JP2012530749A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2012530749A5 JP2012530749A5 JP2012516645A JP2012516645A JP2012530749A5 JP 2012530749 A5 JP2012530749 A5 JP 2012530749A5 JP 2012516645 A JP2012516645 A JP 2012516645A JP 2012516645 A JP2012516645 A JP 2012516645A JP 2012530749 A5 JP2012530749 A5 JP 2012530749A5
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- isocyanate
- stream
- solvent stream
- bar
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002904 solvent Substances 0.000 description 10
- 239000012948 isocyanate Substances 0.000 description 6
- 150000002513 isocyanates Chemical class 0.000 description 6
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US22074009P | 2009-06-26 | 2009-06-26 | |
| US61/220,740 | 2009-06-26 | ||
| PCT/EP2010/058421 WO2010149544A2 (en) | 2009-06-26 | 2010-06-16 | Process for the production of isocyanates, preferably diisocyanates and polyisocyanates with solvent recirculation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2012530749A JP2012530749A (ja) | 2012-12-06 |
| JP2012530749A5 true JP2012530749A5 (enExample) | 2015-07-16 |
Family
ID=43127609
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012516645A Pending JP2012530749A (ja) | 2009-06-26 | 2010-06-16 | イソシアネート、好適には溶媒の再循環を伴うジイソシアネート及びポリイソシアネートの製造方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8759569B2 (enExample) |
| EP (1) | EP2445869B1 (enExample) |
| JP (1) | JP2012530749A (enExample) |
| KR (1) | KR101773630B1 (enExample) |
| CN (1) | CN102482205B (enExample) |
| BR (1) | BRPI1015061A2 (enExample) |
| ES (1) | ES2532761T3 (enExample) |
| PL (1) | PL2445869T3 (enExample) |
| PT (1) | PT2445869E (enExample) |
| WO (1) | WO2010149544A2 (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102596900B (zh) | 2009-10-21 | 2015-09-09 | 巴斯夫欧洲公司 | 生产氨基甲酸酯的方法 |
| CN102666479B (zh) | 2009-12-04 | 2014-11-05 | 巴斯夫欧洲公司 | 制备异氰酸酯的方法 |
| US8609899B2 (en) | 2010-05-17 | 2013-12-17 | Basf Se | Process for preparing toluenediamine by hydrogenation of dinitrotoluene |
| US8907124B2 (en) | 2010-11-17 | 2014-12-09 | Basf Se | Process for preparing methylenedi(phenyl isocyanate) |
| US9505711B2 (en) | 2010-11-17 | 2016-11-29 | Basf Se | Method for purifying mixtures comprising 4,4′-methylenediphenyl diisocyanate |
| US8969615B2 (en) | 2011-03-31 | 2015-03-03 | Basf Se | Process for preparing isocyanates |
| US8933262B2 (en) | 2011-05-24 | 2015-01-13 | Basf Se | Process for preparing polyisocyanates from biomass |
| DE102011087654A1 (de) | 2011-12-02 | 2013-06-06 | Bayer Materialscience Aktiengesellschaft | Verfahren zur Herstellung von Isocyanaten |
| CN103877738A (zh) * | 2012-12-19 | 2014-06-25 | 海安海太铸造有限公司 | 一种带有降膜蒸发器的蒸馏塔 |
| CN103739520B (zh) * | 2013-12-26 | 2016-03-30 | 安徽广信农化股份有限公司 | 一种3,4-二氯苯异氰酸酯精制方法 |
| CN104974010B (zh) | 2014-04-01 | 2016-10-26 | 万华化学集团股份有限公司 | 一种光气法制异氰酸酯的溶剂精制方法及所使用的装置 |
| CN104402765B (zh) * | 2014-10-10 | 2015-09-30 | 青岛科技大学 | 一种以异氰酸酯为中间体制备农药的方法 |
| EP3352896B1 (de) * | 2015-09-24 | 2019-10-23 | Covestro Deutschland AG | Verfahren zur herstellung von isocyanaten |
| CN107935889B (zh) * | 2017-11-29 | 2020-08-28 | 万华化学集团股份有限公司 | 一种单异氰酸酯的制备方法及装置 |
| CN109651201A (zh) * | 2018-12-30 | 2019-04-19 | 安徽广信农化股份有限公司 | 一种合成异氰酸环己酯的废料处理工艺 |
| HUE068310T2 (hu) | 2019-09-17 | 2024-12-28 | Covestro Deutschland Ag | Eljárás izocianátok elõállítására |
| US11731936B2 (en) * | 2019-12-06 | 2023-08-22 | Skc Co., Ltd. | Diisocyanate composition, preparation method thereof and optical material using same |
| CN114380714B (zh) * | 2020-10-16 | 2023-08-11 | 万华化学集团股份有限公司 | 光气化反应生产中的循环溶剂及其除杂方法 |
| CN112552209A (zh) * | 2020-12-09 | 2021-03-26 | 浙江丽水有邦新材料有限公司 | 一种环己基异氰酸酯的制备方法及装置 |
| CN114149345B (zh) * | 2021-12-09 | 2023-04-21 | 万华化学集团股份有限公司 | 一种制备异氰酸酯的方法 |
| CN115093349B (zh) * | 2022-06-28 | 2024-06-25 | 万华化学集团股份有限公司 | 一种甲苯二异氰酸酯副产固体残渣净化溶剂的方法 |
| CN116217439B (zh) * | 2023-01-03 | 2025-05-13 | 万华化学集团股份有限公司 | 一种光气化制备mdi的循环溶剂及其提纯方法 |
| CN117603093A (zh) * | 2023-11-30 | 2024-02-27 | 甘肃银光聚银化工有限公司 | 一种生物基1，4-丁二异氰酸酯的合成方法 |
| CN118812394A (zh) * | 2024-07-26 | 2024-10-22 | 青岛科技大学 | 光气法合成1,5-戊二异氰酸酯的精制工艺及设备 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD139955A3 (de) | 1975-09-23 | 1980-01-30 | Siegbert Loeschau | Verfahren zur sofortigen feststellung von wassereintritten in phosgen bzw.phosgenfuehrenden systemen |
| DE4412327A1 (de) * | 1994-04-11 | 1995-10-12 | Bayer Ag | Verfahren zur Herstellung von Diisocyanaten |
| DE19523851A1 (de) * | 1995-06-30 | 1997-01-02 | Basf Ag | Verfahren zur Herstellung von Mischungen aus Diphenylmethan-diisocyanaten und Polyphenyl-polymethylen-polyisocyanaten mit einer verminderten Iodfarbzahl und einem reduzierten Chlorgehalt |
| DE19817691A1 (de) * | 1998-04-21 | 1999-10-28 | Basf Ag | Verfahren zur Herstellung von Mischungen aus Diphenylmehandiisocyanaten und Polyphenylen-polymethylen-polyisocyanaten mit vermindertem Gehalt an chlorierten Nebenprodukten und verminderter Jodfarbzahl |
| DE19942299A1 (de) | 1999-09-04 | 2001-03-08 | Basf Ag | Verbessertes Verfahren zur Herstellung von Mono- und Oligo-Isocyanaten |
| EP1371634A1 (en) | 2002-06-14 | 2003-12-17 | Bayer Ag | Process for the purification of mixtures of toluenediisocyanate |
| EP1371633A1 (en) * | 2002-06-14 | 2003-12-17 | Bayer Ag | Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column |
| DE10260027A1 (de) * | 2002-12-19 | 2004-07-08 | Basf Ag | Verfahren zur Abtrennung und Reinigung von Lösungsmittel von einem Reaktionsgemisch aus einer Isocyanatsynthese |
| DE10333929A1 (de) * | 2003-07-25 | 2005-02-24 | Bayer Materialscience Ag | Herstellung von Mischungen von Di- und Polyisocyanaten der Diphenylmethanreihe mit hohen Gehalten an 4,4'-Methylendiphenyldiisocyanat und 2,4'-Methylendiphenyldiisocyanat |
| DE102006004041A1 (de) * | 2006-01-28 | 2007-08-02 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| DE102006022448A1 (de) * | 2006-05-13 | 2007-11-15 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten |
| US8273915B2 (en) | 2007-08-31 | 2012-09-25 | Basf Se | Process for preparing isocyanates |
| WO2009037179A1 (de) | 2007-09-19 | 2009-03-26 | Basf Se | Verfahren zur herstellung von isocyanaten |
| JP2011516593A (ja) | 2008-04-14 | 2011-05-26 | ビーエーエスエフ ソシエタス・ヨーロピア | イソシアネートの製造で生じる残渣を処理する方法 |
| WO2010015667A1 (de) | 2008-08-07 | 2010-02-11 | Basf Se | Verfahren zur herstellung von aromatischen isocyanaten |
| EP2367783B1 (de) | 2008-11-19 | 2013-01-09 | Basf Se | Verfahren zur herstellung eines isocyanats |
| US8609899B2 (en) | 2010-05-17 | 2013-12-17 | Basf Se | Process for preparing toluenediamine by hydrogenation of dinitrotoluene |
| KR20130089233A (ko) | 2010-06-22 | 2013-08-09 | 바스프 에스이 | 고체 루이스 산 위의 이소시아네이트의 합성을 위한 불균일하게 촉매화된 카바메이트 해리 |
| US9505711B2 (en) | 2010-11-17 | 2016-11-29 | Basf Se | Method for purifying mixtures comprising 4,4′-methylenediphenyl diisocyanate |
-
2010
- 2010-06-16 PT PT107236077T patent/PT2445869E/pt unknown
- 2010-06-16 CN CN201080037436.8A patent/CN102482205B/zh active Active
- 2010-06-16 BR BRPI1015061A patent/BRPI1015061A2/pt not_active IP Right Cessation
- 2010-06-16 WO PCT/EP2010/058421 patent/WO2010149544A2/en not_active Ceased
- 2010-06-16 ES ES10723607.7T patent/ES2532761T3/es active Active
- 2010-06-16 EP EP10723607.7A patent/EP2445869B1/en active Active
- 2010-06-16 JP JP2012516645A patent/JP2012530749A/ja active Pending
- 2010-06-16 KR KR1020127001771A patent/KR101773630B1/ko active Active
- 2010-06-16 US US13/380,680 patent/US8759569B2/en active Active
- 2010-06-16 PL PL10723607T patent/PL2445869T3/pl unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2012530749A5 (enExample) | ||
| JP2009541553A5 (enExample) | ||
| JP2008540615A5 (enExample) | ||
| WO2008131856A3 (de) | Verfahren zur rückgewinnung von ruthenium aus einem rutheniumhaltigen geträgerten katalysatormaterial | |
| JP2009196991A5 (enExample) | ||
| JP2012532160A5 (enExample) | ||
| SA519410718B1 (ar) | استخلاص الهيليوم من تيارات غازية | |
| WO2010053571A3 (en) | Methanol carbonylation with aldehyde removal | |
| WO2012158872A3 (en) | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene | |
| SG131033A1 (en) | Process for gas purification | |
| WO2012067980A3 (en) | Process for producing 2,3,3,3-tetrafluoropropene and a process for purifying 2-chloro-1,1,1,2-tetrafluoropropane | |
| JP2012507455A5 (enExample) | ||
| WO2008087657A3 (en) | A process for preparing epichlorohydrin | |
| WO2003097847A3 (en) | A process for producing ethanol from organic material | |
| WO2011059210A3 (en) | Process for purification of monosilane | |
| WO2008000957A3 (fr) | Procédé de préparation d'hydroquinone purifiée | |
| PT1993990E (pt) | Processo para a separação por destilação de dinitrotolueno a partir de água residual resultante do processo de preparação de dinitrotolueno por nitração de tolueno através de ácidos de nitração | |
| ATE517076T1 (de) | Reinigung von propylenglycolmonoalkylether | |
| EA201000464A1 (ru) | Способ получения очищенного синтез-газа из синтез-газа, содержащего следовые количества примеси сернистых соединений, с помощью металлорганической структуры | |
| SG11201901292YA (en) | Method for separating and purifying isobutylene and method for producing isobutylene | |
| UA111318C2 (uk) | Спосіб одержання кристалів адипінової кислоти | |
| CN104364196B (zh) | 用于纯化氨气或氮气和氢气的混合物或氮气、氢气和氨气的混合物的方法 | |
| WO2011097189A3 (en) | Process for purifying ethanol | |
| DE502008001207D1 (de) | Verfahren zur herstellung polymerisierbarer silicone | |
| JP2010235536A5 (enExample) |