JP2007168184A - 樹脂被覆ステンレス鋼箔,容器及び2次電池 - Google Patents
樹脂被覆ステンレス鋼箔,容器及び2次電池 Download PDFInfo
- Publication number
- JP2007168184A JP2007168184A JP2005366763A JP2005366763A JP2007168184A JP 2007168184 A JP2007168184 A JP 2007168184A JP 2005366763 A JP2005366763 A JP 2005366763A JP 2005366763 A JP2005366763 A JP 2005366763A JP 2007168184 A JP2007168184 A JP 2007168184A
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- Prior art keywords
- resin
- stainless steel
- steel foil
- layer
- coated stainless
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Abstract
【解決手段】 ステンレス鋼箔の少なくとも一方の面に,2nm以上200nm以下のクロメート処理層を有し,該クロメート処理層の上に,極性を持つ官能基を含有するポリオレフィン系樹脂(A)層を少なくとも有することを特徴とする樹脂被覆ステンレス鋼箔,これを用いた容器,及び2次電池。
【選択図】 図1
Description
(1) ステンレス鋼箔の少なくとも一方の面に,2nm以上200nm以下のクロメート処理層を有し,該クロメート処理層の上に,極性を持つ官能基を含有するポリオレフィン系樹脂(A)層を少なくとも有することを特徴とする,樹脂被覆ステンレス鋼箔。
(2) 前記ステンレス鋼箔の一方の面に,2nm以上200nm以下のクロメート処理層を有し,該クロメート処理層の上に,極性を持つ官能基を含有するポリオレフィン系樹脂(A)層を少なくとも有すると共に,前記ステンレス鋼箔の他方の面に樹脂層を有することを特徴とする,(1)に記載の樹脂被覆ステンレス鋼箔。
(3) 前記ポリオレフィン系樹脂(A)中の前記極性を持つ官能基の含有量が0.0005〜5mmol/gであることを特徴とする,(1)又は(2)に記載の樹脂被覆ステンレス鋼箔。
(4) 前記ポリオレフィン系樹脂(A)中に,層状無機物(B)が0.01〜50質量%分散されることを特徴とする,(1)〜(3)のいずれかに記載の樹脂被覆ステンレス鋼箔。
(5) 前記層状無機物(B)の最長径が1μm以下であることを特徴とする,(4)に記載の樹脂被覆ステンレス鋼箔。
(6) 前記層状無機物(B)がモンモリロナイトであることを特徴とする,(4)又は(5)に記載の樹脂被覆ステンレス鋼箔。
(7) 前記クロメート処理層と前記ステンレス鋼箔との間に,ストライクめっき層を有することを特徴とする,(1)〜(6)のいずれかに記載の樹脂被覆ステンレス鋼箔。
(8) 前記ストライクめっきのめっき種がニッケルであることを特徴とする,(7)に記載の樹脂被覆ステンレス鋼箔。
(9) 前記ステンレス鋼箔の他方の面の樹脂層が,ポリオレフィン,ポリエステル,ポリアミド,及びポリイミドからなる群より選ばれる1種又は2種以上を主成分とする樹脂組成物からなる少なくとも1層の樹脂層であることを特徴とする,(2)に記載の樹脂被覆ステンレス鋼箔。
(10) 前記ステンレス鋼箔の他方の面の樹脂層が,極性基を含有するビニル重合体(C)でカプセル化したゴム状弾性体樹脂(D)が微細分散されたポリエステル系樹脂(E)からなる少なくとも1層の樹脂層であることを特徴とする,(2)又は(9)に記載の樹脂被覆ステンレス鋼箔。
(11) 前記ステンレス鋼箔の他方の面の樹脂層と前記ステンレス鋼箔との間に,下地処理層を有することを特徴とする,(2),(9)又は(10)に記載の樹脂被覆ステンレス鋼箔。
(12) 前記下地処理層が,クロメート処理層,化成処理層または接着剤層の1種又は2種以上であることを特徴とする,(11)に記載の樹脂被覆ステンレス鋼箔。
(13) (1)〜(12)のいずれかに記載の樹脂被覆ステンレス鋼箔を成形加工してなる容器。
(14) (13)に記載の容器を用いてなる2次電池。
(式1中,R1,R2は各々独立に炭素数1〜12のアルキル基または水素を示し,R3は炭素数1〜12のアルキル基,アリール基又は水素を示す)
(式2中,R4,R5は各々独立に炭素数1〜12のアルキル基若しくは水素を,R6は炭素数1〜12のアルキル基,フェニル基若しくは水素を示す。)
本実施例に使用するステンレス鋼箔は,50μm厚の新日本製鐵(株)製SUS316LブライトAを使用した。
実施例と同様にして,表3に示す組合せで比較例1〜5を作成した。比較例5のアルミ箔は厚さ100μmの純Al製の箔を使用した。
(a) 一次密着強度試験
実施例1〜16及び比較例1〜5の樹脂被覆金属箔を10mm×120mmに切り出し,被覆した表面側の樹脂層の密着強度をピール試験(23℃,180°ピール:JIS K6854−2と同形式,引張り速度20mm/min)で測定した。10N/cm以上の密着強度を有することが好ましい。
(b) 加工性評価試験
実施例1〜16及び比較例1〜5の樹脂被覆金属箔を,電池ケースとしてよく使用される形状である角筒形状に絞り加工した。角筒絞りのプレス加工は以下の条件にて実施した。ダイス142mm×142mmでコーナー部径4mm,ポンチ140mm×140mmでコーナー部径4mm,しわ押え力6トン,潤滑剤はJohnson WAX122とマシン油を1:1に混合したものを用い,プレス速度60mm/分で,ブランクサイズ200mm×200mmの供試材を,表面側をポンチ側にして,深さ5mmにプレス加工した。
プレス加工後の樹脂被覆金属箔の外観を以下のようにして評価して,加工性評価とした。角筒絞り加工の折り曲げ部位全域における被覆樹脂,及び被覆樹脂と金属箔との界面の亀裂や剥離を20倍ルーペで観察した。加工性評価結果は以下のようにした。◎:亀裂,剥離が認められない,○:亀裂が認められない,△:微細な亀裂が認められる,×:亀裂が認められる。ここで,○以上の評価を合格とした。
(c) 耐腐食性評価試験
(b)の加工性評価試験で得られた角筒を用いて,角筒内面(金属箔の表面)の電解液中での耐腐食性を以下のようにして評価した。角筒絞り加工済みの各金属箔の底面から試料片を10mm×120mmに切り出し,蓋を用いて密閉できるガラス製の瓶中で電解液に完全に浸漬して75℃で1週間保持した。その後,一次密着試験と同様にして,ピール試験で密着強度を測定し,20倍ルーペで樹脂剥離面を観察して腐食の有無を確認した。なお,電解液は,六フッ化リン酸リチウム(LiPF6)をエチレンカーボネートとジエチルカーボネートとを1:1に混合した溶媒で1mol/Lの濃度に希釈したものを用いた。
(d) 突き刺し強度試験
突き刺し強度は以下のようにして測定した。樹脂被覆金属箔を固定し,表面側に垂直に長さ50mm,直径0.5mm,先端半径0.15mmの針を突立てて荷重をかけ,針が貫通するまでの最大荷重を突き刺し強度とした。電池ケースとして要求される強度は1200g以上が好ましく,2000g以上がさらに好ましい。
Claims (14)
- ステンレス鋼箔の少なくとも一方の面に,2nm以上200nm以下のクロメート処理層を有し,該クロメート処理層の上に,極性を持つ官能基を含有するポリオレフィン系樹脂(A)層を少なくとも有することを特徴とする,樹脂被覆ステンレス鋼箔。
- 前記ステンレス鋼箔の一方の面に,2nm以上200nm以下のクロメート処理層を有し,該クロメート処理層の上に,極性を持つ官能基を含有するポリオレフィン系樹脂(A)層を少なくとも有すると共に,
前記ステンレス鋼箔の他方の面に樹脂層を有することを特徴とする,請求項1に記載の樹脂被覆ステンレス鋼箔。 - 前記ポリオレフィン系樹脂(A)中の前記極性を持つ官能基の含有量が0.0005〜5mmol/gであることを特徴とする,請求項1又は2に記載の樹脂被覆ステンレス鋼箔。
- 前記ポリオレフィン系樹脂(A)中に,層状無機物(B)が0.01〜50質量%分散されることを特徴とする,請求項1〜3のいずれかに記載の樹脂被覆ステンレス鋼箔。
- 前記層状無機物(B)の最長径が1μm以下であることを特徴とする,請求項4に記載の樹脂被覆ステンレス鋼箔。
- 前記層状無機物(B)がモンモリロナイトであることを特徴とする,請求項4又は5に記載の樹脂被覆ステンレス鋼箔。
- 前記クロメート処理層と前記ステンレス鋼箔との間に,ストライクめっき層を有することを特徴とする,請求項1〜6のいずれかに記載の樹脂被覆ステンレス鋼箔。
- 前記ストライクめっきのめっき種がニッケルであることを特徴とする,請求項7に記載の樹脂被覆ステンレス鋼箔。
- 前記ステンレス鋼箔の他方の面の樹脂層が,ポリオレフィン,ポリエステル,ポリアミド,及びポリイミドからなる群より選ばれる1種又は2種以上を主成分とする樹脂組成物からなる少なくとも1層の樹脂層であることを特徴とする,請求項2に記載の樹脂被覆ステンレス鋼箔。
- 前記ステンレス鋼箔の他方の面の樹脂層が,極性基を含有するビニル重合体(C)でカプセル化したゴム状弾性体樹脂(D)が微細分散されたポリエステル系樹脂(E)からなる少なくとも1層の樹脂層であることを特徴とする,請求項2又は9に記載の樹脂被覆ステンレス鋼箔。
- 前記ステンレス鋼箔の他方の面の樹脂層と前記ステンレス鋼箔との間に,下地処理層を有することを特徴とする,請求項2,9又は10に記載の樹脂被覆ステンレス鋼箔。
- 前記下地処理層が,クロメート処理層,化成処理層または接着剤層の1種又は2種以上であることを特徴とする,請求項11に記載の樹脂被覆ステンレス鋼箔。
- 請求項1〜12のいずれかに記載の樹脂被覆ステンレス鋼箔を成形加工してなる容器。
- 請求項13に記載の容器を用いてなる2次電池。
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CN2006800476971A CN101331020B (zh) | 2005-12-20 | 2006-07-28 | 树脂被覆不锈钢箔、容器及二次电池 |
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US12/086,830 US9719185B2 (en) | 2005-12-20 | 2006-07-28 | Resin-coated stainless steel foil, container and secondary battery |
CA2634108A CA2634108C (en) | 2005-12-20 | 2006-07-28 | Resin-coated stainless steel foil, container and secondary battery |
EP06782294.0A EP1964667B1 (en) | 2005-12-20 | 2006-07-28 | Resin-coated stainless steel foil, container and secondary battery |
PCT/JP2006/315434 WO2007072604A1 (ja) | 2005-12-20 | 2006-07-28 | 樹脂被覆ステンレス鋼箔、容器及び2次電池 |
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Also Published As
Publication number | Publication date |
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EP1964667B1 (en) | 2014-04-30 |
KR101024790B1 (ko) | 2011-03-24 |
TW200731604A (en) | 2007-08-16 |
EP1964667A1 (en) | 2008-09-03 |
WO2007072604A1 (ja) | 2007-06-28 |
TWI403014B (zh) | 2013-07-21 |
US9719185B2 (en) | 2017-08-01 |
JP5080738B2 (ja) | 2012-11-21 |
KR20080084978A (ko) | 2008-09-22 |
CA2634108A1 (en) | 2007-06-28 |
CA2634108C (en) | 2013-11-19 |
CN101331020B (zh) | 2012-09-12 |
CN101331020A (zh) | 2008-12-24 |
US20090029245A1 (en) | 2009-01-29 |
EP1964667A4 (en) | 2011-08-24 |
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