JP2015134906A - 粘着剤組成物、粘着剤層、粘着テープ、及び、両面粘着テープ - Google Patents
粘着剤組成物、粘着剤層、粘着テープ、及び、両面粘着テープ Download PDFInfo
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- JP2015134906A JP2015134906A JP2014247970A JP2014247970A JP2015134906A JP 2015134906 A JP2015134906 A JP 2015134906A JP 2014247970 A JP2014247970 A JP 2014247970A JP 2014247970 A JP2014247970 A JP 2014247970A JP 2015134906 A JP2015134906 A JP 2015134906A
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- Prior art keywords
- polyester
- sensitive adhesive
- pressure
- adhesive layer
- tackifier
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
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Abstract
【解決手段】本発明のポリエステル系粘着剤組成物は、ポリエステル、耐加水分解剤、粘着付与剤、及び、架橋剤を含有するポリエステル系粘着剤組成物であって、前記粘着付与剤の酸価が、8以下であり、前記粘着付与剤の軟化点が、80〜170℃であり、前記ポリエステル100重量部に対して、前記粘着付与剤を20〜100重量部含有することを特徴とする。
【選択図】なし
Description
本発明に用いられるポリエステルとしては、少なくとも、ジカルボン酸成分と、ジオール成分とを重縮合して得られるポリエステルが用いられることが好ましい。なお、ポリエステルの合成方法としては、特に限定されるものではなく、公知の重合方法を用いることができる。
粘着剤層のバイオマス度(重量%)=100×[植物由来の原料の重量(g)]/[粘着剤層の総重量(g)]
本発明の粘着剤組成物は、前記ポリエステルと共に、架橋剤を含有するものであり、前記架橋剤を用いて粘着剤組成物を架橋反応させることにより、粘着剤層を形成することができる。前記架橋剤として、特に限定されるものではなく、従来公知のものを使用することができ、例えば、多価イソシアヌレート、多官能性イソシアネート化合物、多官能性メラミン化合物、多官能性エポキシ化合物、多官能性オキサゾリン化合物、多官能性アジリジン化合物、金属キレート化合物などを用いることができ、特に汎用性という観点から、多価イソシアヌレートや多官能性イソシアネート化合物を用いることが好ましい態様である。これらは、1種または2種以上を組み合わせて使用できる。
また、本発明の粘着剤組成物は、前記ポリエステルと共に、粘着付与剤を含有するものであり、前記粘着付与剤を含有することにより、所望の特性を有する粘着剤層を得ることができ、特に粘着特性だけでなく、耐久性(加温加湿保存性)の向上(耐久性の悪化を抑制)が期待できる。
本発明の粘着剤組成物は、前記ポリエステルと共に、耐加水分解剤を含有するものであり、前記耐加水分解剤を含有することにより、所望の特性を有する粘着剤層を得ることができ、特に耐久性(加温加湿保存性)の向上が期待できる。
前記支持体としては、特に限定されず、従来公知のものを使用することができ、プラスチックフィルムや、紙、不織布などの多孔質材料など、各種の支持体(基材)を使用することができる。なお、耐久性等の観点から、プラスチックフィルムを用いることが好ましい態様である。前記プラスチックフィルムとしては、たとえば、ポリエチレン、ポリプロピレン、ポリ−1−ブテン、ポリ−4−メチル−1−ペンテン、エチレン・プロピレン共重合体、エチレン・1−ブテン共重合体、エチレン・酢酸ビニル共重合体、エチレン・エチルアクリリレート共重合体、エチレン・ビニルアルコール共重合体等のポリオレフィンフィルム、ポリエチレンテレフタレート、ポリエチレンナフタレート、ポリブチレンテレフタレート等のポリエステルフィルム、ポリアクリレートフィルム、ポリスチレンフィルム、また、ナイロン6、ナイロン6,6、部分芳香族ポリアミド等のポリアミドフィルム、ポリ塩化ビルフィルム、ポリ塩化ビニリデンフィルム、ポリカーボネートフィルム等を挙げることができる。また、植物由来の原料から得られるポリ乳酸やセルロースなどからなる支持体を好適に用いることができる。
本発明のポリエステル系粘着テープや両面粘着テープは、部材や部品の固定、ラベルの貼り合わせ、包装材、壁紙などの建材、化粧シートなど、汎用されるところで使用できる。
三つ口セパラブルフラスコに攪拌機、温度計、真空ポンプを付し、これにダイマー酸(商品名「プリポール1009」、分子量567、クローダ社製)97.8g、ダイマージオール(商品名「プリポール2033」、分子量537、クローダ社製)102.2g、触媒として酸化ジブチルスズ(関東化学社製)0.2gを仕込み、減圧雰囲気(2.0kPa以下)で撹拌しながら200℃まで昇温し、この温度を保持した。約5時間反応を続けてポリエステルを得た。重量平均分子量(Mw)は2.8万であった。
ポリエステル100部に、架橋剤としてヘキサメチレンジイソシアネート(商品名「TPA−100」、旭化成ケミカルズ社製)3.75部、粘着付与剤であるテルペンフェノール(商品名「YSポリスターS145」、ヤスハラケミカル社製)40部、耐加水分解剤としてカルボジイミド基含有化合物(商品名「カルボジライトV-03」、日清紡ケミカル社製)0.5部を配合し、固形分が60%になるようトルエンを加え、粘着剤組成物(粘着剤溶液)を調整した。これを乾燥後の厚みが30μmになるように剥離処理したポリエチレンテレフタレート(PET)フィルム(商品名「ダイアホイルMRF♯38」、三菱樹脂社製)の剥離処理面に塗工し、120℃で3分乾燥させ、粘着剤層を得た。その後、剥離処理したポリエチレンテレフタレート(PET)フィルム(商品名「ダイアホイルMRE♯38」、三菱樹脂社製)の剥離処理面に前記粘着剤層を貼り合わせて、さらに40℃3日間放置し、粘着テープを得た。
架橋剤を3.5部にし、粘着付与剤を20部にし、耐加水分解剤をカルボジイミド基含有化合物(商品名「カルボジライトV−07」)にした以外は、実施例1と同様にして粘着テープを得た。
架橋剤を4部にし、耐加水分解剤をカルボジイミド基含有化合物(商品名「カルボジライトV−07」、日清紡ケミカル社製)にした以外は、実施例1と同様にして粘着剤組成物を調整した。これを乾燥後の厚みが19μmになるように剥離処理したポリエチレンテレフタレート(PET)フィルム(商品名「ダイアホイルMRF♯38」、三菱樹脂社製)の剥離処理面に塗工し、120℃で3分乾燥させ、粘着剤層を得た。同様にもう一方の剥離処理したPETフィルム(商品名「ダイアホイルMRE♯38」、三菱樹脂社製)にも塗工し、2枚の粘着剤層を得た。この2枚の粘着剤層で、厚み12μmのPETフィルム(商品名「ルミラー12S10」パナック社製)を挟み、PET基材ありの粘着テープを得た(PET基材両面テープの構成)。
架橋剤を2.75部にし、粘着付与剤をテルペン樹脂(商品名「YSレジンPX1250」、ヤスハラケミカル社製)40部にした以外は、実施例2と同様にして粘着テープを得た。
粘着付与剤をテルペンフェノール(商品名「YSポリスターT145」、ヤスハラケミカル社製)20部とテルペン樹脂(商品名「YSレジンPX1250」、ヤスハラケミカル社製)20部にし、耐加水分解剤をカルボジイミド基含有化合物(商品名「カルボジライトV−03」、日清紡ケミカル社製)1部にした以外は、実施例4と同様にして粘着テープを得た。
架橋剤を3.5部にし、粘着付与剤をテルペンフェノール(商品名「YSポリスターS145」、ヤスハラケミカル社製)30部と水添テルペン樹脂(商品名「クリアロンP125」、ヤスハラケミカル社製)10部にした以外は、実施例1と同様にして粘着テープを得た。
架橋剤を3部にし、粘着付与剤を芳香族変性テルペン(商品名「YSレジンTO115」、ヤスハラケミカル社製)40部にした以外は、実施例2と同様にして粘着テープを得た。
架橋剤を4部にし、粘着付与剤をテルペンフェノール(商品名「YSポリスターS145」、ヤスハラケミカル社製)30部とロジンエステル(商品名「ペンセルD135」、荒川化学社製)10部にし、耐加水分解剤を0.1部にした以外は、実施例2と同様にして粘着テープを得た。
粘着付与剤をテルペンフェノール(商品名「YSポリスターS145」、ヤスハラケミカル社製)20部とロジンエステル(商品名「ペンセルD135」、荒川化学社製)20部にし、耐加水分解剤を0.5部にした以外は、実施例8と同様にして粘着テープを得た。
粘着付与剤をテルペンフェノール(商品名「YSポリスターS145」、ヤスハラケミカル社製)10部とロジンエステル(商品名「ペンセルD135」、荒川化学社製)30部にし、耐加水分解剤を2部にした以外は、実施例2と同様にして粘着テープを得た。
架橋剤を3.5部、粘着付与剤をロジンエステル(商品名「ペンセルD135」、荒川化学社製)にした以外は、実施例1と同様にして粘着テープを得た。
耐加水分解剤をカルボジイミド基含有化合物(商品名「カルボジライトV−07」、日清紡ケミカル社製)0.1部にした以外は、比較例1と同様にして粘着テープを得た。
耐加水分解剤を1部にした以外は、比較例2と同様にして粘着テープを得た。
粘着付与剤をロジンエステル(商品名「ペンセルD135」、荒川化学社製)にし、耐加水分解剤を添加しない以外は、実施例3と同様にして粘着テープを得た。
耐加水分解剤を添加しない以外は、実施例5と同様にして粘着テープを得た。
重量平均分子量(Mw)は、ポリマー(ポリエステル)をテトラヒドロフラン(THF)で溶解した溶液をゲル・パーミエイション・クロマトグラフィ(GPC)法を用い、標準ポリスチレンにより作成した検量線から、分子量を測定した。
装置名:東ソー社製、HLC−8220GPC
試験片濃度:0.1重量%(THF溶液)
試験片注入量:20μl
溶離液:THF
流速:0.300ml/min
測定(カラム)温度:40℃
カラム: 試験片カラム;TSKguardcolumn SuperHZ−L(1本)+TSKgel SuperHZM−M(2本)、リファレンスカラム;TSKgel
SuperH−RC(1本)、東ソー製
検出器:示差屈折計(RI)
粘着付与剤の軟化点は、JIS K5601に記載の環球法に準じて、測定した。
粘着付与剤の酸価は、JIS K0070に記載の方法に準じて、測定した。
得られた粘着テープから一方の剥離処理されたフィルムを剥離し、露出させた粘着面を厚さが25μmのポリエチレンテレフタレート(PET)フィルム(商品名「ルミラー25S10」、パナック社製)に貼り合わせて試験体を得た。前記試験体を幅20mmにカットし、もう一方の剥離処理されたフィルムを剥離し、露出させた粘着面をポリカーボネート板(商品名「PC1600」、タキロン社製)に貼り合わせて、試験片とし、対PC板接着力(N/20mm)を測定した。
なお、貼り合せの際の圧着は、2kgのローラーを1往復して行い、貼り合わせ30分後に引張圧縮試験機(装置名「TG−1kN」、ミネベア社製)にて、180°ピール接着力(粘着力)の測定を以下の条件下で行った。
引張り(剥離)速度:300mm/分
測定条件:温度:23±2℃、湿度:65±5%RH
得られた粘着テープから一方の剥離処理されたフィルムを剥離し、露出させた粘着面を厚さが25μmのポリエチレンテレフタレート(PET)フィルム(商品名「ルミラー25S10」、パナック社製)に貼り合わせて試験体を得た。前記試験体を幅10mm×長さ100mmにカットし、もう一方の剥離処理されたフィルムを剥離し、露出させた粘着面を幅25mm×長さ125mm×厚さ2mmのベークライト板に、幅方向および長さ方向をそれぞれ対応させて、ベークライト板の幅方向の中心部付近に、幅10mm×長さ20mmラップするように2kgのローラーで1往復して圧着して貼り合わせ、測定片とした。この測定片を用い、40℃の雰囲気下で30分放置した後、0.5kgの荷重を加えた状態で40℃の雰囲気下に1時間(60分)放置後の試験片のズレ長さ(mm/60分)を測定した。
得られた粘着テープから一方の剥離処理されたフィルムを剥離し、露出させた粘着面を厚さが25μmのポリエチレンテレフタレート(PET)フィルム(商品名「ルミラー25S10」、パナック社製)に貼り合わせて試験片を得た。前記試験片を幅20mmにカットし、もう一方の剥離処理されたフィルムを剥離し、露出させた粘着面をSUS304板に貼り合わせて、試験片とした。この試験片を85℃で85%RHの条件下に500時間放置し、剥がれや浮き、糊はみ出しやズレなどがないか観察した。
剥がれや浮き、糊はみ出しやズレがない場合:○
剥がれや浮き、糊はみ出しやズレがある場合:×
2 粘着剤層
3 支持体
10 両面粘着テープ(支持体なし)
10’ 両面粘着テープ(支持体あり)
10'' 粘着テープ(支持体あり)
Claims (9)
- ポリエステル、耐加水分解剤、粘着付与剤、及び、架橋剤を含有するポリエステル系粘着剤組成物であって、
前記粘着付与剤の酸価が、8以下であり、
前記粘着付与剤の軟化点が、80〜170℃であり、
前記ポリエステル100重量部に対して、前記粘着付与剤を20〜100重量部含有することを特徴とするポリエステル系粘着剤組成物。 - 前記耐加水分解剤が、カルボジイミド基含有化合物であり、
前記ポリエステル100重量部に対して、前記カルボジイミド基含有化合物を0.05〜5重量部含有することを特徴とする請求項1に記載のポリエステル系粘着剤組成物。 - 前記ポリエステルが、少なくとも、ジカルボン酸成分と、ジオール成分とを重縮合して得られることを特徴とする請求項1又は2に記載のポリエステル系粘着剤組成物。
- 前記粘着付与剤が、少なくとも1種のテルペン系樹脂を含有することを特徴とする請求項1〜3のいずれかに記載のポリエステル系粘着剤組成物。
- 請求項1〜4のいずれかに記載のポリエステル系粘着剤組成物により形成されるポリエステル系粘着剤層であって、
ポリカーボネート板に対する接着力が、7N/20mm以上であることを特徴とするポリエステル系粘着剤層。 - 40℃における保持力が、0.8mm/60分以下であることを特徴とする請求項5に記載のポリエステル系粘着剤層。
- 少なくとも片面に、剥離ライナーを有することを特徴とする請求項5又は6に記載のポリエステル系粘着剤層。
- 請求項5〜7のいずれかに記載のポリエステル系粘着剤層の少なくとも片面に、支持体を有することを特徴とするポリエステル系粘着テープ。
- 請求項5〜7のいずれかに記載のポリエステル系粘着剤層が、少なくとも2層あり、
前記ポリエステル系粘着剤層の少なくとも片面に、支持体を有することを特徴とするポリエステル系両面粘着テープ。
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
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JP2014247970A JP6687997B2 (ja) | 2013-12-20 | 2014-12-08 | 粘着剤組成物、粘着剤層、粘着テープ、及び、両面粘着テープ |
PCT/JP2014/083402 WO2015093526A1 (ja) | 2013-12-20 | 2014-12-17 | 粘着剤組成物、粘着剤層、粘着テープ、及び、両面粘着テープ |
KR1020217023973A KR102316685B1 (ko) | 2013-12-20 | 2014-12-17 | 점착제 조성물, 점착제층, 점착 테이프, 및 양면 점착 테이프 |
CN201480069454.2A CN105829482B (zh) | 2013-12-20 | 2014-12-17 | 粘合剂组合物、粘合剂层、粘合带以及双面粘合带 |
US15/103,574 US10087345B2 (en) | 2013-12-20 | 2014-12-17 | Pressure-sensitive adhesive composition, pressure-sensitive adhesive layer, pressure-sensitive adhesive tape, and double-coated pressure-sensitive adhesive tape |
KR1020167019184A KR20160102226A (ko) | 2013-12-20 | 2014-12-17 | 점착제 조성물, 점착제층, 점착 테이프, 및 양면 점착 테이프 |
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JP7299428B2 (ja) | 2021-02-26 | 2023-06-27 | 日東電工株式会社 | 粘着剤組成物および粘着シート |
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CN105829482B (zh) | 2021-06-08 |
JP6687997B2 (ja) | 2020-04-28 |
KR20160102226A (ko) | 2016-08-29 |
US20160312073A1 (en) | 2016-10-27 |
KR20210096322A (ko) | 2021-08-04 |
KR102316685B1 (ko) | 2021-10-22 |
WO2015093526A1 (ja) | 2015-06-25 |
US10087345B2 (en) | 2018-10-02 |
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