもよい。
毛髪基材
International Hair Importers & Products Inc.から供給され、白人由来のものである4グラム、8インチの未処理の毛束(すなわち、化学処理なし)。
毛束を、シンクの上に垂らし、事前に水で約30秒間濡らす。毛束は、続いて、人差し指と中指との間で挟まれ、これらの指の間を通って引かれて、余分な水分が除去される。0.4ccの洗浄組成物を、各毛束の前側に載せ、各ヘアピースの長さの端から端までジグザグに塗布する。洗浄組成物は、小さく硬めの櫛毛を有するプラスチック製のブラシであるGoody(登録商標)を使用して、約30秒間、それぞれの毛束にブラッシングで塗布する。その後、それぞれの毛束を約30秒間水で洗い流す。毛束は、続いて、人差し指と中指との間で挟まれ、これらの指の間を通って引かれて、余分な水分が除去される。次いで、毛束をひっくり返し、0.4ccの洗浄組成物を、各毛束の後側に載せ、各束の長さの端から端までジグザグに塗布する。その後、それぞれの毛束を約30秒間水で洗い流す。毛束は、続いて、人差し指と中指との間で挟まれ、これらの指の間を通って引かれて、余分な水分が除去される。次いで、毛束を風乾させる。毛束を予め濡らし、すすぐために使用した水は、典型的には、約100°Fの温度及び約1.5ガロン/分の圧力である。水は、典型的には、約7グレイン/ガロン〜約13グレイン/ガロンの硬度である。毛髪処理後、毛髪が乾燥するまで、毛束を80℃のホットボックス内に入れておく。
毛髪サンプルを20% RHの一定湿度のチャンバ内で一晩平衡化する。各サンプルごとに、0.1gの毛髪を20〜40mmのセグメントに切断してバイアル瓶に入れる(n=4)。まず、毛髪をヘキサンで穏やかに抽出して、外部のセチルアルコールを除去する。ヘキサン抽出は、毛髪をヘキサンで2回抽出し、次いで、第2の溶媒(超臨界流体クロマトグラフィー質量分析(SFC−MSMS)については移動相)及びガスクロマトグラフィー(GC)についてはN,O−ビス(トリメチルシリルトリフルオロアセトアミド(BSTFA)誘導体化試薬)中で、乾燥した残渣を濃縮することからなる。次に、2:1、次いで、1:1のクロロホルム:メタノールを用いて内部のセチルアルコールを抽出する。クロロホルムは、10mMジメチルヘキシルアミン(DMHA)及びメタノール1%ギ酸を含有する。各抽出物を、65℃で30分間毛髪と共に加熱し、次いで、合わせ、乾燥した残渣を第2の溶媒(SFCMS−MSについては移動相及びGCについてはBSTFA誘導体化試薬)に再溶解させる。水素移動相を有するポリジメチルシロキサンキャピラリーカラムを使用し、炎イオン化検出を備えるガスクロマトグラフィーによって、セチルアルコールを定量する。ノナデカン酸及びエイコサン酸を内部標準として使用する。
1個のビーズを、洗浄シャーシ(chassis)を収容する2.5mmのODキャピラリー(壁厚0.01mm)の張り出し端(flared end)に落下させ、キャピラリの首部に穏やかに押し込んで、確実に完全に沈める。この準備は、回収された各時点で用い、経時的に変化したときにビーズ自体のSAXSパターンを捕捉するために、サンプルビームにおいてビーズを含有するキャピラリの位置を中心にする。ビーズはキャピラリの本体よりもわずかに大きいが、キャピラリは開口端に向かうにつれ広がっており、この広がりにより、開口端のサイズはビーズが分析の全日にわたって定位置に保持されるものになっている。
離散粒子は、最終製品に組み込まれたならば十分に膨潤又は「水和」して、そのなかで、製品が消費者によりパッケージから分注された際に、当該粒子が、洗浄連続層とのブレンドを開始することが望ましい。図1は、粒子の水和を示す。図1は、無水粒子10及び離散粒子12を含む。結果として、時間並びに粒子及びシャーシの組成14の関数として、粒子構造内に異なる水和ドメインが生じる。異なるドメインは、以下のように記載される。
−非水和固体相16=顕著な水和をほとんど経験しておらず、その相の圧縮が、本明細書に記載のKawabata KES−FB3−Auto Compression試験法の50g力限度以上であり、無水粒子に最も近い、離散粒子の最小水和相。
−半水和ゲル相18=離散粒子が部分的に水和された相であり、経時的に水和し続け、かつその相の圧縮がKawabata KES−FB3−Auto Compression Tester及び以下に記載する対応する方法を使用して測定可能である相。
−水和ゲル相20=マイクロスケールで、分散したゲルネットワーク相に最も密接に類似している、離散粒子のほとんど水和している相。
ビーズが製品によって効果的にコーティングされるように、(例えば、約5グラムのシャンプーなどの洗浄組成物に約10個のビーズを組み込む比で)ビーズを最終製品に組み込むことによって、製品サンプルを調製する。抽出中にビーズが変形しないように注意しながら、小さなスパチュラを使用して、様々な時間間隔でこれらのビーズを1つずつ製品からサンプリングする。特定の時間スケールに限定されるものではないが、以下の時間間隔(時間):0、1、3、6、及び24時間でビーズの圧縮を行う。適切な設備較正及び測定設定の後、サンプル分析の準備として、ビーズを製品から慎重に抽出し、KS−FB3−A圧縮試験機のサンプル台の中心、圧縮プローブの真下に置く。
以下の実施例に示される組成物は、組成物の具体的な実施形態を説明したものであるが、これらに限定されない。当業者によって、本発明の趣旨及び範囲から逸脱することなく他の変更がなされ得る。本明細書に記載されている組成物のこれらの例示された実施形態は、毛髪への増強されたコンディショニング効果をもたらす。
(2)Croda Chemicalsから入手可能
(3)Emery Oleochemicalsから入手可能
(4)Clariant Int.Ltd.から入手可能
(5)P&G Chemicalsから入手可能
(6)Stepan Companyから入手可能
(7)Genamin(登録商標)BTMS(Clariant)
(8)Incromine(商標)SD(Croda)
(9)PRESTIGE Ruby(Sudarshan Chemical)
(10)二酸化チタン(Kobo)
(11)Jordapon Ci Prilled(BASF)
(12)Sigma Aldrichから入手可能
(13)Cf330m(Momentive Performance Materials)
(14)Belsil(登録商標)DM 5500 E(Wacker)
(15)Dow Corning 1872(Dow Corning Corporation)
(16)Mirapol 100S(Solvay USA Inc.)
(17)DLパンテノール(DSM Nutritional Products Inc)
(18)D/DIパンテニルエチルエーテル(DSM Nutritional Products Inc)
(19)アルガニアスピノサ(Argania Spinosa)核油(BASF Corporation)
(20)ココナッツミルク5432472(IFF)
(21)LAEVO MENTHOL(Symrise)
(22)BASFから入手可能
洗浄性界面活性剤及び最終洗浄組成物の他の成分と共に組み込む前の離散粒子の実施例。
(2)カチオン性ガラクトマンナン(分子量−200,000、電荷密度=3.0meq/g)
(3)カチオン性ガラクトマンナン(分子量−200,000、電荷密度=0.7meq/g)
(4)Jaguar C17(Rhodia)
(5)ADPP−5043H1VPW(分子量−1,200,000及び電荷密度2.0meq/g)、Aqualon/Herculesから入手可能
(6)Polymer LR30M(Dow Chemical Company)
(7)Mirapol 100S(Solvay USA Inc.)
(8)Cf330m(Momentive Performance Materials)
(9)Belsil(登録商標)DM 5500 E(Wacker)
(10)Dow Corning 1872(Dow Corning Corporation)
(11)トリヒドロキシステアリン−PrimG(Elementis Specialties Inc.)
(12)Carbopol Aqua SF 1(Lubrizol Advanced Materials)
(13)Jaguar Excel(Solvay)
(14)Polymer KG30M(Dow Chemical Company)
(15)Carbopol Aqua SF 2(Lubrizol Advanced Materials)
Claims (10)
- 洗浄組成物であって、
(a)洗浄性界面活性剤と、
(b)水性キャリアと、
(c)前記洗浄組成物の約0.5重量%〜約30重量%の、無水粒子及び水相を含む離散粒子と、
を含み、
前記無水粒子が、
(1)脂肪アルコール、脂肪酸エステル、脂肪酸、脂肪族アミド、及びこれらの混合物からなる群から選択される1種以上の脂肪両親媒性物質、
(2)アニオン性界面活性剤、非イオン性界面活性剤、双性イオン性界面活性剤、カチオン性界面活性剤、又はこれらの混合物からなる群から選択される1種以上の二次界面活性剤、を含み、
前記離散粒子が、約200マイクロメートル〜約15000マイクロメートルのサイズを有し、前記洗浄組成物が、約75%以上の透過率%を有する、洗浄組成物。 - 前記脂肪両親媒性物質が、前記洗浄組成物の約0.25重量%〜約15重量%である、請求項1に記載の洗浄組成物。
- 前記離散粒子が、約500マイクロメートル〜約7000マイクロメートルである、請求項1に記載の洗浄組成物。
- 前記無水粒子が、約0.2マイクロメートル〜約200マイクロメートルのサイズスケールを有する、請求項1に記載の組成物。
- 前記無水粒子が、約200マイクロメートル〜約0.5mmのサイズスケールを有する、請求項1に記載の組成物。
- 前記無水粒子が、約0.5mm〜約20mmのサイズスケールを有する、請求項1に記載の組成物。
- 前記無水粒子が、約1mm〜約10mmのサイズスケールを有する、請求項1に記載の組成物。
- 前記離散粒子が半水和ゲル相中に存在し、KES−FB3−A Compression Testerを使用して測定したときに約0.5グラム重量単位〜約50グラム重量単位の圧縮を有する、請求項1に記載の組成物。
- 前記離散粒子が、約0.3mm未満のスケールサイズを有する非水和固相中に存在する、請求項1に記載の組成物。
- 前記非水和固相が、KES−FB3−A Compression Testerを使用して測定したときに約50グラム重量単位を超える圧縮を有する、請求項9に記載の組成物。
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JP7274507B2 (ja) | 2023-05-16 |
CN112261931B (zh) | 2023-12-08 |
WO2019236646A1 (en) | 2019-12-12 |
JP2023087001A (ja) | 2023-06-22 |
US11628126B2 (en) | 2023-04-18 |
US20190365611A1 (en) | 2019-12-05 |
CN112261931A (zh) | 2021-01-22 |
MX2020013252A (es) | 2021-02-22 |
US20230210730A1 (en) | 2023-07-06 |
CN117562814A (zh) | 2024-02-20 |
EP3801443A1 (en) | 2021-04-14 |
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