KR101250153B1 - 트리메틸갈륨, 이의 제조 방법 및 트리메틸갈륨으로부터형성된 질화갈륨 박막 - Google Patents
트리메틸갈륨, 이의 제조 방법 및 트리메틸갈륨으로부터형성된 질화갈륨 박막 Download PDFInfo
- Publication number
- KR101250153B1 KR101250153B1 KR1020050096398A KR20050096398A KR101250153B1 KR 101250153 B1 KR101250153 B1 KR 101250153B1 KR 1020050096398 A KR1020050096398 A KR 1020050096398A KR 20050096398 A KR20050096398 A KR 20050096398A KR 101250153 B1 KR101250153 B1 KR 101250153B1
- Authority
- KR
- South Korea
- Prior art keywords
- trimethylgallium
- ppm
- tma
- content
- trimethylaluminum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/40—AIIIBV compounds wherein A is B, Al, Ga, In or Tl and B is N, P, As, Sb or Bi
- C30B29/403—AIII-nitrides
- C30B29/406—Gallium nitride
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G15/00—Compounds of gallium, indium or thallium
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
- C30B25/02—Epitaxial-layer growth
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Vapour Deposition (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004298564A JP4470682B2 (ja) | 2004-10-13 | 2004-10-13 | トリメチルガリウムの製造方法 |
| JPJP-P-2004-00298564 | 2004-10-13 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20060053239A KR20060053239A (ko) | 2006-05-19 |
| KR101250153B1 true KR101250153B1 (ko) | 2013-04-04 |
Family
ID=35430195
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020050096398A Expired - Fee Related KR101250153B1 (ko) | 2004-10-13 | 2005-10-13 | 트리메틸갈륨, 이의 제조 방법 및 트리메틸갈륨으로부터형성된 질화갈륨 박막 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20060075959A1 (enExample) |
| JP (1) | JP4470682B2 (enExample) |
| KR (1) | KR101250153B1 (enExample) |
| CN (1) | CN1763049B (enExample) |
| DE (1) | DE102005048680A1 (enExample) |
| GB (1) | GB2420118B (enExample) |
| TW (1) | TWI363059B (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008024617A (ja) | 2006-07-19 | 2008-02-07 | Ube Ind Ltd | 高純度トリアルキルアルミニウム及びその製法 |
| JP4462251B2 (ja) * | 2006-08-17 | 2010-05-12 | 日立電線株式会社 | Iii−v族窒化物系半導体基板及びiii−v族窒化物系発光素子 |
| JP2008050268A (ja) * | 2006-08-22 | 2008-03-06 | Ube Ind Ltd | 高純度トリアルキルガリウム及びその製法 |
| JP2008081451A (ja) * | 2006-09-28 | 2008-04-10 | Ube Ind Ltd | 高純度トリアルキルガリウム及びその製法 |
| JP2008263023A (ja) * | 2007-04-11 | 2008-10-30 | Sumitomo Electric Ind Ltd | Iii−v族化合物半導体の製造方法、ショットキーバリアダイオード、発光ダイオード、レーザダイオード、およびそれらの製造方法 |
| JP2008266196A (ja) * | 2007-04-19 | 2008-11-06 | Nippon Shokubai Co Ltd | ボラジン化合物の製造方法 |
| JP2009126835A (ja) * | 2007-11-27 | 2009-06-11 | Ube Ind Ltd | 高純度トリアルキルガリウム及びその製法 |
| KR100965270B1 (ko) * | 2008-07-04 | 2010-06-22 | 주식회사 한솔케미칼 | 새로운 전자 주개 리간드를 가지는 갈륨 착화합물 및 이의제조방법 |
| JP5423039B2 (ja) * | 2009-02-23 | 2014-02-19 | 宇部興産株式会社 | 高純度トリアルキルガリウム及びその製造方法 |
| JP5348186B2 (ja) * | 2011-06-16 | 2013-11-20 | 宇部興産株式会社 | 高純度トリアルキルガリウム及びその製法 |
| DE102012013941A1 (de) | 2012-07-16 | 2014-01-16 | Umicore Ag & Co. Kg | Verfahren zur Herstellung von Galliumtrialkylverbindungen |
| TWI632149B (zh) | 2011-11-28 | 2018-08-11 | 烏明克股份有限兩合公司 | 第iii a族金屬的三烷基化合物之製法 |
| KR101326554B1 (ko) * | 2012-06-22 | 2013-11-07 | 한국기초과학지원연구원 | 트리메틸갈륨(TMGa)의 재활용 방법 |
| KR101436590B1 (ko) * | 2013-05-28 | 2014-09-02 | 한국기초과학지원연구원 | 회수 TMIn 재이용방법 |
| JP5761401B2 (ja) * | 2014-02-27 | 2015-08-12 | 宇部興産株式会社 | 高純度トリアルキルガリウム及びその製法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5288885A (en) * | 1991-11-19 | 1994-02-22 | Shell Research Limited | Purification of tri-alkyl compounds of Group 3a metals |
| JP2002533348A (ja) * | 1998-12-19 | 2002-10-08 | エピケム リミテッド | 有機金属化合物の製造のための改良された方法および装置 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62132888A (ja) * | 1985-12-03 | 1987-06-16 | Sumitomo Chem Co Ltd | 有機金属化合物の精製方法 |
| US4847399A (en) * | 1987-01-23 | 1989-07-11 | Morton Thiokol, Inc. | Process for preparing or purifying Group III-A organometallic compounds |
| US5043462A (en) * | 1989-04-28 | 1991-08-27 | Messer Greisheim | Process for the production of gallium-alkyl compounds |
| US5455364A (en) * | 1993-12-14 | 1995-10-03 | Sumitomo Chemical Company, Ltd. | Process for removing an impurity in organometallic compound |
| JP3230029B2 (ja) * | 1994-05-30 | 2001-11-19 | 富士通株式会社 | Iii−v族化合物半導体結晶成長方法 |
| JP2927685B2 (ja) * | 1994-08-19 | 1999-07-28 | 信越化学工業株式会社 | 有機金属化合物の精製方法 |
| MY112590A (en) * | 1994-09-02 | 2001-07-31 | Sec Dep For Defence Acting Through His Defence Evaluation And Research Agency United Kingdom | Semi-conductor devices and their production |
| WO2000071551A2 (en) * | 1999-05-21 | 2000-11-30 | Akzo Nobel N.V. | Purification of an organometallic compound by recrystallization |
| TW574762B (en) * | 2002-10-16 | 2004-02-01 | Univ Nat Cheng Kung | Method for growing monocrystal GaN on silicon substrate |
| JP4488186B2 (ja) * | 2004-06-18 | 2010-06-23 | 信越化学工業株式会社 | トリメチルアルミニウムの精製方法 |
| JP2006001896A (ja) * | 2004-06-18 | 2006-01-05 | Shin Etsu Chem Co Ltd | 高純度トリメチルアルミニウム及びトリメチルアルミニウムの精製方法 |
-
2004
- 2004-10-13 JP JP2004298564A patent/JP4470682B2/ja not_active Expired - Fee Related
-
2005
- 2005-10-11 DE DE102005048680A patent/DE102005048680A1/de not_active Withdrawn
- 2005-10-11 GB GB0520663A patent/GB2420118B/en not_active Expired - Fee Related
- 2005-10-11 US US11/246,550 patent/US20060075959A1/en not_active Abandoned
- 2005-10-13 TW TW094135671A patent/TWI363059B/zh not_active IP Right Cessation
- 2005-10-13 KR KR1020050096398A patent/KR101250153B1/ko not_active Expired - Fee Related
- 2005-10-13 CN CN2005101083835A patent/CN1763049B/zh not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5288885A (en) * | 1991-11-19 | 1994-02-22 | Shell Research Limited | Purification of tri-alkyl compounds of Group 3a metals |
| JP2002533348A (ja) * | 1998-12-19 | 2002-10-08 | エピケム リミテッド | 有機金属化合物の製造のための改良された方法および装置 |
Non-Patent Citations (2)
| Title |
|---|
| Journal of Cluster Science, 2002, Volume 13, Number 4, 631-636 * |
| Journal of Cluster Science, 2002, Volume 13, Number 4, 631-636* |
Also Published As
| Publication number | Publication date |
|---|---|
| GB0520663D0 (en) | 2005-11-16 |
| US20060075959A1 (en) | 2006-04-13 |
| DE102005048680A1 (de) | 2006-04-20 |
| TWI363059B (en) | 2012-05-01 |
| TW200611908A (en) | 2006-04-16 |
| GB2420118B (en) | 2006-12-13 |
| CN1763049A (zh) | 2006-04-26 |
| KR20060053239A (ko) | 2006-05-19 |
| GB2420118A (en) | 2006-05-17 |
| CN1763049B (zh) | 2011-12-14 |
| JP2006111546A (ja) | 2006-04-27 |
| JP4470682B2 (ja) | 2010-06-02 |
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