WO2007118474A3 - Verfahren zur herstellung von wasserstoffreichen silanen, sowie neue chemische verbindungen - Google Patents

Verfahren zur herstellung von wasserstoffreichen silanen, sowie neue chemische verbindungen Download PDF

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Publication number
WO2007118474A3
WO2007118474A3 PCT/DE2007/000724 DE2007000724W WO2007118474A3 WO 2007118474 A3 WO2007118474 A3 WO 2007118474A3 DE 2007000724 W DE2007000724 W DE 2007000724W WO 2007118474 A3 WO2007118474 A3 WO 2007118474A3
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WO
WIPO (PCT)
Prior art keywords
silanes
rich
hydrogen
type
production
Prior art date
Application number
PCT/DE2007/000724
Other languages
English (en)
French (fr)
Other versions
WO2007118474A2 (de
Inventor
Gerrit Fester
Gerhard Roewer
Edwin Kroke
Original Assignee
Univ Freiberg Tech Bergakad
Gerrit Fester
Gerhard Roewer
Edwin Kroke
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE200610019016 external-priority patent/DE102006019016A1/de
Application filed by Univ Freiberg Tech Bergakad, Gerrit Fester, Gerhard Roewer, Edwin Kroke filed Critical Univ Freiberg Tech Bergakad
Priority to DE112007000952T priority Critical patent/DE112007000952A5/de
Publication of WO2007118474A2 publication Critical patent/WO2007118474A2/de
Publication of WO2007118474A3 publication Critical patent/WO2007118474A3/de

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/025Silicon compounds without C-silicon linkages

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)

Abstract

Die vorliegende Erfindung betrifft ein Verfahren zur Synthese von wasserstoffreichen Silanen des Typs HnSi(AR1)4-n mit n = 1 oder 2 und A = O, NR2 oder S, insbesondere Di- und Trialkoxysilanen vom Typ HnSi(OR)4-n mit n = 1 oder 2 durch Umsetzen: a.) eines Dihalogensilans des Typs H2SiX2 mit X = Halogen, b.) einer Verbindung mit der allgemeinen Formel HAR1 mit A = O, NR2 oder S, wie z. B. eines Alkohols mit der allgemeinen Formel HOR, wobei R z. B. ein Alkyl- oder Arylrest ist, der wenn n = 2 mindestens 3 Kohlenstoffatome aufweist, c.) mit einem Überschuss eines tertiären aliphatischen oder cyclischen Amins Durch das erfindungsgemäße Verfahren können vorteilhaft die wasserstoffreichen Silane selektiv in einer einfachen Reaktion in Reinheiten von > 90 % erhalten werden.
PCT/DE2007/000724 2006-04-19 2007-04-19 Verfahren zur herstellung von wasserstoffreichen silanen, sowie neue chemische verbindungen WO2007118474A2 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE112007000952T DE112007000952A5 (de) 2006-04-19 2007-04-19 Verfahren zur Herstellung von Wasserstoffreichen Silanen, sowie neue chemische Verbindungen

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102006019016.5 2006-04-19
DE200610019016 DE102006019016A1 (de) 2006-04-19 2006-04-19 Verfahren zur Herstellung von Di- und Trialkoxysilanen
DE102006034335 2006-07-17
DE102006034335.2 2006-07-17

Publications (2)

Publication Number Publication Date
WO2007118474A2 WO2007118474A2 (de) 2007-10-25
WO2007118474A3 true WO2007118474A3 (de) 2007-12-21

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DE2007/000724 WO2007118474A2 (de) 2006-04-19 2007-04-19 Verfahren zur herstellung von wasserstoffreichen silanen, sowie neue chemische verbindungen

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DE (1) DE112007000952A5 (de)
WO (1) WO2007118474A2 (de)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006019015A1 (de) 2006-04-19 2007-10-25 Technische Universität Bergakademie Freiberg Verfahren zur Herstellung von wasserstoffreichen Cyclosiloxanen
US8728955B2 (en) 2012-02-14 2014-05-20 Novellus Systems, Inc. Method of plasma activated deposition of a conformal film on a substrate surface
KR102276834B1 (ko) 2016-10-12 2021-07-14 다우 실리콘즈 코포레이션 티오(다이)실란
US20220162138A1 (en) * 2019-04-05 2022-05-26 Mcmaster University Process for cleaving sulfur-sulfur and sulfur-hydrogen bonds in organic compounds

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1543513A1 (de) * 1965-12-07 1969-08-28 Dynamit Nobel Ag Verfahren zur Herstellung von halogenierten Phenoxysilanen
US5288889A (en) * 1992-05-18 1994-02-22 Shin-Etsu Chemical Co. Fluorinated organic silicon compounds and method for making
US5976512A (en) * 1997-03-03 1999-11-02 Roche Vitamins Inc. Symetrical hydroxyphenyl-s-triazine compositions

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1543513A1 (de) * 1965-12-07 1969-08-28 Dynamit Nobel Ag Verfahren zur Herstellung von halogenierten Phenoxysilanen
US5288889A (en) * 1992-05-18 1994-02-22 Shin-Etsu Chemical Co. Fluorinated organic silicon compounds and method for making
US5976512A (en) * 1997-03-03 1999-11-02 Roche Vitamins Inc. Symetrical hydroxyphenyl-s-triazine compositions

Non-Patent Citations (9)

* Cited by examiner, † Cited by third party
Title
BELLEGARDE, B. ET AL., C. R. HEBD. SEANCES ACAD. SCI. SER. C, vol. 264, 1967, pages 340 - 342 *
BROOK, M. ET AL., J. ORG. CHEM., vol. 55, no. 11, 1990, pages 3609 - 3616 *
DATABASE BEILSTEIN [online] BEILSTEIN INSTITUTE FOR ORGANIC CHEMISTRY, FRANKFURT-MAIN, DE; XP002446452, retrieved from XFIRE Database accession no. Reaction ID 4465146; Reaction ID 4465145 *
DATABASE BEILSTEIN [online] BEILSTEIN INSTITUTE FOR ORGANIC CHEMISTRY, FRANKFURT-MAIN, DE; XP002446453, retrieved from XFIRE Database accession no. BRN 1859526 *
DATABASE BEILSTEIN [online] BEILSTEIN INSTITUTE FOR ORGANIC CHEMISTRY, FRANKFURT-MAIN, DE; XP002446454, retrieved from XFIRE Database accession no. BRN 3627304, BRN 3625052 *
DATABASE BEILSTEIN [online] BEILSTEIN INSTITUTE FOR ORGANIC CHEMISTRY, FRANKFURT-MAIN, DE; XP002446455, retrieved from XFIRE Database accession no. BRN 3047361, BRN 1765642 *
HENSEN, K. ET AL., CHEM. BER., vol. 129, no. 7, 1996, pages 765 - 772 *
HENSEN, K. ET AL.: "Experimental Investigations and ab Inition Studies on Hexacoordinated Complexes of Dichlorosilane", J. AM. CHEM. SOC, vol. 120, 1998, pages 10402 - 10408, XP002446447 *
SHERGINA ET AL., J. GEN. CHEM. USSR (ENGL. TRANSL.), vol. 46, 1976, pages 303 *

Also Published As

Publication number Publication date
WO2007118474A2 (de) 2007-10-25
DE112007000952A5 (de) 2009-01-15

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