TWI860477B - 真空凍結乾燥裝置及真空凍結乾燥方法 - Google Patents

真空凍結乾燥裝置及真空凍結乾燥方法 Download PDF

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Publication number
TWI860477B
TWI860477B TW110117714A TW110117714A TWI860477B TW I860477 B TWI860477 B TW I860477B TW 110117714 A TW110117714 A TW 110117714A TW 110117714 A TW110117714 A TW 110117714A TW I860477 B TWI860477 B TW I860477B
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Taiwan
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aforementioned
temperature
cylindrical
cylindrical portion
drying device
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TW110117714A
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English (en)
Chinese (zh)
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TW202202792A (zh
Inventor
盛本修司
竹原誠
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日商Ｍｉｉ股份有限公司
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
    • F26B5/065—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing the product to be freeze-dried being sprayed, dispersed or pulverised
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B11/00—Machines or apparatus for drying solid materials or objects with movement which is non-progressive
    • F26B11/02—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles
    • F26B11/024—Arrangements for gas-sealing the drum
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B11/00—Machines or apparatus for drying solid materials or objects with movement which is non-progressive
    • F26B11/02—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles
    • F26B11/026—Arrangements for charging or discharging the materials to be dried, e.g. discharging by reversing drum rotation, using spiral-type inserts
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B11/00—Machines or apparatus for drying solid materials or objects with movement which is non-progressive
    • F26B11/02—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles
    • F26B11/04—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles rotating about a horizontal or slightly-inclined axis
    • F26B11/0436—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles rotating about a horizontal or slightly-inclined axis comprising multiple stages, e.g. multiple rotating drums subsequently receiving the material to be dried; Provisions for heat recuperation
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B11/00—Machines or apparatus for drying solid materials or objects with movement which is non-progressive
    • F26B11/02—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles
    • F26B11/04—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles rotating about a horizontal or slightly-inclined axis
    • F26B11/0463—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles rotating about a horizontal or slightly-inclined axis having internal elements, e.g. which are being moved or rotated by means other than the rotating drum wall
    • F26B11/0477—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles rotating about a horizontal or slightly-inclined axis having internal elements, e.g. which are being moved or rotated by means other than the rotating drum wall for mixing, stirring or conveying the materials to be dried, e.g. mounted to the wall, rotating with the drum
    • F26B11/0481—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in moving drums or other mainly-closed receptacles rotating about a horizontal or slightly-inclined axis having internal elements, e.g. which are being moved or rotated by means other than the rotating drum wall for mixing, stirring or conveying the materials to be dried, e.g. mounted to the wall, rotating with the drum the elements having a screw- or auger-like shape, or form screw- or auger-like channels
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
    • F26B17/18—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by rotating helical blades or other rotary conveyors which may be heated moving materials in stationary chambers, e.g. troughs
    • F26B17/20—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by rotating helical blades or other rotary conveyors which may be heated moving materials in stationary chambers, e.g. troughs the axis of rotation being horizontal or slightly inclined
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
    • F26B17/26—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by reciprocating or oscillating conveyors propelling materials over stationary surfaces; with movement performed by reciprocating or oscillating shelves, sieves, or trays
    • F26B17/266—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by reciprocating or oscillating conveyors propelling materials over stationary surfaces; with movement performed by reciprocating or oscillating shelves, sieves, or trays the materials to be dried being moved in a helical, spiral or circular path, e.g. vibrated helix
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00—Arrangements for supplying or controlling air or other gases for drying solid materials or objects
    • F26B21/30—Controlling, e.g. regulating, parameters of gas supply
    • F26B21/35—Temperature; Pressure
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B23/00—Heating arrangements
    • F26B23/10—Heating arrangements using tubes or passages containing heated fluids, e.g. acting as radiative elements; Closed-loop systems
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00—Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/06—Chambers, containers, or receptacles
    • F26B25/14—Chambers, containers, receptacles of simple construction
    • F26B25/16—Chambers, containers, receptacles of simple construction mainly closed, e.g. drum
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/041—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum for drying flowable materials, e.g. suspensions, bulk goods, in a continuous operation, e.g. with locks or other air tight arrangements for charging/discharging

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Sustainable Development (AREA)
  • Drying Of Solid Materials (AREA)
TW110117714A 2020-05-18 2021-05-17 真空凍結乾燥裝置及真空凍結乾燥方法 TWI860477B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2020086652 2020-05-18
JP2020-086652 2020-05-18

Publications (2)

Publication Number Publication Date
TW202202792A TW202202792A (zh) 2022-01-16
TWI860477B true TWI860477B (zh) 2024-11-01

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Country Link
US (1) US11644236B2 (https=)
EP (1) EP4155642A4 (https=)
JP (1) JP7218484B2 (https=)
KR (1) KR20220154833A (https=)
CN (1) CN115943283B (https=)
TW (1) TWI860477B (https=)
WO (1) WO2021235459A1 (https=)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114111302B (zh) * 2021-11-08 2022-10-25 西安交通大学 一种螺旋烘干输送机
CN116717962B (zh) * 2023-07-12 2025-01-14 山东迪乐能食品科技有限公司 一种婴幼儿冻干饼干制备用的冻干设备及制备方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55112980A (en) * 1979-02-26 1980-09-01 Nippon Oxygen Co Ltd Freezing drier
US8341854B2 (en) * 2007-06-14 2013-01-01 Ulvac, Inc. Vacuum freeze-drying apparatus and method for vacuum freeze drying
TW201708780A (zh) * 2015-07-13 2017-03-01 愛發科股份有限公司 真空乾燥裝置及真空乾燥方法
CN208108631U (zh) * 2018-04-19 2018-11-16 陕西森弗天然制品有限公司 植物提取用真空冷冻干燥装置

Family Cites Families (85)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US548573A (en) * 1895-10-22 moller g
US1303982A (en) * 1919-05-20 stevens
US474568A (en) * 1892-05-10 Grain drier or moistener
US236677A (en) * 1881-01-18 Grain-drier
US430652A (en) * 1890-06-24 Grain steamer and drier for mills
US676165A (en) * 1901-03-30 1901-06-11 Charles Wacker Drier.
US986107A (en) * 1910-09-21 1911-03-07 Franz Wertenbruch Drying-machine.
US1051359A (en) * 1912-01-05 1913-01-21 Carl Wille Drying apparatus.
US1179192A (en) * 1912-03-28 1916-04-11 Frank Kleinschmidt Drying apparatus.
US1172479A (en) * 1913-05-19 1916-02-22 Mary A Motter Ore-roasting furnace.
US1328027A (en) 1919-01-30 1920-01-13 Sakizo Dry battery
US1735396A (en) * 1924-07-07 1929-11-12 Stanley Hiller, Inc. A cobpobation of califobnia
US1735393A (en) * 1924-07-07 1929-11-12 Stanley Hiller Inc Apparatus for treating materials
US2038904A (en) * 1934-10-24 1936-04-28 Allison J Gibbs Dehydrating machine
US2067506A (en) * 1936-05-11 1937-01-12 Frank V Silva Casein drier
US2616604A (en) * 1941-05-02 1952-11-04 Theodore R Folsom Method for freezing and drying liquids and semisolids
US2411152A (en) * 1941-05-02 1946-11-19 Theodore R Folsom Method for freezing and drying liquids and semisolids
US2388917A (en) * 1941-10-13 1945-11-13 Hormel & Co Geo A Process for preservation of biological materials and products resulting therefrom
US2743168A (en) * 1944-09-09 1956-04-24 Krohn Roy Sublimation apparatus
US2552360A (en) * 1945-01-10 1951-05-08 Zichis Joseph Method of and apparatus for dehydrating materials
US2515098A (en) * 1945-08-01 1950-07-11 Chain Belt Co Continuous low-temperature dehydration
US2636284A (en) * 1948-07-12 1953-04-28 Miami Boiler & Machine Company Handling of materials and apparatus therefor
US2751687A (en) * 1952-05-21 1956-06-26 Proctor Drying And Freezing Co Process and apparatus for producing stabilized products
US2803888A (en) * 1954-04-27 1957-08-27 Cerletti Santiago Apparatus for lyophilising products contained in small bottles
DE1098448B (de) * 1959-02-26 1961-01-26 Erwin Lothar Holland Merten Beschickungsvorrichtung fuer eine Trocknungstrommel
US3088222A (en) * 1959-07-01 1963-05-07 Robert C Mace Freeze drying system
US3266169A (en) * 1962-10-31 1966-08-16 Hupp Corp Vacuum freeze drying apparatus
DE1604803A1 (de) * 1962-03-01 1971-01-07 Carlo Barbareschi Verfahren zur kontinuierlichen Absorbierung und Beseitigung von Wasserdampf oder anderen Loesungsmitteln durch Verdampfung oder Sublimation bei niedriger Temperatur unter Vakuum
US3362835A (en) * 1964-01-15 1968-01-09 Fmc Corp Spray freeze drying system
US3264747A (en) * 1964-05-13 1966-08-09 Pennsalt Chemical Corp Method and apparatus for continuous freeze drying
US3445247A (en) * 1964-10-08 1969-05-20 Basic Vegetable Products Inc Freeze dried product and process for producing the same
DE1924793U (de) * 1965-05-20 1965-09-30 Erwin Lothar Holland-Merten Beschikkungsvorrichtung fuer eine trocknungstrommel zur behandlung von schuett- und rieselgutern.
US3316652A (en) * 1965-10-24 1967-05-02 Sun Freeze Inc Continuous dehydrating process
US3310881A (en) * 1966-03-14 1967-03-28 Pillsbury Co Apparatus and method for continuous drying
US3324565A (en) * 1966-07-21 1967-06-13 Hupp Corp Apparatus and method for freeze drying
GB1199285A (en) * 1966-12-07 1970-07-22 H J Heinz Company Ltd Improvements in or Relating to Freeze Drying Apparatus
DE1779393B1 (de) * 1968-08-06 1972-05-04 Leybold Heraeus Gmbh & Co Kg Vakuumtrocknungskammer zur kontinuierlichen Gefriertrocknung von grobstueckig anfallendem,im Endzustand kleinteiligem Gut
US3531872A (en) * 1968-09-13 1970-10-06 Envirotech Corp Process and apparatus for deliquifying fluent material
US3952541A (en) * 1968-11-05 1976-04-27 Mario Rigoli Apparatus for quick freezing of aqueous solutions or suspensions to be submitted to lyophilization
US3616542A (en) * 1969-02-24 1971-11-02 Earl L Rader Apparatus and processes for producing freeze dried products
US3601901A (en) * 1969-09-12 1971-08-31 Earl L Rader Freeze drying apparatus with removable conveyor and heater structures
US3605273A (en) * 1970-01-16 1971-09-20 Nat Distillers Chem Corp Continuous process and apparatus for drying titanium sponge
FR2298777A2 (fr) * 1975-01-22 1976-08-20 Air Liquide Appareil de lyophilisation
JPS56127168A (en) * 1980-03-13 1981-10-05 Nikku Ind Co Method of and apparatus for continuous vacuum drying of particulate matter
WO1984000604A1 (fr) * 1982-08-05 1984-02-16 Buss Ag Four a tambour rotatif chauffe de maniere ininterrompue
JPS59161774A (ja) 1983-03-04 1984-09-12 Hitachi Ltd 乗算型ａ／ｄ変換器
JPS60191179A (ja) * 1984-03-12 1985-09-28 日本真空技術株式会社 インライン式凍結真空乾燥装置
JPS60191177A (ja) * 1984-03-12 1985-09-28 日本真空技術株式会社 インライン式凍結真空乾燥装置
JPH0627624B2 (ja) * 1985-08-06 1994-04-13 株式会社大川原製作所 液状物質の凍結乾燥装置
US4746968A (en) * 1987-03-30 1988-05-24 Mcdonnell Douglas Corporation Combined microwave and thermal drying apparatus
GB9505523D0 (en) * 1995-03-18 1995-05-03 Wellcome Found Lyophilization process
FR2760524A1 (fr) * 1997-03-10 1998-09-11 Paul Christophe Four tournant etanche pour le sechage ou le traitement thermique de produits organiques
JP3005657B2 (ja) 1997-11-19 2000-01-31 彰 堀金 凍結乾燥方法、装置および凍結乾燥物
US7140122B1 (en) * 2001-10-13 2006-11-28 Micronics, Llc Vacuum treatment of waste stream with anti-incrustation measures
JP3942093B2 (ja) * 2003-01-28 2007-07-11 株式会社アルバック 噴霧式真空凍結乾燥装置
MXPA06012614A (es) * 2004-05-01 2007-07-18 Agres Ltd Proceso y aparato de secado.
JP2006177640A (ja) * 2004-12-24 2006-07-06 Ulvac Japan Ltd 凍結真空乾燥装置
JP4145905B2 (ja) * 2005-08-01 2008-09-03 セイコーエプソン株式会社 減圧乾燥装置
JP3117061U (ja) * 2005-09-26 2006-01-05 共和真空技術株式会社 食品・薬品等の密閉式粉末充填装置における粉末体の供給装置
EP2101131A1 (en) 2007-12-31 2009-09-16 Terruzzi Fercalx S.p.A. Lyophilization method and system therefor
US8978268B2 (en) * 2008-07-10 2015-03-17 Ulvac, Inc. Freeze-drying apparatus and freeze-drying method
CN201974015U (zh) 2011-01-25 2011-09-14 张红霞 磷脂真空连续式冷冻干燥机
US9488410B2 (en) * 2011-02-08 2016-11-08 Kyowa Vacuum Engineering, Ltd. Calculation method and calculation device for sublimation interface temperature, bottom part temperature, and sublimation rate of material to be dried in freeze-drying device
RU2623225C2 (ru) * 2011-05-18 2017-06-23 Биоэндев Аб Противоточная усиленная кислородом торрефакция
DE102011103021B4 (de) * 2011-05-24 2013-07-04 Mineralit Gmbh Trommeltrockner
EP2745064B1 (en) * 2011-09-06 2017-04-05 Rheavita B.V. Method and system for freeze-drying injectable compositions, in particular pharmaceutical compositions
EP2578975A1 (en) * 2011-10-05 2013-04-10 Sanofi Pasteur Sa Rotary drum freeze-dryer
EP2578974A1 (en) * 2011-10-05 2013-04-10 Sanofi Pasteur Sa Process line for the production of freeze-dried particles
CN103292582A (zh) * 2013-06-06 2013-09-11 南通瑞翔新材料有限公司 一种氢氧化钴回转干燥装置
BR112016031039B1 (pt) * 2014-07-21 2022-02-15 Sanofi Pasteur Sa Dispositivo de alimentação de líquido para a geração de gotículas, linha de processo para a produção de partículas liofilizadas e processos para preparar uma composição de vacina compreendendo
CN104110950B (zh) * 2014-07-24 2015-12-30 山西大学 一种湿物料烘干装置
JP2017003146A (ja) * 2015-06-05 2017-01-05 研機株式会社 乾燥装置
EP3167877A1 (en) * 2015-11-12 2017-05-17 Bayer Pharma Aktiengesellschaft Method for the production of freeze-dried pellets comprising factor viii
CN105318665B (zh) * 2015-11-17 2018-06-29 上海东富龙科技股份有限公司 一种全自动密闭式喷雾冻干生产设备及方法
EP3443286B1 (fr) * 2016-04-14 2021-01-27 Jean Delaveau Dispositif de sublimation et procédé de lyophilisation
CN105712607B (zh) * 2016-04-28 2019-04-16 湖南科技大学 一种污泥的喷雾颗粒化冷冻真空干燥装置及方法
FR3052544B1 (fr) * 2016-06-08 2020-12-04 Haffner Energy Dispositif de deshydratation
KR101941109B1 (ko) * 2017-01-24 2019-01-22 (주)조은인터내셔널 버섯분말 제조 장치
WO2018204484A1 (en) * 2017-05-02 2018-11-08 Massachusetts Institute Of Technology Freeze-drying methods and related products
WO2019235036A1 (ja) 2018-06-08 2019-12-12 株式会社アルバック 凍結真空乾燥装置及び凍結真空乾燥方法
CN108731429A (zh) * 2018-06-15 2018-11-02 山东鲁北企业集团总公司 一种磷酸铁连续脱水及晶型可控系统及其控制方法
KR102028654B1 (ko) * 2019-03-08 2019-10-04 대성기계공업 주식회사 이차전지의 양극재 제조를 위한 분말원료 건조장치 및 이를 이용하는 분말원료 처리방법
CN209840540U (zh) * 2019-04-29 2019-12-24 四川百可馨生物制药有限公司 一种用于百可欣抑菌喷雾的密闭式冻干生产设备
CN110595193A (zh) * 2019-09-30 2019-12-20 苏州蒂珀克制冷科技有限公司 铰龙式连续真空低温冻干机
JP6777350B1 (ja) 2020-05-18 2020-10-28 株式会社エムアイアイ 真空凍結乾燥装置及び真空凍結乾燥方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55112980A (en) * 1979-02-26 1980-09-01 Nippon Oxygen Co Ltd Freezing drier
US8341854B2 (en) * 2007-06-14 2013-01-01 Ulvac, Inc. Vacuum freeze-drying apparatus and method for vacuum freeze drying
TW201708780A (zh) * 2015-07-13 2017-03-01 愛發科股份有限公司 真空乾燥裝置及真空乾燥方法
CN208108631U (zh) * 2018-04-19 2018-11-16 陕西森弗天然制品有限公司 植物提取用真空冷冻干燥装置

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Publication number Publication date
WO2021235459A1 (ja) 2021-11-25
JPWO2021235459A1 (https=) 2021-11-25
US11644236B2 (en) 2023-05-09
CN115943283A (zh) 2023-04-07
EP4155642A1 (en) 2023-03-29
KR20220154833A (ko) 2022-11-22
US20230100406A1 (en) 2023-03-30
EP4155642A4 (en) 2024-06-05
TW202202792A (zh) 2022-01-16
CN115943283B (zh) 2025-02-25
JP7218484B2 (ja) 2023-02-07

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