JP2005156840A - 樹脂シート、液晶セル基板、液晶表示装置、エレクトロルミネッセンス表示装置用基板、エレクトロルミネッセンス表示装置および太陽電池用基板 - Google Patents
樹脂シート、液晶セル基板、液晶表示装置、エレクトロルミネッセンス表示装置用基板、エレクトロルミネッセンス表示装置および太陽電池用基板 Download PDFInfo
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- JP2005156840A JP2005156840A JP2003394044A JP2003394044A JP2005156840A JP 2005156840 A JP2005156840 A JP 2005156840A JP 2003394044 A JP2003394044 A JP 2003394044A JP 2003394044 A JP2003394044 A JP 2003394044A JP 2005156840 A JP2005156840 A JP 2005156840A
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- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 description 2
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- VYKXQOYUCMREIS-UHFFFAOYSA-N methylhexahydrophthalic anhydride Chemical compound C1CCCC2C(=O)OC(=O)C21C VYKXQOYUCMREIS-UHFFFAOYSA-N 0.000 description 2
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Abstract
【解決手段】 ガラス繊維製布状体と無機粒子を樹脂中に含有してなる樹脂硬化層を備え、ヘイズ値が10%以下となるように構成されたことを特徴とする樹脂シートによる。
【選択図】 図1
Description
また、プラスチック基板は、機械的強度が比較的低いという問題も有している。
また、本発明に係る樹脂シートは、前記樹脂中に無機粒子を含有しているため、樹脂硬化層の熱による収縮・膨張をより一層効果的に防止することができ、しかも、樹脂を加熱して硬化させた後の冷却工程において、ガラス繊維製布状体と樹脂との線膨張係数の差によって凹凸が生じるのを防止することが可能となる。しかも、該樹脂シートは、ヘイズ値が10%以下となるように構成されているために透過光の拡散が少なく、極めて光透過性に優れた樹脂シートとなる。よって、例えば液晶セル基板やエレクトロルミネッセンス表示装置用基板として使用した場合、表示装置の表示品位が優れたものとなる。さらに、該樹脂シートを備えた太陽電池用基板は太陽電池の発電効率向上に寄与し得るものとなる。
そして、樹脂硬化層中において、斯かる粒子径の無機粒子を15〜60重量%とすることが好ましく、25〜50重量%とすることがより好ましい。無機粒子の添加量が15重量%よりも少ない場合には、樹脂硬化層の線膨張係数が低下し、前記ガラス繊維製布状体との収縮率差が大きくなり、硬化後の冷却工程において凹凸を生じ、表面平滑性に悪影響を及ぼすおそれがある。また、無機粒子の添加量が60重量%よりも多い場合には、樹脂硬化層を形成する際の樹脂の粘度が高くなり過ぎ、作業性が悪化するおそれがある。
添加剤としては、例えば、硬化剤、硬化促進剤、老化防止剤、変成剤、界面活性剤、染料、顔料、変色防止剤、紫外線吸収剤等が挙げられる。
また、前記変性剤としては、特に制限されないが、例えば、グリコール類、シリコーン類、アルコール類等の従来公知のものを使用することができる。
尚、屈折率は、アッベ屈折率測定機により、25℃、589nmの条件で測定することができる。
尚、線膨張係数は、被測定物について、JIS K 7197に規定されるTMA法によりTMA測定値を得て、これを下記式に代入することによって算出される。下記式において、ΔIs(T1)およびΔIs(T2)は、測定時の温度T1(℃)及びT2(℃)におけるTMA測定値(μm)をそれぞれ示し、L0は、室温23℃における被測定物の長さ(mm)を示す。
線膨張係数=[1/(L0×103)]・[(ΔIs(T2)-ΔIs(T1))/(T2-T1)]
尚、光透過率は、高速分光光度計を用いて波長550nmの全光線透過率を測定することによって求めることができる。
前記珪素窒化物としては、例えば、珪素原子数(Si)に対する窒素原子数(N)の割合(Si:N)が1:1〜3:4であるものが好ましい。
また、ガラス繊維製布状体に樹脂が含浸してなる樹脂硬化層は、常圧下において、ガラス繊維製布状体に液状の樹脂を含浸させた後、樹脂を硬化させることによっても形成することができる。
無機粒子は、前記ガラス繊維製布状体に樹脂を塗布する際、該樹脂中に例えばゾル−ゲル反応によって分散させておけばよい。
また、樹脂硬化層を構成する樹脂をガラス繊維製布状体に含浸させる際には、該樹脂を溶媒に分散または溶解して樹脂液を調製し、これを使用しても良い。
よって、例えば、視認側の偏光板の上に設ける光拡散板、アンチグレア層、反射防止膜、保護層、保護板、或いは液晶セルと視認側の偏光板の間に設ける補償用位相差板などの適宜な光学部品を前記樹脂シートに適宜組み合わせることができる。
無機粒子としてのシリカ粒子(平均粒子径15nm)がゾル−ゲル反応によって均一に分散された下記化学式(3)で示される3,4−エポキシシクロヘキシルメチル−3,4−エポキシシクロヘキサンカルボキシレート(商品名「NANOPOX XP22/0316」、hanse chemie社製)をエポキシ樹脂が24.6部(重量部、以下同じ)となる量だけ用い、さらに、下記化学式(4)で示されるジシクロペンタジエン型エポキシ樹脂(商品名「EXA−7320」(エポキシ当量259)、大日本インキ化学工業社製)6.9部、硬化剤としてメチルナジック酸無水物36.2部、硬化促進剤として下記化学式(5)で示されるテトラ−n−ブチルホスホニウムo,o−ジエチルホスホジチオエート0.72部を攪拌混合し、樹脂硬化層中におけるシリカ粒子の含有量が31.5重量%であるエポキシ樹脂液を調製した。
次に、下記化学式(6)で示されるウレタンアクリレート17重量%のトルエン溶液を、ダイよりステンレス製エンドレスベルトに走行速度0.3m/分で流延塗布し、風乾してトルエンを揮発させた後、UV硬化装置を用いて硬化させることにより、膜厚2μmのハードコート層を形成した。続いて、その上に、前記エポキシ樹脂液を含浸させたガラス繊維製布状体を貼り合わせ、加熱装置を用いて硬化させた。こうして、ハードコート層と樹脂硬化層とが積層された膜厚100μmの積層体を得た。尚、樹脂硬化層のうちガラス繊維製布状体を除く部位の屈折率を別途測定したところ1.516であり、ガラス繊維製布状体と、それを除く部位との屈折率差は0.003であった。
樹脂硬化層中におけるシリカ粒子の含有量を23重量%とする以外は、実施例1と同様にして樹脂シートを作製した。
シリカ粒子を添加しない点を除き、他は実施例1と同様にして樹脂シートを作製した。
ガラス繊維製布状体として、屈折率1.558、厚み100μmのガラスクロス(日東紡社製)を用いる以外は、実施例1と同様にして樹脂シートを作製した。樹脂硬化層において、ガラス繊維製布状体と、それを除く部位との屈折率差は0.042であった。
実施例および比較例の樹脂シートに関し、線膨張係数、屈曲性、光透過率、表面粗さの各項目について測定した。尚、各々の測定方法は、下記の通りとした。
しかしながら、比較例1の樹脂シートを用いた液晶表示装置は、樹脂シートの表面平滑性に起因すると思われる画質の低下が認められた。
また、比較例2の樹脂シートを用いた透過型液晶表示装置は、画面が白濁して表示装置としての機能を十分に果たしえないものであった。
2 ガラス繊維製布状体
3 無機粒子
4 ガスバリア層
5 ハードコート層
10 樹脂シート
Claims (14)
- ガラス繊維製布状体と無機粒子を樹脂中に含有してなる樹脂硬化層を備え、ヘイズ値が10%以下となるように構成されたことを特徴とする樹脂シート。
- 前記樹脂硬化層を構成する樹脂とガラス繊維製布状体との屈折率差が、0.01以下であることを特徴とする請求項1記載の樹脂シート。
- 前記無機粒子の添加量が、前記樹脂硬化層中において15〜60重量%であることを特徴とする請求項1又は2に記載の樹脂シート。
- 前記無機粒子がシリカ粒子であることを特徴とする請求項1〜3の何れかに記載の樹脂シート。
- 前記樹脂硬化層を構成する樹脂がエポキシ系樹脂であることを特徴とする請求項1〜4の何れかに記載の樹脂シート。
- 25〜160℃における線膨張係数が5.0×10-5/℃以下であることを特徴とする請求項1〜5の何れかに記載の樹脂シート。
- 光透過率が88%以上であることを特徴とする請求項1〜6の何れかに記載の樹脂シート。
- さらに、ガスバリア層が積層されてなることを特徴とする請求項1〜7の何れかに記載の樹脂シート。
- さらに、ハードコート層が積層されてなることを特徴とする請求項1〜8の何れかに記載の樹脂シート。
- 請求項1〜9の何れかに記載の樹脂シートを備えてなることを特徴とする液晶セル基板。
- 請求項10に記載の液晶セル基板を備えてなることを特徴とする液晶表示装置。
- 請求項1〜9の何れかに記載の樹脂シートを備えてなることを特徴とするエレクトロルミネッセンス表示装置用基板。
- 請求項12に記載のエレクトロルミネッセンス表示装置用基板を備えてなることを特徴とするエレクトロルミネッセンス表示装置。
- 請求項1〜9の何れかに記載の樹脂シートを備えてなることを特徴とする太陽電池用基板。
Priority Applications (5)
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JP2003394044A JP4241340B2 (ja) | 2003-11-25 | 2003-11-25 | 樹脂シート、液晶セル基板、液晶表示装置、エレクトロルミネッセンス表示装置用基板、エレクトロルミネッセンス表示装置および太陽電池用基板 |
KR1020067009553A KR20060097031A (ko) | 2003-11-25 | 2004-11-24 | 수지 시트, 액정셀 기판, 액정 표시 장치,일렉트로루미네선스 표시 장치용 기판,일렉트로루미네선스 표시 장치 및 태양 전지용 기판 |
PCT/JP2004/017416 WO2005052037A1 (ja) | 2003-11-25 | 2004-11-24 | 樹脂シート、液晶セル基板、液晶表示装置、エレクトロルミネッセンス表示装置用基板、エレクトロルミネッセンス表示装置および太陽電池用基板 |
CN2004800345961A CN1886447B (zh) | 2003-11-25 | 2004-11-24 | 树脂片材、液晶单元基板、液晶显示装置、电致发光显示装置用基板、电致发光显示装置以及太阳电池用基板 |
US10/580,714 US20070128376A1 (en) | 2003-11-25 | 2004-11-24 | Resin sheet, liquid crystal cell substrate, liquid crytal display device, substrate for an electroluminescence display device, electroluminescence display device, and substrate for a solar cell |
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JP2003394044A JP4241340B2 (ja) | 2003-11-25 | 2003-11-25 | 樹脂シート、液晶セル基板、液晶表示装置、エレクトロルミネッセンス表示装置用基板、エレクトロルミネッセンス表示装置および太陽電池用基板 |
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JP (1) | JP4241340B2 (ja) |
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JP2014116427A (ja) * | 2012-12-07 | 2014-06-26 | Fuji Electric Co Ltd | 太陽電池一体型膜材 |
US10396224B2 (en) | 2012-12-07 | 2019-08-27 | Chukoh Chemical Industries, Ltd. | Solar cell integrated film material |
JP2014208798A (ja) * | 2013-03-29 | 2014-11-06 | 日本化薬株式会社 | 硬化性樹脂組成物及びガラス繊維を含む硬化物 |
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CN1886447A (zh) | 2006-12-27 |
US20070128376A1 (en) | 2007-06-07 |
WO2005052037A1 (ja) | 2005-06-09 |
CN1886447B (zh) | 2011-04-27 |
KR20060097031A (ko) | 2006-09-13 |
JP4241340B2 (ja) | 2009-03-18 |
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