ES8701743A1 - Procedimiento para la preparacion de acido acetoacetamido-n-sulfonico o sussales - Google Patents

Procedimiento para la preparacion de acido acetoacetamido-n-sulfonico o sussales

Info

Publication number
ES8701743A1
ES8701743A1 ES551338A ES551338A ES8701743A1 ES 8701743 A1 ES8701743 A1 ES 8701743A1 ES 551338 A ES551338 A ES 551338A ES 551338 A ES551338 A ES 551338A ES 8701743 A1 ES8701743 A1 ES 8701743A1
Authority
ES
Spain
Prior art keywords
salts
oxathiazin
dihydro
dioxide
methyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES551338A
Other languages
English (en)
Other versions
ES551338A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=6231216&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES8701743(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Hoechst AG filed Critical Hoechst AG
Publication of ES8701743A1 publication Critical patent/ES8701743A1/es
Publication of ES551338A0 publication Critical patent/ES551338A0/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D291/00—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms
    • C07D291/02—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms not condensed with other rings
    • C07D291/06—Six-membered rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Seasonings (AREA)
  • Catalysts (AREA)
  • Cephalosporin Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

PROCEDIMIENTO PARA LA PREPARACION DE ACIDO ACERAMIDO-N-SULFONICO. COMPRENDE: A) HACER REACCIONAR UN DERIVADO DE ACIDO AMIDOSULFONICO COMO LAS SALES DE LITIO, DE AMONIO PRIMARIAS, SECUNDARIAS, TERCIARIAS Y CUATERNARIAS DEL ACIDO AMIDOSULFONICO CON UN EXCESO DE HASTA APROXIMADAMENTE 30% EN MOLES DE UN AGENTE ACETOACETILANTE COMO LA DICETENA, EN UN DISOLVENTE ORGANICO INERTE QUE DISUELVA PARCIALMENTE LAS SALES DEL ACIDO AMIDOSULFONICO COMO EL CLORURO DE METILENO, CLOROFORMO Y OTROS, CON AMINAS O FOSFINAS, ESPECIALMENTE TERCIARIAS COMO CATALIZADOR, PARA FORMAR UN ACETOAMIDO-N-SULFONATO; U B) CICLAR EL ACETOACETAMIDO-N-SULFONATO OBTENIDO CON UN EXCESO HASTA 20 VECES MAYOR QUE LA CANTIDAD EQUIMOLAR DE SO, EN UN DISOLVENTE INORGANICO U ORGANICO INERTE COMO EL CLORURO DE METILENO, TRICLOROETILENO U OTROS, A UNA TEMPERATURA ENTRE C40 Y 10JC, PARA OBTENER LOS COMPUESTOS DE FORMULA (I). SUS SALES NO TOXICAS SON UTILIZABLES COMO EDULCORANTES.
ES551338A 1984-03-22 1986-01-28 Procedimiento para la preparacion de acido acetoacetamido-n-sulfonico o sussales Expired ES8701743A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19843410439 DE3410439A1 (de) 1984-03-22 1984-03-22 Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und dessen nichttoxischen salzen sowie der dabei als zwischenprodukt(e) auftretenden acetoacetamind-n-sulfonsaeure(salze)

Publications (2)

Publication Number Publication Date
ES8701743A1 true ES8701743A1 (es) 1986-12-16
ES551338A0 ES551338A0 (es) 1986-12-16

Family

ID=6231216

Family Applications (2)

Application Number Title Priority Date Filing Date
ES541417A Expired ES8606315A1 (es) 1984-03-22 1985-03-20 Procedimiento para la preparacion de 6-metil-3,4-dihidro-1,2,3-oxatiazin-4-on-2,2-dioxido y de sus sales no toxicas'
ES551338A Expired ES8701743A1 (es) 1984-03-22 1986-01-28 Procedimiento para la preparacion de acido acetoacetamido-n-sulfonico o sussales

Family Applications Before (1)

Application Number Title Priority Date Filing Date
ES541417A Expired ES8606315A1 (es) 1984-03-22 1985-03-20 Procedimiento para la preparacion de 6-metil-3,4-dihidro-1,2,3-oxatiazin-4-on-2,2-dioxido y de sus sales no toxicas'

Country Status (21)

Country Link
US (4) US4607100A (es)
EP (1) EP0155634B1 (es)
JP (2) JPS60209578A (es)
KR (1) KR930000806B1 (es)
AT (1) ATE53579T1 (es)
AU (2) AU587970B2 (es)
BR (1) BR8501306A (es)
CA (1) CA1273923A (es)
CS (3) CS249549B2 (es)
DD (3) DD234007A5 (es)
DE (2) DE3410439A1 (es)
DK (2) DK170401B1 (es)
ES (2) ES8606315A1 (es)
FI (1) FI83076C (es)
HU (2) HU196954B (es)
IE (1) IE58342B1 (es)
IL (1) IL74676A (es)
MX (1) MX162880B (es)
NO (3) NO163771C (es)
SU (1) SU1342418A3 (es)
ZA (1) ZA852116B (es)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3410233A1 (de) * 1984-03-21 1985-09-26 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung kristalliner salze des acetoacetamid-n-sulfofluorids
DE3410440A1 (de) * 1984-03-22 1985-09-26 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und dessen nichttoxischen salzen
DE3527070A1 (de) * 1985-07-29 1987-01-29 Hoechst Ag Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid
DE3531359A1 (de) * 1985-09-03 1987-03-12 Hoechst Ag Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid sowie zu dessen reinigung
DE3531358A1 (de) * 1985-09-03 1987-03-12 Hoechst Ag Verfahren zur herstellung der nicht-toxischen salze des 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxids
TW223067B (es) * 1992-03-17 1994-05-01 Hoechst Ag
DE10013259A1 (de) 2000-03-17 2001-09-20 Nutrinova Gmbh Acesulfam-Metall-Komplexe Verfahren zu ihrer Herstellung und ihre Verwendung
DE10130298A1 (de) 2001-06-22 2003-01-23 Nutrinova Gmbh Antimikrobiell wirksame Acesulfam-Komplexe, Verfahren zu ihrer Herstellung und ihre Verwendung
DE10130504B4 (de) 2001-06-25 2005-02-03 Nutrinova Nutrition Specialties & Food Ingredients Gmbh Xanthin- und Phenazon-Acesulfam-H-Komplexe mit verbessertem Geschmack, Verfahren zu ihrer Herstellung und ihre Verwendung
JP2003026671A (ja) * 2001-07-13 2003-01-29 Daicel Chem Ind Ltd オキサチアジン類の製造方法
CN1336363A (zh) 2001-07-25 2002-02-20 张元宾 乙酰磺胺酸钾的合成制备方法
DE10253773B3 (de) * 2002-11-19 2004-06-24 Nutrinova Nutrition Specialties & Food Ingredients Gmbh Verwendung von Acesulfamsäure zur pH-Wert-Absenkung
AU2003304021A1 (en) 2002-11-19 2004-10-18 Nutrinova Nutrition Specialties And Food Ingredients Gmbh Use of sweetener acids for the microbiological stabilisation of foodstuffs, cosmetic products, consumer goods and pharmaceutical products
US8043647B1 (en) 2003-03-10 2011-10-25 Perry Stephen C Sugar replacement
DE10330025A1 (de) * 2003-07-03 2005-01-20 Nutrinova Nutrition Specialties & Food Ingredients Gmbh Verfahren zur Herstellung eines Süßstoffsalzes basierend auf Aspartam und Acesulfam
JP2005263779A (ja) * 2004-02-17 2005-09-29 Daicel Chem Ind Ltd ３，４−ジヒドロ−１，２，３−オキサチアジン−４−オン−２，２−ジオキサイド化合物又はその塩の製造法
CN100410246C (zh) * 2006-09-24 2008-08-13 张家港浩波化学品有限公司 一种合成乙酰磺胺酸钾过程中的水解工艺及该工艺的专用设备
CN100516054C (zh) * 2006-09-24 2009-07-22 张家港浩波化学品有限公司 一种合成乙酰磺胺酸钾过程中的磺化环合工艺及该工艺的专用设备
UA103492C2 (ru) 2008-07-08 2013-10-25 Борд Оф Риджентс, Дзе Юниверсити Оф Техас Систем Ингибиторы пролиферации и активации переносчика сигнала и активатора транскрипции (stats)
EP2382237A1 (en) 2008-12-23 2011-11-02 Schering Corporation Purification of recombinantly produced interferon
EP2407146A1 (en) 2010-07-15 2012-01-18 Nutrinova Nutrition Specialties & Food Ingredients GmbH Use of acesulfame K as a flavour modulator
US9024016B2 (en) * 2012-06-08 2015-05-05 Nutrinova Nutrition Specialists & Food Ingredients GmbH Process for producing acesulfame potassium
CN103450114B (zh) * 2013-08-19 2015-09-02 苏州浩波科技股份有限公司 5-氯-6-甲基-1,2,3-氧噁嗪-4(3h)-酮-2,2-二氧化物的合成方法
CN104292181B (zh) * 2014-09-27 2016-10-26 安徽金禾实业股份有限公司 一种mvr系统浓缩安赛蜜母液的方法
SI3319949T1 (sl) 2016-09-21 2020-11-30 Celanese International Corporation, Sestavki kalijevega acesulfama in postopki za njihovo izdelavo
RS59840B1 (sr) * 2016-09-21 2020-02-28 Celanese Int Corp Kompozicije acesulfam-kalijuma i postupci za njihovu proizvodnju
JP6912582B2 (ja) 2016-09-21 2021-08-04 セラニーズ・インターナショナル・コーポレーション アセスルファムカリウム組成物及びその製造方法
DK3319948T3 (da) 2016-09-21 2021-09-27 Celanese Int Corp Acesulfam-kaliumsammensætninger og fremgangsmåder til fremstilling af disse
CA3168761A1 (en) 2020-03-19 2021-09-23 Minna HASSINEN Temperature-responsive virus storage system
BR112022019660A2 (pt) 2020-03-30 2022-11-29 Trizell Ltd Composições e métodos para tratamento de câncer
CN113454060B (zh) * 2021-05-28 2022-11-25 安徽金禾实业股份有限公司 乙酰乙酰胺-n-磺酸三乙胺盐的制备方法
WO2022246865A1 (zh) * 2021-05-28 2022-12-01 安徽金禾实业股份有限公司 乙酰磺胺酸钾的制备方法
CN113454056B (zh) * 2021-05-28 2022-11-04 安徽金禾实业股份有限公司 乙酰乙酰胺-n-磺酸三乙胺盐的制备方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL157304B (nl) * 1970-01-10 1978-07-17 Hoechst Ag Werkwijze voor het bereiden van zoetmiddelen, onder toepassing van deze werkwijze verkregen gevormd voortbrengsel, alsmede werkwijze voor het bereiden van zoetsmakende verbindingen.
DE2001017C3 (de) * 1970-01-10 1978-05-18 Hoechst Ag, 6000 Frankfurt 3,4-Dihydro-1,23-oxathiazin-4on-2,2-dioxide, ihre Herstellung und Verwendung
DE2228423C3 (de) * 1972-06-10 1982-05-13 Hoechst Ag, 6000 Frankfurt 3,4-Dihydro-1,2,3-oxathiazin-4-one und Verfahren zu ihrer Herstellung
DE2434549A1 (de) * 1974-07-18 1976-01-29 Hoechst Ag Verfahren zur herstellung des suesstoffes 6-methyl-3,4-dihydro-1,2,3-oxathiazin4-on-2,2-dioxid
DE2434564A1 (de) * 1974-07-18 1976-01-29 Hoechst Ag Verfahren zur herstellung von 6-methyl3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und seine verwendung als suesstoff
DE2453063A1 (de) * 1974-11-08 1976-05-13 Hoechst Ag Verfahren zur herstellung von acetoacetamid-n-sulfofluorid
DE3410440A1 (de) * 1984-03-22 1985-09-26 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und dessen nichttoxischen salzen
DE3429039A1 (de) * 1984-08-07 1986-02-20 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und dessen nichttoxischen salzen
DE3527070A1 (de) * 1985-07-29 1987-01-29 Hoechst Ag Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid

Also Published As

Publication number Publication date
SU1342418A3 (ru) 1987-09-30
ZA852116B (en) 1985-11-27
AU4021085A (en) 1985-09-26
DD244551A5 (de) 1987-04-08
IL74676A (en) 1988-12-30
ES541417A0 (es) 1986-04-16
ES551338A0 (es) 1986-12-16
NO851143L (no) 1985-09-23
HUT36467A (en) 1985-09-30
KR850006192A (ko) 1985-10-02
DK129185D0 (da) 1985-03-21
CS249549B2 (en) 1987-03-12
FI851104A0 (fi) 1985-03-20
US5011982A (en) 1991-04-30
KR930000806B1 (ko) 1993-02-05
DK129185A (da) 1985-09-23
US5103046A (en) 1992-04-07
US4695629A (en) 1987-09-22
FI83076B (fi) 1991-02-15
DK42394A (da) 1994-04-13
DK171986B1 (da) 1997-09-08
AU2237288A (en) 1988-12-22
NO163771C (no) 1990-07-18
NO166364B (no) 1991-04-02
DK170401B1 (da) 1995-08-21
BR8501306A (pt) 1985-11-19
MX162880B (es) 1991-07-02
ES8606315A1 (es) 1986-04-16
NO163771B (no) 1990-04-09
AU598698B2 (en) 1990-06-28
IL74676A0 (en) 1985-06-30
NO163773C (no) 1990-07-18
ATE53579T1 (de) 1990-06-15
DD244554A5 (de) 1987-04-08
IE58342B1 (en) 1993-09-08
NO854605L (no) 1985-09-23
IE850723L (en) 1985-09-22
CA1273923A (en) 1990-09-11
AU587970B2 (en) 1989-09-07
NO163773B (no) 1990-04-09
NO166364C (no) 1991-07-10
EP0155634A2 (de) 1985-09-25
JPH0647571B2 (ja) 1994-06-22
JPS60209578A (ja) 1985-10-22
EP0155634A3 (en) 1987-03-04
DE3410439A1 (de) 1985-09-26
FI83076C (fi) 1991-05-27
HU196954B (en) 1989-02-28
NO854604L (no) 1985-09-23
CS249540B2 (en) 1987-03-12
US4607100A (en) 1986-08-19
DD234007A5 (de) 1986-03-19
CS249550B2 (en) 1987-03-12
DE3578174D1 (de) 1990-07-19
JPH0570627B2 (es) 1993-10-05
JPH03184948A (ja) 1991-08-12
HU196976B (en) 1989-02-28
FI851104L (fi) 1985-09-23
EP0155634B1 (de) 1990-06-13

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 20061021