RU2133753C1 - Кристаллический полугидрат типа b соли бензойной кислоты 4''-деокси-4''-эпи- метиламиноавермектина bia/bib, способ ее получения, инсектицидная композиция и способ борьбы с сельскохозяйственными насекомыми-вредителями - Google Patents

Кристаллический полугидрат типа b соли бензойной кислоты 4''-деокси-4''-эпи- метиламиноавермектина bia/bib, способ ее получения, инсектицидная композиция и способ борьбы с сельскохозяйственными насекомыми-вредителями Download PDF

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Publication number
RU2133753C1
RU2133753C1 RU96107041A RU96107041A RU2133753C1 RU 2133753 C1 RU2133753 C1 RU 2133753C1 RU 96107041 A RU96107041 A RU 96107041A RU 96107041 A RU96107041 A RU 96107041A RU 2133753 C1 RU2133753 C1 RU 2133753C1
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RU
Russia
Prior art keywords
deoxy
salt
water
bib
benzoic acid
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RU96107041A
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English (en)
Russian (ru)
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RU96107041A (ru
Inventor
Кветович Раймонд
Демчак Ричард
А.Макколи Джеймс
Дж.Варсалона Ричард
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Мерк Энд Ко., Инк.
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H19/00—Compounds containing a hetero ring sharing one ring hetero atom with a saccharide radical; Nucleosides; Mononucleotides; Anhydro-derivatives thereof
    • C07H19/01—Compounds containing a hetero ring sharing one ring hetero atom with a saccharide radical; Nucleosides; Mononucleotides; Anhydro-derivatives thereof sharing oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H17/00—Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
    • C07H17/04—Heterocyclic radicals containing only oxygen as ring hetero atoms
    • C07H17/08—Hetero rings containing eight or more ring members, e.g. erythromycins
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Molecular Biology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Pest Control & Pesticides (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • Genetics & Genomics (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Saccharide Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
RU96107041A 1993-08-19 1994-08-15 Кристаллический полугидрат типа b соли бензойной кислоты 4''-деокси-4''-эпи- метиламиноавермектина bia/bib, способ ее получения, инсектицидная композиция и способ борьбы с сельскохозяйственными насекомыми-вредителями RU2133753C1 (ru)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US10918993A 1993-08-19 1993-08-19
US109189 1993-08-19
US109,189 1993-08-19
PCT/US1994/009207 WO1995005390A1 (en) 1993-08-19 1994-08-15 THERMODYNAMICALLY STABLE CRYSTAL FORM OF 4'-DEOXY-4'-EPI-METHYLAMINO AVERMECTIN B1a/B1b BENZOIC ACID SALT AND PROCESSES FOR ITS PREPARATION

Publications (2)

Publication Number Publication Date
RU96107041A RU96107041A (ru) 1998-05-20
RU2133753C1 true RU2133753C1 (ru) 1999-07-27

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
RU96107041A RU2133753C1 (ru) 1993-08-19 1994-08-15 Кристаллический полугидрат типа b соли бензойной кислоты 4''-деокси-4''-эпи- метиламиноавермектина bia/bib, способ ее получения, инсектицидная композиция и способ борьбы с сельскохозяйственными насекомыми-вредителями

Country Status (25)

Country Link
EP (1) EP0714400B1 (ko)
JP (3) JP3954093B2 (ko)
KR (1) KR100370697B1 (ko)
CN (1) CN1041523C (ko)
AT (1) ATE187735T1 (ko)
AU (1) AU684828B2 (ko)
BR (1) BR9407300A (ko)
CA (1) CA2168843C (ko)
CY (1) CY2181B1 (ko)
CZ (1) CZ287929B6 (ko)
DE (1) DE69422182T2 (ko)
DK (1) DK0714400T3 (ko)
ES (1) ES2139753T3 (ko)
FI (2) FI110783B (ko)
GR (1) GR3032164T3 (ko)
HU (1) HU217769B (ko)
LV (1) LV12571B (ko)
NO (1) NO305658B1 (ko)
NZ (1) NZ273129A (ko)
PL (1) PL176300B1 (ko)
PT (1) PT714400E (ko)
RU (1) RU2133753C1 (ko)
SK (1) SK281684B6 (ko)
WO (1) WO1995005390A1 (ko)
ZA (1) ZA946203B (ko)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6486195B1 (en) * 1993-08-19 2002-11-26 Merck & Co., Inc. Thermodynamically stable crystal form of 4″-deoxy-4″-epi-methylamino avermectin B1a/B1b benzoic acid salt and processes for its preparation
CR6574A (es) 2001-02-27 2004-10-28 Syngenta Participations Ag Sales de avermectinas substituidas en la posicion 4 con propiedades plaguicidas
CA2790921A1 (en) * 2010-02-23 2011-09-01 Nippon Kayaku Co., Ltd. Stabilized crystal of 2-ethyl-3,7-dimethyl-6-(4-(trifluoromethoxy)phenoxy)quinoline-4-yl methyl carbonate, process for producing the crystal, and agricultural chemical compositioncomprising the crystal
CN106995476B (zh) * 2017-05-16 2018-03-13 河北美荷药业有限公司 一种甲氨基阿维菌素b2苯甲酸盐的制备方法
CN108840893A (zh) * 2018-07-01 2018-11-20 李万强 一种甲氨基阿维菌素苯甲酸盐的新晶型及其制备方法
CN109912671B (zh) * 2019-04-12 2022-04-26 宁夏泰益欣生物科技有限公司 一种利用阿维菌素结晶母液提取阿维菌素B2a的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57212200A (en) * 1981-06-23 1982-12-27 Takeda Chem Ind Ltd Preparation of echinoside a
GB8518422D0 (en) * 1985-07-22 1985-08-29 Beecham Group Plc Compounds
IT1216059B (it) * 1988-03-11 1990-02-22 Crc Ricerca Chim Procedimento per la separazione di diastereomeri macrociclici.
JPH0631302B2 (ja) * 1988-11-16 1994-04-27 日本化薬株式会社 エトポシド−２−ジメチルアミノ体塩酸二水和結晶及びその製造法
JPH0615557B2 (ja) * 1990-02-19 1994-03-02 ヤマサ醤油株式会社 ２’―デオキシ―２’―メチリデンシチジンの２水和物結晶
JPH0446192A (ja) * 1990-06-12 1992-02-17 Nippon Kayaku Co Ltd オキセタノシンｇ無水物結晶及びその製造法
IL98599A (en) * 1990-06-28 1995-06-29 Merck & Co Inc Stable salts of "4-deoxy-" 4-epi-methylamino abramectin and insecticides containing them
JP2652272B2 (ja) * 1990-12-31 1997-09-10 住化ファインケム株式会社 １−（４−アミノ−６，７−ジメトキシ−２−キナゾリニル）−４−（２−テトラヒドロフロイル）ピペラジン塩酸塩の新規な結晶体および該結晶体の製造方法
WO1992020683A1 (en) * 1991-05-15 1992-11-26 Yamanouchi Pharmaceutical Co., Ltd. (-)-(s)-2,8-dimethyl-3-methylene-1-oxa-8-azaspiro[4,5]decane l-tartrate
JP2848721B2 (ja) * 1991-08-09 1999-01-20 森永乳業株式会社 結晶ラクチュロース三水和物とその製造法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Седых А.С. и др. Авермектины - новая группа инсектоакарицидов и нематоцидов: Обзор инф. - М.: НИИТЭХИМ, 1990, с.34. *

Also Published As

Publication number Publication date
ATE187735T1 (de) 2000-01-15
WO1995005390A1 (en) 1995-02-23
CN1129453A (zh) 1996-08-21
PL176300B1 (pl) 1999-05-31
JP2011207899A (ja) 2011-10-20
HUT73552A (en) 1996-08-28
DK0714400T3 (da) 2000-04-10
FI110783B (fi) 2003-03-31
PL313043A1 (en) 1996-05-27
CA2168843C (en) 2004-10-19
AU684828B2 (en) 1998-01-08
SK20996A3 (en) 1996-06-05
GR3032164T3 (en) 2000-04-27
FI20021120A (fi) 2002-06-11
FI960725A0 (fi) 1996-02-16
BR9407300A (pt) 1996-10-08
CZ45996A3 (en) 1996-05-15
FI111165B (fi) 2003-06-13
CN1041523C (zh) 1999-01-06
KR100370697B1 (ko) 2003-06-11
CA2168843A1 (en) 1995-02-23
AU7631994A (en) 1995-03-14
FI960725A (fi) 1996-02-16
JP3954093B2 (ja) 2007-08-08
DE69422182T2 (de) 2000-06-21
CY2181B1 (en) 2002-08-23
HU9600345D0 (en) 1996-04-29
DE69422182D1 (de) 2000-01-20
PT714400E (pt) 2000-05-31
SK281684B6 (sk) 2001-06-11
NZ273129A (en) 1996-08-27
HU217769B (hu) 2000-04-28
JP2007176946A (ja) 2007-07-12
NO960618D0 (no) 1996-02-16
EP0714400B1 (en) 1999-12-15
NO960618L (no) 1996-02-16
ZA946203B (en) 1995-03-31
NO305658B1 (no) 1999-07-05
LV12571A (en) 2000-11-20
CZ287929B6 (cs) 2001-03-14
LV12571B (en) 2001-04-20
JPH09502169A (ja) 1997-03-04
ES2139753T3 (es) 2000-02-16
KR960703936A (ko) 1996-08-31
EP0714400A1 (en) 1996-06-05

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