CN101506173A - 制备3-二卤代甲基吡唑-4-羧酸衍生物的方法 - Google Patents
制备3-二卤代甲基吡唑-4-羧酸衍生物的方法 Download PDFInfo
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- CN101506173A CN101506173A CNA200780031363XA CN200780031363A CN101506173A CN 101506173 A CN101506173 A CN 101506173A CN A200780031363X A CNA200780031363X A CN A200780031363XA CN 200780031363 A CN200780031363 A CN 200780031363A CN 101506173 A CN101506173 A CN 101506173A
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- thiazolinyl
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
Abstract
Description
Claims (12)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102006039909.9 | 2006-08-25 | ||
DE102006039909A DE102006039909A1 (de) | 2006-08-25 | 2006-08-25 | Verfahren zum Herstellen von 3-Dihalomethyl-pyrazol-4-carbonsäurederivaten |
PCT/EP2007/007377 WO2008022777A2 (de) | 2006-08-25 | 2007-08-22 | Verfahren zum herstellen von 3-dihalomethyl-pyrazol-4-carbonsäurederivaten |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101506173A true CN101506173A (zh) | 2009-08-12 |
CN101506173B CN101506173B (zh) | 2012-05-30 |
Family
ID=39015935
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN200780031363XA Active CN101506173B (zh) | 2006-08-25 | 2007-08-22 | 制备3-二卤代甲基吡唑-4-羧酸衍生物的方法 |
Country Status (16)
Country | Link |
---|---|
US (1) | US7939673B2 (zh) |
EP (1) | EP2057126B1 (zh) |
JP (2) | JP5511380B2 (zh) |
KR (1) | KR101445326B1 (zh) |
CN (1) | CN101506173B (zh) |
AT (1) | ATE487702T1 (zh) |
BR (1) | BRPI0715674B1 (zh) |
CA (1) | CA2661407C (zh) |
DE (2) | DE102006039909A1 (zh) |
DK (1) | DK2057126T3 (zh) |
ES (1) | ES2355309T3 (zh) |
IL (1) | IL196894A (zh) |
MX (1) | MX2009001840A (zh) |
RU (1) | RU2470015C2 (zh) |
TW (1) | TWI419880B (zh) |
WO (1) | WO2008022777A2 (zh) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101720317B (zh) * | 2007-06-15 | 2014-07-09 | 巴斯夫欧洲公司 | 生产二氟甲基取代的吡唑化合物的方法 |
CN104245676A (zh) * | 2012-02-01 | 2014-12-24 | 拜耳农作物科学股份公司 | 用于制备3,5-双(氟烷基)吡唑-4-甲酸衍生物和3,5-双(氟烷基)吡唑类化合物的方法 |
CN104529899A (zh) * | 2014-12-19 | 2015-04-22 | 浙江泰达作物科技有限公司 | 高区域选择性制备1-烷基-3-卤代烷基吡唑衍生物的方法 |
CN105541716A (zh) * | 2015-03-26 | 2016-05-04 | 旭硝子株式会社 | 吡唑衍生物的制造方法 |
CN105722827A (zh) * | 2013-11-11 | 2016-06-29 | 拜耳作物科学股份公司 | 由α,α-二卤代胺类制备3,5-双(卤代烷基)吡唑衍生物的方法 |
CN106164049A (zh) * | 2014-03-24 | 2016-11-23 | 拜耳作物科学股份公司 | 由α,α‑二卤胺和酮亚胺制备3,5‑二(卤代烷基)吡唑衍生物的方法 |
CN107960078A (zh) * | 2015-06-26 | 2018-04-24 | 拜耳作物科学股份公司 | 由α,α-二卤代烷基胺和酮亚胺制备含有卤代烷氧基和卤代烷硫基的取代的吡唑的方法 |
CN112041303A (zh) * | 2018-05-21 | 2020-12-04 | Pi工业有限公司 | 制备取代的杂环化合物的方法 |
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KR101517254B1 (ko) | 2007-06-01 | 2015-04-30 | 바스프 에스이 | N-치환된 (3-디할로메틸-1-메틸-피라졸-4-일)카르복사미드의 제조 방법 |
WO2009021987A1 (en) | 2007-08-16 | 2009-02-19 | Solvay (Société Anonyme) | Process for the preparation of esters of 4-fluorosubstituted 3-oxo-alcanoic acids |
EP2133341A1 (de) | 2008-02-25 | 2009-12-16 | Bayer CropScience AG | Verfahren zur regioselektiven Synthese von 1-Alkyl-3-haloalkyl-pyrazol-4-carbonsäure-Derivaten |
EP2100883A1 (de) | 2008-03-10 | 2009-09-16 | Bayer CropScience AG | Verfahren zur regioselektiven Synthese von 1-Alkyl-3-haloalkyl-pyrazol-4carbonsäure-Derivaten |
PL2300417T3 (pl) | 2008-05-02 | 2015-12-31 | Basf Se | Sposób wytwarzania estrów kwasu 2-(aminometylideno)-4,4-difluoro-3-oksomasłowego |
ES2386940T3 (es) * | 2008-05-02 | 2012-09-06 | Basf Se | Método para la preparación de ésteres halosustituidos de ácido 2-(aminometiliden)-3-oxobutírico |
UA106470C2 (uk) | 2008-05-05 | 2014-09-10 | Басф Се | Спосіб одержання 1,3,4-заміщених піразольних сполук |
ATE555098T1 (de) | 2008-07-21 | 2012-05-15 | Basf Se | Verfahren zur herstellung 1,3-disubstituierter pyrazolcarbonsäureester |
GB0908435D0 (en) * | 2009-05-15 | 2009-06-24 | Syngenta Ltd | Processes |
EP2496560B1 (en) * | 2009-11-05 | 2015-04-22 | Basf Se | Process for preparing 1,3-disubstituted pyrazole compounds |
CN102596911B (zh) | 2009-11-05 | 2015-04-08 | 巴斯夫欧洲公司 | 制备缩醛胺的方法及其在制备1,3-二取代的吡唑化合物中的用途 |
JP5819938B2 (ja) | 2010-04-23 | 2015-11-24 | バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツングBayer Intellectual Property GmbH | 5−フルオロ−1−アルキル−3−フルオロアルキル−1h−ピラゾール−4−カルボニルクロリドおよびフルオリドの調製方法 |
CN103619822A (zh) | 2011-06-21 | 2014-03-05 | 拜耳知识产权有限责任公司 | 制备吡唑基甲酰苯胺类化合物的方法 |
JP5931291B2 (ja) | 2012-08-30 | 2016-06-08 | バイエル・クロップサイエンス・アクチェンゲゼルシャフト | 3,5−ビス(ハロアルキル)−ピラゾール−4−カルボン酸誘導体の脱カルボキシル化手順 |
US8871947B2 (en) | 2013-02-04 | 2014-10-28 | KingChem LLC | Preparation of alkyl 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid ester |
BR112015028751B1 (pt) * | 2013-05-22 | 2021-01-12 | Bayer Cropscience Aktiengesellschaft | Processo para a preparação de derivados de 3,5-bis (fluoralquil)pirazol a partir de alfa, alfa-dihaloaminas e uso destes para preparação de ingredientes fungicidas ativos |
MX2015016119A (es) | 2013-05-22 | 2016-03-31 | Bayer Cropscience Ag | Metodo para preparar derivados de 3,5-bis(fluoroalquil)pirazol. |
CN104379551B (zh) | 2013-12-09 | 2017-03-08 | 金凯有限责任公司 | 3‑二氟甲基‑1‑甲基‑1h‑吡唑‑4‑羧酸烷基酯及其类似物的制备方法 |
EP3015458A1 (en) | 2014-11-03 | 2016-05-04 | Bayer CropScience AG | Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives from a,a-dihaloamines and ketimines |
KR102430607B1 (ko) | 2014-06-11 | 2022-08-08 | 바이엘 크롭사이언스 악티엔게젤샤프트 | 케트이민의 아실화를 통한 3,5-비스(할로알킬)피라졸의 제조 방법 |
EP3154946B1 (en) | 2014-06-11 | 2018-04-18 | Bayer CropScience Aktiengesellschaft | Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives via acylation of hydrazones |
EP3312161B1 (en) * | 2015-06-19 | 2020-11-04 | Zhejiang Yongtai Technology Co., Ltd. | Method for preparing pyrazolecarboxylic acid derivative, and intermediate thereof |
EP3178813A1 (en) | 2015-12-09 | 2017-06-14 | Basf Se | Method for preparing halogenated 3-oxocarboxylates carrying a 2-alkoxymethylidene or a 2-dialkylaminomethylidene group |
JP2019502723A (ja) | 2016-01-21 | 2019-01-31 | バイエル・クロップサイエンス・アクチェンゲゼルシャフト | ポリフルオロアルキル化キノリン類の製造方法 |
MX2019003255A (es) | 2016-09-21 | 2019-07-18 | Bayer Cropscience Ag | Proceso para la preparacion de 3-fluoroalquil-5-pirazolcarboxilato s y acidos 3-fluoroalquil-5-pirazolcarboxilicos. |
WO2018234184A1 (en) | 2017-06-22 | 2018-12-27 | Bayer Aktiengesellschaft | PROCESS FOR THE PREPARATION OF 2,3,4-TRISUBSTITUTED QUINOLINES |
JP2021506879A (ja) | 2017-12-22 | 2021-02-22 | ソルヴェイ(ソシエテ アノニム) | ピラゾールカルボン酸誘導体及びその前駆体の製造のための方法 |
KR20210022049A (ko) | 2018-06-18 | 2021-03-02 | 바이엘 악티엔게젤샤프트 | 이치환된 5(3)-피라졸 카르복실레이트, 및 에놀레이트 및 플루오로알킬아미노시약 (far) 시약으로부터의 그의 제조 방법 |
WO2020093715A1 (en) | 2018-11-07 | 2020-05-14 | Fujian Yongjing Technology Co., Ltd | New process for manufacture of pyrazoles or pyrimidones |
CN110577503A (zh) * | 2019-08-02 | 2019-12-17 | 宿迁市科莱博生物化学有限公司 | 一种卤素取代化合物及其制备方法和应用 |
Family Cites Families (10)
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US5489624A (en) * | 1992-12-01 | 1996-02-06 | Minnesota Mining And Manufacturing Company | Hydrophilic pressure sensitive adhesives |
DE4302156A1 (de) * | 1993-01-27 | 1994-07-28 | Bayer Ag | Verfahren zur Herstellung von Aminomethylenverbindungen |
US5359089A (en) * | 1993-12-22 | 1994-10-25 | American Cyanamid Company | Process for the preparation of 2,4,5-tribromopyrrole-3-carbonitrile |
GB0101996D0 (en) * | 2001-01-25 | 2001-03-14 | Syngenta Participations Ag | Organtic compounds |
DE10161978A1 (de) * | 2001-12-17 | 2003-06-26 | Bayer Ag | Verfahren zur Herstellung von 2-Halogenacyl-3-amino-acrylsäure-derivate |
CA2477931C (en) | 2002-03-05 | 2011-02-01 | Josef Ehrenfreund | O-cyclopropyl-carboxanilides and their use as fungicides |
DE10349500A1 (de) * | 2003-10-23 | 2005-06-02 | Bayer Cropscience Ag | Verfahren zum Herstellen von 2-Dihalogenacyl-3-amino-acrylsäureestern und 3-Dihalogenmethyl-pyrazol-4-carbonsäureestern |
GB0415764D0 (en) * | 2004-07-14 | 2004-08-18 | Syngenta Participations Ag | Chemical process |
JP4971170B2 (ja) * | 2004-10-21 | 2012-07-11 | シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト | ピラゾールの調製のための方法 |
JP5559678B2 (ja) * | 2007-06-15 | 2014-07-23 | ビーエーエスエフ ソシエタス・ヨーロピア | ジフルオロメチル置換ピラゾール化合物の製造方法 |
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2006
- 2006-08-25 DE DE102006039909A patent/DE102006039909A1/de not_active Withdrawn
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2007
- 2007-08-22 CN CN200780031363XA patent/CN101506173B/zh active Active
- 2007-08-22 BR BRPI0715674-0A patent/BRPI0715674B1/pt active IP Right Grant
- 2007-08-22 US US12/438,732 patent/US7939673B2/en active Active
- 2007-08-22 JP JP2009524958A patent/JP5511380B2/ja active Active
- 2007-08-22 EP EP07801808A patent/EP2057126B1/de active Active
- 2007-08-22 KR KR1020097005762A patent/KR101445326B1/ko active IP Right Grant
- 2007-08-22 DE DE502007005625T patent/DE502007005625D1/de active Active
- 2007-08-22 MX MX2009001840A patent/MX2009001840A/es active IP Right Grant
- 2007-08-22 RU RU2009110413/04A patent/RU2470015C2/ru active
- 2007-08-22 ES ES07801808T patent/ES2355309T3/es active Active
- 2007-08-22 AT AT07801808T patent/ATE487702T1/de active
- 2007-08-22 DK DK07801808.2T patent/DK2057126T3/da active
- 2007-08-22 WO PCT/EP2007/007377 patent/WO2008022777A2/de active Application Filing
- 2007-08-22 CA CA2661407A patent/CA2661407C/en active Active
- 2007-08-24 TW TW096131325A patent/TWI419880B/zh active
-
2009
- 2009-02-04 IL IL196894A patent/IL196894A/en active IP Right Grant
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2013
- 2013-08-16 JP JP2013169060A patent/JP5805717B2/ja active Active
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101720317B (zh) * | 2007-06-15 | 2014-07-09 | 巴斯夫欧洲公司 | 生产二氟甲基取代的吡唑化合物的方法 |
TWI609006B (zh) * | 2012-02-01 | 2017-12-21 | 拜耳作物科學股份有限公司 | 製備3,5-雙(氟烷基)吡唑-4-羧酸衍生物及3,5-雙(氟烷基)吡唑類之方法 |
CN104245676A (zh) * | 2012-02-01 | 2014-12-24 | 拜耳农作物科学股份公司 | 用于制备3,5-双(氟烷基)吡唑-4-甲酸衍生物和3,5-双(氟烷基)吡唑类化合物的方法 |
CN105722827B (zh) * | 2013-11-11 | 2019-01-22 | 拜耳作物科学股份公司 | 由α, α-二卤代胺类制备3,5-双(卤代烷基)吡唑衍生物的方法 |
CN105722827A (zh) * | 2013-11-11 | 2016-06-29 | 拜耳作物科学股份公司 | 由α,α-二卤代胺类制备3,5-双(卤代烷基)吡唑衍生物的方法 |
CN106164049B (zh) * | 2014-03-24 | 2019-04-12 | 拜耳作物科学股份公司 | 由α,α-二卤胺和酮亚胺制备3,5-二(卤代烷基)吡唑衍生物的方法 |
CN106164049A (zh) * | 2014-03-24 | 2016-11-23 | 拜耳作物科学股份公司 | 由α,α‑二卤胺和酮亚胺制备3,5‑二(卤代烷基)吡唑衍生物的方法 |
CN104529899A (zh) * | 2014-12-19 | 2015-04-22 | 浙江泰达作物科技有限公司 | 高区域选择性制备1-烷基-3-卤代烷基吡唑衍生物的方法 |
CN105541716A (zh) * | 2015-03-26 | 2016-05-04 | 旭硝子株式会社 | 吡唑衍生物的制造方法 |
TWI703119B (zh) * | 2015-03-26 | 2020-09-01 | 日商Agc股份有限公司 | 吡唑衍生物之製造方法 |
CN105541716B (zh) * | 2015-03-26 | 2024-02-23 | Agc株式会社 | 吡唑衍生物的制造方法 |
CN107960078A (zh) * | 2015-06-26 | 2018-04-24 | 拜耳作物科学股份公司 | 由α,α-二卤代烷基胺和酮亚胺制备含有卤代烷氧基和卤代烷硫基的取代的吡唑的方法 |
CN112041303A (zh) * | 2018-05-21 | 2020-12-04 | Pi工业有限公司 | 制备取代的杂环化合物的方法 |
Also Published As
Publication number | Publication date |
---|---|
WO2008022777A3 (de) | 2008-04-17 |
WO2008022777A8 (de) | 2009-04-09 |
KR20090043580A (ko) | 2009-05-06 |
RU2470015C2 (ru) | 2012-12-20 |
US20090326242A1 (en) | 2009-12-31 |
BRPI0715674B1 (pt) | 2015-06-16 |
TW200817335A (en) | 2008-04-16 |
IL196894A (en) | 2015-03-31 |
JP5805717B2 (ja) | 2015-11-04 |
ATE487702T1 (de) | 2010-11-15 |
ES2355309T3 (es) | 2011-03-24 |
DK2057126T3 (da) | 2011-02-28 |
DE102006039909A1 (de) | 2008-03-13 |
DE502007005625D1 (de) | 2010-12-23 |
CN101506173B (zh) | 2012-05-30 |
IL196894A0 (en) | 2009-11-18 |
BRPI0715674A2 (pt) | 2013-07-09 |
WO2008022777A2 (de) | 2008-02-28 |
RU2009110413A (ru) | 2010-09-27 |
JP2010501502A (ja) | 2010-01-21 |
EP2057126A2 (de) | 2009-05-13 |
EP2057126B1 (de) | 2010-11-10 |
CA2661407C (en) | 2014-07-15 |
KR101445326B1 (ko) | 2014-09-29 |
TWI419880B (zh) | 2013-12-21 |
US7939673B2 (en) | 2011-05-10 |
JP2014001226A (ja) | 2014-01-09 |
JP5511380B2 (ja) | 2014-06-04 |
MX2009001840A (es) | 2009-03-03 |
CA2661407A1 (en) | 2008-02-28 |
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