JP2006111546A5 - - Google Patents
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- Publication number
- JP2006111546A5 JP2006111546A5 JP2004298564A JP2004298564A JP2006111546A5 JP 2006111546 A5 JP2006111546 A5 JP 2006111546A5 JP 2004298564 A JP2004298564 A JP 2004298564A JP 2004298564 A JP2004298564 A JP 2004298564A JP 2006111546 A5 JP2006111546 A5 JP 2006111546A5
- Authority
- JP
- Japan
- Prior art keywords
- raw material
- trimethylaluminum
- trimethylgallium
- methyltriethylsilane
- ppm
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XCZXGTMEAKBVPV-UHFFFAOYSA-N trimethylgallium Chemical compound C[Ga](C)C XCZXGTMEAKBVPV-UHFFFAOYSA-N 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 7
- JLTRXTDYQLMHGR-UHFFFAOYSA-N trimethylaluminium Chemical compound C[Al](C)C JLTRXTDYQLMHGR-UHFFFAOYSA-N 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 5
- JCSVHJQZTMYYFL-UHFFFAOYSA-N triethyl(methyl)silane Chemical compound CC[Si](C)(CC)CC JCSVHJQZTMYYFL-UHFFFAOYSA-N 0.000 claims description 5
- 229910002601 GaN Inorganic materials 0.000 claims description 3
- JMASRVWKEDWRBT-UHFFFAOYSA-N Gallium nitride Chemical compound [Ga]#N JMASRVWKEDWRBT-UHFFFAOYSA-N 0.000 claims description 3
- 239000010409 thin film Substances 0.000 claims description 3
- 150000003961 organosilicon compounds Chemical class 0.000 claims description 2
- 238000004821 distillation Methods 0.000 claims 2
- 238000000746 purification Methods 0.000 claims 2
- UPWPDUACHOATKO-UHFFFAOYSA-K gallium trichloride Chemical compound Cl[Ga](Cl)Cl UPWPDUACHOATKO-UHFFFAOYSA-K 0.000 claims 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 claims 1
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 150000003377 silicon compounds Chemical class 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004298564A JP4470682B2 (ja) | 2004-10-13 | 2004-10-13 | トリメチルガリウムの製造方法 |
| GB0520663A GB2420118B (en) | 2004-10-13 | 2005-10-11 | A trimethylgallium, a method for producing the same and a gallium nitride thin film grown from the trimethylgallium |
| US11/246,550 US20060075959A1 (en) | 2004-10-13 | 2005-10-11 | Trimethylgallium, a method for producing the same and a gallium nitride thin film grown from the trimethylgallium |
| DE102005048680A DE102005048680A1 (de) | 2004-10-13 | 2005-10-11 | Trimethylgallium, Verfahren zur Herstellung desselben und aus dem Trimethylgallium gezüchteter Galliumnitriddünnfilm |
| KR1020050096398A KR101250153B1 (ko) | 2004-10-13 | 2005-10-13 | 트리메틸갈륨, 이의 제조 방법 및 트리메틸갈륨으로부터형성된 질화갈륨 박막 |
| TW094135671A TWI363059B (en) | 2004-10-13 | 2005-10-13 | A method for producing trimethylgallium |
| CN2005101083835A CN1763049B (zh) | 2004-10-13 | 2005-10-13 | 三甲基镓的制造方法以及氮化镓薄膜的制造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004298564A JP4470682B2 (ja) | 2004-10-13 | 2004-10-13 | トリメチルガリウムの製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2006111546A JP2006111546A (ja) | 2006-04-27 |
| JP2006111546A5 true JP2006111546A5 (enExample) | 2006-07-27 |
| JP4470682B2 JP4470682B2 (ja) | 2010-06-02 |
Family
ID=35430195
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2004298564A Expired - Fee Related JP4470682B2 (ja) | 2004-10-13 | 2004-10-13 | トリメチルガリウムの製造方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20060075959A1 (enExample) |
| JP (1) | JP4470682B2 (enExample) |
| KR (1) | KR101250153B1 (enExample) |
| CN (1) | CN1763049B (enExample) |
| DE (1) | DE102005048680A1 (enExample) |
| GB (1) | GB2420118B (enExample) |
| TW (1) | TWI363059B (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008024617A (ja) | 2006-07-19 | 2008-02-07 | Ube Ind Ltd | 高純度トリアルキルアルミニウム及びその製法 |
| JP4462251B2 (ja) * | 2006-08-17 | 2010-05-12 | 日立電線株式会社 | Iii−v族窒化物系半導体基板及びiii−v族窒化物系発光素子 |
| JP2008050268A (ja) * | 2006-08-22 | 2008-03-06 | Ube Ind Ltd | 高純度トリアルキルガリウム及びその製法 |
| JP2008081451A (ja) * | 2006-09-28 | 2008-04-10 | Ube Ind Ltd | 高純度トリアルキルガリウム及びその製法 |
| JP2008263023A (ja) * | 2007-04-11 | 2008-10-30 | Sumitomo Electric Ind Ltd | Iii−v族化合物半導体の製造方法、ショットキーバリアダイオード、発光ダイオード、レーザダイオード、およびそれらの製造方法 |
| JP2008266196A (ja) * | 2007-04-19 | 2008-11-06 | Nippon Shokubai Co Ltd | ボラジン化合物の製造方法 |
| JP2009126835A (ja) * | 2007-11-27 | 2009-06-11 | Ube Ind Ltd | 高純度トリアルキルガリウム及びその製法 |
| KR100965270B1 (ko) * | 2008-07-04 | 2010-06-22 | 주식회사 한솔케미칼 | 새로운 전자 주개 리간드를 가지는 갈륨 착화합물 및 이의제조방법 |
| JP5423039B2 (ja) * | 2009-02-23 | 2014-02-19 | 宇部興産株式会社 | 高純度トリアルキルガリウム及びその製造方法 |
| JP5348186B2 (ja) * | 2011-06-16 | 2013-11-20 | 宇部興産株式会社 | 高純度トリアルキルガリウム及びその製法 |
| DE102012013941A1 (de) | 2012-07-16 | 2014-01-16 | Umicore Ag & Co. Kg | Verfahren zur Herstellung von Galliumtrialkylverbindungen |
| TWI632149B (zh) | 2011-11-28 | 2018-08-11 | 烏明克股份有限兩合公司 | 第iii a族金屬的三烷基化合物之製法 |
| KR101326554B1 (ko) * | 2012-06-22 | 2013-11-07 | 한국기초과학지원연구원 | 트리메틸갈륨(TMGa)의 재활용 방법 |
| KR101436590B1 (ko) * | 2013-05-28 | 2014-09-02 | 한국기초과학지원연구원 | 회수 TMIn 재이용방법 |
| JP5761401B2 (ja) * | 2014-02-27 | 2015-08-12 | 宇部興産株式会社 | 高純度トリアルキルガリウム及びその製法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62132888A (ja) * | 1985-12-03 | 1987-06-16 | Sumitomo Chem Co Ltd | 有機金属化合物の精製方法 |
| US4847399A (en) * | 1987-01-23 | 1989-07-11 | Morton Thiokol, Inc. | Process for preparing or purifying Group III-A organometallic compounds |
| US5043462A (en) * | 1989-04-28 | 1991-08-27 | Messer Greisheim | Process for the production of gallium-alkyl compounds |
| TW217415B (enExample) * | 1991-11-19 | 1993-12-11 | Shell Internat Res Schappej B V | |
| US5455364A (en) * | 1993-12-14 | 1995-10-03 | Sumitomo Chemical Company, Ltd. | Process for removing an impurity in organometallic compound |
| JP3230029B2 (ja) * | 1994-05-30 | 2001-11-19 | 富士通株式会社 | Iii−v族化合物半導体結晶成長方法 |
| JP2927685B2 (ja) * | 1994-08-19 | 1999-07-28 | 信越化学工業株式会社 | 有機金属化合物の精製方法 |
| MY112590A (en) * | 1994-09-02 | 2001-07-31 | Sec Dep For Defence Acting Through His Defence Evaluation And Research Agency United Kingdom | Semi-conductor devices and their production |
| GB2344822A (en) * | 1998-12-19 | 2000-06-21 | Epichem Ltd | Organometallic compound production using distillation |
| WO2000071551A2 (en) * | 1999-05-21 | 2000-11-30 | Akzo Nobel N.V. | Purification of an organometallic compound by recrystallization |
| TW574762B (en) * | 2002-10-16 | 2004-02-01 | Univ Nat Cheng Kung | Method for growing monocrystal GaN on silicon substrate |
| JP4488186B2 (ja) * | 2004-06-18 | 2010-06-23 | 信越化学工業株式会社 | トリメチルアルミニウムの精製方法 |
| JP2006001896A (ja) * | 2004-06-18 | 2006-01-05 | Shin Etsu Chem Co Ltd | 高純度トリメチルアルミニウム及びトリメチルアルミニウムの精製方法 |
-
2004
- 2004-10-13 JP JP2004298564A patent/JP4470682B2/ja not_active Expired - Fee Related
-
2005
- 2005-10-11 DE DE102005048680A patent/DE102005048680A1/de not_active Withdrawn
- 2005-10-11 GB GB0520663A patent/GB2420118B/en not_active Expired - Fee Related
- 2005-10-11 US US11/246,550 patent/US20060075959A1/en not_active Abandoned
- 2005-10-13 TW TW094135671A patent/TWI363059B/zh not_active IP Right Cessation
- 2005-10-13 KR KR1020050096398A patent/KR101250153B1/ko not_active Expired - Fee Related
- 2005-10-13 CN CN2005101083835A patent/CN1763049B/zh not_active Expired - Fee Related
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