CN103281900A - 氟吡菌酰胺用于防治作物中的线虫以及提高产量的用途 - Google Patents
氟吡菌酰胺用于防治作物中的线虫以及提高产量的用途 Download PDFInfo
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Classifications
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- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01C—PLANTING; SOWING; FERTILISING
- A01C1/00—Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
- A01C1/06—Coating or dressing seed
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G7/00—Botany in general
- A01G7/06—Treatment of growing trees or plants, e.g. for preventing decay of wood, for tingeing flowers or wood, for prolonging the life of plants
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Environmental Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
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- Zoology (AREA)
- Agronomy & Crop Science (AREA)
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- Forests & Forestry (AREA)
- Biodiversity & Conservation Biology (AREA)
- Ecology (AREA)
- Toxicology (AREA)
- Botany (AREA)
- Soil Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pretreatment Of Seeds And Plants (AREA)
- Catching Or Destruction (AREA)
- Cultivation Of Plants (AREA)
Abstract
本发明通常涉及吡啶基乙基苯甲酰胺衍生物防治线虫的用途以及对于防治线虫和/或提高作物产量特别有效的方法。
Description
背景技术
本发明通常涉及N-{[3-氯-5-(三氟甲基)-2-吡啶基]乙基}-2,6-二氯苯甲酰胺(氟吡菌酰胺)和包含氟吡菌酰胺的组合物用于防治蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄中的线虫的用途,以及用于防治在由蔬菜(尤其是番茄和葫芦)、马铃薯、胡椒、胡萝卜、洋葱、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄、木本作物 - 梨果、木本作物 - 核果、木本作物 - 坚果、花组成的作物中的线虫和/或提高作物产量和用于提高产量特别有效的方法。
将氟吡菌酰胺定义为式(I)的化合物
以及其化合物的N-氧化物。
氟吡菌酰胺是具有渗透和经板(translaminar)特性的广谱杀真菌剂,其用于在大范围的不同作物中针对多种经济上重要的植物疾病进行叶面、滴灌、浇灌和种子处理施用。它在针对白粉菌类、灰霉和白霉类的预防性施用是十分有效的。它具有抵抗许多其它植物疾病的效能。氟吡菌酰胺已在孢子萌发、芽管伸长和菌丝体生长试验中显示出活性。在生物化学水平上,氟吡菌酰胺通过阻断琥珀酸脱氢酶呼吸链中的电子传递来抑制线粒体呼吸(复合物II-SDH抑制剂)。
在EP-A- 1 389 614和WO 2004/016088中描述了氟吡菌酰胺及其从公知并市售的化合物开始的生产方法。
吡啶基乙基苯甲酰胺衍生物的杀线虫活性的一般描述可发现于WO-A 2008/126922中。
线虫是微小的、蠕虫类的、适于水中生存的多细胞动物。线虫种的数目估计有五十万个。作为土壤动物区系的重要部分,线虫生活在称为孔的相互连接的通路形成的迷宫中,所述孔是由土壤作用而产生。它们在附在土壤颗粒上的水膜中移动。植物寄生性线虫中的大部分是根进食者,发现其与大部分植物相关。一些线虫是内寄生性的,在根、块茎、芽、种子等的组织内生活并进食。其它是外寄生性的,经植物壁外部进食。一只内寄生线虫可以杀死一株植物或降低其生产力。内寄生根进食者包括这样的经济上重要的害虫如根结线虫(根结线虫属(Meloidogyne)种)、肾状线虫(肾状线虫属(Rotylenchulus)种)、胞囊线虫(胞囊线虫属(Heterodera)种)和根腐线虫(根腐线虫属(Pratylenchus)种)。线虫的直接进食可以严重降低植物的营养和水分摄入。当种子萌发后线虫立即攻击幼苗的根时,它们对作物的生产力具有最大的影响。线虫进食还产生了开放性创伤,其为多种植物致病真菌和细菌提供了入口。相比于线虫进食的直接作用,这些微生物感染通常造成更严重的经济损害。
目前线虫防治基本关注于防止线虫攻击植物。一旦植物被寄生,要杀死线虫而又不破坏植物实际上是不可能的。因此,提供线虫防治化合物以及处理植物来预防或降低线虫损害的方法是有利的。
发明概述
本发明现在提供氟吡菌酰胺防治线虫侵袭选自蔬菜、番茄、葫芦、马铃薯、胡椒、胡萝卜、洋葱、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果、柑橘属水果、菠萝和香蕉、和葡萄、木本作物 - 梨果、木本作物 - 核果、木本作物 - 坚果、花的作物并提高产量的有利用途。
本发明现在提供氟吡菌酰胺防治线虫侵袭选自蔬菜、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果、木本作物 - 坚果、花的作物并提高产量的有利用途。
本发明现在提供氟吡菌酰胺防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、胡椒、胡萝卜、洋葱、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄、木本作物 - 梨果、木本作物 - 核果、木本作物 - 坚果、花的作物并提高产量的有利用途。
本发明现在提供氟吡菌酰胺防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄的作物并提高产量的有利用途。
本发明还涉及氟吡菌酰胺防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄的作物的用途,所述线虫选自以下属:滑刃线虫属(Aphelenchoides
spp.)、松材线虫属(Bursaphelenchus spp.)、茎线虫属(Ditylenchus spp.)、球异皮线虫属(Globodera spp.)、异皮线虫属(Heterodera spp.)、长针线虫属(Longidorus spp.)、根结线虫属(Meloidogyne
spp.)、短体线虫属(Pratylenchus spp.)、穿孔线虫属(Radopholus spp.)、毛刺线虫属(Trichodorus
spp.)、半穿刺线虫属(Tylenchulus spp.)、剑线虫属(Xiphinema spp.)、螺旋线虫属(Helicotylenchus
spp.)、矮化线虫属(Tylenchorhynchus spp.)、盾线虫属(Scutellonema spp.)、异毛刺线虫属(Paratrichodorus
spp.)、Meloinema spp.、拟滑刃线虫属(Paraphelenchus spp.)、垫刃线虫属(Aglenchus spp.)、刺线虫属(Belonolaimus
spp.)、珍珠线虫属(Nacobbus spp.)、肾状线虫属(Rotylenchulus spp.)、盘旋线虫属(Rotylenchus
spp.)、拟茎线虫属(Neotylenchus spp.)、异滑刃线虫属(Paraphelenchus spp.)、锥线虫属(Dolichodorus spp.)、纽带线虫属(Hoplolaimus
spp.)、克点胞囊线虫属(Punctodera spp.)、小环线虫属(Criconemella spp.)、五沟属(Quinisulcius
spp.)、鞘线虫属(Hemicycliophora spp.)、粒线虫属(Anguina spp.)、Subanguina
spp.、半轮线虫属(Hemicriconemoides spp.)、平滑线虫属(Psilenchus spp.)、Pseudohalenchus
spp.、轮线虫属(Criconemoides spp.)、坏死线虫属(Cacopaurus spp.)。
本发明还涉及氟吡菌酰胺防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、胡椒、胡萝卜、洋葱、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄、木本作物 - 梨果、木本作物 - 核果、木本作物 - 坚果、花的作物并提高产量的用途,所述线虫选自以下属:滑刃线虫属(Aphelenchoides
spp.)、松材线虫属(Bursaphelenchus spp.)、茎线虫属(Ditylenchus spp. )、球异皮线虫属(Globodera spp. )、异皮线虫属(Heterodera spp.)、长针线虫属(Longidorus spp.)、根结线虫属(Meloidogyne
spp.)、短体线虫属(Pratylenchus spp.)、穿孔线虫属(Radopholus spp.)、毛刺线虫属(Trichodorus
spp.)、半穿刺线虫属(Tylenchulus spp.)、剑线虫属(Xiphinema spp.)、螺旋线虫属(Helicotylenchus
spp.)、矮化线虫属(Tylenchorhynchus spp.)、盾线虫属(Scutellonema spp.)、异毛刺线虫属(Paratrichodorus
spp.)、Meloinema spp.、拟滑刃线虫属(Paraphelenchus spp.)、垫刃线虫属(Aglenchus spp.)、刺线虫属(Belonolaimus
spp.)、珍珠线虫属(Nacobbus spp.)、肾状线虫属(Rotylenchulus spp.)、盘旋线虫属(Rotylenchus
spp.)、拟茎线虫属(Neotylenchus spp.)、异滑刃线虫属(Paraphelenchus spp.)、锥线虫属(Dolichodorus spp.)、纽带线虫属(Hoplolaimus
spp.)、克点胞囊线虫属(Punctodera spp.)、小环线虫属(Criconemella spp.)、五沟属(Quinisulcius
spp.)、鞘线虫属(Hemicycliophora spp.)、粒线虫属(Anguina spp.)、Subanguina
spp.、半轮线虫属(Hemicriconemoides spp.)、平滑线虫属(Psilenchus spp.)、Pseudohalenchus
spp.、轮线虫属(Criconemoides spp.)、坏死线虫属(Cacopaurus spp.)。
本发明还涉及氟吡菌酰胺防治线虫种的用途,所述线虫种选自:居农野外垫刃线虫(Aglenchus
agricola)、小麦粒线虫(Anguina tritici)、花生滑刃线虫(Aphelenchoides arachidis)、草莓滑刃线虫(Aphelenchoidesfragariae)、Belonolaimusgracilis、长尾刺线虫(Belonolaimuslongicaudatus)、Belonolaimusnortoni、Cacopauruspestis、弯曲小环线虫(Criconemellacurvata)、Criconemella onoensis、装饰小环线虫(Criconemella
ornata)、Criconemella rusium、薄叶小环线虫(Criconemella xenoplax=环腐线虫(Mesocriconema xenoplax))和通常的小环线虫属、Criconemoides
ferniae、Criconemoides onoense、Criconemoides ornatum和通常的轮线虫属、马铃薯茎线虫(Ditylenchus
destructor)、鳞球茎茎线虫(Ditylenchus dipsaci)、食菌茎线虫(Ditylenchus myceliophagus)和通常的茎线虫属、Dolichodorus heterocephalus、马铃薯白线虫(Globodera pallida=马铃薯白线虫(Heterodera
pallida))、Globodera rostochiensis、Globodera solanacearum、烟草胞囊线虫(Globodera
tabacum)、Globodera virginiae、双角螺旋线虫(Helicotylenchus digonicus)、双宫螺旋线虫(Helicotylenchus dihystera)、Helicotylenchus erythrine、多带螺旋线虫(Helicotylenchus multicinctus)、Helicotylenchus nannus、假强壮螺旋线虫(Helicotylenchus
pseudorobustus)和通常的螺旋线虫属、加利福尼亚半轮线虫(Hemicriconemoides)、裸鞘线虫(Hemicycliophoraarenaria)、Hemicycliophoranudata、Hemicycliophoraparvana、燕麦胞囊线虫(Heteroderaavenae)、十字花科胞囊线虫(Heteroderacruciferae)、大豆胞囊线虫(Heteroderaglycines)、水稻胞囊线虫(Heteroderaoryzae)、甜菜胞囊线虫(Heteroderaschachtii)、玉米胞囊线虫(Heteroderazeae)和通常的胞囊线虫属、Hoplolaimus
aegyptii、Hoplolaimuscalifornicus、哥伦布纽带线虫(Hoplolaimuscolumbus)、盔形纽带线虫(Hoplolaimusgaleatus)、印度纽带线虫(Hoplolaimusindicus)、Hoplolaimusmagnistylus、拟强壮纽带线虫(Hoplolaimuspararobustus)、Longidorusafricanus、Longidorusbreviannulatus、横带长针线虫(Longidoruselongatus)、Longidoruslaevicapitatus、Longidorusvineacola和通常的长针线虫属、高粱根结线虫(Meloidogyneacronea)、非洲根结线虫(Meloidogyneafricana)、花生根结线虫(Meloidogynearenaria)、Meloidogynearenariathamesi、Meloidogyneartiella、奇特伍德根结线虫(Meloidogynechitwoodi)、咖啡根结线虫(Meloidogynecoffeicola)、埃塞俄比亚根结线虫(Meloidogyneethiopica)、短小根结线虫(Meloidogyneexigua)、禾草根结线虫(Meloidogynegraminicola)、禾本科根结线虫(Meloidogynegraminis)、北方根结线虫(Meloidogynehapla)、南方根结线虫(Meloidogyneincognita)、Meloidogyneincognitaacrita、爪哇根结线虫(Meloidogynejavanica)、吉库尤根结线虫(Meloidogynekikuyensis)、纳西根结线虫(Meloidogynenaasi)、Meloidogyneparanaensis、泰晤士根结线虫(Meloidogynethamesi)和通常的根结线虫属、Meloinemaspp.、异常珍珠线虫(Nacobbusaberrans)、Neotylenchusvigissi、假墙草异滑刃线虫(Paraphelenchus pseudoparietinus)、葱属拟毛刺线虫(Paratrichodorusallius)、Paratrichodoruslobatus、较小拟毛刺线虫(Paratrichodorusminor)、短小拟毛刺线虫(Paratrichodorusnanus)、多孔拟毛刺线虫(Paratrichodorus porosus)、光滑拟毛刺线虫(Paratrichodorusteres)和通常的拟毛刺线虫属、钩针线虫(Paratylenchushamatus)、微小针线虫(Paratylenchusminutus)、突出针线虫(Paratylenchusprojectus)和通常的针线虫属、敏捷短体线虫(Pratylenchusagilis)、艾伦短体线虫(Pratylenchusalleni)、安第斯短体线虫(Pratylenchusandinus)、最短尾短体线虫(Pratylenchusbrachyurus)、Pratylenchuscerealis、咖啡短体线虫(Pratylenchuscoffeae)、刻痕短体线虫(Pratylenchuscrenatus)、德拉特短体线虫(Pratylenchusdelattrei)、Pratylenchusgiibbicaudatus、古迪短体线虫(Pratylenchusgoodeyi)、Pratylenchushamatus、六裂短体线虫(Pratylenchushexincisus)、卢斯短体线虫(Pratylenchusloosi)、落选短体线虫(Pratylenchusneglectus)、穿刺短体线虫(Pratylenchuspenetrans)、草地短体线虫(Pratylenchuspratensis)、斯克里布纳短体线虫(Pratylenchusscribneri)、光滑短体线虫(Pratylenchusteres)、桑尼短体线虫(Pratylenchusthornei)、伤残短体线虫(Pratylenchusvulnus)、玉米短体线虫(Pratylenchuszeae)和通常的短体线虫属、Pseudohalenchus minutus、Psilenchusmagnidens、Psilenchustumidus、墨西哥玉米胞囊线虫(Punctoderachalcoensis)、Quinisulcius acutus、柑橘穿孔线虫(Radopholuscitrophilus)、香蕉穿孔线虫(Radopholussimilis)、Rotylenchulusborealis、小肾状线虫(Rotylenchulusparvus)、肾形肾状线虫(Rotylenchulusreniformis)和通常的肾状线虫属、直沟盘旋线虫(Rotylenchuslaurentinus)、Rotylenchusmacrodoratus、强壮盘旋线虫(Rotylenchus robustus)、Rotylenchusuniformis和通常的盘旋线虫属、小尾盾线虫(Scutellonemabrachyurum)、薯蓣盾线虫(Scutellonemabradys)、格尾盾线虫(Scutellonemaclathricaudatum)和通常的盾线虫属、Subanguinaradiciola、Tetylenchusnicotianae、圆桶毛刺线虫(Trichodorus
cylindricus)、较小毛刺线虫(Trichodorusminor)、原始毛刺线虫(Trichodorus primitivus)、Trichodorusproximus、相似毛刺线虫(Trichodorussimilis)、Trichodorussparsus和通常的毛刺线虫属、农田矮化线虫(Tylenchorhynchusagri)、甘蓝矮化线虫(Tylenchorhynchusbrassicae)、清亮矮化线虫(Tylenchorhynchusclarus)、克莱顿矮化线虫(Tylenchorhynchusclaytoni)、Tylenchorhynchusdigitatus、Tylenchorhynchusebriensis、最大矮化线虫(Tylenchorhynchusmaximus)、裸矮化线虫(Tylenchorhynchusnudus)、普通矮化线虫(Tylenchorhynchusvulgaris)和通常的矮化线虫属、半穿刺线虫(Tylenchulussemipenetrans)、美洲剑线虫(Xiphinemaamericanum)、短颈剑线虫(Xiphinemabrevicolle)、Xiphinemadimorphicaudatum、标准剑线虫(Xiphinemaindex)和通常的剑线虫属。
因此,本发明还涉及组合物防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄的作物并提高产量的用途,除填充剂和/或表面活性剂之外,所述组合物包含
A)氟吡菌酰胺和
B)至少一种农用化学活性化合物。
因此,本发明还涉及组合物防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、胡椒、胡萝卜、洋葱、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄、木本作物 - 梨果、木本作物 - 核果、木本作物 - 坚果、花的作物并提高产量的用途,除填充剂和/或表面活性剂之外,所述组合物包含
A)氟吡菌酰胺和
B)至少一种农用化学活性化合物。
因此,本发明还涉及组合物防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄的作物并提高产量的用途,除填充剂和/或表面活性剂之外,所述组合物包含
A)氟吡菌酰胺和
B)至少一种农用化学活性化合物,
所述线虫选自以下属:滑刃线虫属(Aphelenchoides
spp.)、松材线虫属(Bursaphelenchus spp.)、茎线虫属(Ditylenchus spp. )、球异皮线虫属(Globodera spp. )、异皮线虫属(Heterodera spp.)、长针线虫属(Longidorus spp.)、根结线虫属(Meloidogyne
spp.)、短体线虫属(Pratylenchus spp.)、穿孔线虫属(Radopholus spp.)、毛刺线虫属(Trichodorus
spp.)、半穿刺线虫属(Tylenchulus spp.)、剑线虫属(Xiphinema spp.)、螺旋线虫属(Helicotylenchus
spp.)、矮化线虫属(Tylenchorhynchus spp.)、盾线虫属(Scutellonema spp.)、异毛刺线虫属(Paratrichodorus
spp.)、Meloinema spp.、拟滑刃线虫属(Paraphelenchus spp.)、垫刃线虫属(Aglenchus spp.)、刺线虫属(Belonolaimus
spp.)、珍珠线虫属(Nacobbus spp.)、肾状线虫属(Rotylenchulus spp.)、盘旋线虫属(Rotylenchus
spp.)、拟茎线虫属(Neotylenchus spp.)、异滑刃线虫属(Paraphelenchus spp.)、锥线虫属(Dolichodorus spp.)、纽带线虫属(Hoplolaimus
spp.)、克点胞囊线虫属(Punctodera spp.)、小环线虫属(Criconemella spp.)、五沟属(Quinisulcius
spp.)、鞘线虫属(Hemicycliophora spp.)、粒线虫属(Anguina spp.)、Subanguina
spp.、半轮线虫属(Hemicriconemoides spp.)、平滑线虫属(Psilenchus spp.)、Pseudohalenchus
spp.、轮线虫属(Criconemoides spp.)、坏死线虫属(Cacopaurus spp.)。
因此,本发明还涉及组合物防治线虫侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、胡椒、胡萝卜、洋葱、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄、木本作物 - 梨果、木本作物 - 核果、木本作物 - 坚果、花的作物并提高产量的用途,除填充剂和/或表面活性剂之外,所述组合物包含
A)氟吡菌酰胺和
B)至少一种农用化学活性化合物,
所述线虫选自以下属:滑刃线虫属(Aphelenchoides
spp.)、松材线虫属(Bursaphelenchus spp.)、茎线虫属(Ditylenchus spp. )、球异皮线虫属(Globodera spp. )、异皮线虫属(Heterodera spp.)、长针线虫属(Longidorus spp.)、根结线虫属(Meloidogyne
spp.)、短体线虫属(Pratylenchus spp.)、穿孔线虫属(Radopholus spp.)、毛刺线虫属(Trichodorus
spp.)、半穿刺线虫属(Tylenchulus spp.)、剑线虫属(Xiphinema spp.)、螺旋线虫属(Helicotylenchus
spp.)、矮化线虫属(Tylenchorhynchus spp.)、盾线虫属(Scutellonema spp.)、异毛刺线虫属(Paratrichodorus
spp.)、Meloinema spp.、拟滑刃线虫属(Paraphelenchus spp.)、垫刃线虫属(Aglenchus spp.)、刺线虫属(Belonolaimus
spp.)、珍珠线虫属(Nacobbus spp.)、肾状线虫属(Rotylenchulus spp.)、盘旋线虫属(Rotylenchus
spp.)、拟茎线虫属(Neotylenchus spp.)、异滑刃线虫属(Paraphelenchus spp.)、锥线虫属(Dolichodorus spp.)、纽带线虫属(Hoplolaimus
spp.)、克点胞囊线虫属(Punctodera spp.)、小环线虫属(Criconemella spp.)、五沟属(Quinisulcius
spp.)、鞘线虫属(Hemicycliophora spp.)、粒线虫属(Anguina spp.)、Subanguina
spp.、半轮线虫属(Hemicriconemoides spp.)、平滑线虫属(Psilenchus spp.)、Pseudohalenchus
spp.、轮线虫属(Criconemoides spp.)、坏死线虫属(Cacopaurus spp.)。
因此,本发明还涉及组合物防治线虫种侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄的作物并提高产量的用途,除填充剂和/或表面活性剂之外,所述组合物包含
A)氟吡菌酰胺和
B)至少一种农用化学活性化合物,
所述线虫种选自:居农野外垫刃线虫(Aglenchus
agricola)、小麦粒线虫(Anguina tritici)、花生滑刃线虫(Aphelenchoides arachidis)、草莓滑刃线虫(Aphelenchoides fragariae)、Belonolaimusgracilis、长尾刺线虫(Belonolaimuslongicaudatus)、Belonolaimusnortoni、Cacopauruspestis、弯曲小环线虫(Criconemellacurvata)、Criconemellaonoensis、装饰小环线虫(Criconemellaornata)、Criconemellarusium、薄叶小环线虫(Criconemellaxenoplax=环腐线虫(Mesocriconemaxenoplax))和通常的小环线虫属、Criconemoidesferniae、Criconemoidesonoense、Criconemoidesornatum)和通常的轮线虫属、马铃薯茎线虫(Ditylenchusdestructor)、鳞球茎茎线虫(Ditylenchusdipsaci)、食菌茎线虫(Ditylenchusmyceliophagus)和通常的茎线虫属、(Dolichodorusheterocephalus)、马铃薯白线虫(Globoderapallida=马铃薯白线虫(Heterodera pallida))、Globoderarostochiensis、Globoderasolanacearum、烟草胞囊线虫(Globoderatabacum)、Globoderavirginiae、双角螺旋线虫(Helicotylenchusdigonicus)、双宫螺旋线虫(Helicotylenchusdihystera)、Helicotylenchuserythrine、多带螺旋线虫(Helicotylenchusmulticinctus)、Helicotylenchusnannus、假强壮螺旋线虫(Helicotylenchus
pseudorobustus)和通常的螺旋线虫属、加利福尼亚半轮线虫(Hemicriconemoides)、裸鞘线虫(Hemicycliophoraarenaria)、Hemicycliophoranudata、Hemicycliophoraparvana、燕麦胞囊线虫(Heteroderaavenae)、十字花科胞囊线虫(Heteroderacruciferae)、大豆胞囊线虫(Heteroderaglycines)、水稻胞囊线虫(Heteroderaoryzae)、甜菜胞囊线虫(Heteroderaschachtii)、玉米胞囊线虫(Heterodera zeae)和通常的胞囊线虫属、Hoplolaimus aegyptii、Hoplolaimuscalifornicus、哥伦布纽带线虫(Hoplolaimuscolumbus)、盔形纽带线虫(Hoplolaimusgaleatus)、印度纽带线虫(Hoplolaimusindicus)、Hoplolaimusmagnistylus、拟强壮纽带线虫(Hoplolaimuspararobustus)、Longidorusafricanus、Longidorusbreviannulatus、横带长针线虫(Longidoruselongatus)、Longidoruslaevicapitatus、Longidorusvineacola)和通常的长针线虫属、高粱根结线虫(Meloidogyneacronea)、非洲根结线虫(Meloidogyneafricana)、花生根结线虫(Meloidogynearenaria)、Meloidogynearenariathamesi、Meloidogyneartiella、奇特伍德根结线虫(Meloidogynechitwoodi)、咖啡根结线虫(Meloidogynecoffeicola)、埃塞俄比亚根结线虫(Meloidogyneethiopica)、短小根结线虫(Meloidogyneexigua)、禾草根结线虫(Meloidogynegraminicola)、禾本科根结线虫(Meloidogynegraminis)、北方根结线虫(Meloidogynehapla)、南方根结线虫(Meloidogyneincognita)、Meloidogyneincognitaacrita、爪哇根结线虫(Meloidogynejavanica)、吉库尤根结线虫(Meloidogynekikuyensis)、纳西根结线虫(Meloidogynenaasi)、Meloidogyneparanaensis、泰晤士根结线虫(Meloidogynethamesi)和通常的根结线虫属、Meloinemaspp.、异常珍珠线虫(Nacobbusaberrans)、Neotylenchusvigissi、假墙草异滑刃线虫(Paraphelenchuspseudoparietinus)、葱属拟毛刺线虫(Paratrichodorus allius)、Paratrichodoruslobatus、较小拟毛刺线虫(Paratrichodorusminor)、短小拟毛刺线虫(Paratrichodorus nanus)、多孔拟毛刺线虫(Paratrichodorusporosus)、光滑拟毛刺线虫(Paratrichodorusteres)和通常的拟毛刺线虫属、钩针线虫(Paratylenchushamatus)、微小针线虫(Paratylenchusminutus)、突出针线虫(Paratylenchusprojectus)和通常的针线虫属、敏捷短体线虫(Pratylenchusagilis)、艾伦短体线虫(Pratylenchusalleni)、安第斯短体线虫(Pratylenchusandinus)、最短尾短体线虫(Pratylenchusbrachyurus)、Pratylenchuscerealis、咖啡短体线虫(Pratylenchuscoffeae)、刻痕短体线虫(Pratylenchuscrenatus)、德拉特短体线虫(Pratylenchusdelattrei)、Pratylenchusgiibbicaudatus、古迪短体线虫(Pratylenchusgoodeyi)、Pratylenchus hamatus、六裂短体线虫(Pratylenchushexincisus)、卢斯短体线虫(Pratylenchus loosi)、落选短体线虫(Pratylenchus
neglectus)、穿刺短体线虫(Pratylenchus penetrans)、草地短体线虫(Pratylenchus pratensis)、斯克里布纳短体线虫(Pratylenchus scribneri)、光滑短体线虫(Pratylenchus teres)、桑尼短体线虫(Pratylenchus
thornei)、伤残短体线虫(Pratylenchus vulnus)、玉米短体线虫(Pratylenchus zeae)和通常的短体线虫属、Pseudohalenchus
minutus、Psilenchus magnidens、Psilenchus tumidus、墨西哥玉米胞囊线虫(Punctodera
chalcoensis)、Quinisulcius
acutus、柑橘穿孔线虫(Radopholus citrophilus)、香蕉穿孔线虫(Radopholus similis)、Rotylenchulus
borealis、小肾状线虫(Rotylenchulus parvus)、肾形肾状线虫(Rotylenchulus reniformis)和通常的肾状线虫属、直沟盘旋线虫(Rotylenchus laurentinus)、Rotylenchus macrodoratus、强壮盘旋线虫(Rotylenchus robustus)、Rotylenchus uniformis和通常的盘旋线虫属、小尾盾线虫(Scutellonema
brachyurum)、薯蓣盾线虫(Scutellonema bradys)、格尾盾线虫(Scutellonema clathricaudatum)和通常的盾线虫属、Subanguina radiciola、Tetylenchus nicotianae、圆桶毛刺线虫(Trichodorus
cylindricus)、较小毛刺线虫(Trichodorusminor)、原始毛刺线虫(Trichodorusprimitivus)、Trichodorusproximus、相似毛刺线虫(Trichodorussimilis)、Trichodorussparsus和通常的毛刺线虫属、农田矮化线虫(Tylenchorhynchusagri)、甘蓝矮化线虫(Tylenchorhynchusbrassicae)、清亮矮化线虫(Tylenchorhynchusclarus)、克莱顿矮化线虫(Tylenchorhynchus claytoni)、Tylenchorhynchusdigitatus、Tylenchorhynchusebriensis、最大矮化线虫(Tylenchorhynchusmaximus)、裸矮化线虫(Tylenchorhynchus nudus)、普通矮化线虫(Tylenchorhynchusvulgaris)和通常的矮化线虫属、半穿刺线虫(Tylenchulussemipenetrans)、美洲剑线虫(Xiphinemaamericanum)、短颈剑线虫(Xiphinemabrevicolle)、Xiphinemadimorphicaudatum、标准剑线虫(Xiphinemaindex)和通常的剑线虫属。
因此,本发明还涉及组合物防治线虫种侵袭选自蔬菜(尤其是番茄和葫芦)、马铃薯、胡椒、胡萝卜、洋葱、玉米、大豆、棉花、烟草、咖啡、甘蔗、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄、木本作物 - 梨果、木本作物 - 核果、木本作物 - 坚果、花的作物并提高产量的用途,除填充剂和/或表面活性剂之外,所述组合物包含
A)氟吡菌酰胺和
B)至少一种农用化学活性化合物,
所述线虫种选自:居农野外垫刃线虫(Aglenchus
agricola)、小麦粒线虫(Anguina tritici)、花生滑刃线虫(Aphelenchoides arachidis)、草莓滑刃线虫(Aphelenchoides fragariae)、Belonolaimusgracilis 、长尾刺线虫(Belonolaimus longicaudatus)、Belonolaimus nortoni、Cacopaurus
pestis、弯曲小环线虫(Criconemella curvata)、Criconemella onoensis、装饰小环线虫(Criconemella
ornata)、Criconemella rusium、薄叶小环线虫(Criconemella xenoplax=环腐线虫(Mesocriconema xenoplax))和通常的小环线虫属、Criconemoides
ferniae、Criconemoides onoense、Criconemoides ornatum和通常的轮线虫属、马铃薯茎线虫(Ditylenchus
destructor)、鳞球茎茎线虫(Ditylenchus dipsaci)、食菌茎线虫(Ditylenchus myceliophagus)和通常的茎线虫属、Dolichodorus heterocephalus、马铃薯白线虫(Globodera pallida=马铃薯白线虫(Heterodera
pallida))、Globodera rostochiensis、Globodera solanacearum、烟草胞囊线虫(Globodera
tabacum)、Globodera virginiae、双角螺旋线虫(Helicotylenchus digonicus)、双宫螺旋线虫(Helicotylenchus dihystera)、Helicotylenchus erythrine、多带螺旋线虫(Helicotylenchus multicinctus)、Helicotylenchus nannus、假强壮螺旋线虫(Helicotylenchus
pseudorobustus)和通常的螺旋线虫属、加利福尼亚半轮线虫(Hemicriconemoides)、裸鞘线虫(Hemicycliophoraarenaria)、Hemicycliophoranudata、Hemicycliophoraparvana、燕麦胞囊线虫(Heteroderaavenae)、十字花科胞囊线虫(Heteroderacruciferae)、大豆胞囊线虫(Heterodera glycines)、水稻胞囊线虫(Heterodera oryzae)、甜菜胞囊线虫(Heterodera
schachtii)、玉米胞囊线虫(Heterodera zeae)和通常的胞囊线虫属、Hoplolaimus aegyptii、Hoplolaimuscalifornicus、哥伦布纽带线虫(Hoplolaimuscolumbus)、盔形纽带线虫(Hoplolaimusgaleatus)、印度纽带线虫(Hoplolaimusindicus)、Hoplolaimus
magnistylus、拟强壮纽带线虫(Hoplolaimuspararobustus)、Longidorusafricanus、Longidorusbreviannulatus、横带长针线虫(Longidoruselongatus)、Longidoruslaevicapitatus、Longidorusvineacola和通常的长针线虫属、高粱根结线虫(Meloidogyneacronea)、非洲根结线虫(Meloidogyne africana)、花生根结线虫(Meloidogynearenaria)、Meloidogyne arenaria thamesi、Meloidogyne artiella、奇特伍德根结线虫(Meloidogynechitwoodi)、咖啡根结线虫(Meloidogynecoffeicola)、埃塞俄比亚根结线虫(Meloidogyneethiopica)、短小根结线虫(Meloidogyneexigua)、禾草根结线虫(Meloidogynegraminicola)、禾本科根结线虫(Meloidogynegraminis)、北方根结线虫(Meloidogynehapla)、南方根结线虫(Meloidogyneincognita)、Meloidogyne incognitaacrita、爪哇根结线虫(Meloidogynejavanica)、吉库尤根结线虫(Meloidogynekikuyensis)、纳西根结线虫(Meloidogynenaasi)、Meloidogyneparanaensis、泰晤士根结线虫(Meloidogyne thamesi)和通常的根结线虫属、Meloinemaspp.、异常珍珠线虫(Nacobbusaberrans)、Neotylenchusvigissi、假墙草异滑刃线虫(Paraphelenchuspseudoparietinus)、葱属拟毛刺线虫(Paratrichodorus allius)、Paratrichodoruslobatus、较小拟毛刺线虫(Paratrichodorus minor)、短小拟毛刺线虫(Paratrichodorusnanus)、多孔拟毛刺线虫(Paratrichodorus porosus)、光滑拟毛刺线虫(Paratrichodorusteres)和通常的拟毛刺线虫属、钩针线虫(Paratylenchushamatus)、微小针线虫(Paratylenchusminutus)、突出针线虫(Paratylenchusprojectus)和通常的针线虫属、敏捷短体线虫(Pratylenchusagilis)、艾伦短体线虫(Pratylenchusalleni)、安第斯短体线虫(Pratylenchusandinus)、最短尾短体线虫(Pratylenchusbrachyurus)、Pratylenchuscerealis、咖啡短体线虫(Pratylenchuscoffeae)、刻痕短体线虫(Pratylenchuscrenatus)、德拉特短体线虫(Pratylenchusdelattrei)、Pratylenchusgiibbicaudatus、古迪短体线虫(Pratylenchusgoodeyi)、Pratylenchushamatus、六裂短体线虫(Pratylenchushexincisus)、卢斯短体线虫(Pratylenchusloosi)、落选短体线虫(Pratylenchus
neglectus)、穿刺短体线虫(Pratylenchuspenetrans)、草地短体线虫(Pratylenchuspratensis)、斯克里布纳短体线虫(Pratylenchusscribneri)、光滑短体线虫(Pratylenchusteres)、桑尼短体线虫(Pratylenchusthornei)、伤残短体线虫(Pratylenchusvulnus)、玉米短体线虫(Pratylenchuszeae)和通常的短体线虫属、Pseudohalenchus minutus、Psilenchusmagnidens、Psilenchustumidus、墨西哥玉米胞囊线虫(Punctoderachalcoensis)、Quinisulciusacutus、柑橘穿孔线虫(Radopholuscitrophilus)、香蕉穿孔线虫(Radopholussimilis)、Rotylenchulusborealis、小肾状线虫(Rotylenchulusparvus)、肾形肾状线虫(Rotylenchulusreniformis)和通常的肾状线虫属、直沟盘旋线虫(Rotylenchuslaurentinus)、Rotylenchusmacrodoratus、强壮盘旋线虫(Rotylenchusrobustus)、Rotylenchusuniformis和通常的盘旋线虫属、小尾盾线虫(Scutellonemabrachyurum)、薯蓣盾线虫(Scutellonemabradys)、格尾盾线虫(Scutellonemaclathricaudatum)和通常的盾线虫属、Subanguinaradiciola、Tetylenchusnicotianae、圆桶毛刺线虫(Trichodoruscylindricus)、较小毛刺线虫(Trichodorusminor)、原始毛刺线虫(Trichodorusprimitivus)、Trichodorusproximus、相似毛刺线虫(Trichodorussimilis)、Trichodorussparsus和通常的毛刺线虫属、农田矮化线虫(Tylenchorhynchus agri)、甘蓝矮化线虫(Tylenchorhynchusbrassicae)、清亮矮化线虫(Tylenchorhynchusclarus)、克莱顿矮化线虫(Tylenchorhynchus claytoni)、Tylenchorhynchusdigitatus、Tylenchorhynchusebriensis、最大矮化线虫(Tylenchorhynchusmaximus)、裸矮化线虫(Tylenchorhynchusnudus)、普通矮化线虫(Tylenchorhynchusvulgaris)和通常的矮化线虫属、半穿刺线虫(Tylenchulussemipenetrans)、美洲剑线虫(Xiphinemaamericanum)、短颈剑线虫(Xiphinemabrevicolle)、Xiphinemadimorphicaudatum、标准剑线虫(Xiphinemaindex)和通常的剑线虫属。
本发明的示例性方法包括向土壤或植物(如种子或叶面)施用本发明的氟吡菌酰胺以防治线虫损害和/或提高作物产量。
优选实施方式说明
蔬菜例如是绿花椰菜、花椰菜、朝鲜蓟、甜玉米(玉米)、豌豆、豆、无头甘蓝、羽衣甘蓝、菠菜、芝麻菜、 beet
green、小白菜、牛皮菜、菜心、芜菁、菊苣、莴苣、芥菜、水田芥、韭菜、芥蓝、韭葱、布鲁塞尔豆芽、马槟榔、苤蓝、芹菜、大黄、刺菜蓟、中国芹菜、香茅、芦笋、竹笋、高良姜和姜、马铃薯、洋姜、甘薯、芋头、山药豆芽、绿豆、urad、苜蓿、胡萝卜、荷兰防风草、甜菜、水萝卜、芜菁甘蓝、萝卜、牛蒡、洋葱、青葱、大蒜、番茄、葫芦科植物(黄瓜、笋瓜、南瓜、甜瓜、丝瓜、葫芦、西瓜)、密生西葫芦、胡椒、茄子、绿茄果、佛手瓜、秋葵、面包果和鳄梨、四季豆、兵豆、荷兰豆。
优选的蔬菜是番茄、葫芦科植物、马铃薯、胡椒、胡萝卜、洋葱。
木本作物-核果例如是杏、樱桃、杏仁和桃。
木本作物-梨果例如是苹果、梨。
木本作物-坚果例如是山毛榉、巴西坚果、石栗、腰果、板栗(包括中国板栗、甜板栗)、药西瓜、黑籽南瓜、榛子(Filbert)、智利榛、山核桃 (包括美洲山核桃、薄皮山核桃)、榄仁树、榛子(Hazelnut)、印度山毛榉、可乐果、夏威夷果、马拉巴栗、黄连木、蜜果、Maya坚果、Mongongo、橡树橡子(Oak acorn)、Ogbono坚果、Paradise nut、比列橄榄、胡桃、黑胡桃、菱角。
在本上下文中,将农用化学活性化合物理解为表示用于或可以通常用于处理植物的所有物质。杀真菌剂、杀细菌剂、杀虫剂、杀螨剂、杀线虫剂、杀软体动物剂、安全剂、植物生长调节剂和植物营养物以及生物防治剂可以优选提及。
混合伴侣
可以提及的杀真菌剂的实例是:
1)麦角固醇生物合成的抑制剂,例如(1.1)十二吗啉(1704-28-5)、(1.2)阿扎康唑(60207-31-0)、(1.3)联苯三唑醇(55179-31-2)、(1.4)糠菌唑(116255-48-2)、(1.5)环丙唑醇(113096-99-4)、(1.6)苄氯三唑醇(75736-33-3)、(1.7)苯醚甲环唑(119446-68-3)、(1.8)烯唑醇(83657-24-3)、(1.9)烯唑醇-M(83657-18-5)、(1.10)吗菌灵(1593-77-7)、(1.11)吗菌灵乙酸酯(31717-87-0)、(1.12)氟环唑(106325-08-0)、(1.13)乙环唑(60207-93-4)、(1.14)氯苯嘧啶醇(60168-88-9)、(1.15)腈苯唑(114369-43-6)、(1.16)环酰菌胺(126833-17-8)、(1.17)苯锈啶(67306-00-7)、(1.18)粉锈啉(67306-03-0)、(1.19)氟喹唑(136426-54-5)、(1.20)呋嘧醇(56425-91-3)、(1.21)氟硅唑(85509-19-9)、(1.22)粉唑醇(76674-21-0)、(1.23)呋菌唑(112839-33-5)、(1.24)呋醚唑(112839-32-4)、(1.25)己唑醇(79983-71-4)、(1.26)抑霉唑(60534-80-7)、(1.27)抑霉唑硫酸酯(58594-72-2)、(1.28)亚胺唑(86598-92-7)、(1.29)种菌唑(125225-28-7)、(1.30)叶菌唑(125116-23-6)、(1.31)腈菌唑(88671-89-0)、(1.32)萘替芬(65472-88-0)、(1.33)噻菌醇(63284-71-9)、(1.34)噁咪唑(174212-12-5)、(1.35)多效唑(76738-62-0)、(1.36)稻瘟酯(101903-30-4)、(1.37)戊菌唑(66246-88-6)、(1.38)哌丙灵(3478-94-2)、(1.39)咪鲜胺(67747-09-5)、(1.40)丙环唑(60207-90-1)、(1.41)丙硫菌唑(178928-70-6)、(1.42)稗草丹(88678-67-5)、(1.43)啶斑肟(88283-41-4)、(1.44)氯苯喹唑(103970-75-8)、(1.45)硅氟唑(149508-90-7)、(1.46)螺环菌胺(118134-30-8)、(1.47)戊唑醇(107534-96-3)、(1.48)特比萘芬(91161-71-6)、(1.49)氟醚唑(112281-77-3)、(1.50)三唑酮(43121-43-3)、(1.51)三唑醇(89482-17-7)、(1.52)十三吗啉(81412-43-3)、(1.53)氟菌唑(68694-11-1)、(1.54)嗪氨灵(26644-46-2)、(1.55)灭菌唑(131983-72-7)、(1.56)烯效唑(83657-22-1)、(1.57)烯效唑-p(83657-17-4)、(1.58)烯霜苄唑(77174-66-4)、(1.59)伏立康唑(137234-62-9)、(1.60)1-(4-氯苯基)-2-(1H-1,2,4-三唑-1-基)环庚醇(129586-32-9)、(1.61)1-(2,2-二甲基-2,3-二氢-1H-茚-1-基)-1H-咪唑-5-甲酸甲酯(110323-95-0)、(1.62)N'-{5-(二氟甲基)-2-甲基-4-[3-(三甲基甲硅烷基)丙氧基]苯基}-N-乙基-N-甲基亚氨基甲酰胺、(1.63)N-乙基-N-甲基-N'-{2-甲基-5-(三氟甲基)-4-[3-(三甲基甲硅烷基)丙氧基]苯基}亚氨基甲酰胺和(1.64)O-[1-(4-甲氧基苯氧基)-3,3-二甲基丁-2-基] 1H-咪唑-1-硫代甲酸酯(111226-71-2)。
(2)复合物I或II的呼吸链抑制剂,例如(2.1)联苯吡菌胺(581809-46-3)、(2.2)啶酰菌胺(188425-85-6)、(2.3)萎锈灵(5234-68-4)、(2.4)二氟林(130339-07-0)、(2.5)甲呋酰胺(24691-80-3)、(2.6)氟吡菌酰胺(658066-35-4)、(2.7)氟酰胺(66332-96-5)、(2.8)氟唑菌酰胺(907204-31-3)、(2.9)福拉比(123572-88-3)、(2.10)茂谷乐(60568-05-0)、(2.11)萘吡菌胺(同侧差向异构外消旋体1RS,4SR,9RS和异侧差向异构外消旋体1RS,4SR,9SR的混合物)(881685-58-1)、(2.12)萘吡菌胺(异侧差向异构外消旋体1RS,4SR,9SR)、(2.13)萘吡菌胺(异侧差向异构外消旋体1R,4S,9S)、(2.14)萘吡菌胺(异侧差向异构外消旋体1S,4R,9R)、(2.15)萘吡菌胺(同侧差向异构外消旋体1RS,4SR,9RS)、(2.16)萘吡菌胺(同侧差向异构外消旋体1R,4S,9R)、(2.17)萘吡菌胺(同侧差向异构外消旋体1S,4R,9S)、(2.18)灭锈胺(55814-41-0)、(2.19)氧化萎锈灵(5259-88-1)、(2.20)戊苯吡菌胺(494793-67-8)、(2.21)吡噻菌胺(183675-82-3)、(2.22)环丙吡菌胺(874967-67-6)、(2.23)噻氟菌胺(130000-40-7)、(2.24)1-甲基-N-[2-(1,1,2,2-四氟乙氧基)苯基]-3-(三氟甲基)-1H-吡唑-4-甲酰胺、(2.25)3-(二氟甲基)-1-甲基-N-[2-(1,1,2,2-四氟乙氧基)苯基]-1H-吡唑-4-甲酰胺、(2.26)3-(二氟甲基)-N-[4-氟-2-(1,1,2,3,3,3-六氟丙氧基)苯基]-1-甲基-1H-吡唑-4-甲酰胺、(2.27)N-[1-(2,4-二氯苯基)-1-甲氧基丙烷-2-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺(1092400-95-7)(WO
2008148570)、(2.28)5,8-二氟-N-[2-(2-氟-4-{[4-(三氟甲基)吡啶-2-基]氧基}苯基)乙基]喹唑啉-4-胺(1210070-84-0)(WO2010025451)、(2.29)N-[9-(二氯亚甲基)-1,2,3,4-四氢-1,4-桥亚甲基萘-5-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺、(2.30) N-[(1S,4R)-9-(二氯亚甲基)-1,2,3,4-四氢-1,4-桥亚甲基萘-5-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺和(2.31) N-[(1R,4S)-9-(二氯亚甲基)-1,2,3,4-四氢-1,4-桥亚甲基萘-5-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺。
(3)复合物III的呼吸链抑制剂,例如(3.1)辛唑嘧菌胺(865318-97-4)、(3.2)吲唑磺菌胺(348635-87-0)、(3.3)嘧菌酯(131860-33-8)、(3.4)氰霜唑(120116-88-3)、(3.5)甲香菌酯(850881-30-0)、(3.6)丁香菌酯(850881-70-8)、(3.7)醚菌胺(141600-52-4)、(3.8)烯肟菌酯(238410-11-2)(WO 2004/058723)、(3.9)噁唑菌酮(131807-57-3)(WO
2004/058723)、(3.10)咪唑菌酮(161326-34-7)(WO
2004/058723)、(3.11)fenoxystrobin(918162-02-4)、(3.12)氟嘧菌酯(361377-29-9)(WO
2004/058723)、(3.13)醚菌酯(143390-89-0)(WO
2004/058723)、(3.14)苯氧菌胺(133408-50-1)(WO
2004/058723)、(3.15)肟醚菌胺(189892-69-1)(WO
2004/058723)、(3.16)啶氧菌酯(117428-22-5)(WO
2004/058723)、(3.17)吡唑醚菌酯(175013-18-0)(WO
2004/058723)、(3.18)唑胺菌酯(915410-70-7)(WO
2004/058723)、(3.19)唑菌酯(862588-11-2)(WO
2004/058723)、(3.20)吡菌苯威(799247-52-2)(WO
2004/058723)、(3.21)氯啶菌酯(902760-40-1)、(3.22)三氟敏(141517-21-7)(WO
2004/058723)、(3.23)(2E)-2-(2-{[6-(3-氯-2-甲基苯氧基)-5-氟嘧啶-4-基]氧基}苯基)-2-(甲氧基亚氨基)-N-甲基乙酰胺(WO 2004/058723)、(3.24)(2E)-2-(甲氧基亚氨基)-N-甲基-2-(2-{[({(1E)-1-[3-(三氟甲基)苯基]亚乙基}氨基)氧基]甲基}苯基)乙酰胺(WO 2004/058723)、(3.25)(2E)-2-(甲氧基亚氨基)-N-甲基-2-{2-[(E)-({1-[3-(三氟甲基)苯基]乙氧基}亚胺基)甲基]苯基}乙酰胺(158169-73-4)、(3.26)(2E)-2-{2-[({[(1E)-1-(3-{[(E)-1-氟-2-苯基乙烯基]氧基}苯基)亚乙基]氨基}氧基)甲基]苯基}-2-(甲氧基亚氨基)-N-甲基乙酰胺(326896-28-0)、(3.27)(2E)-2-{2-[({[(2E,3E)-4-(2,6-二氯苯基)亚丁-3-烯-2-基]氨基}氧基)甲基]苯基}-2-(甲氧基亚氨基)-N-甲基乙酰胺、(3.28)2-氯-N-(1,1,3-三甲基-2,3-二氢-1H-茚-4-基)吡啶-3-甲酰胺(119899-14-8)、(3.29)5-甲氧基-2-甲基-4-(2-{[({(1E)-1-[3-(三氟甲基)苯基]亚乙基}氨基)氧基]甲基}苯基)-2,4-二氢-3H-1,2,4-三唑-3-酮、(3.30)(2E)-2-{2-[({环丙基 [(4-甲氧基苯基)亚氨基]甲基}硫烷基)甲基]苯基}-3-甲氧基丙-2-烯酸甲酯(149601-03-6)、(3.31)N-(3-乙基-3,5,5-三甲基环己基)-3-(甲酰基氨基)-2-羟基苯甲酰胺(226551-21-9)、(3.32)2-{2-[(2,5-二甲基苯氧基)甲基]苯基}-2-甲氧基-N-甲基乙酰胺(173662-97-0)和(3.33)(2R)-2-{2-[(2,5-二甲基苯氧基)甲基]苯基}-2-甲氧基-N-甲基乙酰胺(394657-24-0)。
(4)有丝分裂和细胞分裂的抑制剂,例如(4.1)苯菌灵(17804-35-2)、(4.2)多菌灵(10605-21-7)、(4.3)氯苯咪唑(3574-96-7)、(4.4)乙霉威(87130-20-9)、(4.5)噻唑菌胺(162650-77-3)、(4.6)氟吡菌胺(239110-15-7)、(4.7)麦穗宁(3878-19-1)、(4.8)戊菌隆(66063-05-6)、(4.9)噻苯咪唑(148-79-8)、(4.10)甲基硫菌灵(23564-05-8)、(4.11)硫菌灵(23564-06-9)、(4.12)苯酰菌胺(156052-68-5)、(4.13)5-氯-7-(4-甲基哌啶-1-基)-6-(2,4,6-三氟苯基)[1,2,4]三唑并[1,5-a]嘧啶(214706-53-3)和(4.14)3-氯-5-(6-氯吡啶-3-基)-6-甲基-4-(2,4,6-三氟苯基)哒嗪(1002756-87-7)。
(5)能够具有多位点作用的化合物,如例如(5.1)波尔多混合物(8011-63-0)、(5.2)敌菌丹(2425-06-1)、(5.3)克菌丹(133-06-2)(WO
02/12172)、(5.4)百菌清(1897-45-6)、(5.5)氢氧化铜(20427-59-2)、(5.6)环烷酸铜(1338-02-9)、(5.7)氧化铜(1317-39-1)、(5.8)氧氯化铜(1332-40-7)、(5.9)硫酸铜(2+)(7758-98-7)、(5.10)抑菌灵(1085-98-9)、(5.11)二噻农(3347-22-6)、(5.12)多果定(2439-10-3)、(5.13)多果定游离碱、(5.14)福美铁(14484-64-1)、(5.15)N-邻苯二甲酰亚胺(719-96-0)、(5.16)灭菌丹(133-07-3)、(5.17)双胍盐(108173-90-6)、(5.18)双胍辛乙酸盐、(5.19)双胍辛胺(13516-27-3)、(5.20)双胍辛胺苯磺酸盐(169202-06-6)、(5.21)双胍辛胺三乙酸盐(57520-17-9)、(5.22)代森锰铜(53988-93-5)、(5.23)代森锰锌(8018-01-7)、(5.24)代森锰(12427-38-2)、(5.25)代森联(9006-42-2)、(5.26)代森联锌(9006-42-2)、(5.27)喹啉铜(10380-28-6)、(5.28)普罗帕脒(104-32-5)、(5.29)甲基代森锌(12071-83-9)、(5.30)硫磺和硫磺制剂包括多硫化钙(7704-34-9)、(5.31)福美双(137-26-8)、(5.32)对甲抑菌灵(731-27-1)、(5.33)代森锌(12122-67-7)和(5.34)福美锌(137-30-4)。
(6)能够诱导宿主防御的化合物,例如(6.1)阿拉酸式苯-S-甲基(135158-54-2)、(6.2)异噻菌胺(224049-04-1)、(6.3)噻菌灵(27605-76-1)和(6.4)噻酰菌胺(223580-51-6)。
(7)氨基酸和/或蛋白质生物合成抑制剂,例如(7.1)胺扑灭(23951-85-1)、(7.2)灭瘟素(2079-00-7)、(7.3)嘧菌环胺(121552-61-2)、(7.4)春雷霉素(6980-18-3)、(7.5)盐酸春雷霉素水合物(19408-46-9)、(7.6)嘧菌胺(110235-47-7)、(7.7)嘧霉胺(53112-28-0)和(7.8)3-(5-氟-3,3,4,4-四甲基-3,4-二氢异喹啉-1-基)喹啉(861647-32-7)(WO2005070917)。
(8)ATP生产的抑制剂,例如(8.1)薯瘟锡(900-95-8)、(8.2)三苯锡氯(639-58-7)、(8.3)毒菌锡(76-87-9)和(8.4)硅噻菌胺(175217-20-6)。
(9)细胞壁合成的抑制剂,例如(9.1)苯并噻菌威(177406-68-7)、(9.2)烯酰吗啉(110488-70-5)、(9.3)氟吗啉(211867-47-9)、(9.4)缬霉威(140923-17-7)、(9.5)双炔酰菌胺(374726-62-2)、(9.6)多氧霉素(11113-80-7)、(9.7)多抗霉素(22976-86-9)、(9.8)井冈霉素(37248-47-8)和(9.9)valifenalate(283159-94-4;283159-90-0)。
(10)脂质和膜合成的抑制剂,例如(10.1)联苯(92-52-4)、(10.2)地茂散(2675-77-6)、(10.3)氯硝胺(99-30-9)、(10.4)克瘟散(17109-49-8)、(10.5)依得利(2593-15-9)、(10.6)iodocarb(55406-53-6)、(10.7)异稻瘟净(26087-47-8)、(10.8)稻瘟灵(50512-35-1)、(10.9)霜霉威(25606-41-1)、(10.10)盐酸霜霉威(25606-41-1)、(10.11)胺丙威(19622-08-3)、(10.12)定菌磷(13457-18-6)、(10.13)五氯硝基苯(82-68-8)、(10.14)四氯硝基苯(117-18-0)和(10.15)甲基立枯磷(57018-04-9)。
(11)黑色素生物合成抑制剂,例如(11.1)加普胺(104030-54-8)、(11.2)双氯氰菌胺(139920-32-4)、(11.3)稻瘟酰胺(115852-48-7)、(11.4)四氯苯酞(27355-22-2)、(11.5)乐喹酮(57369-32-1)、(11.6)三环唑(41814-78-2)和(11.7) {3-甲基-1-[(4-甲基苯甲酰基)氨基]丁烷-2-基}氨基甲酸2,2,2-三氟乙酯(851524-22-6)(WO2005042474)。
(12)核酸合成的抑制剂,例如(12.1)苯霜灵(71626-11-4)、(12.2)苯霜灵-M(kiralaxyl)(98243-83-5)、(12.3)布瑞莫(41483-43-6)、(12.4)clozylacon(67932-85-8)、(12.5)甲菌定(5221-53-4)、(12.6)乙菌定(23947-60-6)、(12.7)呋霜灵(57646-30-7)、(12.8)噁霉灵(10004-44-1)、(12.9)甲霜灵(57837-19-1)、(12.10)甲霜灵-M(精甲霜灵)(70630-17-0)、(12.11)甲呋酰胺(58810-48-3)、(12.12)噁霜灵(77732-09-3)和(12.13)噁喹酸(14698-29-4)。
(13)信号转导的抑制剂,例如(13.1)乙菌利(84332-86-5)、(13.2)拌种咯(74738-17-3)、(13.3)咯菌腈(131341-86-1)、(13.4)异菌脲(36734-19-7)、(13.5)腐霉利(32809-16-8)、(13.6)喹氧灵(124495-18-7)和(13.7)乙烯菌核利(50471-44-8)。
(14)能够充当解偶联剂的化合物,例如(14.1)乐杀螨(485-31-4)、(14.2)阿乐丹(131-72-6)、(14.3)嘧菌腙(89269-64-7)、(14.4)氟啶胺(79622-59-6)和(14.5)消螨多(131-72-6)。
(15)其他化合物,例如(15.1)苯噻硫氰(21564-17-0)、(15.2)3-苯并[b]噻吩-2-基-5,6-二氢-1,4,2-噻嗪4-氧化物(163269-30-5)、(15.3)卡巴西霉素(70694-08-5)、(15.4)香芹酮(99-49-0)、(15.5)灭螨猛(2439-01-2)、(15.6)pyriofenone(chlazafenone)(688046-61-9)、(15.7)硫杂灵(11096-18-7)、(15.8)环氟菌胺(180409-60-3)、(15.9)霜脲氰(57966-95-7)、(15.10)啶酰菌胺(221667-31-8)、(15.11)棉隆(533-74-4)、(15.12)咪菌威(62732-91-6)、(15.13)二氯芬(97-23-4)、(15.14)哒菌清(62865-36-5)、(15.15)野燕枯(49866-87-7)、(15.16)野燕枯甲基硫酸盐(43222-48-6)、(15.17)二苯胺(122-39-4)、(15.18)ecomate、(15.19)胺苯吡菌酮(473798-59-3)、(15.20)氟酰菌胺(154025-04-4)、(15.21)氟里醚(41205-21-4)、(15.22)磺菌胺(106917-52-6)、(15.23)氟噻菌净 (304900-25-2)、(15.24)三乙膦酸铝(39148-24-8)、(15.25)三乙膦酸钙、(15.26)三乙膦酸钠(39148-16-8)、(15.27)六氯苯(118-74-1)、(15.28)人间霉素(81604-73-1)、(15.29)磺菌威(66952-49-6)、(15.30)异硫氰酸甲酯(556-61-6)、(15.31)苯菌酮(220899-03-6)、(15.32)灭粉霉素(67527-71-3)、(15.33)游霉素(7681-93-8)、(15.34)福美镍(15521-65-0)、(15.35)酞菌酯(10552-74-6)、(15.36)辛噻酮(26530-20-1)、(15.37)oxamocarb(917242-12-7)、(15.38) oxyfenthiin (34407-87-9)、(15.39)五氯苯酚和盐(87-86-5)、(15.40)苯氧司林、(15.41)亚磷酸及其盐(13598-36-2)、(15.42)霜霉威-三乙磷酸酯、(15.43)丙醇菌素钠(88498-02-6)、(15.44)碘喹唑酮(189278-12-4)、(15.45)丁吡吗啉(868390-90-3)、(15.45e)(2E)-3-(4-叔-丁基苯基)-3-(2-氯吡啶-4-基)-1-(吗啉-4-基)丙-2-烯-1-酮(1231776-28-5)、(15.45z)(2Z)-3-(4-叔-丁基苯基)-3-(2-氯吡啶-4-基)-1-(吗啉-4-基)丙-2-烯-1-酮(1231776-29-6)、(15.46)硝吡咯菌素(1018-71-9) (EP-A 1 559 320)、(15.47)异丁乙氧喹啉(376645-78-2)、(15.48)叶枯酞(76280-91-6)、(15.49)甲磺菌胺(304911-98-6)、(15.50)咪唑嗪(72459-58-6)、(15.51)酰菌胺(70193-21-4)、(15.52)氰菌胺(84527-51-5)、(15.53)2-甲基丙酸(3S,6S,7R,8R)-8-苄基-3-[({3-[(异丁酰氧基)甲氧基]-4-甲氧基吡啶-2-基}羰基)氨基]-6-甲基-4,9-二氧代-1,5-二氧杂环己烷-7-基酯(517875-34-2) (WO2003035617)、(15.54)1-(4-{4-[(5R)-5-(2,6-二氟苯基)-4,5-二氢-1,2-噁唑-3-基]-1,3-噻唑-2-基}哌啶-1-基)-2-[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]乙酮(1003319-79-6) (WO 2008013622)、(15.55)1-(4-{4-[(5S)-5-(2,6-二氟苯基)-4,5-二氢-1,2-噁唑-3-基]-1,3-噻唑-2-基}哌啶-1-基)-2-[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]乙酮(1003319-80-9) (WO 2008013622)、(15.56)1-(4-{4-[5-(2,6-二氟苯基)-4,5-二氢-1,2-噁唑-3-基]-1,3-噻唑-2-基}哌啶-1-基)-2-[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]乙酮(1003318-67-9)
(WO 2008013622)、(15.57)1H-咪唑-1-甲酸1-(4-甲氧基苯氧基)-3,3-二甲基丁烷-2-基酯(111227-17-9)、(15.58)2,3,5,6-四氯-4-(甲基磺酰基)吡啶(13108-52-6)、(15.59)2,3-二丁基-6-氯噻吩并[2,3-d]嘧啶-4(3H)-酮(221451-58-7)、(15.60)2,6-二甲基-1H,5H-[1,4]二噻烯并[2,3-c:5,6-c']二吡咯-1,3,5,7(2H,6H)-四酮、(15.61)2-[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]-1-(4-{4-[(5R)-5-苯基-4,5-二氢-1,2-噁唑-3-基]-1,3-噻唑-2-基}哌啶-1-基)乙酮(1003316-53-7)
(WO 2008013622)、(15.62)2-[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]-1-(4-{4-[(5S)-5-苯基-4,5-二氢-1,2-噁唑-3-基]-1,3-噻唑-2-基}哌啶-1-基)乙酮(1003316-54-8) (WO 2008013622)、(15.63)2-[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]-1-{4-[4-(5-苯基-4,5-二氢-1,2-噁唑-3-基)-1,3-噻唑-2-基]哌啶-1-基}乙酮(1003316-51-5)
(WO 2008013622)、(15.64)2-丁氧基-6-碘-3-丙基-4H-苯并吡喃-4-酮、(15.65)2-氯-5-[2-氯-1-(2,6-二氟-4-甲氧基苯基)-4-甲基-1H-咪唑-5-基]吡啶、(15.66)2-苯基苯酚和盐(90-43-7)、(15.67)3-(4,4,5-三氟-3,3-二甲基-3,4-二氢异喹啉-1-基)喹啉(861647-85-0)
(WO2005070917)、(15.68)3,4,5-三氯吡啶-2,6-二甲腈(17824-85-0)、(15.69)3-[5-(4-氯苯基)-2,3-二甲基-1,2-噁唑烷-3-基]吡啶、(15.70)3-氯-5-(4-氯苯基)-4-(2,6-二氟苯基)-6-甲基哒嗪、(15.71)4-(4-氯苯基)-5-(2,6-二氟苯基)-3,6-二甲基哒嗪、(15.72)5-氨基-1,3,4-噻二唑-2-硫醇、(15.73)5-氯-N'-苯基-N'-(丙-2-炔-1-基)噻吩-2-噻吩磺酰肼(134-31-6)、(15.74)5-氟-2-[(4-氟苄基)氧基]嘧啶-4-胺(1174376-11-4) (WO2009094442)、(15.75)5-氟-2-[(4-甲基苄基)氧基]嘧啶-4-胺(1174376-25-0)
(WO2009094442)、(15.76)5-甲基-6-辛基[1,2,4]三唑并[1,5-a]嘧啶-7-胺、(15.77)(2Z)-3-氨基-2-氰基-3-苯基丙-2-烯酸乙酯、(15.78)N'-(4-{[3-(4-氯苯基)-1,2,4-噻二唑-5-基]氧基}-2,5-二甲基苯基)-N-乙基-N-甲基亚氨基甲酰胺、(15.79)N-(4-氯苄基)-3-[3-甲氧基-4-(丙-2-炔-1-基氧基)苯基]丙酰胺、(15.80)N-[(4-氯苯基)(氰基)甲基]-3-[3-甲氧基-4-(丙-2-炔-1-基氧基)苯基]丙酰胺、(15.81)N-[(5-溴-3-氯吡啶-2-基)甲基]-2,4-二氯吡啶-3-甲酰胺、(15.82)N-[1-(5-溴-3-氯吡啶-2-基)乙基]-2,4-二氯吡啶-3-甲酰胺、(15.83)N-[1-(5-溴-3-氯吡啶-2-基)乙基]-2-氟-4-碘代吡啶-3-甲酰胺、(15.84)N-{(E)-[(环丙基甲氧基)亚氨基][6-(二氟甲氧基)-2,3-二氟苯基]甲基}-2-苯基乙酰胺(221201-92-9)、(15.85)N-{(Z)-[(环丙基甲氧基)亚氨基][6-(二氟甲氧基)-2,3-二氟苯基]甲基}-2-苯基乙酰胺(221201-92-9)、(15.86)N'-{4-[(3-叔-丁基-4-氰基-1,2-噻唑-5-基)氧基]-2-氯-5-甲基苯基}-N-乙基-N-甲基亚氨基甲酰胺、(15.87)N-甲基-2-(1-{[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]乙酰基}哌啶-4-基)-N-(1,2,3,4-四氢萘-1-基)-1,3-噻唑-4-甲酰胺(922514-49-6)
(WO 2007014290)、(15.88)N-甲基-2-(1-{[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]乙酰基}哌啶-4-基)-N-[(1R)-1,2,3,4-四氢萘-1-基]-1,3-噻唑-4-甲酰胺(922514-07-6)
(WO 2007014290)、(15.89)N-甲基-2-(1-{[5-甲基-3-(三氟甲基)-1H-吡唑-1-基]乙酰基}哌啶-4-基)-N-[(1S)-1,2,3,4-四氢萘-1-基]-1,3-噻唑-4-甲酰胺(922514-48-5)
(WO 2007014290)、(15.90){6-[({[(1-甲基-1H-四唑-5-基)(苯基)亚甲基]氨基}氧基)甲基]吡啶-2-基}氨基甲酸戊酯、(15.91)吩嗪-1-甲酸、(15.92)8-羟基喹啉、(15.93)8-羟基喹啉硫酸盐(2:1)(134-31-6)和(15.94){6-[({[(1-甲基-1H-四唑-5-基)(苯基)亚甲基]氨基}氧基)甲基]吡啶-2-基}氨基甲酸叔丁酯。
(16)进一步的化合物,例如(16.1)1-甲基-3-(三氟甲基)-N-[2'-(三氟甲基)联苯-2-基]-1H-吡唑-4-甲酰胺、(16.2)N-(4'-氯联苯-2-基)-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺、(16.3)N-(2',4'-二氯联苯-2-基)-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺、(16.4)3-(二氟甲基)-1-甲基-N-[4'-(三氟甲基)联苯-2-基]-1H-吡唑-4-甲酰胺、(16.5)N-(2',5'-二氟联苯-2-基)-1-甲基-3-(三氟甲基)-1H-吡唑-4-甲酰胺、(16.6)3-(二氟甲基)-1-甲基-N-[4'-(丙-1-炔-1-基)联苯-2-基]-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.7)5-氟-1,3-二甲基-N-[4'-(丙-1-炔-1-基)联苯-2-基]-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.8)2-氯-N-[4'-(丙-1-炔-1-基)联苯-2-基]吡啶-3-甲酰胺(由WO 2004/058723已知)、(16.9)3-(二氟甲基)-N-[4'-(3,3-二甲基丁-1-炔-1-基)联苯-2-基]-1-甲基-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.10)N-[4'-(3,3-二甲基丁-1-炔-1-基)联苯-2-基]-5-氟-1,3-二甲基-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.11)3-(二氟甲基)-N-(4'-乙炔基联苯-2-基)-1-甲基-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.12)N-(4'-乙炔基联苯-2-基)-5-氟-1,3-二甲基-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.13)2-氯-N-(4'-乙炔基联苯-2-基)吡啶-3-甲酰胺(由WO 2004/058723已知)、(16.14)2-氯-N-[4'-(3,3-二甲基丁-1-炔-1-基)联苯-2-基]吡啶-3-甲酰胺(由WO 2004/058723已知)、(16.15)4-(二氟甲基)-2-甲基-N-[4'-(三氟甲基)联苯-2-基]-1,3-噻唑-5-甲酰胺(由WO 2004/058723已知)、(16.16)5-氟-N-[4'-(3-羟基-3-甲基丁-1-炔-1-基)联苯-2-基]-1,3-二甲基-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.17)2-氯-N-[4'-(3-羟基-3-甲基丁-1-炔-1-基)联苯-2-基]吡啶-3-甲酰胺(由WO 2004/058723已知)、(16.18)3-(二氟甲基)-N-[4'-(3-甲氧基-3-甲基丁-1-炔-1-基)联苯-2-基]-1-甲基-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.19)5-氟-N-[4'-(3-甲氧基-3-甲基丁-1-炔-1-基)联苯-2-基]-1,3-二甲基-1H-吡唑-4-甲酰胺(由WO 2004/058723已知)、(16.20)2-氯-N-[4'-(3-甲氧基-3-甲基丁-1-炔-1-基)联苯-2-基]吡啶-3-甲酰胺(由WO 2004/058723已知)、(16.21)(5-溴-2-甲氧基-4-甲基吡啶-3-基)(2,3,4-三甲氧基-6-甲基苯基)甲酮(由EP-A 1 559 320已知)、(16.22)N-[2-(4-{[3-(4-氯苯基)丙-2-炔-1-基]氧基}-3-甲氧基苯基)乙基]-N2-(甲基磺酰基)缬氨酰胺(220706-93-4)、(16.23)
4-氧代-4-[(2-苯乙基)氨基]丁酸和(16.24){6-[({[(Z)-(1-甲基-1H-四唑-5-基)(苯基)亚甲基]氨基}氧基)甲基]吡啶-2-基}氨基甲酸丁-3-炔-1-酯。
如果其官能团允许的话,(1)至(16)类所有指定的混合伴侣可以任选与合适的碱或酸形成盐。
可以提及的杀细菌剂的实例是:
溴硝丙二醇、双氯酚、氯啶、二甲二硫氨基甲酸镍、春雷霉素、辛噻酮、呋喃甲酸、土霉素、烯丙异噻唑、链霉素、叶枯酞、硫酸铜及其它铜制剂。
本文通过其“通用名”说明的活性组分是公知的并且例如描述于Pesticide Manual (“The Pesticide Manual”, 第14版, British Crop
Protection Council 2006)或者可以在互联网中检索到(例如http://www.alanwood.net/pesticides)。
(1)乙酰胆碱酯酶(AChE)抑制剂,例如
氨基甲酸酯,如棉铃威、涕灭威、恶虫威、丙硫克百威、丁酮威、丁酮砜威、甲萘威、克百威、丁硫克百威、乙硫苯威、仲丁威、伐虫脒、呋线威、异丙威、甲硫威、灭多威、速灭威、杀线威、抗蚜威、残杀威、硫双威、久效威、唑蚜威、混杀威、灭除威和灭杀威;或
有机磷酸盐,如乙酰甲胺磷、甲基吡噁磷、益棉磷、保棉磷、硫线磷、氯氧磷、毒虫畏、氯甲硫磷、毒死蜱、甲基毒死蜱、蝇毒磷、杀螟睛、甲基内吸磷、二嗪磷、敌敌畏/DDVP、百治磷、乐果、甲基毒虫畏、乙拌磷、苯硫磷、乙硫磷、灭线磷、伐灭磷、苯线磷、杀螟硫磷、倍硫磷、噻唑膦、庚烯磷、Imicyafos、异柳磷、O-(甲氧氨基硫代磷酰)水杨酸异丙酯、噁唑磷、马拉硫磷、灭蚜磷、甲胺磷、杀扑磷、速灭磷、久效磷、二溴磷、氧乐果、亚砜磷、对硫磷、甲基对硫磷、稻丰散、甲拌磷、伏杀硫磷、亚胺硫磷、磷胺、辛硫磷、甲基嘧啶磷、丙溴磷、胺丙畏、丙硫磷、吡唑硫磷、哒嗪硫磷、喹硫磷、治螟磷、丁基嘧啶磷、双硫磷、特丁硫磷、杀虫畏、甲基乙拌磷、三唑磷、敌百虫和蚜灭磷。
(2)GABA门控的氯通道拮抗剂,例如
环戊二烯有机氯,例如氯丹和硫丹;或
苯基吡唑(fiproles),例如乙虫腈和氟虫腈。
(3)钠通道调节剂/电压依赖的钠通道阻滞剂,例如
拟除虫菊酯,如氟丙菊酯、烯丙菊酯、右旋-顺式-反式烯丙菊酯、右旋-反式烯丙菊酯、联苯菊酯、生物烯丙菊酯、生物烯丙菊酯S-环戊烯异构体、生物苄呋菊酯、乙氰菊酯、氟氯氰菊酯、β-氟氯氰菊酯、三氯氟氰菊酯、λ-三氯氟氰菊酯、γ-三氯氟氰菊酯、氯氰菊酯、α-氯氰菊酯、β-氯氰菊酯、θ-氯氰菊酯、ζ-氯氰菊酯、苯氰菊酯[(1R)-反式异构体]、溴氰菊酯、右旋烯炔菊酯[(EZ)-(1R)异构体)、高氰戊菊酯、醚菊酯、甲氰菊酯、氰戊菊酯、氟氰戊菊酯、氟氯苯菊酯、氟胺氰菊酯、苄螨醚、炔咪菊酯、噻嗯菊酯、氯菊酯、苯醚菊酯[(1R)-反式异构体)、炔丙菊酯、除虫菊素(pyrethrum)、苄呋菊酯、氟硅菊酯、七氟菊酯、胺菊酯、胺菊酯[(1R)异构体)]、四溴菊酯和四氟苯菊酯;或
滴滴涕;或甲氧滴滴涕。
(4)烟碱乙酰胆碱受体(nAChR)激动剂,例如
新烟碱类,如啶虫脒、噻虫胺、呋虫胺、吡虫啉、烯啶虫胺、噻虫啉和噻虫嗪;或
烟碱。
(5)烟碱乙酰胆碱受体(nAChR)变构活化剂,例如
多杀菌素,如乙基多杀菌素和多杀霉素。
(6)氯通道活化剂,例如
阿维菌素/米尔贝霉素,如阿维菌素、甲氨基阿维菌素苯甲酸盐、雷皮菌素和密灭汀。
(7)保幼激素模拟物,例如
保幼激素类似物,如烯虫乙酯、烯虫炔酯和烯虫酯;或
苯氧威;或吡丙醚。
(8)多方面非特异性(多位点)抑制剂,例如
卤代烷类,如溴甲烷和其它卤代烷类;或
氯化苦;或硫酰氟;或硼砂;或吐酒石。
(9)选择性同翅昆虫进食阻滞剂,如吡蚜酮;或氟啶虫酰胺。
(10)螨生长抑制剂,如四螨嗪、噻螨酮和氟螨嗪;或
乙螨唑。
(11)昆虫中肠膜的微生物破坏剂,如苏云金芽孢杆菌以色列亚种(Bacillus
thuringiensis subspecies israelensis)、球形芽胞杆菌(Bacillus
sphaericus)、苏云金芽孢杆菌鲇泽亚种(Bacillus thuringiensis subspecies
aizawai)、苏云金芽孢杆菌库斯塔克亚种(Bacillus thuringiensis subspecies
kurstaki)、苏云金芽胞杆菌拟步行甲亚种(Bacillus thuringiensis subspecies
tenebrionis)和BT作物蛋白:Cry1Ab、Cry1Ac、Cry1Fa、Cry2Ab、mCry3A、Cry3Ab、Cry3Bb、Cry34/35Ab1。
(12)线粒体ATP合酶抑制剂,例如丁醚脲;或
有机锡杀螨剂,如三唑锡、三环锡和苯丁锡;或
快螨特;或三氯杀螨砜。
(13)经破坏质子梯度的氧化磷酸化解偶联剂,如虫螨腈、二硝酚和氟虫胺。
(14)烟碱乙酰胆碱受体(nAChR)通道阻断剂,例如杀虫磺、杀螟丹氢氯化物、杀虫环和杀虫双。
(15)0型壳多糖生物合成抑制剂,例如双三氟虫脲、氟啶脲、除虫脲、氟环脲、氟虫脲、氟铃脲、虱螨脲、氟酰脲、多氟脲、氟苯脲和杀铃脲。
(16)1型壳多糖生物合成抑制剂,例如噻嗪酮。
(17)蜕皮破坏剂,例如灭蝇胺。
(18)蜕皮激素受体激动剂,例如环虫酰肼、氯虫酰肼、甲氧虫酰肼和虫酰肼。
(19)章鱼胺受体激动剂,例如双甲脒。
(20)线粒体复合物III电子传递抑制剂,例如氟蚁腙;或灭螨醌;或嘧螨酯。
(21)线粒体复合物I电子传递抑制剂,例如
METI杀螨剂,如喹螨醚、唑螨酯、嘧螨醚、哒螨灵、吡螨胺和唑虫酰胺;或
鱼藤酮(鱼藤属)。
(22)电压依赖的钠通道阻断剂,如茚虫威;或氰氟虫腙。
(23)乙酰辅酶A羧化酶抑制剂,例如
特窗酸和特特拉姆酸衍生物,如螺螨酯、螺甲螨酯和螺虫乙酯。
(24)线粒体复合物IV电子传递抑制剂,例如
膦,如磷化铝、磷化钙、磷化氢和磷化锌;或
氰化物。
(25)线粒体复合物II电子传递抑制剂,例如腈吡螨酯。
(28)利阿诺定受体调节剂,例如
二酰胺,如氯虫苯甲酰胺、氰虫酰胺和氟虫酰胺。
具有未知的或不确定的作用方式的其它的活性成分,例如磺胺螨酯、印楝素、Benclothiaz、苯螨特、联苯肼酯、溴螨酯、灭螨猛、冰晶石、溴氰虫酰胺(Cyazypyr)、丁氟螨酯、三氯杀螨醇、氟螨嗪、Fluensulfone、嘧虫胺、丁烯氟虫腈、氟吡菌酰胺、呋喃虫酰肼、氯噻啉、异菌脲、氯氟醚菊酯、三氟甲吡醚、Pyrifluquinazon、四氟醚菊酯和碘甲烷;基于坚硬芽胞杆菌(Bacillus firmus)(包括但不限于菌株CNCM I-1582,如,例如,VOTiVO™,BioNem)的其它产品或一种以下公知的活性化合物:3-溴-N-{2-溴-4-氯-6-[(1-环丙基乙基)氨基甲酰基]苯基}-1-(3-氯吡啶-2-基)-1H-吡唑-5-甲酰胺(由WO2005/077934已知)、4-{[(6-溴吡啶-3-基)甲基](2-氟乙基)氨基}呋喃-2(5H)-酮(由WO2007/115644已知)、4-{[(6-氟吡啶-3-基)甲基](2,2-二氟乙基)氨基}呋喃-2(5H)-酮(由WO2007/115644已知)、4-{[(2-氯-1,3-噻唑-5-基)甲基](2-氟乙基)氨基}呋喃-2(5H)-酮(由WO2007/115644已知)、4-{[(6-氯吡啶-3-基)甲基](2-氟乙基)氨基}呋喃-2(5H)-酮(由WO2007/115644已知)、Flupyradifurone、4-{[(6-氯-5-氟吡啶-3-基)甲基](甲基)氨基}呋喃-2(5H)-酮(由WO2007/115643已知)、4-{[(5,6-二氯吡啶-3-基)甲基](2-氟乙基)氨基}呋喃-2(5H)-酮(由WO2007/115646已知)、4-{[(6-氯-5-氟吡啶-3-基)甲基](环丙基)氨基}呋喃-2(5H)-酮(由WO2007/115643已知)、4-{[(6-氯吡啶-3-基)甲基](环丙基)氨基}呋喃-2(5H)-酮(由EP-A-0 539 588已知)、4-{[(6-氯吡啶-3-基)甲基](甲基)氨基}呋喃-2(5H)-酮(由EP-A-0 539 588已知)、{[1-(6-氯吡啶-3-基)乙基](甲基)氧化-λ4-亚硫烷基}氨腈(由WO2007/149134已知)及其非对映异构体{[(1R)-1-(6-氯吡啶-3-基)乙基](甲基)氧化-λ4-亚硫烷基}氨腈 (A)和{[(1S)-1-(6-氯吡啶-3-基)乙基](甲基)氧化-λ4-亚硫烷基}氨腈 (B) (也由WO2007/149134已知)以及氟啶虫胺腈及其非对映异构体:称为非对映异构体组A(由WO2010/074747、WO2010/074751已知)的[(R)-甲基(氧化){(1R)-1-[6-(三氟甲基)吡啶-3-基]乙基}-λ4-亚硫烷基]氨腈 (A1) 和[(S)-甲基(氧化){(1S)-1-[6-(三氟甲基)吡啶-3-基]乙基}-λ4-亚硫烷基]氨腈 (A2)、称为非对映异构体组B(也由WO2010/074747、WO2010/074751已知)的[(R)-甲基(氧化){(1S)-1-[6-(三氟甲基)吡啶-3-基]乙基}-λ4-亚硫烷基]氨腈 (B1) 和[(S)-甲基(氧化){(1R)-1-[6-(三氟甲基)吡啶-3-基]乙基}-λ4-亚硫烷基]氨腈 (B2)、和11-(4-氯-2,6-二甲基苯基)-12-羟基-1,4-二氧杂-9-氮杂二螺[4.2.4.2]十四-11-烯-10-酮(由WO2006/089633已知)、3-(4'-氟-2,4-二甲基联苯-3-基)-4-羟基-8-氧杂-1-氮杂螺[4.5]癸-3-烯-2-酮(由WO2008/067911已知)、1-{2-氟-4-甲基-5-[(2,2,2-三氟乙基)亚硫酰基]苯基}-3-(三氟甲基)-1H-1,2,4-三唑-5-胺(由WO2006/043635已知)、[(3S,4aR,12R,12aS,12bS)-3-[(环丙基羰基)氧基]-6,12-二羟基-4,12b-二甲基-11-氧代-9-(吡啶-3-基)-1,3,4,4a,5,6,6a,12,12a,12b-十氢-2H,11H-苯并[f]吡喃并[4,3-b]苯并吡喃-4-基]甲基环丙烷甲酸酯(由WO2008/066153已知)、2-氰基-3-(二氟甲氧基)-N,N-二甲基苯磺酰胺(由WO2006/056433已知)、2-氰基-3-(二氟甲氧基)-N-甲基苯磺酰胺(由WO2006/100288已知)、2-氰基-3-(二氟甲氧基)-N-乙基苯磺酰胺(由WO2005/035486已知)、4-(二氟甲氧基)-N-乙基-N-甲基-1,2-苯并噻唑-3-胺1,1-二氧化物(由WO2007/057407已知)、N-[1-(2,3-二甲基苯基)-2-(3,5-二甲基苯基)乙基]-4,5-二氢-1,3-噻唑-2-胺(由WO2008/104503已知)、{1'-[(2E)-3-(4-氯苯基)丙-2-烯-1-基]-5-氟螺[吲哚-3,4'-哌啶]-1(2H)-基}(2-氯吡啶-4-基)甲酮(由WO2003/106457已知)、3-(2,5-二甲基苯基)-4-羟基-8-甲氧基-1,8-二氮杂螺[4.5]癸-3-烯-2-酮(由WO2009/049851已知)、3-(2,5-二甲基苯基)-8-甲氧基-2-氧代-1,8-二氮杂螺[4.5]癸-3-烯-4-基乙基碳酸酯(由WO2009/049851已知)、4-(丁-2-炔-1-基氧基)-6-(3,5-二甲基哌啶-1-基)-5-氟嘧啶(由WO2004/099160已知)、(2,2,3,3,4,4,5,5-八氟戊基)(3,3,3-三氟丙基)丙二腈(由WO2005/063094已知)、(2,2,3,3,4,4,5,5-八氟戊基)(3,3,4,4,4-五氟丁基)丙二腈(由WO2005/063094已知)、8-[2-(环丙基甲氧基)-4-(三氟甲基)苯氧基]-3-[6-(三氟甲基)哒嗪-3-基]-3-氮杂双环[3.2.1]辛烷(由WO2007/040280已知)、Flometoquin、PF1364
(CAS-Reg.No. 1204776-60-2) (由JP2010/018586已知)、5-[5-(3,5-二氯苯基)-5-(三氟甲基)-4,5-二氢-1,2-噁唑-3-基]-2-(1H-1,2,4-三唑-1-基)苄腈(由WO2007/075459已知)、5-[5-(2-氯吡啶-4-基)-5-(三氟甲基)-4,5-二氢-1,2-噁唑-3-基]-2-(1H-1,2,4-三唑-1-基)苄腈(由WO2007/075459已知)、4-[5-(3,5-二氯苯基)-5-(三氟甲基)-4,5-二氢-1,2-噁唑-3-基]-2-甲基-N-{2-氧代-2-[(2,2,2-三氟乙基)氨基]乙基}苯甲酰胺(由WO2005/085216已知)、4-{[(6-氯吡啶-3-基)甲基](环丙基)氨基}-1,3-噁唑-2(5H)-酮、4-{[(6-氯吡啶-3-基)甲基](2,2-二氟乙基)氨基}-1,3-噁唑-2(5H)-酮、4-{[(6-氯吡啶-3-基)甲基](乙基)氨基}-1,3-噁唑-2(5H)-酮、4-{[(6-氯吡啶-3-基)甲基](甲基)氨基}-1,3-噁唑-2(5H)-酮(均由WO2010/005692已知)、NNI-0711 (由WO2002/096882已知)、1-乙酰基-N-[4-(1,1,1,3,3,3-六氟-2-甲氧基丙烷-2-基)-3-异丁基苯基]-N-异丁酰基-3,5-二甲基-1H-吡唑-4-甲酰胺(由WO2002/096882已知)、2-[2-({[3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-基]羰基}氨基)-5-氯-3-甲基苯甲酰基]-2-甲基肼甲酸甲酯(由WO2005/085216已知)、2-[2-({[3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-基]羰基}氨基)-5-氰基-3-甲基苯甲酰基]-2-乙基肼甲酸甲酯(由WO2005/085216已知)、2-[2-({[3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-基]羰基}氨基)-5-氰基-3-甲基苯甲酰基]-2-甲基肼甲酸甲酯(由WO2005/085216已知)、2-[3,5-二溴-2-({[3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-基]羰基}氨基)苯甲酰基]-1,2-二乙基肼甲酸甲酯(由WO2005/085216已知)、2-[3,5-二溴-2-({[3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-基]羰基}氨基)苯甲酰基]-2-乙基肼甲酸甲酯(由WO2005/085216已知)、(5RS,7RS;5RS,7SR)-1-(6-氯-3-吡啶基甲基)-1,2,3,5,6,7-六氢-7-甲基-8-硝基-5-丙氧基咪唑并[1,2-a]吡啶 (由WO2007/101369已知)、N-[2-(5-氨基-1,3,4-噻二唑-2-基)-4-氯-6-甲基苯基]-3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-甲酰胺(由CN102057925已知)和2-[3,5-二溴-2-({[3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-基]羰基}氨基)苯甲酰基]-2-乙基-1-甲基肼甲酸甲酯(由WO2011/049233已知)。
可以提及的杀软体动物剂的实例是四聚乙醛和甲硫威。
可以提及的安全剂的实例是:
(1)杂环羧酸衍生物,例如二氯苯基吡唑啉-3-羧酸衍生物,如由WO 91/07874已知的1-(2,4-二氯苯基)-5-(乙氧基羰基)-5-甲基-4,5-二氢-1H-吡唑-3-甲酸、1-(2,4-二氯苯基)-4,5-二氢-5-甲基-1H-吡唑-3,5-二甲酸二乙酯(“吡唑解草酯”)和类似化合物;例如二氯苯基吡唑羧酸衍生物,如由EP-A 0 333 131和EP-A 0 269 806已知的1-(2,4-二氯苯基)-5-甲基-1H-吡唑-3-甲酸乙酯、1-(2,4-二氯苯基)-5-异丙基-1H-吡唑-3-甲酸乙酯、5-叔-丁基-1-(2,4-二氯苯基)-1H-吡唑-3-甲酸乙酯和类似化合物;例如1,5-二苯基吡唑-3-羧酸衍生物,如由EP-A 0 268 554已知的1-(2,4-二氯苯基)-5-苯基-1H-吡唑-3-甲酸乙酯、1-(2-氯苯基)-5-苯基-1H-吡唑-3-甲酸甲酯和类似化合物;例如三唑羧酸衍生物,如由EP-A
0 174 562和EP-A
0 346 620已知的解草唑、正解草唑和类似化合物;例如2-异噁唑啉-3-羧酸衍生物,如由WO 91/08202已知的5-(2,4-二氯苄基)-4,5-二氢-1,2-噁唑-3-甲酸乙酯、5-苯基-4,5-二氢-1,2-噁唑-3-甲酸乙酯和类似化合物、或由WO 95/07897已知的5,5-二苯基-4,5-二氢-1,2-噁唑-3-甲酸、5,5-二苯基-4,5-二氢-1,2-噁唑-3-甲酸乙酯(“双苯噁唑酸”)、5,5-二苯基-4,5-二氢-1,2-噁唑-3-甲酸丙酯、5-(4-氟苯基)-5-苯基-4,5-二氢-1,2-噁唑-3-甲酸乙酯。
(2)8-羟基喹啉的衍生物,例如(喹啉-8-基氧基)乙酸的衍生物,如由EP-A 0 086 750、EP-A 0 094 349、EP-A
0 191 736或EP-A 0 492 366已知的[(5-氯喹啉-8-基)氧基]乙酸庚-2-酯(“解毒喹”)、[(5-氯喹啉-8-基)氧基]乙酸4-甲基戊-2-酯、[(5-氯喹啉-8-基)氧基]乙酸4-(烯丙氧基)丁酯、[(5-氯喹啉-8-基)氧基]乙酸1-(烯丙氧基)丙-2-酯、[(5-氯喹啉-8-基)氧基]乙酸乙酯、[(5-氯喹啉-8-基)氧基]乙酸甲酯、[(5-氯喹啉-8-基)氧基]乙酸烯丙酯、[(5-氯喹啉-8-基)氧基]乙酸2-{[亚丙基氨基]氧基}乙酯、[(5-氯喹啉-8-基)氧基]乙酸2-氧丙酯和类似的化合物,以及[(5-氯喹啉-8-基)氧基]乙酸、它的水合物和盐,如由WO 02/34048已知的锂、钠、钾、钙、镁、铝、铁、铵、季铵、锍或鏻盐;例如[(5-氯喹啉-8-基)氧基]丙二酸的衍生物,如由EP-A 0 582 198已知的[(5-氯喹啉-8-基)氧基]丙二酸二乙酯、[(5-氯喹啉-8-基)氧基]丙二酸二烯丙酯、[(5-氯喹啉-8-基)氧基]丙二酸乙基甲酯和类似的化合物。
(3)二氯乙酰胺,其通常用作出芽前安全剂(土壤活性安全剂),如“二氯丙烯胺”(N,N-二烯丙基-2,2-二氯乙酰胺)、Stauffer公司的“R-29148”(3二氯乙酰基-2,2,5-三甲基-1,3-噁唑烷)和“R-28725”(3-二氯乙酰基-2,2-二甲基-1,3-噁唑烷)、“解草嗪”(4 - 二氯乙酰基-3,4-二氢-3-甲基-2H-1,4-苯并噁嗪)、PPG Industries的“PPG-1292”(N-烯丙基-N-[(1,3-二氧杂环戊烷-2-基)-甲基]-二氯乙酰胺)、Sagro-Chem的“DKA-24”(N-烯丙基-N-[(烯丙基氨基羰基)甲基]-二氯乙酰胺)、Nitrokemia和Monsanto的“AD-67”或“MON4660”(3-二氯乙酰基-1-氧杂-3-氮杂-螺[4,5]癸烷)、TRI-Chemical RT的“TI-35”(1-二氯乙酰基-氮杂环庚烷)、BASF的“diclonon”(dicyclonon)或“BAS145138”或“LAB145138”(3-二氯乙酰基-2,5,5-三甲基-1,3-二氮杂双环[4.3.0]壬烷)、“Furilazol”或“MON13900”[(RS)-3-二氯乙酰基-5-(2-呋喃基)-2,2-二甲基噁唑烷]以及其(R)-异构体。
(4)酰基磺酰胺,例如式(II)的N-酰基磺酰胺
或其盐(由WO 97/45016已知),其中
R1表示(C1-C6)烷基,其是未取代的或被选自卤素、(C1-C4)烷氧基、(C1-C6)卤代烷氧基和(C1-C4)烷硫基的取代基单取代至三取代;
R2表示卤素、(C1-C4)烷基、(C1-C4)烷氧基、CF3;
m是1或2;
或例如式(III)的4-(苯甲酰基氨磺酰基)苯甲酰胺
或其盐(由WO 99/16744已知),其中
R3、R4互相独立地表示氢、(C1-C6)烷基、(C3-C6)烯基、(C3-C6)炔基、(C3-C6)环烷基,
R5表示卤素、(C1-C4)烷基、(C1-C4)卤代烷基或(C1-C4)烷氧基
n是1或2,
具体是式(III)的化合物,其中
R3 = 环丙基、R4 = 氢并且R5 n = 2-OMe,(“环丙磺酰胺”),
R3 = 环丙基、R4 = 氢并且R5 n = 5-Cl-2-OMe,
R3 = 乙基、R4 = 氢并且R5 n = 2-OMe,
R3 = 异丙基、R4 = 氢并且R5 n = 5-Cl-2-OMe,
R3 = 异丙基、R4 = 氢并且R5 n = 2-OMe,
或例如式(IV)的苯甲酰基氨磺酰基苯基脲
(由EP-A 0 365 484已知),其中
R6、R7互相独立地表示氢、(C1-C8)烷基、(C3-C6)烯基、(C3-C6)炔基,
R8表示卤素、(C1-C4)烷基、(C1-C4)烷氧基、CF3
r是1或2;
具体是
1-[4-(N-2-甲氧基苯甲酰基氨磺酰基)苯基]-3-甲基脲、
1-[4-(N-2-甲氧基苯甲酰基氨磺酰基)苯基]-3,3-二甲基脲、
1-[4-(N-4,5-二甲基苯甲酰基氨磺酰基)苯基]-3-甲基脲。
(5)羟基芳香族化合物和芳香族-脂肪族羧酸衍生物,如3,4,5-三乙酸基苯甲酸乙酯、4-羟基-3,5-二甲氧基苯甲酸、3,5-二羟基苯甲酸、2,4-二羟基苯甲酸、4-氟-2-羟基苯甲酸、2-羟基肉桂酸、2,4-二氯肉桂酸(参见WO 2004/084631、WO 2005/015994、WO
2005/016001)。
(6)1,2-二氢喹喔啉-2-酮,如1-甲基-3-(2-噻吩基)-1,2-二氢喹喔啉-2-酮、1-甲基-3-(2-噻吩基)-1,2-二氢喹喔啉-2-硫铜、1-(2-氨基乙基)-3-(2-噻吩基)-1,2-二氢喹喔啉-2-酮氢氯化物、1-(2-甲基磺酰基氨基乙基)-3-(2-噻吩基)-1,2-二氢喹喔啉-2-酮(参见WO 2005/112630)。
(7)二苯基甲氧基乙酸衍生物,如(二苯基甲氧基)乙酸甲酯(CAS-Reg.
No. 41858-19-9)、(二苯基甲氧基)乙酸乙酯或(二苯基甲氧基)乙酸(参见WO 98/38856)。
(8)式(V)的化合物
或其盐(由WO 98/27049已知),其中
R9代表卤素、(C1-C4)烷基、(C1-C4)卤代烷基、(C1-C4)烷氧基、(C1-C4)卤代烷氧基,
R10代表氢或(C1-C4)烷基,
R10代表氢,在每一种情况下为未取代或单取代至三取代的(C1-C8)烷基、(C2-C4)烯基、(C2-C4)炔基或芳基,其中取代基选自卤素和(C1-C8)烷氧基,
s是0、1或2。
(9)
3-(5-四唑基羰基)-2-喹诺酮,如1,2-二氢-4-羟基-1-乙基-3-(5-四唑基羰基)-2-喹诺酮 (CAS-Reg. No. 219479-18-2)、1,2-二氢-4-羟基-1-甲基-3-(5-四唑基羰基)-2-喹诺酮 (CAS-Reg. No.
95855-00-8) (参见WO 99/00020)。
(10)
式(VI-a)和(VI-b)的化合物
(由WO 2007/023719和WO 2007/023764已知),其中
R12表示卤素、(C1-C4)烷基、甲氧基、硝基、氰基、CF3、OCF3,
Y、Z独立地表示O或S,
t是0、1、2、3或4,
R13表示(C1-C16)烷基、(C2-C6)烯基、芳基、苄基、卤代苄基,
R14表示氢或(C1-C6)烷基,
(11) 氧代亚氨基化合物,公知作为种子处理剂,如“解草腈” [(Z)-1,3-二氧杂环戊烷-2-基甲氧基亚胺基(苯基)乙腈]、“氟草肟” [1-(4-氯苯基)-2,2,2-三氟-1-乙酮-O-(1,3-二氧戊环-2-基甲基)-肟]和“解草胺腈”或“CGA-43089” [(Z)-氰基甲氧基亚胺基(苯基)乙腈],均已知为用于高粱抵抗异丙甲草胺损伤的种子处理安全剂。
(12)
异硫代苯并二氢吡喃酮,如由WO 98/13361已知的[(3-氧代-1H-2-苯并噻喃-4(3H)-亚基)甲氧基]乙酸甲酯(CAS-Reg. No.
205121-04-6)和类似的化合物。
(13)选自下列的化合物:“萘酐”(1,8-萘二甲酸酐),其已知为用于玉米(玉米)抵抗硫代氨基甲酸酯除草剂损伤的种子处理安全剂、“解草啶”(4,6-二氯-2-苯基嘧啶),其已知为用于播种的稻抵抗丙草胺损伤的种子处理安全剂、“解草胺”(苄基-2-氯-4-三氟甲基-1,3-噻唑-5-甲酸酯),其已知为用于高粱抵抗甲草胺和异丙甲草胺损伤的种子处理安全剂、American Cyanamid的“CL 304415” (CAS-Reg. No.
31541-57-8)(4-羧基-3,4-二氢-2H-1-苯并吡喃-4-乙酸),其已知为用于玉米(玉米)抵抗咪唑啉酮损伤的安全剂、Nitrokemia的“MG
191” (CAS-Reg. No. 96420-72-3) (2-二氯甲基-2-甲基-1,3-二氧杂环戊烷),已知为用于玉米(玉米)的安全剂、Nitrokemia的“MG-838” (CAS-Reg. No.
133993-74-5)(2-丙烯基1-氧杂-4-氮杂螺[4.5]癸烷-4-二硫代甲酸酯) 、“乙拌磷” (O,O-二乙基-S-2-乙基硫代乙基二硫代磷酸酯) 、“增效磷” (O,O-二乙基-O-苯基硫代磷酸酯) 、“mephenate”(4-氯苯基-甲基氨基甲酸酯)。
(14)除了除草剂活性之外在作物如稻中还具有安全剂活性的化合物,如“哌草丹”或“MY-93” (S-1-甲基-1-苯乙基-哌啶-1-硫代甲酸酯),其已知为用于稻抵抗禾草敌损伤的安全剂、“杀草隆”或“SK 23” [1-(1-甲基-1-苯乙基)-3-p-甲苯基-脲],其已知为用于稻抵抗唑吡嘧磺隆损伤的安全剂、“苄草隆” = “JC-940” [3-(2-氯苯基甲基)-1-(1-甲基-1-苯基-乙基)脲] (参见JP-A 60-087254),其已知为用于稻抵抗某些除草剂损伤的安全剂、“苯草酮”或“NK 049” (3,3'-二甲基-4-甲氧基-二苯甲酮),其已知为用于稻抵抗某些除草剂损伤的安全剂、Kumiai的“CSB” [1-溴-4-(氯甲基磺酰基)苯](CAS-Reg. No.
54091-06-4),其已知为用于稻抵抗某些除草剂损伤的安全剂。
(15)主要用作除草剂但也在某些作物中具有安全剂活性的化合物,如(2,4-二氯苯氧基)乙酸(2,4-D)、(4-氯苯氧基)乙酸、(R,S)-2-(4-氯-邻-甲苯基氧基)丙酸(2-甲-4-氯丙酸)、4-(2,4-二氯苯氧基)丁酸(2,4-DB)、(4-氯-邻-甲苯基氧基)乙酸(MCPA)、4-(4 - 氯 - 邻-甲苯基氧基)丁酸、4-(4-氯苯氧基)丁酸、3,6-二氯-2-甲氧基苯甲酸(麦草畏)、1-(乙氧基羰基)乙基-1,6 - 二氯-2-甲氧基苯甲酸酯(lactidichlor-ethyl)。
可以提及的植物生长调节剂的实例是矮壮素和乙烯利。
可以提及的植物营养物的实例是用于向植物提供大量和/或微量营养素的常规无机或有机肥料。
在优选实施方式中,本发明涉及包含氟吡菌酰胺和一种或多种以下杀虫剂的组合物的用途:
氨基甲酸酯,优选涕灭威、甲硫威、杀线威和硫双威;
有机磷酸盐,优选苯线磷、噻唑膦、灭线磷、Imicyafos;
Fiproles,优选氟虫腈和乙虫腈;
Chlornicotinyls(新烟碱类杀虫剂),优选吡虫啉、噻虫胺、噻虫啉和噻虫嗪;
拟除虫菊酯,优选β-氟氯氰菊酯、λ-三氯氟氰菊酯、溴氰菊酯、七氟菊酯、四氟苯菊酯;
利阿诺定受体调节剂(Anthranilamids),优选Rynaxypyr(氯虫苯甲酰胺)、Cyazypyr(Cyantraniliprole);
Macrolids (多杀霉素类),优选刺糖菌素、乙基多杀菌素;
阿维菌素/米尔贝霉素,优选阿维菌素;
特窗酸和特特拉姆酸衍生物(Ketoenols),优选螺虫乙酯、螺螨酯和螺甲螨酯。
多方面非特异性(多位点)抑制剂,优选氟啶虫酰胺。
具有未知的或不确定的作用方式的活性成分,优选4-[(2,2-二氯乙基)氨基]呋喃-2(5H)-酮-2-氯-5-乙基吡啶(1:1)、氟啶虫胺腈。
在优选实施方式中,本发明涉及包含氟吡菌酰胺和一种或多种以下杀真菌剂的组合物的用途
(2.1)联苯吡菌胺(581809-46-3)、(2.2)啶酰菌胺(188425-85-6)、(2.8)氟唑菌酰胺(907204-31-3)、(2.9)(2.11)萘吡菌胺(同侧差向异构外消旋体1RS,4SR,9RS和异侧差向异构外消旋体1RS,4SR,9SR的混合物)(881685-58-1)、(2.12)萘吡菌胺(异侧差向异构外消旋体1RS,4SR,9SR)、(2.13)萘吡菌胺(异侧差向异构外消旋体1R,4S,9S)、(2.14)萘吡菌胺(异侧差向异构外消旋体1S,4R,9R)、(2.15)萘吡菌胺(同侧差向异构外消旋体1RS,4SR,9RS)、(2.16)萘吡菌胺(同侧差向异构外消旋体1R,4S,9R)、(2.17)萘吡菌胺(同侧差向异构外消旋体1S,4R,9S)、(2.20)戊苯吡菌胺(494793-67-8)、(2.21)吡噻菌胺(183675-82-3)、(2.22)环丙吡菌胺(874967-67-6)、(2.23)噻氟菌胺(130000-40-7)、(2.24)1-甲基-N-[2-(1,1,2,2-四氟乙氧基)苯基]-3-(三氟甲基)-1H-吡唑-4-甲酰胺、(2.25)3-(二氟甲基)-1-甲基-N-[2-(1,1,2,2-四氟乙氧基)苯基]-1H-吡唑-4-甲酰胺、(2.26)3-(二氟甲基)-N-[4-氟-2-(1,1,2,3,3,3-六氟丙氧基)苯基]-1-甲基-1H-吡唑-4-甲酰胺、(2.27)N-[1-(2,4-二氯苯基)-1-甲氧基丙烷-2-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺(1092400-95-7)(WO
2008148570)、(2.28)5,8-二氟-N-[2-(2-氟-4-{[4-(三氟甲基)吡啶-2-基]氧基}苯基)乙基]喹唑啉-4-胺(1210070-84-0)(WO2010025451)、(2.29)N-[9-(二氯亚甲基)-1,2,3,4-四氢-1,4-桥亚甲基萘-5-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺、(2.30) N-[(1S,4R)-9-(二氯亚甲基)-1,2,3,4-四氢-1,4-桥亚甲基萘-5-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺和(2.31) N-[(1R,4S)-9-(二氯亚甲基)-1,2,3,4-四氢-1,4-桥亚甲基萘-5-基]-3-(二氟甲基)-1-甲基-1H-吡唑-4-甲酰胺、(7.7)嘧霉胺(53112-28-0)、(3.22)三氟敏(141517-21-7)。
在本发明中,“防治”表示与未处理作物相比,线虫侵袭的预防性或治愈性的降低,更优选基本抵制了侵袭,最优选完全抑制了侵袭。
病害系统
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治咖啡中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:最短尾短体线虫、咖啡短体线虫、短小根结线虫、南方根结线虫、咖啡根结线虫、螺旋线虫属以及Meloidogyne
paranaensis、盘旋线虫属、剑线虫属、矮化线虫属、盾线虫属。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治马铃薯中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:最短尾短体线虫、草地短体线虫、斯克里布纳短体线虫、穿刺短体线虫、咖啡短体线虫、鳞球茎茎线虫以及艾伦短体线虫、安第斯短体线虫、Pratylenchus
cerealis、刻痕短体线虫、六裂短体线虫、卢斯短体线虫、落选短体线虫、光滑短体线虫、桑尼短体线虫、伤残短体线虫、长尾刺线虫、圆桶毛刺线虫、原始毛刺线虫、Trichodorusproximus、相似毛刺线虫、Trichodorussparsus、较小拟毛刺线虫、葱属拟毛刺线虫、短小拟毛刺线虫、光滑拟毛刺线虫、花生根结线虫、北方根结线虫、泰晤士根结线虫、南方根结线虫、奇特伍德根结线虫、爪哇根结线虫、异常珍珠线虫、Globoderarostochiensis、马铃薯白线虫、马铃薯茎线虫、香蕉穿孔线虫、肾形肾状线虫、Neotylenchusvigissi、假墙草异滑刃线虫、草莓滑刃线虫、Meloinemaspp.。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治番茄中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:花生根结线虫、北方根结线虫、爪哇根结线虫、南方根结线虫、穿刺短体线虫以及最短尾短体线虫、咖啡短体线虫、斯克里布纳短体线虫、伤残短体线虫、较小拟毛刺线虫、短小根结线虫、异常珍珠线虫、Globoderasolanacearum、Dolichodorusheterocephalus、肾形肾状线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治番茄中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:螺旋线虫属、花生根结线虫、北方根结线虫、爪哇根结线虫、南方根结线虫、穿刺短体线虫以及最短尾短体线虫、咖啡短体线虫、斯克里布纳短体线虫、伤残短体线虫、较小拟毛刺线虫、短小根结线虫、异常珍珠线虫、Globoderasolanacearum、Dolichodorusheterocephalus、肾形肾状线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治胡椒中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:最短尾短体线虫、草地短体线虫、斯克里布纳短体线虫、穿刺短体线虫、咖啡短体线虫、鳞球茎茎线虫以及艾伦短体线虫、安第斯短体线虫、Pratylenchuscerealis、刻痕短体线虫、六裂短体线虫、卢斯短体线虫、落选短体线虫、光滑短体线虫、桑尼短体线虫、伤残短体线虫、长尾刺线虫、圆桶毛刺线虫、原始毛刺线虫、Trichodorusproximus、相似毛刺线虫、Trichodorussparsus、较小拟毛刺线虫、葱属拟毛刺线虫、短小拟毛刺线虫、光滑拟毛刺线虫、花生根结线虫、北方根结线虫、泰晤士根结线虫、南方根结线虫、奇特伍德根结线虫、爪哇根结线虫、异常珍珠线虫、Globoderarostochiensis、马铃薯白线虫、马铃薯茎线虫、香蕉穿孔线虫、肾形肾状线虫、Neotylenchusvigissi、假墙草异滑刃线虫、草莓滑刃线虫、Meloinemaspp.。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治胡萝卜中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:最短尾短体线虫、草地短体线虫、斯克里布纳短体线虫、穿刺短体线虫、咖啡短体线虫、鳞球茎茎线虫以及艾伦短体线虫、安第斯短体线虫、Pratylenchuscerealis、刻痕短体线虫、六裂短体线虫、卢斯短体线虫、落选短体线虫、光滑短体线虫、桑尼短体线虫、伤残短体线虫、长尾刺线虫、圆桶毛刺线虫、原始毛刺线虫、Trichodorusproximus、相似毛刺线虫、Trichodorussparsus、较小拟毛刺线虫、葱属拟毛刺线虫、短小拟毛刺线虫、光滑拟毛刺线虫、花生根结线虫、北方根结线虫、泰晤士根结线虫、南方根结线虫、奇特伍德根结线虫、爪哇根结线虫、异常珍珠线虫、Globoderarostochiensis、马铃薯白线虫、马铃薯茎线虫、香蕉穿孔线虫、肾形肾状线虫、Neotylenchusvigissi、假墙草异滑刃线虫、草莓滑刃线虫、Meloinemaspp.。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治洋葱中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:最短尾短体线虫、草地短体线虫、斯克里布纳短体线虫、穿刺短体线虫、咖啡短体线虫、鳞球茎茎线虫以及艾伦短体线虫、安第斯短体线虫、Pratylenchuscerealis、刻痕短体线虫、六裂短体线虫、卢斯短体线虫、落选短体线虫、光滑短体线虫、桑尼短体线虫、伤残短体线虫、长尾刺线虫、圆桶毛刺线虫、原始毛刺线虫、Trichodorusproximus、相似毛刺线虫、Trichodorussparsus、较小拟毛刺线虫、葱属拟毛刺线虫、短小拟毛刺线虫、光滑拟毛刺线虫、花生根结线虫、北方根结线虫、泰晤士根结线虫、南方根结线虫、奇特伍德根结线虫、爪哇根结线虫、异常珍珠线虫、Globoderarostochiensis、马铃薯白线虫、马铃薯茎线虫、香蕉穿孔线虫、肾形肾状线虫、Neotylenchusvigissi、假墙草异滑刃线虫、草莓滑刃线虫、Meloinemaspp.。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治葫芦中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:花生根结线虫、北方根结线虫、爪哇根结线虫、南方根结线虫、肾形肾状线虫以及桑尼短体线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治葫芦中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:花生根结线虫、北方根结线虫、爪哇根结线虫、肾形肾状线虫以及桑尼短体线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治棉花中线虫特别有效,所述线虫属于至少一个选自以下植物寄生性线虫的种:长尾刺线虫、南方根结线虫、哥伦布纽带线虫、盔形纽带线虫、肾形肾状线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治玉米中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:长尾刺线虫、较小拟毛刺线虫以及最短尾短体线虫、德拉特短体线虫、六裂短体线虫、穿刺短体线虫、玉米短体线虫、Belonolaimus
gracilis、Belonolaimus nortoni、Longidorus breviannulatus、花生根结线虫、Meloidogyne arenaria thamesi、禾本科根结线虫、南方根结线虫、Meloidogyne incognita acrita、爪哇根结线虫、纳西根结线虫、燕麦胞囊线虫、水稻胞囊线虫、玉米胞囊线虫、墨西哥玉米胞囊线虫、鳞球茎茎线虫、Hoplolaimus
aegyptii、Hoplolaimus magnistylus、盔形纽带线虫、印度纽带线虫、双角螺旋线虫、双宫螺旋线虫、假强壮螺旋线虫、美洲剑线虫、Dolichodorus
heterocephalus、装饰小环线虫、Criconemella
onoensis、香蕉穿孔线虫、Rotylenchulus borealis、小肾状线虫、农田矮化线虫、清亮矮化线虫、克莱顿矮化线虫、最大矮化线虫、裸矮化线虫、普通矮化线虫、Quinisulcius
acutus、微小针线虫、Hemicycliophora parvana、居农野外垫刃线虫、小麦粒线虫、花生滑刃线虫、小尾盾线虫、Subanguina radiciola。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治大豆中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:最短尾短体线虫、草地短体线虫、穿刺短体线虫、斯克里布纳短体线虫、长尾刺线虫、大豆胞囊线虫、哥伦布纽带线虫以及咖啡短体线虫、六裂短体线虫、落选短体线虫、刻痕短体线虫、艾伦短体线虫、敏捷短体线虫、玉米短体线虫、伤残短体线虫、Belonolaimus
gracilis、花生根结线虫、南方根结线虫、爪哇根结线虫、北方根结线虫、哥伦布纽带线虫、盔形纽带线虫、肾形肾状线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治大豆中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:最短尾短体线虫、草地短体线虫、穿刺短体线虫、斯克里布纳短体线虫、长尾刺线虫、大豆胞囊线虫、哥伦布纽带线虫以及咖啡短体线虫、六裂短体线虫、落选短体线虫、刻痕短体线虫、艾伦短体线虫、敏捷短体线虫、玉米短体线虫、伤残短体线虫、Belonolaimus
gracilis、花生根结线虫、南方根结线虫、爪哇根结线虫、北方根结线虫、哥伦布纽带线虫、盔形纽带线虫、肾形肾状线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治烟草中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:南方根结线虫、爪哇根结线虫以及最短尾短体线虫、草地短体线虫、六裂短体线虫、穿刺短体线虫、落选短体线虫、刻痕短体线虫、桑尼短体线虫、伤残短体线虫、玉米短体线虫、横带长针线虫、Paratrichodorus
lobatus、毛刺线虫属、花生根结线虫、北方根结线虫、烟草胞囊线虫、Globodera
solanacearum、Globodera
virginiae、鳞球茎茎线虫、盘旋线虫属、螺旋线虫属、美洲剑线虫、小环线虫属、肾形肾状线虫、克莱顿矮化线虫、针线虫属、Tetylenchus
nicotianae。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治柑橘中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:咖啡短体线虫以及最短尾短体线虫、伤残短体线虫、长尾刺线虫、较小拟毛刺线虫、多孔拟毛刺线虫、毛刺线虫属、南方根结线虫、Meloidogyne
incognita acrita、爪哇根结线虫、Rotylenchus
macrodoratus、美洲剑线虫、短颈剑线虫、标准剑线虫、小环线虫属、半轮线虫属、(香蕉穿孔线虫)、柑橘穿孔线虫、裸鞘线虫、Hemicycliophora
nudata、半穿刺线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治香蕉中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:咖啡短体线虫、香蕉穿孔线虫以及Pratylenchus
giibbicaudatus、卢斯短体线虫、根结线虫属、多带螺旋线虫、双宫螺旋线虫、肾状线虫属。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治菠萝中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:玉米短体线虫、草地短体线虫、最短尾短体线虫、古迪短体线虫、根结线虫属、肾形肾状线虫以及横带长针线虫、Longidorus
laevicapitatus、原始毛刺线虫、较小毛刺线虫、异皮线虫属、食菌茎线虫、Hoplolaimuscalifornicus、拟强壮纽带线虫、印度纽带线虫、双宫螺旋线虫、Helicotylenchusnannus、多带螺旋线虫、Helicotylenchuserythrine、Xiphinemadimorphicaudatum、香蕉穿孔线虫、Tylenchorhynchusdigitatus、Tylenchorhynchusebriensis、微小针线虫、格尾盾线虫、薯蓣盾线虫、Psilenchustumidus、Psilenchusmagnidens、Pseudohalenchusminutus、Criconemoidesferniae、Criconemoidesonoense、Criconemoidesornatum。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治甘蔗中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:最短尾短体线虫、草地短体线虫、斯克里布纳短体线虫、穿刺短体线虫、咖啡短体线虫、鳞球茎茎线虫以及艾伦短体线虫、安第斯短体线虫、Pratylenchuscerealis、刻痕短体线虫、六裂短体线虫、卢斯短体线虫、落选短体线虫、光滑短体线虫、桑尼短体线虫、伤残短体线虫、花生根结线虫、高粱根结线虫、Meloidogyneartiella、南方根结线虫、禾草根结线虫、爪哇根结线虫、泰晤士根结线虫、北方根结线虫、埃塞俄比亚根结线虫、非洲根结线虫、吉库尤根结线虫、双角螺旋线虫、双宫螺旋线虫、假强壮螺旋线虫、Rotylenchulusborealis、小肾状线虫、肾形肾状线虫、小尾盾线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治葡萄中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:伤残短体线虫、花生根结线虫、南方根结线虫、爪哇根结线虫、美洲剑线虫、标准剑线虫以及草地短体线虫、斯克里布纳短体线虫、落选短体线虫、最短尾短体线虫、桑尼短体线虫、半穿刺线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治木本作物 - 梨果中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:穿刺短体线虫以及伤残短体线虫、横带长针线虫、南方根结线虫、北方根结线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治木本作物 - 核果中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:穿刺短体线虫、伤残短体线虫、花生根结线虫、北方根结线虫、爪哇根结线虫、南方根结线虫、薄叶小环线虫以及最短尾短体线虫、咖啡短体线虫、斯克里布纳短体线虫、玉米短体线虫、长尾刺线虫、双宫螺旋线虫、美洲剑线虫、弯曲小环线虫、克莱顿矮化线虫、钩针线虫、突出针线虫、小尾盾线虫、盔形纽带线虫。
氟吡菌酰胺和包含氟吡菌酰胺的组合物对于防治木本作物 - 坚果中线虫特别有效,所述线虫属于至少一个选自植物寄生性线虫的种,尤其是:毛刺线虫属、Criconemella
rusium以及伤残短体线虫、异毛刺线虫属、南方根结线虫、螺旋线虫属、矮化线虫属、Cacopauruspestis。
植物部位的定义
根据本发明,所有的植物和植物部位均可以被处理。植物表示所有的植物和植物种群,如想要的和不想要的野生植物、栽培种和植物品种(无论是否受植物品种或植物育种者权利的保护)。栽培种和植物品种可以是通过常规繁殖和育种方法获得的植物,所述方法可以由一种或多种生物技术方法如利用双单倍体、原生质体融合、随机和定向诱变、分子或遗传学标记或由生物工程和遗传工程方法来辅助或补充。植物部位表示植物的所有地上和地下部位及器官,如茎、叶、花和根,由此列出了例如叶、针叶、茎、枝、花、子实体、果实和种子以及根、块根、球茎和根茎。作物和无性及有性繁殖材料,例如插条、球茎、根茎、块根、纤枝 和种子也属于植物部位。
如上文已提及的,根据本发明处理所有植物和它们的部位是可以的。在一个实施方式中,对野生植物种和植物栽培种、或通过常规生物学育种如杂交或原生质体融合获得的那些以及其部位进行处理。在进一步的实施方式中,对通过遗传工程(如合适的话与常规方法组合)获得的转基因植物和植物栽培种(基因改造生物)及其部位进行处理。术语“部位”或“植物的部位”或“植物部位”已在上文进行了解释。
GMOs
根据本发明可以对在每种情况下市售或正在使用的植物栽培种的植物进行处理。可以将植物栽培种理解为表示这样的植物,所述植物具有可以通过常规育种、通过诱变或通过重组DNA技术获得的新特性(“性状”)。这可以是生物型和基因型品种。
可以根据本发明进行处理的转基因植物或植物栽培种(即通过遗传工程获得的那些)包括所有的在遗传修饰中获得了遗传物质的植物,所述遗传物质向这些植物传递了特别有利且有益的性状。此类特性的实例是更好的植物生长、对高温或低温的耐受性增加、对干旱或对水或土壤盐含量的耐受性增加、提高的开花性能、更易于收获、加速成熟、更高的收获产量、收获产物的更好品质和/或更高营养价值、收获产物的更好的储存稳定性和/或加工性。此类特性进一步并且特别强调的实例是植物对动物和微生物害虫,如针对线虫、昆虫、螨、致植物病真菌、细菌和/或病毒的更好的防御,以及还有植物对某些除草活性化合物的耐受性增加。特别强调的是蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄。
本发明的处理方法可以用于处理基因改造生物(GMO),如植物或种子。基因改造植物(或转基因植物)是外源基因已稳定地整合入基因组中的植物。表述“异源基因”基本上表示这样的基因,所述基因在植物之外提供或装配,当引入核基因组、叶绿体基因组或线粒体基因组中时,通过表达目的蛋白或多肽或通过下调或沉默存在于植物中的其它基因(例如使用反义技术、共抑制技术或RNA干扰– RNAi -技术),给予转化的植物新的或改进的农学或其它特性。位于基因组内的异源基因也称为转基因。将通过它在植物基因组中具体位置来确定的转基因称为转化或转基因事件。
根据植物种或植物栽培种、它们的位置和生长条件(土壤、气候、生长期、食物),本发明的处理也可以导致超加性(“协同的”)效应。因此,例如,根据本发明可以使用的活性化合物和组合物降低的施用率和/或拓宽的活性谱和/或活性的增加、更好的植物生长、对高温或低温的耐受性增加、对干旱或对水或土壤盐含量的耐受性增加、提高的开花性能、更易于收获、加速成熟、更高的收获产量、更大的果实、更大的植物高度、更绿的叶片颜色、更早开花、收获产物的更好品质和/或更高营养价值、果实中更高的糖浓度、收获产物的更好的储存稳定性和/或加工性都是可能的,其超出了实际预期的效果。
在某种施用率下,本发明的氟吡菌酰胺和包含氟吡菌酰胺的组合物在植物中也可以具有强化效果。因此,它们也适合于动员植物的防御系统对抗不想要的微生物的攻击。如果合适的话,这可以是本发明的氟吡菌酰胺和包含氟吡菌酰胺的组合物例如针对线虫活性增强的原因之一。在本上下文中,应将植物强化(抗性诱导)物质理解为表示能够以这样的方式刺激植物的防御系统的那些物质或物质的组合,当随后接种不想要的微生物时,处理后的植物表现出对这些微生物一定程度上的抗性。在这种情况下,应将不想要的微生物理解为是指致植物病真菌、细菌和病毒。因此,可以使用本发明的氟吡菌酰胺和包含氟吡菌酰胺的组合物用于在处理后某一时期内保护植物对抗上述病原体的攻击。在用活性化合物处理植物之后,保护有效的时期通常从1天延长至10天,优选1-7天。在某种施用率下,本发明的氟吡菌酰胺和包含氟吡菌酰胺的组合物在植物中也可以具有提高产量的效果。
根据本发明优选处理的植物和植物栽培种包括具有向这些植物传递特别有利的、有益的性状的遗传物质的所有植物(不论通过育种和/或生物技术方法获得)。
根据本发明还优选处理的植物和植物栽培种对一种或多种生物性胁迫具有抗性,即所述植物对动物和微生物害虫如对昆虫、螨、致植物病真菌、细菌、病毒和/或类病毒具有更好的防御。
根据本发明还可以处理的植物和植物栽培种是对一种或多种非生物性胁迫具有抗性的那些植物。非生物性胁迫条件可以包括例如干旱、低温暴露、热暴露、渗透胁迫、浸没、增加的土壤盐度、增加的矿物质暴露、臭氧暴露、高光暴露、氮营养的有限可用性、磷营养的有限可用性、避荫。
根据本发明还可以处理的植物和植物栽培种是特征在于提高的产量特性的那些植物。所述植物中提高的产量可以是下列情形的结果,例如改善的植物生理、生长和发育,如用水率、保水率、改善的氮利用、增强的碳同化、改善的光合作用、提高的萌发率和加速成熟。产量还可以受改善的植物构造(在胁迫和非胁迫条件下)的影响,包括但不限于早开花、杂种制种的开花控制、幼苗活力、植株大小、节间数目和距离、根生长、种子大小、果实大小、荚果大小、荚果或谷穗数目、每一荚果或谷穗的种子数目、种子质量、提高的种子充实、降低的种子散布、降低的荚果开裂和抗倒伏性。进一步的产量性状包括种子组成,如碳水化合物含量、蛋白含量、油含量和组成、营养价值、抗营养化合物的减少、改善的加工性和更好的储存稳定性。
可以根据本发明处理的植物是已经表现出杂种优势(heterosis)或杂种活力(hybrid
vigor)的特性的杂交植物,所述杂种优势或杂种活力特性通常产生更高的产量、活力、健康和对生物性和非生物性胁迫的抗性。此类植物通常通过将近交雄性不育亲代系(母本)与另一近交雄性可育亲代系(父本)杂交来产生。通常从雄性不育植物收获杂种种子并出售给种植者。有时(如在玉米中)可以通过去雄即机械去除雄性生殖器官(或雄花)来产生雄性不育植物,但更典型的是,雄性不育是植物基因组中遗传定子的结果。在那种情况下,并且尤其是当种子是要从杂交植物中收获的所需产物时,保证杂交植物中的雄性育性完全恢复通常是有用的。这可以通过确保父本具有合适的育性恢复基因来实现,所述育性恢复基因能够恢复包含负责雄性不育的遗传定子的杂交植物的雄性育性。雄性不育的遗传定子可以位于细胞质中。细胞质雄性不育(CMS)的实例例如描述于芸苔属的种中(W0 92/05251、WO
95/09910、WO 98/27806、WO 05/002324、WO
06/021972和US 6,229,072)。然而,雄性不育的遗传定子也可以位于核基因组中。也可以通过植物生物技术方法如遗传工程来获得雄性不育植物。获得雄性不育植物特别有效的方法描述于WO
89/10396中,其中,例如将核糖核酸酶如芽孢杆菌RNA酶选择性表达于雄蕊的绒毡层细胞中。随后可以通过核糖核酸酶抑制剂如芽孢杆菌RNA酶抑制剂在绒毡层细胞中表达来恢复育性(如WO 91/02069)。
可以根据本发明处理的植物或植物栽培种(通过植物生物技术方法如遗传工程来获得的)是除草剂耐受性植物,即对一种或多种给定除草剂产生耐受性的植物。可以通过遗传转化或通过选择包含传递此类除草剂耐受性的突变的植物来获得此类植物。
除草剂耐受性植物例如草甘磷耐受性植物,即对除草剂草甘磷或其盐产生耐受性的植物。可以通过不同方法使植物产生对草甘磷的耐受性。例如,可以通过用编码酶5-烯醇丙酮酰莽草酸-3-磷酸合酶(EPSPS)的基因转化植物来获得草甘磷耐受性植物。此类EPSPS基因的实例是细菌鼠伤寒沙门氏菌(Salmonella
typhimurium)的AroA基因(突变株CT7)(Comai等, 1983, Science 221, 370-371)、细菌农杆菌属(Agrobacterium sp.)的CP4基因(Barry等, 1992, Curr.
Topics Plant Physiol. 7, 139-145)、编码矮牵牛EPSPS的基因(Shah等, 1986, Science
233, 478-481)、番茄EPSPS (Gasser等, 1988, J. Biol. Chem. 263, 4280-4289)或牛筋草属EPSPS (WO 01/66704)。它也可以为描述于例如EP 0837944、WO 00/66746、WO 00/66747或WO02/26995中的突变的EPSPS。如U.S. Patent Nos. 5,776,760和5,463,175中所描述,也可以通过表达编码草甘磷氧化还原酶的基因来获得草甘磷耐受性植物,如美国专利Nos. 5,776,760和5,463,175所述。例如WO 02/36782、WO 03/092360、WO
05/012515和WO 07/024782所述,也可以通过表达编码草甘磷乙酰转移酶的基因来获得草甘磷耐受性植物。例如WO 01/024615或WO 03/013226所述,也可以通过选择包含天然存在的上述基因的突变的植物来获得草甘磷耐受性植物。表达赋予草甘磷耐受性的 EPSPS 基因的植物描述于例如美国专利申请 Nos 11/517,991 、 10/739,610 、 12/139,408 、 12/352,532 、 11/312,866 、 11/315,678 、 12/421,292 、 11/400,598 、 11/651,752 、 11/681,285 、 11/605,824 、 12/468,205 、 11/760,570 、 11/762,526 、 11/769,327 、 11/769,255 、 11/943801 或 12/362,774 中。包含赋予草甘磷耐受性的其它基因如脱羧酶基因的植物描述于例如美国专利申请 11/588,811 、 11/185,342 、 12/364,724 、 11/185,560 或 12/423,926 中。
其它除草剂抗性植物是例如对抑制酶谷氨酰胺合酶的除草剂如双丙氨膦、草丁膦或草铵膦产生耐受性的植物。例如美国专利申请 No
11/760,602 所述,可以通过表达使除草剂解毒的酶或对抑制作用具有抗性的突变型谷氨酰胺合酶来获得此类植物。一种此类有效的解毒酶是编码草丁膦乙酰转移酶的酶(如来自链霉菌属种的bar或pat蛋白)。表达外源草丁膦乙酰转移酶的植物例如描述于美国专利Nos.
5,561,236; 5,648,477; 5,646,024; 5,273,894; 5,637,489; 5,276,268; 5,739,082;
5,908,810和7,112,665中。
其它的除草剂耐受性植物也是对抑制酶羟基苯基丙酮酸双加氧酶(HPPD)的除草剂产生耐受性的植物。羟基苯基丙酮酸双加氧酶HPPD是催化对羟基苯基丙酮酸(HPP)转化为尿黑酸的反应的酶。如WO 96/38567、WO 99/24585和WO 99/24586、WO 2009/144079 、 WO
2002/046387 或 US 6,768,044中所述,可以用编码天然存在的抗性HPPD酶的基因、或编码突变的或嵌合的HPPD酶的基因转化对HPPD抑制剂耐受的植物。也可以通过用编码某些酶的基因转化植物来获得对HPPD抑制剂的耐受性,所述酶尽管受HPPD抑制剂对天然HPPD酶的抑制作用但仍能够形成尿黑酸。此类的植物和基因描述于WO 99/34008和WO 02/36787中。如WO
2004/024928所述,除编码HPPD耐受性酶的基因之外,也可以通过用编码具有预苯酸脱氢酶(PDH)活性的酶的基因转化植物来改善植物对HPPD抑制剂的耐受性。此外,可以通过向其基因组中加入编码能够代谢或降解 HPPD 抑制剂的酶(如 WO 2007/103567 和 WO
2008/150473 中显示的 CYP450 酶)的基因而使植物对 HPPD 抑制剂除草剂更耐受。
更进一步的除草剂耐受性植物是对乙酰乳酸合酶(ALS)抑制剂产生耐受性的植物。已知的ALS抑制剂包括例如磺酰脲、咪唑啉酮、三唑并嘧啶、嘧啶氧基(硫基)苯甲酸酯和/或磺酰基氨基羰基三唑啉酮除草剂。例如Tranel和Wright
(2002, Weed Science 50:700-712)所述,也如美国专利No. 5,605,011、5,378,824、5,141,870和5,013,659所述,公知ALS酶(也称为乙酰羟酸合酶,AHAS)中的不同突变对不同的除草剂和除草剂的组赋予耐受性。磺酰脲耐受性植物和咪唑啉酮耐受性植物的产生描述于美国专利Nos.
5,605,011; 5,013,659; 5,141,870; 5,767,361; 5,731,180; 5,304,732; 4,761,373;
5,331,107; 5,928,937; 和5,378,824; 以及国际公开WO 96/33270中。其它的咪唑啉酮耐受性植物也描述于例如WO 2004/040012、WO 2004/106529、WO 2005/020673、WO 2005/093093、WO 2006/007373、WO 2006/015376、WO 2006/024351和WO 2006/060634中。其它的磺酰脲和咪唑啉酮耐受性植物也描述于例如WO
07/024782和美国专利申请 No 61/288958 中。
可以通过诱变、存在除草剂的情况下在细胞培养物中选择或突变育种来获得其它对咪唑啉酮和/或磺酰脲耐受的植物,例如对美国专利5,084,082的大豆、WO
97/41218中的稻、美国专利5,773,702和WO
99/057965中的糖用甜菜、美国专利5,198,599中的莴苣或WO
01/065922中的向日葵所述。
也可以根据本发明处理的植物或植物栽培种(通过植物生物技术方法如遗传工程来获得的)是抗昆虫转基因植物,即对某些目标昆虫的攻击产生抗性的植物。可以通过遗传转化或通过选择包含传递此类昆虫抗性的突变的植物来获得此类植物。
本文中使用的“昆虫抗性转基因植物”包括任何包含至少一个转基因的植物,所述转基因包含编码下列的编码序列:
1) 来自苏云金芽胞杆菌(Bacillus thuringiensis)的杀虫晶体蛋白或其杀虫部分,如由Crickmore等列出的杀虫晶体蛋白(1998,
Microbiology and Molecular Biology Reviews, 62: 807-813)、由Crickmore等(2005)在苏云金芽孢杆菌毒素命名法(在线:http://www.lifesci.sussex.ac.uk/Home/Neil_Crickmore/Bt/)中更新的杀虫晶体蛋白,或其杀虫部分,如Cry蛋白分类Cry1Ab、Cry1Ac、Cry1B、Cry1C、Cry1D、Cry1F、Cry2Ab、Cry3Aa或Cry3Bb的蛋白或其杀虫部分(如EP 1999141和WO 2007/107302)、或由如美国专利申请 No
12/249,016 中描述的合成基因编码的此类蛋白;或
2)来自苏云金芽孢杆菌的晶体蛋白或其部分,所述晶体蛋白或其部分在存在第二个来自苏云金芽孢杆菌的其它晶体蛋白或其部分的情况下具有杀虫性,如由Cry34和Cry35晶体蛋白构成的二元毒素(Moellenbeck等 2001, Nat. Biotechnol. 19: 668-72; Schnepf等 2006, Applied Environm. Microbiol. 71, 1765-1774)或由Cry1A或Cry1F蛋白和Cry2Aa或Cry2Ab或Cry2Ae蛋白构成的二元毒素(美国专利申请No. 12/214,022和EP
08010791.5);或
3)包含来自苏云金芽孢杆菌的不同杀虫晶体蛋白的部分的杂种杀虫蛋白,如上述1)中的蛋白的杂种或上述2)中的蛋白的杂种,如通过玉米品系MON89034产生的Cry1A.105蛋白(WO 2007/027777);或
4)上述1)至3)中任一项的蛋白,其中某些(具体1-10)氨基酸已由另一氨基酸所替代以获得对于目标昆虫种更高的杀虫活性和/或扩展影响的目标昆虫种的范围,和/或由于在克隆或转化中引入编码DNA中的改变所引起,如在玉米品系MON863或MON88017中的Cry3Bb1蛋白或在玉米品系MIR604中的Cry3A蛋白;或
5)来自苏云金芽孢杆菌或蜡样芽胞杆菌(Bacillus cereus)的杀虫分泌性蛋白或其杀虫部分,如列于:
http://www.lifesci.sussex.ac.uk/home/Neil_Crickmore/Bt/vip.html的营养期杀虫蛋白(VIP),如来自VIP3Aa蛋白分类的蛋白;或
6)来自苏云金芽孢杆菌或蜡样芽胞杆菌的分泌性蛋白,所述分泌性蛋白在存在第二个来自苏云金芽孢杆菌或蜡样芽胞杆菌的分泌性蛋白时具有杀虫性,如由VIP1A和VIP2A蛋白构成的二元毒素(WO 94/21795);或
7)包含来自苏云金芽孢杆菌或蜡样芽胞杆菌的不同分泌性蛋白的部分的杂种杀虫蛋白,如上述1)中的蛋白的杂种或上述2)中的蛋白的杂种;或
8)上述5)至7)中任一项的蛋白,其中某些(具体1-10)氨基酸已由另一氨基酸所替代,以获得对于目标昆虫种更高的杀虫活性和/或扩展影响的目标昆虫种的范围,和/或由于在克隆或转化中引入编码DNA中的改变(而仍编码杀虫蛋白)所引起,如在棉花品系COT102中的VIP3Aa蛋白;或
9)来自苏云金芽孢杆菌或蜡样芽胞杆菌的分泌性蛋白,所述分泌性蛋白在存在第二个来自苏云金芽孢杆菌的晶体蛋白时具有杀虫性,如由VIP3和Cry1A或Cry1F构成的二元毒素(美国专利申请No. 61/126083 和61/195019)或由VIP3蛋白和Cry2Aa或Cry2Ab 或Cry2Ae蛋白构成的二元毒素(美国专利申请No. 12/214,022和EP
08010791.5)。
10)上述9)中的蛋白,其中某些(具体1-10)氨基酸已由另一氨基酸所替代,以获得对于目标昆虫种更高的杀虫活性和/或扩展影响的目标昆虫种的范围,和/或由于在克隆或转化中引入编码DNA中的改变(而仍编码杀虫蛋白)所引起。
当然,如本文使用的昆虫抗性转基因植物也包括任何包含编码上述1-10类别的任一个蛋白的基因的组合的植物。在一个实施方式中,昆虫抗性植物包含多于一个编码上述1-10类别的任一个蛋白的转基因,目的在于当使用针对不同目标昆虫种的不同蛋白时扩展影响的目标昆虫种的范围、或通过使用对相同目标昆虫种具有杀虫作用但具有不同作用方式(如结合到昆虫中的不同受体结合位点上)的不同蛋白来延缓昆虫对植物的抗性发育。
本文中使用的“昆虫抗性转基因植物”还包括任何包含至少一个包含表达后产生双链RNA的序列的转基因的植物,所述双链RNA由植物虫害摄入后抑制该虫害的生长,例如WO
2007/080126、 WO 2006/129204 、 WO 2007/074405 、 WO
2007/080127 和 WO 2007/035650 中所描述。
也可以根据本发明处理的植物或植物栽培种(通过植物生物技术方法如遗传工程来获得的)对非生物胁迫是耐受的。可以通过遗传转化或通过选择包含传递此类胁迫抗性的突变的植物来获得此类植物。特别有效的胁迫耐受性植物包括:
1)如WO 00/04173、WO/2006/045633、EP
04077984.5或EP 06009836.5中所描述,包含能够降低植物细胞或植物中多聚(ADP核糖)聚合酶(PARP)基因的表达和/或活性的转基因的植物。
2)例如WO 2004/090140所述,包含能够降低植物或植物细胞的PARG编码基因的表达和/或活性的胁迫耐受性增强转基因的植物。
3)例如EP 04077624.7、WO
2006/133827、PCT/EP07/002433、EP 1999263或WO
2007/107326所述,包含编码烟酰胺腺嘌呤二核苷酸补救合成途径的植物功能性酶的胁迫耐受性增强转基因的植物,所述酶包括烟酰胺酶、烟酸盐磷酸核糖转移酶、烟酸单核苷酸腺嘌呤转移酶、烟酰胺腺嘌呤二核苷酸合酶或烟酰胺磷酸核糖转移酶。
也可以根据本发明处理的植物或植物栽培种(通过植物生物技术方法如遗传工程来获得的)显示出收获产物改变的数量、质量和/或储存稳定性和/或收获产物的特定成分的改变的特性,如:
1)合成修饰的淀粉的转基因植物,所述修饰的淀粉在其理化特性中,尤其是直链淀粉含量或直链淀粉/支链淀粉比、支化度、平均链长、侧链分布、黏度性能、凝胶强度、淀粉粒大小和/或淀粉粒形态,与野生型植物细胞或植物中的合成淀粉相比发生了改变,从而这更加适合于特殊应用。所述合成修饰淀粉的转基因植物例如公开于EP
0571427、 WO 95/04826、 EP 0719338、 WO
96/15248、 WO 96/19581、 WO 96/27674、 WO
97/11188、 WO 97/26362、 WO 97/32985、 WO
97/42328、 WO 97/44472、 WO 97/45545、 WO
98/27212、 WO 98/40503、 WO99/58688、 WO
99/58690、 WO 99/58654、 WO 00/08184、 WO
00/08185、 WO 00/08175、 WO 00/28052、 WO
00/77229、 WO 01/12782、 WO 01/12826、 WO
02/101059、 WO 03/071860、 WO 2004/056999、 WO
2005/030942、 WO 2005/030941、 WO 2005/095632、 WO 2005/095617、 WO 2005/095619、 WO
2005/095618、 WO 2005/123927、 WO 2006/018319、 WO
2006/103107、 WO 2006/108702、 WO 2007/009823、 WO
00/22140、 WO 2006/063862、 WO 2006/072603、 WO
02/034923、 EP 06090134.5、 EP 06090228.5、 EP
06090227.7、 EP 07090007.1、 EP 07090009.7、 WO
01/14569、 WO 02/79410、 WO 03/33540、 WO
2004/078983、 WO 01/19975、 WO 95/26407、 WO
96/34968、 WO 98/20145、 WO 99/12950、 WO
99/66050、 WO 99/53072、 US 6、734、341、 WO 00/11192、 WO 98/22604、 WO
98/32326、 WO 01/98509、 WO 01/98509、 WO
2005/002359、 US 5、824、790、 US 6、013、861、 WO 94/04693、 WO
94/09144、 WO 94/11520、 WO 95/35026、 WO
97/20936。
2)合成非淀粉碳水化合物聚合物或合成与未进行遗传修饰的野生型植物相比具有改变特性的非淀粉碳水化合物聚合物的转基因植物。实例是公开于EP
0663956、 WO 96/01904、 WO 96/21023、 WO
98/39460和WO 99/24593中的产生多聚果糖尤其是菊粉和果聚糖类多聚果糖的植物,公开于WO 95/31553、 US 2002031826、 US
6,284,479、US 5,712,107、 WO 97/47806、 WO
97/47807、 WO 97/47808和WO 00/14249中的产生α-1,4-葡聚糖的植物、 公开于WO 00/73422中的产生α-1,6支化α-1,4-葡聚糖的植物、 公开于例如WO 00/47727、 WO 00/73422、 EP
06077301.7、 US 5,908,975和EP 0728213中的产生alternan的植物,
3)例如公开于WO 2006/032538、WO 2007/039314、WO
2007/039315、WO 2007/039316、JP 2006304779和WO
2005/012529的产生透明质酸的转基因植物。
4)如描述于美国专利申请No. 12/020,360和61/054,026的转基因植物或杂交植物,例如具有例如‘高可溶性固体含量’、‘低刺激性’(LP)和/或‘长期储存’(LS)特性的洋葱。
也可以根据本发明处理的植物或植物栽培种(其可以通过植物生物技术方法如遗传工程来获得)是具有改变的纤维特性的植物如棉花植物。此类植物可以通过遗传转化或通过选择包含传递此类改变的纤维特性的突变的植物来获得,并且包括:
a)如描述于WO 98/00549中的包含改变形式的纤维素合酶基因的植物,如棉花植物;
b)如描述于WO 2004/053219中的包含改变形式的rsw2或rsw3同源核酸的植物,如棉花植物;
c)如描述于WO 01/17333中的具有升高表达的蔗糖磷酸合酶的植物,如棉花植物;
d)如描述于WO 02/45485中的具有升高表达的蔗糖合酶的植物,如棉花植物;
e)如描述于WO 2005/017157中或如描述于EP 08075514.3或美国专利申请No.
61/128,938中的植物如棉花植物,其中例如通过下调纤维选择性β-1,3-葡聚糖酶改变了纤维状细胞基础上的胞间连丝门控时机;
f)如描述于WO 2006/136351中的例如通过表达包括nodC在内的N-乙酰葡糖胺转移酶基因和几丁质合酶基因而具有改变的反应性的纤维的植物,如棉花植物。
也可以根据本发明处理的植物或植物栽培种(其可以通过植物生物技术方法如遗传工程来获得)是这样的植物,如具有改变的油分布特性的油菜或相关的芸苔属植物。此类植物可以通过遗传转化或通过选择包含传递此类改变的油分布特性的突变的植物来获得,并且包括:
a)例如描述于US 5,969,169、US 5,840,946或US
6,323,392或US 6,063,947中的产生具有高油酸含量的油的植物,如油菜植物;
b)例如描述于US 6,270,828、US 6,169,190或US
5,965,755中的产生具有低亚麻酸含量的油的植物,如油菜植物;
c)例如描述于美国专利No. 5,434,283或美国专利申请 No 12/668303 中的产生具有低水平的饱和脂肪酸的油的植物,如油菜植物。
也可以根据本发明处理的植物或植物栽培种(其可以通过植物生物技术方法如遗传工程来获得)是这样的植物,例如,对如马铃薯Y病毒具有病毒抗性的马铃薯(来自Tecnoplant, Argentina的品系SY230和SY233)、对如马铃薯晚疫病具有疾病抗性的马铃薯(如RB基因)、表现出冷诱导甜化降低的马铃薯(携带Nt-Inhh、IIR-INV基因)或具有矮化表型的马铃薯(基因A-20氧化酶)。
也可以根据本发明处理的植物或植物栽培种(其可以通过植物生物技术方法如遗传工程来获得)是这样的植物,如具有改变的落粒特性的油菜或相关的芸苔属植物。此类植物可以通过遗传转化或通过选择包含传递此类改变的落粒特性的突变的植物来获得,并且包括这样的植物,如具有延迟或降低的落粒的油菜植物,如美国专利申请No.
61/135,230和EP 08075648.9、 WO09/068313 和 WO10/006732所述。
可以根据本发明进行处理的特别有用的转基因植物是包含转化品系或转化品系的组合的植物,在美国,其是向美国农业部(USDA)的动植物健康检查局(APHIS)的非管制身份的请求主题,无论此类请求已授权或仍待决定。任何时候均可以从APHIS
(4700 River Road Riverdale, MD 20737, USA)方便地获得这些信息,例如在其互联网网址(URL
http://www.aphis.usda.gov/brs/not_reg.html)上。在本申请的申请日,APHIS待决定的或APHIS已授权的非管制身份的请求是列于表B中的那些,其包含以下信息:
- 请求:请求的标识号。转化品系的技术说明书可以在从APHIS可获的各个请求文件中找到,例如在APHIS网站上通过参考该请求号。这些说明书通过引用并入本文。
- 请求范围:参考要求范围的之前请求。
- 机构:提交请求的实体名称。
- 管制事物:相关植物种。
- 转基因表型:通过转化品系赋予植物的性状。
- 转化品系或株系:请求非管制身份的一种或多种品系(有时也称为株系或株系)的名称。
-
APHIS文件:由APHIS发布与请求相关的和APHIS可以要求的不同文件。
另外的包含单一转化品系或转化品系组合的特别有效的植物例如列于不同国家或区域监管机构的数据库中(例如见
http://gmoinfo.jrc.it/gmp_browse.aspx 和http://www.agbios.com/dbase.php)。
本发明还涉及氟吡菌酰胺和包含氟吡菌酰胺的组合物防治包含转化品系或转化品系的组合的植物中线虫的用途,所述植物例如列于不同国家或区域监管机构的数据库中,包括:品系1143-14A
(棉花, 昆虫防治, 未保藏, 描述于WO2006/128569); 品系1143-51B (棉花, 昆虫防治, 未保藏, 描述于WO2006/128570); 品系1445
(棉花, 除草剂耐受性, 未保藏, 描述于US2002120964或WO2002/034946); 品系17053
(稻, 除草剂耐受性, 保藏为PTA-9843, 描述于WO2010/117737);
品系17314 (稻, 除草剂耐受性, 保藏为PTA-9844, 描述于WO2010/117735); 品系281-24-236
(棉花, 昆虫防治 - 除草剂耐受性, 保藏为PTA-6233, 描述于WO2005/103266或US2005216969);
品系3006-210-23 (棉花, 昆虫防治 - 除草剂耐受性, 保藏为PTA-6233, 描述于US2007143876或WO2005/103266);
品系3272 (玉米, 质量性状, 保藏为PTA-9972, 描述于WO2006098952或US2006230473);
品系40416 (玉米, 昆虫防治 - 除草剂耐受性, 保藏为ATCC PTA-11508, 描述于WO2011/075593);
品系43A47 (玉米, 昆虫防治 - 除草剂耐受性, 保藏为ATCC PTA-11509, 描述于WO2011/075595);
品系5307 (玉米, 昆虫防治, 保藏为ATCC PTA-9561, 描述于WO2010/077816); 品系ASR-368
(糠穗草, 除草剂耐受性, 保藏为ATCC PTA-4816, 描述于US2006162007或WO2004053062); 品系B16 (玉米, 除草剂耐受性, 未保藏, 描述于US2003126634); 品系BPS-CV127-9 (大豆, 除草剂耐受性, 保藏为NCIMB No. 41603,
描述于WO2010/080829); 品系CE43-67B (棉花, 昆虫防治, 保藏为DSM ACC2724, 描述于US2009217423或WO2006/128573);
品系CE44-69D (棉花, 昆虫防治, 未保藏, 描述于US20100024077); 品系CE44-69D
(棉花, 昆虫防治, 未保藏, 描述于WO2006/128571); 品系CE46-02A (棉花, 昆虫防治, 未保藏, 描述于WO2006/128572); 品系COT102
(棉花, 昆虫防治, 未保藏, 描述于US2006130175或WO2004039986); 品系COT202
(棉花, 昆虫防治, 未保藏, 描述于US2007067868或WO2005054479); 品系COT203
(棉花, 昆虫防治, 未保藏, 描述于WO2005/054480); 品系DAS40278 (玉米, 除草剂耐受性, 保藏为ATCC PTA-10244, 描述于WO2011/022469); 品系DAS-59122-7
(玉米, 昆虫防治 - 除草剂耐受性, 保藏为ATCC PTA 11384 ,
描述于US2006070139); 品系DAS-59132 (玉米, 昆虫防治 - 除草剂耐受性, 未保藏, 描述于WO2009/100188); 品系DAS68416 (大豆, 除草剂耐受性, 保藏为ATCC PTA-10442, 描述于WO2011/066384或WO2011/066360);
品系DP-098140-6 (玉米, 除草剂耐受性, 保藏为ATCC PTA-8296, 描述于US2009137395或WO2008/112019); 品系DP-305423-1
(大豆, 质量性状, 未保藏, 描述于US2008312082或WO2008/054747); 品系DP-32138-1
(玉米, 杂交系统, 保藏为ATCC PTA-9158, 描述于US20090210970或WO2009/103049); 品系DP-356043-5
(大豆, 除草剂耐受性, 保藏为ATCC PTA-8287, 描述于US20100184079或WO2008/002872); 品系EE-1
(茄子, 昆虫防治, 未保藏, 描述于WO2007/091277); 品系FI117 (玉米, 除草剂耐受性, 保藏为ATCC 209031, 描述于US2006059581或WO1998/044140);
品系GA21 (玉米, 除草剂耐受性, 保藏为ATCC 209033, 描述于US2005086719或WO1998/044140);
品系GG25 (玉米, 除草剂耐受性, 保藏为ATCC 209032, 描述于US2005188434或WO1998/044140);
品系GHB119 (棉花, 昆虫防治 - 除草剂耐受性, 保藏为ATCC PTA-8398, 描述于WO2008/151780);
品系GHB614 (棉花, 除草剂耐受性, 保藏为ATCC PTA-6878, 描述于US2010050282或WO2007/017186);
品系GJ11 (玉米, 除草剂耐受性, 保藏为ATCC 209030, 描述于US2005188434或WO1998/044140);
品系GM RZ13 (糖用甜菜, 病毒抗性, 保藏为NCIMB-41601, 描述于WO2010/076212); 品系H7-1
(糖用甜菜, 除草剂耐受性, 保藏为NCIMB 41158或
NCIMB 41159, 描述于US2004172669或WO2004/074492); 品系JOPLIN1
(小麦, 疾病耐受性, 未保藏, 描述于US2008064032); 品系LL27 (大豆, 除草剂耐受性, 保藏为NCIMB41658, 描述于WO2006/108674或US2008320616);
品系LL55 (大豆, 除草剂耐受性, 保藏为NCIMB 41660, 描述于WO2006/108675或US2008196127);
品系LL棉花25 (棉花, 除草剂耐受性, 保藏为ATCC PTA-3343, 描述于WO2003013224或US2003097687); 品系LLRICE06
(稻, 除草剂耐受性, 保藏为ATCC-23352, 描述于US6468747或 WO2000/026345); 品系LLRICE601
(稻, 除草剂耐受性, 保藏为ATCC PTA-2600, 描述于US20082289060或WO2000/026356); 品系LY038
(玉米, 质量性状, 保藏为ATCC PTA-5623, 描述于US2007028322或WO2005061720); 品系MIR162
(玉米, 昆虫防治, 保藏为PTA-8166, 描述于US2009300784或WO2007/142840); 品系MIR604
(玉米, 昆虫防治, 未保藏, 描述于US2008167456或WO2005103301); 品系MON15985
(棉花, 昆虫防治, 保藏为ATCC PTA-2516, 描述于US2004-250317或WO2002/100163); 品系MON810
(玉米, 昆虫防治, 未保藏, 描述于US2002102582); 品系MON863 (玉米, 昆虫防治, 保藏为ATCC PTA-2605, 描述于WO2004/011601或US2006095986);
品系MON87427 (玉米, 传粉防治, 保藏为ATCC PTA-7899, 描述于WO2011/062904); 品系MON87460
(玉米, 胁迫耐受性, 保藏为ATCC PTA-8910, 描述于WO2009/111263或US20110138504); 品系MON87701
(大豆, 昆虫防治, 保藏为ATCC PTA-8194, 描述于US2009130071或WO2009/064652); 品系MON87705
(大豆, 质量性状 - 除草剂耐受性, 保藏为ATCC PTA-9241, 描述于US20100080887或WO2010/037016);
品系MON87708 (大豆, 除草剂耐受性, 保藏为ATCC PTA9670, 描述于WO2011/034704); 品系MON87754
(大豆, 质量性状, 保藏为ATCC PTA-9385, 描述于WO2010/024976);
品系MON87769 (大豆, 质量性状, 保藏为ATCC PTA-8911, 描述于US20110067141或WO2009/102873);
品系MON88017 (玉米, 昆虫防治 - 除草剂耐受性, 保藏为ATCC PTA-5582, 描述于US2008028482或WO2005/059103); 品系MON88913
(棉花, 除草剂耐受性, 保藏为ATCC PTA-4854, 描述于WO2004/072235或US2006059590); 品系MON89034
(玉米, 昆虫防治, 保藏为ATCC PTA-7455, 描述于WO2007/140256或US2008260932); 品系MON89788
(大豆, 除草剂耐受性, 保藏为ATCC PTA-6708, 描述于US2006282915或WO2006/130436); 品系MS11
(油菜, 传粉防治-除草剂耐受性, 保藏为ATCC PTA-850或PTA-2485, 描述于WO2001/031042);
品系MS8 (油菜, 传粉防治 - 除草剂耐受性, 保藏为ATCC PTA-730, 描述于WO2001/041558或US2003188347); 品系NK603
(玉米, 除草剂耐受性, 保藏为ATCC PTA-2478, 描述于US2007-292854);
品系PE-7 (稻, 昆虫防治, 未保藏, 描述于WO2008/114282); 品系RF3 (油菜, 传粉防治 - 除草剂耐受性, 保藏为ATCC PTA-730, 描述于WO2001/041558或US2003188347);
品系RT73 (糖用油菜, 除草剂耐受性, 未保藏, 描述于WO2002/036831或US2008070260);
品系T227-1 (糖用甜菜, 除草剂耐受性, 未保藏, 描述于WO2002/44407或US2009265817);
品系T25 (玉米, 除草剂耐受性, 未保藏, 描述于US2001029014或WO2001/051654);
品系T304-40 (棉花, 昆虫防治 - 除草剂耐受性, 保藏为ATCC PTA-8171, 描述于US2010077501或WO2008/122406); 品系T342-142
(棉花, 昆虫防治, 未保藏, 描述于WO2006/128568); 品系TC1507 (玉米, 昆虫防治 - 除草剂耐受性, 未保藏, 描述于US2005039226或WO2004/099447); 品系VIP1034
(玉米, 昆虫防治 - 除草剂耐受性, 保藏为ATCC PTA-3925., 描述于WO2003/052073), 品系32316
(玉米,昆虫防治-除草剂耐受性,保藏为PTA-11507, 描述于WO2011/084632), 品系4114
(玉米,昆虫防治-除草剂耐受性,保藏为PTA-11506, 描述于WO2011/084621)。
本发明还涉及氟吡菌酰胺和包含氟吡菌酰胺的组合物防治植物中线虫的用途,所述植物携带有一种或多种列于下表A中的品系:
制剂
可包含于本发明组合物中的合适的填充剂和/或表面活性剂是通常用于植物处理组合物中的所有制剂辅助剂。
在本发明组合物中,氟吡菌酰胺与组(B)的农用化学活性化合物的比例可以在比较宽的范围内变化。通常,每重量份的农用化学活性化合物使用0.02-2.0重量份、优选0.05-1.0重量份的氟吡菌酰胺。
当使用根据本发明可以使用的式(I)的活性化合物时,根据施用类型,施用率可以在某一范围内变化。在种子处理中,式(I)的活性化合物的施用率通常为每千克种子10-10000 mg,优选每千克种子10-300 mg。当以固体制剂使用时,式(I)的活性化合物的施用率通常为每千克制剂20-800 mg,优选每千克制剂30-700
mg。
根据本发明,载体的含义应理解为天然的或合成的、有机的或无机的物质,该物质与活性化合物混合或结合以获得更好的施用性,特别是施用于植物或植物部位或种子。该载体可以是固体或液体,通常是惰性的且应适用于农业。
合适的固体载体是:例如铵盐和粉碎的天然矿物,如高岭土、粘土、滑石、白垩、石英、绿坡缕石、蒙脱石或硅藻土;以及粉碎的合成矿物,如细分散二氧化硅、氧化铝和天然或合成硅酸盐、树脂、蜡、固体肥料、水、醇(特别是丁醇)、有机溶剂、矿物油和植物油,及其衍生物。也可以使用该载体的混合物。适用于颗粒剂的固体载体是:例如粉碎并分级(fractionated)的天然矿物,如方解石、大理石、浮石、海泡石、白云石以及合成的无机及有机粉颗粒,以及有机材料的颗粒如锯屑、椰壳、玉米穗轴和烟草茎。合适的乳化剂和/或成泡剂(foam-formers)是:例如非离子和阴离子乳化剂,如聚氧乙烯脂肪酸酯、聚氧乙烯脂肪醇醚,例如烷基芳基聚乙二醇醚、烷基磺酸盐、烷基硫酸盐、芳基磺酸盐以及蛋白水解物。合适的分散剂是:例如木素亚硫酸盐(lignosulphite)废液和甲基纤维素。
合适的液化气态填充剂(extender)或载体是在环境温度和大气压下为气态的液体,例如气溶胶喷射剂,如丁烷、丙烷、氮气和二氧化碳。
制剂中可使用增粘剂,如羧甲基纤维素以及粉末、颗粒和胶乳形式的天然和合成聚合物,如阿拉伯胶、聚乙烯醇、聚乙酸乙烯酯,或天然磷脂,如脑磷脂和卵磷脂,以及合成磷脂。其他可能的添加剂是矿物油和植物油。
如果使用的填充剂是水,则也可例如使用有机溶剂作为助溶剂。合适的液体溶剂主要是:芳香族化合物,如二甲苯、甲苯或烷基萘,氯代芳香族化合物或氯代脂肪族烃,如氯苯、氯乙烯或二氯甲烷,脂肪族烃,如环己烷或石蜡,例如矿物油馏分、矿物油和植物油,醇,如丁醇或二醇,及其醚和酯,酮,如丙酮、甲基乙基酮、甲基异丁基酮或环己酮,强极性溶剂,如二甲基甲酰胺和二甲基亚砜,以及水。
本发明的组合物可包含其他额外组分,例如,表面活性剂。合适的表面活性剂是具有离子或非离子特性的乳化剂、分散剂或润湿剂,或这些表面活性剂的混合物。这些的实例是聚丙烯酸的盐、木素磺酸的盐、酚磺酸的盐或萘磺酸的盐、环氧乙烷与脂肪醇或脂肪酸或脂肪胺的缩聚物、取代的酚(优选烷基酚或芳基酚)、磺基丁二酸酯的盐、牛磺酸衍生物(优选牛磺酸烷基酯)、聚乙氧基化醇或酚的磷酸酯、多元醇的脂肪酸酯、以及含硫酸基、磺酸基和磷酸基的化合物的衍生物。如果活性化合物之一和/或惰性载体之一不溶于水且当在水中施用时,则需要存在表面活性剂。表面活性剂的比例在本发明组合物的5至40重量%之间。
可以使用着色剂,如无机颜料,例如氧化铁、氧化钛、普鲁士蓝,以及有机染料如茜素染料、偶氮染料和金属酞菁染料,以及微量营养素,如铁、锰、硼、铜、钴、钼和锌的盐。
如果合适,也可存在其他额外组分,例如保护胶体、粘合剂(binders)、胶粘剂(adhesives)、增稠剂、触变剂、渗透剂、稳定剂、螯合剂(sequestering agents)、络合物形成剂(complex formers)。通常,活性化合物可与常用于制剂目的的任何固体或液体添加剂相组合。
通常,本发明的组合物包含0.05-99重量%的本发明的活性化合物组合,优选10-70重量%、特别优选20-50重量%、最优选25重量%。
本发明的活性化合物组合或组合物可以其本身或者根据其各自的物理和/或化学性能,以其制剂的形式或由该制剂制备的使用形式使用,如气溶胶、胶囊悬浮剂、冷雾剂(cold-fogging
concentrates)、热雾剂、微囊粒剂、细粒剂、处理种子用悬浮剂(flowable
concentrate for the treatment of seeds)、即用溶液剂、粉剂、乳油、水包油型乳剂、油包水型乳剂、大粒剂、微粒剂、油分散性粉剂、油悬剂、油剂、泡沫剂、膏剂、农药种衣剂(pesticide-coated
seed)、水悬剂、悬乳浓缩剂(suspoemulsion concentrate)、可溶性液剂、悬浮剂、可湿性粉剂、可溶性粉剂、粉和颗粒剂、水溶性颗粒剂或片剂、处理种子用水溶性粉剂、可湿性粉剂、活性化合物浸渍的天然产物和合成物质、以及聚合物质中和种衣材料中的微胶囊剂,以及ULV冷雾化和热雾化制剂。
所述制剂可以本身已知的方式,例如通过将活性化合物或活性化合物组合与至少一种添加剂混合进行制备。合适的添加剂为所有常用制剂助剂,如有机溶剂、填充剂、溶剂或稀释剂、固体载体和填料、表面活性剂(如佐剂、乳化剂、分散剂、保护胶体、润湿剂和增粘剂)、分散剂和/或粘合剂或固定剂、防腐剂、染料和颜料、消泡剂、无机和有机增稠剂、防水剂、若适用,干燥剂和UV稳定剂、赤霉素以及水和其他加工助剂。取决于各自待制备的制剂种类,可能需要其他加工步骤,例如,湿磨、干磨或造粒。
可存在的有机稀释剂是通常用于此目的的所有极性和非极性有机溶剂。优选为酮,如甲基异丁基酮和环己酮,此外为酰胺,如二甲基甲酰胺和烷甲酰胺,如N,N-二甲基癸酰胺和N,N-二甲基辛酰胺,此外为环状化合物,如N-甲基吡咯烷酮、N-辛基吡咯烷酮、N-十二烷基吡咯烷酮、N-辛基己内酰胺、N-十二烷基己内酰胺和丁内酯,此外为强极性溶剂,如二甲基亚砜,此外为芳香族烃,如二甲苯、Solvesso™、矿物油,例如白酒(white spirit)、石油、烷基苯和锭子油,此外为酯,如丙二醇单甲基醚乙酸酯、己二酸二丁酯、乙酸己酯、乙酸庚酯、柠檬酸三正丁酯和邻苯二甲酸二正丁酯,并且此外为醇,例如苯甲醇和1-甲氧基-2-丙醇。
适合于颗粒剂的固体载体是:例如粉碎并分级的天然矿物,如方解石、大理石、浮石、海泡石、白云石,以及合成的无机和有机粉颗粒,以及有机材料的颗粒,如锯屑、椰壳、玉米穗轴和烟草茎。
合适的表面活性剂(佐剂、乳化剂、分散剂、保护胶体、润湿剂和增粘剂)是常用的离子和非离子物质。可能提及的实例是乙氧基化的壬基酚、直链或支链醇的聚烯烃乙二醇醚、烷基酚与环氧乙烷和/或环氧丙烷的反应产物、脂肪胺与环氧乙烷和/或环氧丙烷的反应产物,此外为脂肪酯、烷基磺酸盐、烷基硫酸盐、烷基醚硫酸盐、烷基醚磷酸盐、芳基硫酸盐、乙氧基化的芳基烷基苯酚,例如三苯乙烯基苯酚乙氧基化物,此外为乙氧基化和丙氧基化的芳基烷基苯酚以及硫酸化或磷酸化的芳基烷基苯酚乙氧基化物或乙氧基和丙氧基化物。还可能提及天然和合成水溶性聚合物,如木素磺酸盐、明胶、阿拉伯胶、磷脂、淀粉、疏水改性淀粉和纤维素衍生物,特别是纤维素酯和纤维素醚,此外为聚乙烯醇、聚乙酸乙烯酯、聚乙烯吡咯烷酮、聚丙烯酸、聚甲基丙烯酸和(甲基)丙烯酸与(甲基)丙烯酸酯的共聚物,并且还有甲基丙烯酸与甲基丙烯酸酯的碱金属氢氧化物中和的共聚物和任选被甲醛取代的萘磺酸盐的缩合物。
合适的固体填料和载体是在作物保护组合物中常用于此目的的所有物质。可以优选提及的无机颗粒,如具有0.005-20 µm、特别优选0.02-10 µm的平均颗粒大小的碳酸盐、硅酸盐、硫酸盐和氧化物。可以提及的实例是硫酸铵、磷酸铵、尿素、碳酸钙、硫酸钙、硫酸镁、氧化镁、氧化铝、二氧化硅、细分散的硅酸、硅胶、天然和合成的硅酸盐和铝硅酸盐和植物产品,如谷物粉、木粉和纤维素粉。
可存在于根据本发明使用的拌种剂中的合适的着色剂包括常用于此目的的所有着色剂。可以使用在水中具有少量溶解度的颜料和在水中可溶的染料。可以提及的实例包括公知的名为罗丹明B(Rhodamin B)、C.I.颜料红112(C.I. Pigment Red
112 )和C.I.溶剂红1(C.I. Solvent Red 1)的着色剂。使用的着色剂可以是无机色素,例如氧化铁、氧化钛、普鲁士蓝,和有机染料如茜素、偶氮和金属酞菁染料,以及微量营养素,如铁、锰、硼、铜、钴、钼和锌的盐。
可存在于根据本发明使用的拌种剂中的合适的润湿剂包括促进湿润并且常用于农用化学活性化合物制剂中的所有物质。优选使用烷基萘磺酸盐,如二异丙基萘磺酸盐或二异丁基萘磺酸盐。
可存在于根据本发明使用的拌种剂中的合适的分散剂和/或乳化剂包括常用于农用化学活性化合物制剂的所有非离子、阴离子和阳离子分散剂。优选使用非离子或阴离子分散剂、或非离子或阴离子分散剂混合物。特别合适的非离子分散剂是环氧乙烷/环氧丙烷嵌段聚合物、烷基酚聚乙二醇醚、以及三苯乙烯基酚聚乙二醇醚,及其磷酸化或硫酸化衍生物。特别合适的阴离子分散剂是木素磺酸盐、聚丙烯酸盐和芳基磺酸盐/甲醛缩合物。
可存在于根据本发明使用的拌种剂中的消泡剂包括常用于农用化学活性化合物制剂的所有泡沫抑制化合物。优选使用硅酮消泡剂、硬脂酸镁、硅酮乳剂、长链醇、脂肪酸及其盐以及有机氟化合物及其混合物。
可存在于根据本发明使用的拌种剂中的防腐剂包括可为此目的用于农用化学组合物的所有化合物。例如,可提到双氯酚和苯甲醇半缩甲醛。
可存在于根据本发明使用的拌种剂中的二次增稠剂包括可为此目的用于农用化学组合物的所有化合物。优选的是纤维素衍生物、丙烯酸衍生物、多糖,如黄原胶或硅酸镁铝、改性粘土、层状硅酸盐(phyllosilicates),如绿坡缕石和膨润土,以及细分散的硅酸。
可存在于根据本发明使用的拌种剂中的合适的胶粘剂包括可用于拌种的所有常规粘合剂。可作为优选提及的是聚乙烯吡咯烷酮、聚乙酸乙烯酯、聚乙烯醇和甲基纤维素(tylose)。
可存在于根据本发明使用的拌种剂中的合适的赤霉素优选为赤霉素A1、A3(=赤霉酸)、A4和A7;特别优选使用赤霉酸。赤霉素是已知的(参见R.Wegler “Chemie der
Pflanzenschutz- and Schädlingsbekämpfungsmittel”[Chemistry
of Crop Protection Agents and Pesticides],Vol.2,Springer Verlag,1970,第401-412页)。
制剂通常包含0.1-95重量%的活性化合物,优选0.5-90%。
本发明的活性化合物组合可以市售制剂的形式以及由所述制剂与其他活性化合物的混合物制备的使用形式存在,所述其他活性化合物如杀虫剂、引诱剂、绝育剂、杀细菌剂、杀螨剂、杀线虫剂、杀真菌剂、生长调节剂或除草剂。肥料的混合物也是可以的。
本发明的用活性化合物组合或组合物对植物和植物部位进行处理是通过常规处理方法直接进行或通过作用于其环境、生境或贮存空间而进行,所述常规处理方法例如浸渍、喷雾、雾化、灌溉、蒸发、撒粉、弥雾、撒播、发泡、涂抹、涂布、浇水(浇灌)、滴灌,并且,对于繁殖材料,特别是对于种子,还可通过包以外皮(incrust)、涂布一层或多层包衣等作为粉剂用于干处理种子、作为溶液用于处理种子、作为水溶性粉剂用于浆料处理。优选通过浸渍、喷雾、雾化、灌溉、蒸发、撒粉、弥雾、撒播、发泡、涂抹、涂布、浇水(浇灌)和滴灌施用。
与常规农业实践一致,以适合于施用形式的方式进行制剂施用。常规施用例如是用水稀释并将所获的喷雾液体喷雾、用油稀释后施用、不稀释直接施用、载体颗粒的拌种或土壤施用。
从市售制剂制备的施用形式的活性化合物含量可以在宽的范围内变化。施用形式的活性化合物浓度可以是从0.0000001高至95重量%的活性化合物,优选0.0001-2重量%。
本发明的组合物不仅仅包含可以用合适的装置向植物或种子施用的即用组合物,也包含使用前需要用水稀释的市售浓缩物。
施用方法
本发明的用氟吡菌酰胺或组合物对植物和植物部位进行处理是通过常规处理方法直接进行或通过作用于其环境、生境或贮存空间而进行,所述常规处理方法例如浸渍、喷雾、雾化、灌溉、茎注射、垄沟中施用(in-furrow
application)、蒸发、撒粉、弥雾、撒播、发泡、涂抹、涂布、浇水(浇灌)、滴灌,并且,对于繁殖材料,特别是对于种子,还可通过包以外皮(incrust)、涂布一层或多层包衣等作为粉剂用于干处理种子、作为溶液用于处理种子、作为水溶性粉剂用于浆料处理。此外可通过超低容量法施用活性化合物,或将活性化合物制剂或活性化合物本身注入土壤。
通常,以每公顷10 g-20 kg的比例施用氟吡菌酰胺,优选每公顷50
g-10 kg,最优选每公顷100 g-5 kg。
此外本发明包括一种处理种子的方法。本发明还涉及根据前述段落描述的方法之一处理的种子。
本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物尤其适用于处理种子。由有害生物引起的作物植物的大部分损害是由储存期间或播种后以及植物萌芽期间和植物萌芽后种子的感染引发的。由于生长中植物的根和芽特别敏感,并且甚至小的伤害也可能导致植物的死亡,因此这一阶段特别关键。因此,通过使用合适的组合物保护种子和发芽的植物受到极大关注。
通过处理植物种子防治线虫已为人所知很长时间并且是不断改进的主题。然而,对种子的处理带来一系列总无法以令人满意的方式解决的问题。因此,希望开发用于保护种子和发芽植物的方法,该方法无需在播种后或植物萌发后额外施用作物保护剂,或至少可显著减少额外施用。此外,还希望以此方式优化所用活性化合物的量,以为种子和发芽植物提供免受线虫侵袭的最大程度的保护,但所用活性化合物不会伤害植物自身。特别地,处理种子的方法还应考虑转基因植物的固有杀线虫特性,以用最少的作物保护剂实现对种子和发芽植物的最佳保护。
因此,本发明还特别涉及一种通过用本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物处理种子来保护种子和发芽植物抵抗线虫侵袭的方法。本发明还涉及本发明组合物用于处理种子以保护种子和发芽植物抵抗线虫的用途。此外,本发明涉及用本发明的组合物处理以保护其抵抗线虫的种子。
对萌发后损害植物的线虫的防治主要通过用作物保护组合物处理土壤和植物的地上部位进行。由于考虑到作物保护组合物对环境以及人类和动物健康的可能的影响,努力降低施用的活性化合物的量。
本发明的优势之一是,由于本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物特定的内吸特性,使用氟吡菌酰胺或这些组合物处理种子不仅保护种子自身,而且还保护萌发长成的植物免受线虫侵袭。以这种方式,可以省却在播种时或此后不久对作物的立即处理。
本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物适合于保护以下作物的种子:蔬菜(尤其是番茄和葫芦)、马铃薯、玉米、大豆、棉花、烟草、咖啡、水果(尤其是柑橘属水果、菠萝和香蕉)和葡萄。
本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物尤其适合于保护大豆的种子,特别是抵抗大豆胞囊线虫。
本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物适合于保护葫芦的种子,特别是抵抗南方根结线虫。
如下文还进一步描述的,用本发明的氟吡菌酰胺或组合物处理转基因种子特别重要。这指的是含有至少一种能表达具有杀虫特性的多肽或蛋白质的异源基因的植物种子。转基因种子中的异源基因可来源于例如以下的微生物:芽孢杆菌属(Bacillus)、根瘤菌属(Rhizobium)、假单胞菌属(Pseudomonas)、沙雷氏菌属(Serratia)、木霉属(Trichoderma)、棒形杆菌属(Clavibacter)、球囊霉菌属(Glomus)或粘帚霉属(Gliocladium)。优选地,该异源基因来源于芽孢杆菌属,基因产物对欧洲玉米螟(European
corn borer)和/或西部玉米根虫(Western
corn rootworm)具有活性。特别优选地,该异源基因来源于苏云金芽孢杆菌。
在本发明的上下文中,本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物可以其本身或以合适制剂的形式施用于种子。优选地,种子以足够稳定的状态进行处理从而使得该处理不会造成任何伤害。通常,对种子的处理可在采收和播种之间的任何时间点进行。通常,使所用种子与植物分离且除去穗轴、外壳、茎、表皮、绒毛或果肉。因此,可以使用例如已采收、清洁且干燥至含水量少于15重量%的种子。可选择地,也可以使用干燥后用例如水处理、随后再次干燥的种子。
当处理种子时,通常必须注意的是,要以这样一种方式选择施用于种子的本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物的量和/或其他添加剂的量,使得种子发芽不会受到不利影响,或长成的植物不受损害。此点必须考虑到,特别是对于在某些施用率下可能具有植物毒性作用的活性化合物。
本发明的氟吡菌酰胺或包含氟吡菌酰胺的组合物可直接施用,也就是说既不包含其他组分也没经过稀释。通常,优选将所述组合物以合适制剂的形式施用于种子。合适制剂和处理种子的方法为本领域技术人员已知并记载于例如下列文件:US
4,272,417 A、US 4,245,432 A、US 4,808,430 A、US 5,876,739
A、US 2003/0176428 A1、WO 2002/080675 A1、WO
2002/028186 A2。
可根据本发明使用的氟吡菌酰胺或包含氟吡菌酰胺的组合物可转化为常规拌种剂,如溶液剂、乳剂、悬浮剂、粉剂、泡沫剂、浆液或其他的种子包衣材料,以及ULV制剂。
这些制剂以已知方式通过将活性化合物或活性化合物组合与常规添加剂混合而制备,所述常规添加剂如常规填充剂以及溶剂或稀释剂、着色剂、润湿剂、分散剂、乳化剂、消泡剂、防腐剂、二次增稠剂、胶粘剂、赤霉素和水。
可存在于可根据本发明使用的拌种剂中的合适的着色剂包括常用于此目的的所有着色剂。可使用微溶于水的颜料和溶于水的染料。可提到的实例包括已知的名为罗丹明B、C.I.颜料红112和C.I.溶剂红1的着色剂。
可存在于可根据本发明使用的拌种剂中的合适的润湿剂包括常用于农用化学活性物质制剂的促进润湿的所有物质。优选可使用烷基萘磺酸盐,如二异丙基萘磺酸盐或二异丁基萘磺酸盐。
可存在于可根据本发明使用的拌种剂中的合适的分散剂和/或乳化剂包括常用于农用化学活性物质制剂的所有非离子、阴离子和阳离子分散剂。优选地,可使用非离子或阴离子分散剂、或非离子或阴离子分散剂混合物。特别合适的非离子分散剂是环氧乙烷-环氧丙烷嵌段聚合物、烷基酚聚乙二醇醚、和三苯乙烯基酚聚乙二醇醚,及其磷酸化或硫酸化衍生物。特别合适的阴离子分散剂是木素磺酸盐、聚丙烯酸盐和芳基磺酸盐-甲醛缩合物。
可存在于根据本发明使用的拌种剂中的消泡剂包括常用于农用化学活性化合物制剂的所有泡沫抑制化合物。优选使用硅酮消泡剂、硬脂酸镁、硅酮乳剂、长链醇、脂肪酸及其盐以及有机氟化合物及其混合物。
可存在于根据本发明使用的拌种剂中的防腐剂包括可为此目的用于农用化学组合物的所有化合物。例如,可提到双氯酚和苯甲醇半缩甲醛。
可存在于根据本发明使用的拌种剂中的二次增稠剂包括可为此目的用于农用化学组合物的所有化合物。优选的是纤维素衍生物、丙烯酸衍生物、多糖,如黄原胶或硅酸镁铝、改性粘土、层状硅酸盐(phyllosilicates),如绿坡缕石和膨润土,以及细分散的硅酸。
可存在于根据本发明使用的拌种剂中的合适的胶粘剂包括可用于拌种的所有常规粘合剂。可作为优选提及的是聚乙烯吡咯烷酮、聚乙酸乙烯酯、聚乙烯醇和甲基纤维素(tylose)。
可存在于根据本发明使用的拌种剂中的合适的赤霉素优选为赤霉素A1、A3(=赤霉酸)、A4和A7;特别优选使用赤霉酸。赤霉素是已知的(参见R.Wegler “Chemie der
Pflanzenschutz- and Schädlingsbekämpfungsmittel”[Chemistry
of Crop Protection Agents and Pesticides],Vol.2,Springer Verlag,1970,第401-412页)。
可根据本发明使用的拌种剂可直接或预先用水稀释后使用以处理极宽范围种类中的任一种种子。可根据本发明使用的拌种剂或其稀释制剂也可用于对转基因植物的种子进行拌种。在上下文中,协同效应也可在与表达形成的物质的相互作用中产生。
用可根据本发明使用的拌种剂或由其通过加水制备的制剂处理种子的合适的混合设备包括通常可用于拌种的所有混合设备。拌种时采用的具体步骤包括:将种子加入混合机中;加入具体所需量的拌种制剂——以其本身或预先用水稀释后;进行混合直到制剂已均匀分布在种子上。任选地,随后进行干燥操作。
本发明的杀线虫组合物可用于治疗性或保护性防治线虫。因此,本发明也涉及使用本发明的氟吡菌酰胺和包含氟吡菌酰胺的组合物防治线虫的治疗性和保护性方法,将所述氟吡菌酰胺和包含氟吡菌酰胺的组合物施用于种子、植物或植物部位、果实或植物生长的土壤。优选的是施用于植物或植物部位、果实或土壤。
用于在作物保护中防治线虫的本发明组合物包含有活性的、但非植物毒性量的本发明化合物。“有活性的、但非植物毒性量”意思是足以防治或完全杀死由线虫引起的植物病害并且同时不显示明显的植物毒性症状的本发明组合物的量。这些施用率通常可在较宽范围内变化,其取决于多种因素,例如线虫、植物或作物、气候条件和本发明组合物的成分。
活性化合物在防治植物病害所需浓度下具有很好的植物耐受性的事实使得可对地上植物部位、无性繁殖材料和种子以及土壤进行处理。
在示例性的种子处理方法中,可以这样的比例施用包含氟吡菌酰胺的含水组合物,所述比例的可以提供的范围为每100 kg (dt)种子0.5 g-10 kg、优选0.8
g-5 kg、最优选1 g-1 kg的氟吡菌酰胺。
在进一步的实施方式中,本发明涉及氟吡菌酰胺用于防治番茄中南方根结线虫的用途。
在进一步的实施方式中,本发明涉及氟吡菌酰胺用于防治番茄中螺旋线虫属的用途。
在进一步的实施方式中,本发明涉及氟吡菌酰胺用于防治马铃薯中北方根结线虫的用途。
在进一步的实施方式中,本发明涉及氟吡菌酰胺用于防治柑橘中半穿刺线虫的用途。
在进一步的实施方式中,本发明涉及氟吡菌酰胺用于防治香蕉中香蕉穿孔线虫的用途。
在进一步的实施方式中,本发明涉及包括以植物浇灌施用方式施用氟吡菌酰胺用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以植物浇灌施用方式施用氟吡菌酰胺用于防治番茄中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以植物垄沟中施用方式施用氟吡菌酰胺用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以植物垄沟中施用方式施用氟吡菌酰胺用于防治马铃薯中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以浇灌施用方式施用氟吡菌酰胺用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以浇灌施用方式施用氟吡菌酰胺用于防治柑橘中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以浇灌施用方式施用氟吡菌酰胺用于防治香蕉中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以茎注射施用方式施用氟吡菌酰胺用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以茎注射施用方式施用氟吡菌酰胺用于防治香蕉中线虫的处理方法。
在进一步的实施方式中,本发明涉及包含氟吡菌酰胺的组合物用于防治番茄中南方根结线虫的用途。
在进一步的实施方式中,本发明涉及包含氟吡菌酰胺的组合物用于防治番茄中螺旋线虫属的用途。
在进一步的实施方式中,本发明涉及包含氟吡菌酰胺的组合物用于防治马铃薯中北方根结线虫的用途。
在进一步的实施方式中,本发明涉及包含氟吡菌酰胺的组合物用于防治柑橘中半穿刺线虫的用途。
在进一步的实施方式中,本发明涉及包含氟吡菌酰胺的组合物用于防治香蕉中香蕉穿孔线虫的用途。
在进一步的实施方式中,本发明涉及包括以植物浇灌施用方式施用包含氟吡菌酰胺的组合物用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以植物浇灌施用方式施用包含氟吡菌酰胺的组合物用于防治番茄中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以植物垄沟中施用方式施用包含氟吡菌酰胺的组合物用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以植物垄沟中施用方式施用包含氟吡菌酰胺的组合物用于防治马铃薯中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以浇灌施用方式施用包含氟吡菌酰胺的组合物用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以浇灌施用方式施用包含氟吡菌酰胺的组合物用于防治柑橘中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以浇灌施用方式施用包含氟吡菌酰胺的组合物用于防治香蕉中线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以茎注射施用方式施用包含氟吡菌酰胺的组合物用于防治线虫的处理方法。
在进一步的实施方式中,本发明涉及包括以茎注射施用方式施用包含氟吡菌酰胺的组合物用于防治香蕉中线虫的处理方法。
本发明的一般概念描述于以下实施例中,不将其作为限定。
实施例
A
番茄中的南方根结线虫-在植物浇灌施用方式下
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂在种植番茄时对包含南方根结线虫(南方根结线虫)的混合种群的土壤进行浇灌。
经过特定时期后,根据虫瘿形成百分比来测定杀线虫活性。100 %表示没有虫瘿形成;0 %表示在处理植物的根上发现的虫瘿数等于未处理的对照植物的根上的虫瘿数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表A:南方根结线虫-番茄中检测
实施例
B
番茄中的螺旋线虫属-在植物浇灌施用方式下
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂在种植番茄时对包含螺旋线虫(螺旋线虫属)的混合种群的土壤进行浇灌。
经过特定时期后,通过对线虫计数来测定杀线虫活性。100 %表示没有发现线虫;0 %表示在处理土壤中发现的线虫数等于未处理土壤中的线虫数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表B:螺旋线虫属-番茄中检测
实施例
C
马铃薯中的北方根结线虫-在植物垄沟中施用方式下
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂以植物垄沟中施用方式在种植马铃薯时对包含北方根结线虫(北方根结线虫)的混合种群的土壤进行处理。
经过特定时期后,根据侵袭的块根的百分比来测定杀线虫活性。100 %表示没有发现侵袭的块根;0 %表示处理植物的侵袭的块根数等于未处理的对照植物的侵袭的块根数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表C:北方根结线虫-马铃薯中检测
实施例
D
柑橘中的半穿刺线虫-浇灌施用
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂对柑橘树冠下包含柑橘线虫(半穿刺线虫)的混合种群的土壤进行浇灌。
经过特定时期后,通过对线虫计数来测定杀线虫活性。100 %表示没有发现线虫;0 %表示在处理土壤中发现的线虫数等于未处理土壤中的线虫数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表D:半穿刺线虫-柑橘中检测
实施例
E
香蕉中的香蕉穿孔线虫-浇灌施用
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂对香蕉下受香蕉根线虫(香蕉穿孔线虫)的混合种群侵袭的土壤进行浇灌。
经过特定时期后,通过对香蕉根中的线虫计数来测定杀线虫活性。100 %表示没有发现线虫;0 %表示在处理样地中发现的线虫数等于未处理样地中的线虫数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表F:香蕉穿孔线虫-香蕉中检测
实施例
G
香蕉中的香蕉穿孔线虫-茎注射
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂对香蕉的茎注射,所述香蕉生长在受香蕉根线虫(香蕉穿孔线虫)的混合种群侵袭的土壤中。
经过特定时期后,通过对香蕉根中的线虫计数来测定杀线虫活性。100 %表示没有发现线虫;0 %表示在处理样地中发现的线虫数等于未处理样地中的线虫数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表G:香蕉穿孔线虫-香蕉中检测
实施例
H
番茄中的南方根结线虫-移植后滴灌施用
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂在番茄移植后6天通过滴灌对包含南方根结线虫(南方根结线虫)的混合种群的土壤进行处理。
经过特定时期后,根据虫瘿形成百分比来测定杀线虫活性。100 %表示没有虫瘿形成;0 %表示在处理植物的根上发现的虫瘿数等于未处理的对照植物的根上的虫瘿数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表H:南方根结线虫-番茄中检测
实施例
I
黄瓜中的爪哇根结线虫-在植物滴灌施用方式下
为了制备合适的制品,用水将制剂稀释至所需浓度。
用制剂通过滴灌在黄瓜种植时对包含根结线虫(爪哇根结线虫)的混合种群的土壤进行处理。
经过特定时期后,根据虫瘿形成百分比来测定杀线虫活性。100 %表示没有虫瘿形成;0 %表示在处理植物的根上发现的虫瘿数等于未处理的对照植物的根上的虫瘿数。
在该检测中,例如,制备实施例中的以下制剂显示出良好的活性:
表I:爪哇根结线虫-黄瓜中检测
Claims (8)
3. 权利要求1或2的用途,其中所述组合物除填充剂和/或表面活性剂之外,包含
A)氟吡菌酰胺和
B)至少一种农用化学活性化合物。
4. 权利要求1至3中任一项的用途,其中氟吡菌酰胺以每公顷100 g-5 kg的比例施用。
5. 防治线虫的方法,其包括向植物施用权利要求1至4的氟吡菌酰胺。
6. 处理种子的方法,其用于防治选自蔬菜、马铃薯、玉米、大豆、棉花和香蕉的作物组中的线虫,所述方法包括向种子施用权利要求1至4的组合物。
7. 提高产量的方法,其包括向植物施用权利要求1至5的氟吡菌酰胺。
8. 提高产量的方法,其包括向种子施用权利要求1至4和6的氟吡菌酰胺。
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CN111602663A (zh) * | 2019-02-25 | 2020-09-01 | 中国农业大学 | 一种悬浮型杀线种衣剂 |
CN110200067A (zh) * | 2019-07-08 | 2019-09-06 | 桂林理工大学 | 一种黄秋葵的保鲜方法 |
CN113115799A (zh) * | 2021-04-01 | 2021-07-16 | 沈阳恩柽研究院有限公司 | 一种姜黄挥发油的应用 |
CN113115799B (zh) * | 2021-04-01 | 2022-01-25 | 沈阳恩柽研究院有限公司 | 一种姜黄挥发油的应用 |
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WO2012072660A1 (en) | 2012-06-07 |
BR112013013670A2 (pt) | 2016-07-12 |
ZA201304854B (en) | 2014-12-23 |
KR20130123416A (ko) | 2013-11-12 |
EP3372081A2 (en) | 2018-09-12 |
JP2014503508A (ja) | 2014-02-13 |
AU2017213496A1 (en) | 2017-08-31 |
US20160270394A1 (en) | 2016-09-22 |
JP2017197561A (ja) | 2017-11-02 |
EP2645856A1 (en) | 2013-10-09 |
JP6412311B2 (ja) | 2018-10-24 |
MX2013005356A (es) | 2013-07-05 |
CN107396929A (zh) | 2017-11-28 |
AP3519A (en) | 2016-01-11 |
AU2016201043A1 (en) | 2016-03-10 |
AP2013006951A0 (en) | 2013-06-30 |
AU2011334989A1 (en) | 2013-06-13 |
US20130253018A1 (en) | 2013-09-26 |
EP3372081A3 (en) | 2018-10-24 |
KR20180096815A (ko) | 2018-08-29 |
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